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Lab 1 Specific Gravity PDF
Lab 1 Specific Gravity PDF
This experiment aimed to determine the specific gravity of a soil sample using a pycnometer.
The specific gravity is generally needed to perform additional testing of the soil. The soil
sample was put in a pycnometer, which was then filled with water, taking care to eliminate
air bubbles. The mass of the pycnometer when filled with water and soil, Mpws, was
determined and then the temperature of the soil-and-water mixture was measured. The soil-
and-water mixture was poured onto a pan and then dried in an oven to determine the mass of
solids, Ms. With the temperature of the soil-and-water mixture known, the mass of the
pycnometer when filled with water, Mpw, was found from the calibration of the pycnometer.
Using the acquired data, the specific gravity of soil was computed. The procedure was
repeated for the second trial. The soil sample was found to have a specific gravity of 2.521.
Groupmates:
Arsenio Esteves Jr.
Romano Guerrero Juarez
Robin James Enclona
Christopher Erick Cruz
Ellaine Mary Paglicauan
1
I. Objectives
This experiment was performed to determine the specific gravity of soil solids that pass
the No. 4 sieve by means of a water pycnometer. Given that the specimen is moist, its
moisture content is determined first.
II. Materials
1. Pycnometer (volumetric flask), with a capacity of 250 mL
2. Balance (with accuracy to 0.01 g)
3. Drying Oven
4. Thermometer
5. Hot Plate or Stove
6. No. 4 Sieve (4.75 mm)
7. Moisture Can
8. Funnel
III. Methodology
Since the soil sample was moist, a portion was placed in a moisture can
and the weight, Wcws, was determined and recorded
The specimen was oven-dried and its weight, Wcs, was determined and
recorded
Wcws - Wcs
ω= × 100%
Wcs - Wc
Using the moisture content, the range of wet masses for specific gravity
specimen was calculated,
2
The pycnometer was cleaned and dried and its weight, Wp, was
determined and recorded
The pycnometer was filled with water up to calibration mark, and the
weight of the pycnometer and water, Wpw, is determined and recorded
Wpw,i - Wp
Vp =
ρw,i
The soil sample (45 g) was transferred into the empty pycnometer
using the funnel
Water was added until the water level is 1/3 to 1/2 of the depth of the
main body of the pycnometer. The water was agitated until a slurry is
formed
Heat the pycnometer on the stove and let it boil for 15 minutes. The
slurry is agitated regularly to prevent any soil from sticking or drying
onto the glass
3
Water was added up to the calibration mark and the weight of the
pycnometer, water and soil, Wpws, was determined and recorded
The test temperature, Tx, was determined and recorded to the nearest
0.01°C
The weight of the pycnometer and water at the test temperature, Wpw,x,
was calculated,
Wpw,x = Mp - Vp ∙ ρw,x
The weight of a pan, Wd, was determined and recorded. The entire
slurry was transferred into the pan and was oven-dried for at least 16
hrs
The specimen was cooled and the weight of the pan and soil, Wds, was
determined and recorded
Ws = Wds - Wd
KWs
G20 =
Wpw,x - Wpws - Ws
Wcws = 50.94 g
Wcs = 50.06 g
Wc = 8.87 g
ω = 2.136%
Wp = 82.67 g
Wpw,i = 330.44 g
Ti = 28.5 °C
5
Wpw,i - Wp 330.44 g - 82.67 g
Vp = = g
ρw,i 0.99609 mL
Vp = 248.743 mL
Tx (°C) 28.5 28
K 0.99788 0.99803
Type of Soil Gs
Sand 2.65-2.67
Silty sand 2.67-2.70
Inorganic clay 2.70-2.80
Soils with mica or iron 2.75-3.00
Organic soils Variable, but may be under 2.00
Also, given that the initial weight of the soil sample is 45 g and the moisture content is
2.14%, the expected value of Ws is 44.06 or lower, considering losses. However the actual
value of Ws in the first trial is 44.29. This implies that either the specimen wasn’t oven-dried
for the sufficient amount of time, or additional soil solids were introduced during the course
of the experiment. Since the specimen was oven-dried for more than 16 hours, 19 hours
exactly, the cause is the latter.
Other factors that may have caused errors in the experiment include nonuniform
temperature of the soil-and-water mixture and imprecise weights due to unclean equipment.
VII. References
1. ASTM D854-10. Standard Test Methods for Specific Gravity of Soil Solids by Water
Pycnometer.
2. Liu, Cheng and Jack B. Evett. Soil Properties: Testing, Measurement, and Evaluation.
5th Ed. New Jersey: Prentice-Hall, 2003.
3. Braja M. Das. Principles of Geotechnical Engineering. 4th Ed. Boston: PWS, 1998.