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Title: Si-29 and C-13 solid state NMR as a tool to study Output This Record
thermal processes in epoxy-silica hybrids
Bibliographic Fields
Author(s): Potrzebowski MJ (Potrzebowski, M. J.), Ciesielski W
(Ciesielski, W.), Ganicz K (Ganicz, K.), Gluszek J (Gluszek, J.),
Szczygiel B (Szczygiel, B.), Kucharczyk B (Kucharczyk, B.),
Masalski J (Masalski, J.)
Source: POLISH JOURNAL OF CHEMISTRY 80 (7): 1185-1194 JUL
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2006
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Document Type: Article
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Language: English
Cited References: 22 Times Cited: 0 [0 articles marked]

Abstract: Si-29 CP/MAS and C-13 CP/MAS measurements were Create Citation Alert
carried out for epoxy-silica hybrids treated at 200 degrees C and
300 degrees C. For each sample, the Si-29 spin lattice relaxation
time was evaluated and compared with the corresponding values Receive e-mail alerts on future
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for reference samples prepared under the same conditions but (Requires registration.)
without epoxy compound. This work clearly shows the sensitivity
of the Si-29 T-1 to the morphology of composite materials. The Context Sensitive Links
mechanism of thermal decomposition is proposed on the basis of
C-13 CP/MAS experiments and analysis of changes of the Si-29 T- View record in
1 relaxation time. Current Contents Connect
Author Keywords: C-13 and Si-29 NMR; hybrid materials; CC Connect Table of Contents
relaxation times; thermal decomposition; solid state NMR Journal Citation Reports
ISI Proceedings
KeyWords Plus: CROSS-POLARIZATION DYNAMICS; GEL
Addresses: Potrzebowski MJ (reprint author), Wroclaw Univ
Technol, Dept Chem, Lab Mat Engn, Wybrzeze Wyspianskiego 27,
PL-50370 Wroclaw, Poland
Polish Acad Sci, NMR Lab, PL-90363 Lodz, Poland
Polish Acad Sci, Ctr Mol & Macromol Studies, Dept Struct Studies,
PL-90363 Lodz, Poland
E-mail Addresses: marekpot@bilbo.cbmm.lodz.pl
Publisher: POLISH CHEMICAL SOCIETY, C/O POLISH ACAD
SCIENCES, INST PHYSICAL CHEMISTRY, UL KASPRZAKA 44/52,
01-224 WARSAW, POLAND
Subject Category: Chemistry, Multidisciplinary
IDS Number: 062XK
ISSN: 0137-5083

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