Overview Pilot Plant

Produksi Bioetanol Berbasis

Lignoselulosa dengan
Kapasitas 10 L/hari
KOICA--LIPI Project 2010-
KOICA 2010-2012

Research Center for Chemistry LIPI

Kawasan PUSPIPTEK Serpong 15314
Tangerang Selatan
Telp. 021-7560929
Fax. 021-7560549

Bioetanol Generasi 1 RC for Chemistry LIPI

Berbasis Gula (Sugar) PUSPIPTEK Serpong

Sweet
Sugar Beet Sorghum
Sugar Cane
(EU) (India, Africa)

Berbasis Tepung (Starch)

Corn Rice Barley wheat

Diatas
Tanah (USA, China) (EU) (EU, Russia)

Dibawah Cassava Potato S.Potato

Tanah (S/W Asia, Africa) (EU)

Lignoselulosa Bioetanol Generasi 2

Agricultural Forestal
Wastes Wastes

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 Unit Operation
RC for Chemistry LIPI
PUSPIPTEK Serpong

Sugar Yeast CO2 Bio-Ethanol

Pre-treatment Fermentation Purification Waste-treatment

juice, bagasse

Starch, Gluten Yeast CO2 Bio-Ethanol Animal feed

Pre-treatment Saccharification Fermentation Purification Waste-treatment

Milling Gelatinization Liquification

Lignin Bio-Ethanol
C5 Fermentation
Pre-treatment Saccharification Yeast CO2 Purification Waste-treatment

C6 Fermentation
Milling Hydrolysis Separation

RC for Chemistry LIPI

BAHAN BAKU PUSPIPTEK Serpong

Komposisi TKKS

Komponen
p Komposisi
p ((%))

Selulosa 41,03

Hemiselulosa 15,88

Lignin 35,74

Abu 0,27

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PUSPIPTEK Serpong

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RC for Chemistry LIPI

PUSPIPTEK Serpong

PRETREATMENT

Chemical Tank

Reactor (Mixer & Exploder)

Belt Press

Washing Tank 1

Washing Tank 2

Buffer Tank
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 RC for Chemistry LIPI
PUSPIPTEK Serpong

Hidrolisa & Fermentasi

Hydrolysis Tank 1&2

Hydrolysis Yeast Propagation Tank 1&2

Fermentor
F t Tank
T k 1,2,3,4
1234
Fermentation
Buffer Tank

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RC for Chemistry LIPI

PUSPIPTEK Serpong

DISTILASI & DEHIDRASI

PSA
drasi
Distilasi

Mash Column (Pressure

(70-80 %Ethanol) Swing
Dehid

Adsorption)
Rectifying Column Anhydrous
(95-96 % Ethanol) Ethanol
(min. 99.5 %)

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 RC for Chemistry LIPI
CONTROL ROOM PUSPIPTEK Serpong

Section #1
PRETREATMENT

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RC for Chemistry LIPI

Section #2 PUSPIPTEK Serpong

HYDROLYSIS & FERMENTATION

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 RC for Chemistry LIPI
Section #3 PUSPIPTEK Serpong

DISTILLATION & DEHYDRATION

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RC for Chemistry LIPI

RINGKASAN HASIL TEST RUN PUSPIPTEK Serpong

Pre-
Distillation &
Tanggal Pretreatment Saccharification SSF
Dehydration

19-26 Kons. NaOH : 10-12% Temperatur : 50-52oC Temperatur : 32-35oC Mash column :
Maret 2012 Temperatur : 130-140oC pH : 4,8-5,5 pH : 4,5-5,5 Feed = 113.4 L/h
Tekanan : 4 bar Substrat : 25 % Substrat : 25 % Tupper : 78.-79oC
Waktu : 30 menit Jumlah FPU : 30 FPU Yeast : 2 % 99 9 100 oC
T bottom : 99.9-100
Bahan Baku per Batch : Buffer pH : Asam Sulfat R reflux = 1:6
- TKKS : 50 Kg Rectifying Column :
- NaOH : 250 L Feed = 90 cc/min
Tupper : 77.7-78oC
T bottom : 100-101 oC
R reflux = 1:8
PSA Dehydration :
T operasi : 125-130 oC
Tekanan : 0,3 kg/cm2

8-14 Kons. NaOH : 9-10% Temperatur

p : 50-52oC Temperatur
p : 32-35oC Mash column :
Juni 2012 Temperatur : 150oC pH : 4,8-5,5 pH : 4,5-5,5 Feed = 70 L/h
Tekanan : 4 bar Substrat : 25 % Substrat : 25 % Tupper : 78.-79oC
Waktu : 30 menit Jumlah FPU : 30 FPU Yeast : 1,5 % T bottom : 99.9-100 oC
Bahan Baku per Batch : Buffer pH : Asam Sulfat R reflux = 1:6
- TKKS : 50 Kg Rectifying Column :
- NaOH : 250 L Feed = 90 cc/min
Tupper : 77.7-78oC
T bottom : 100-101 oC
R reflux = 1:8
PSA Dehydration :
Page 12 T operasi : 125-130 oC
Tekanan : 0,3 kg/cm2

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PUSPIPTEK Serpong

HASIL TEST RUN

Kadar Kadar
Sebelum Setelah
Tanggal Ethanol Pemurnian
Pretreatment Pretreatment
Broth Ethanol
19-26 Selulosa : 41,03
, % Selulosa : 68,68
, % 6,1
, % (v/v)
( ) Mash column :
Maret 2012 % alcohol = 85-90 %
Hemiselulosa : 15,88 % Hemiselulosa : 6,41 %
Rectifying Column :
Lignin : 35,74 % Lignin : 14,13 % % alcohol = 93-94%

PSA Dehydration :
% alcohol = 99.91 %

8-14 Selulosa : 28,23 % Selulosa : 62,86 % 7,8 % (v/v) Mash column :

Juni 2012 % alcohol = 80-85
80 85 %
Hemiselulosa : 14,86 % Hemiselulosa : 7,95 %
Rectifying Column :
Lignin : 36,62 % Lignin : 10,75 % % alcohol = 94-95%

PSA Dehydration :
% alcohol = 99.81 %

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RC for Chemistry LIPI

GRAFIK HASIL PROSES SSF PUSPIPTEK Serpong

19-26 Maret 2012 8-14 Juni 2012

9

8
8

7 Glucose
7
Ethanol
6
6
%Glucose
Xylose
Content % (w/w)

5 5 % Xylose
% % Alcohol
4 4

3 3

2 2

1 1

0 0
0 20 40 60 80 0 20 40 60 80 100
Hour
Time (hours)

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FOTO-FOTO PILOT PLANT PUSPIPTEK Serpong

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Terima Kasih
RC for Chemistry LIPI
PUSPIPTEK Serpong

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