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Distillation Sieve Trays Without Downcomers Prediction of
Distillation Sieve Trays Without Downcomers Prediction of
A large amount of performance data on larger-scale trays without downcomers has become
available recently, and the data have been examined with a view toward understanding and
modeling the contacting mechanisms under distillation conditions. The objective of this paper
is to describe new predictive models for efficiency, pressure drop, and flooding of trays without
downcomers and to show how they can be applied to distillation separations. Such an effort has
not been reported previously. The contacting devices are assigned the generic name of dualflow trays. The models are shown to give reasonable estimates of the performance of these trays
in larger columns with open areas in the range of 15-25%, hole diameters in the range of 1225 mm, and tray spacings in the range of 0.3-0.6 m.
Bubble trays for distillation columns normally involve
liquid flowing between trays through connecting downcomers. Such contacting devices are of the cross-flow
type, and vapor flows only through dispersers on the
trays such as holes, valves, or bubble caps. Less wellknown and -specified are perforated trays without
downcomers, wherein the liquid and vapor flow countercurrently through the same tray openings. These are
often called dual-flow trays, but in specialty forms, they
have other names such as turbogrid trays and ripple
trays. The devices are used for special services, especially when openings of a cross-flow tray might foul.
Their less general use appears to have derived from an
expected narrow operating range of high efficiency, as
well as a general unavailability of design models that
can enable reliable prediction of their performance.
In the mid- to late-1950s Fractionation Research, Inc.
(FRI), undertook an extensive research program on
dual-flow trays, obtaining performance data for several
different systems but not providing a general, fundamental correlation of the data for pressure drop, efficiency, and flooding. Meanwhile, Shell completed an
extensive program of testing its turbogrid trays, similar
in characteristics to dual-flow trays. Recently, FRI
released all of its dual-flow test results, and these data
form a major basis for the modeling in the present
paper. Shell has released none of its turbogrid test
results.
Dual-flow trays have been applied to many situations
in which a broad operating range (high turndown ratio)
is not essential. In its range of application, the tray
provides a very high mass transfer efficiency with low
capital investment. Importantly, the application of such
devices to fouling systems has been eminently successful, the alternating vapor-liquid passage through the
holes providing a self-cleaning action.
Previous Work
Modeling Approach
1634
refa
system
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
5
FRI
FRI
FRI
2
FRI
C6/C7
C6/C7
C6/C7
C6/C7
C6/C7
C6/C7
C6/C7
C6/C7
C6/C7
C6/C7
C4
C4
C4
C4
C4
C4
C4
C4
C4
C4
IPA/H2O
xylenes
xylenes
C8/C10
C8/C10
MeOH/H2O
MeOH/H2O
MeOH/H2O
MeOH/H2O
Bz/Tol
Bz/Tol
pressure
(kPa)
TS
(m)
%
open
hole
diam
(mm)
28
28
28
166
166
166
166
166
345
345
1138
1138
1138
1138
1138
2073
2073
2756
2756
3456
101
16 mm
16 mm
10 mm
10 mm
101
101
101
101
101
101
0.61
0.61
0.61
0.61
0.30
0.91
0.61
0.61
0.61
0.91
0.61
0.30
0.61
0.61
0.91
0.61
0.61
0.61
0.61
0.61
0.61
0.61
0.61
0.61
0.61
0.41
0.41
0.41
0.41
0.51
0.51
13.5
18.9
25.6
13.5
19.1
19.1
18.9
25.6
18.9
29.3
13.5
19.1
18.9
25.6
29.3
13.5
29
13.5
29
13.5
19.1
12.9
17.8
12.9
17.8
10.5
14.2
18.2
23.6
14
14
12.7
25.4
25.4
12.7
12.7
12.7
25.4
25.4
25.4
11.9
0.5
1.0
1.0
1.0
0.47
0.50
0.47
0.50
0.47
0.50
0.5
12.7
12.7
12.7
12.7
b
b
b
b
12.7
12.7
Ep/Fs
Fs
flood
[m/s (kg/m3)0.5]
peak
efficiency
(% flood)
79/1.98
75/2.26
63/2.56
83/1.77
55/1.89
57/3.11
81/2.20
55/2.60
98/2.01
67/2.81
121/0.83
90/1.29
115/1.13
92/1.62
96/1.89
114/0.67
91/0.91
150/0.43
87/0.79
>180/0.24
75/2.34
81/2.01
63/2.01
72/2.81
42/2.56
95/1.27
82/1.92
82/1.98
53/2.3
87/1.63
80/1.96
2.20
2.59
2.93
2.01
1.98
3.39
2.34
2.89
2.34
3.17
1.43
1.46
1.77
1.73
2.07
0.76
1.01
0.52
0.88
0.33
2.46
3.07
3.3
(3.78)
3.2
1.87
2.66
2.78
NA
2.44
2.62
90
87
88
88
96
92
94
90
86
88
58
88
64
94
91
89
90
81
90
74
95
65
61
(74)
(81)
68
72
71
NA
67
75
Column diameters: FRI, 1.2 m; ref 5, 1.0 m; ref 2, 0.45 and 2.50 m. b Slots, 4 mm 150 mm.
m (24 in.). Thus, the 0.30-m spacing has about 81%, and
the 0.91-m spacing about 116%, of the capacity of the
0.61-m spacing.
The effect of open area on flooding is evident but not
well understood. Apparently, the higher hole velocity
for lower open area results in jetting, which increases
liquid entrainment. A small effect of hole size on
flooding is indicated, with 25-mm holes having about
6% less capacity than the more standard 12.5-mm holes.
This difference might be more apparent than real, but
it could be a result of the longer jet length for the larger
holes.
Efficiency at Lower Loadings. The profiles in
Figures 2-4 are typical of dual-flow trays, and it is clear
Ew/Ep )
1
1 + Ep/(1 - )
(1)
1-
Ep + (1 - )
(2)
or
ht ) hgd + hL ) hL - hLd
Figure 6. Fractional entrainment of liquid in vapor. Methanol/
water, 1.0-m-diameter column. Data from ref 5 and Figure 2. The
superimposed curve for cross-flow sieve trays is taken from ref
12.
1 -
1 - 0.70
)
) 0.34 (3)
Ep + (1 - ) 0.70(1 - 0.70)
(4)
ht ) hdG + hL
(5)
with
hdG )
Ux2FL
2gCv2FG
(6)
(7)
1636
hL ) b1
(LML)n[US(FG/FL)0.5]b2
FL(Ah/Aa)b3 (tt/dh)0.42
(8)
n ) 4.3
()
Ah
Aa
1.5
(9)
hdG ) ht,meas - hL )
Ux2FL
2gCv2FG
(10)
from which
Q
Ah
FL
(ht,meas - hL)(2gCv2FG)
(11)
( )( )
)A
Ah/At
0.2
0.8
TS
0.610
0.2
exp -0.35
(12)
where TS is the tray spacing in meters and A, B, and C
are the regression correlation constants (A ) 0.4668, B
) 90, C ) 45).
A representative plot of fractional holes passing vapor
is shown as Figure 8. Although the trend with loading
might seem counterintuitive, until direct measurements
are made, the relationships will remain useful for the
design process, as shown later in a comparison of
calculated and measured overall pressure drop data.
Pressure Drop Model Analysis. The approach
outlined above was used to develop the parity plot in
Figure 9. The plot is based on all of the total reflux FRI
experimental data. The mean absolute deviation is
23.0%, and the average deviation is 0%. Of the 136
points, 13 lie above the (25% range. Most of these
outside points derive from near-flooding conditions,
where measurements are not precise. If the water/2propanol system is excluded, leaving only hydrocarbon
systems, only 9 of the 122 points are outside the (25%
range. In general, pressure drop is underpredicted in
the near-flooding zone. A representative performance
plot showing the pressure drop fit is given in Figure 10.
and methanol/2-propanol systems. The porosity (volume fraction of vapor in the froth) determined by Xu et
al. is
) 1.0 - 0.0946
[ ]
Us2FG
ghLFL
-0.2
refa
(13)
hf )
hL
(1 - )
(14)
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
FRI
system
C6/C7
C6/C7
C6/C7
C6/C7
C6/C7
C6/C7
C6/C7
C6/C7
C6/C7
C6/C7
C4
C4
C4
C4
C4
IPA/H2O
xylenes
xylenes
C8/C10
alcohols
FRI C8/C10
alcohols
5
MeOH/H2O
FRI MeOH/H2O
2
Bz/Tol
hole
efficiency,
pressure TS
% diam peak, calculated
(kPa)
(m) open (mm) meas
(%)b
28
28
28
166
166
166
166
166
345
345
1138
1138
1138
1138
1138
101
16 mm
16 mm
10 mm
0.61
0.61
0.61
0.61
0.61
0.91
0.61
0.61
0.61
0.91
0.61
0.30
0.61
0.61
0.91
0.61
0.61
0.61
0.61
13.5
18.9
25.6
13.5
19.1
19.1
18.9
25.6
18.9
29.3
13.5
19.1
18.9
25.6
29.3
19.1
12.9
17.8
12.9
12.7
25.4
25.4
12.7
12.7
12.7
25.4
25.4
25.4
11.9
12.7
25.4
25.4
25.4
11.0
12.7
12.7
12.7
12.7
79
75
63
83
81
57
81
55
98
67
121
90
115
92
96
75
81
63
72
43
53
54
67
69
71
74
70
75
71
77
71
77
75
74
69
60
62
72
10 mm
0.61 17.8
12.7
42
86
101
101
101
0.41 14.2
0.41 18.2
0.51 14
c
c
12.7
82
82
87
80
80
60
E
)
Ep
1 + Ep
1 -
(15)
1638
Figure 12. Low-loading discount factor for representative experimental data: (a) 12.7-mm holes, 18-20% open area; (b) 25.4-mm
holes, 18-20% open area; (c) 12.7-mm holes or smaller, 13-15% open area; (d) summary plot.
Acknowledgment
This paper would not have been possible without the
generous provision of large-scale performance data by
Fractionation Research, Inc. (FRI). The authors extend
thanks to FRI, as well as to the Separations Research
Program at the University of Texas and to Koch-Glitsch,
Inc., for providing support for the modeling and analysis
effort.
Nomenclature
A, B, C ) constants in eq 12
Aa ) tray active area, m2
Ah ) tray hole area, m2
At ) total column cross-sectional (superficial) area, m2
Ax ) area of holes open to vapor at any instant ) Ah, m2
b1, b2, b3 ) constants in eq 8
Csb ) Souders-Brown capacity parameter, m/s
Cv ) orifice coefficient, eq 6
dh ) hole diameter, mm or m
Ep ) peak efficiency, fractional
Ew ) efficiency corrected for liquid-in-vapor entrainment,
fractional
Fs ) vapor F factor based on superficial area, UsFG0.5, m/s
(kg/m3)0.5
g ) gravitational constant, m/s2
h ) pressure loss, m of tray liquid
hdG ) drop for vapor flow through orifices
hL ) residual drop through two-phase mixture
hLD ) drop for liquid flow through orifices
hL ) head required to force liquid through the orifices
ht ) total pressure drop for a dual-flow tray
ht,meas ) measured total pressure drop for a dual-flow tray
hf ) height of froth on the tray, m
L ) liquid flow, kg mol/s
m ) slope of the equilibrium curve
n ) exponent in eq 8
ML, MG ) molecular weights of liquid and vapor, respectively
Q ) volumetric flow rate of vapor, m3/s
tt ) tray metal thickness, mm
TS ) tray spacing, m
U ) vapor velocity, m/s
Us ) superficial velocity
Ux ) velocity through x fraction of total number of holes
V ) vapor flow, kg mol/s
) fraction of total holes passing vapor at any instant
Greek Letters
) void fraction in the froth
) ratio of slopes, equilibrium curve to operating line )
mV/L
FL ) liquid density, kg/m3
FG ) vapor density, kg/m3
) ratio of wet efficiency (with entrainment) to dry (peak)
efficiency
) ratio of lower loading efficiency to peak efficiency
) efficiency discount factor for entrainment in vapor
) efficiency discount factor for lower loadings
Literature Cited
(1) Zuiderweg, F. J.; Verburg, H.; Gilissen, F. A. H. Comparison
of fractionating devices. Proc. Int. Symp. Distill. 1960, 201.
(2) Zuiderweg, F. J.; de Groot, J. H.; Meeboer, B.; van der Meer,
D. Scaling up distillation plates. Proc. Int. Symp. Distill. 1969, 5,
78.
(3) Huml, M.; Standart, G. The hydraulics of large turbogrid
trays. Brit. Chem. Eng. 1966, 11 (11), 1370.
1640