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Nimonic Alloy 90 PDF
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NIMONIC alloy 90
Silicon ...........................................................................1.0 max. h/1080°C (1975°F)/AC + 16 h/700°C (1290°F)/AC.
Copper..........................................................................0.2 max.
Iron................................................................................1.5 max. Table 1 - Specific Heat
Manganese ...................................................................1.0 max.
Chromium....................................................................18.0-21.0 Temperature Specific Heat
Titanium...........................................................................2.0-3.0
°C °F J/kg•°C Btu/lb•°F
Aluminum ........................................................................1.0-2.0
20 68 446 0.11
Cobalt..........................................................................15.0-21.0
100 212 467 0.11
Boron ..........................................................................0.02 max.
200 392 494 0.12
Sulfur ........................................................................0.015 max.
300 572 520 0.12
Lead........................................................................0.0020 max.
400 752 547 0.13
Zirconium....................................................................0.15 max.
500 932 572 0.14
Nickel .............................................................................Balance
600 1112 600 0.14
®
700 1292 626 0.15
800 1472 652 0.16
Heat Treatment
900 1652 679 0.16
The heat treatments recommended are as follows: 1000 1832 706 0.17
Bar 8 h/1080°C(1975°F)/AC + 16 h/700°C
(1290°F)/AC
Sheet 3 min/1150°C(2100°F)/FBQ or WQ + 1
h/925°C(1700°F)/AC + 4 h/750°C Table 2 - Thermal Conductivity
(1380°F)/AC
Temperature, °C Thermal Conductivity
Welded sheet 3 min/1150°C(2100°F)/FBQ or WQ
+ weld + 1 h/925°C(1700°F)/AC + 4 °C °F W/m•°C Btu•in/ft2•h•°F
h/750°C(1380°F)/AC 20 68 11.47 80.46
Interstage anneal of sheet 20 min/1040°C 100 212 12.77 89.58
(1900°F)/AC or WQ 200 392 14.44 101.30
The data for sheet have been obtained from
300 572 15.99 112.17
material given a second stage interstage anneal (20
400 752 17.54 123.04
min/1040°C(1900°F)/AC), which is purely a softening
treatment. Improved tensile and rupture ductility can be 500 932 18.97 133.07
achieved by using 1 h/925°C(1700°F)/AC as the second 600 1112 20.64 144.79
stage heat treatment. 700 1292 22.32 156.57
800 1472 23.99 168.29
Publication Number SMC-080 900 1652 25.83 181.20
Copyright © Special Metals Corporation, 2004 (Sept 04) 1000 1832 27.88 195.58
Calculated from electrical resistance measurements.
NIMONIC is a trademark of the Special Metals Cold rolled sheet heat-treated 2-3 min/1150°C(2100°F)/FBQ + 20
Corporation group of companies. min/1040°C(1900°F)/AC + 4 h 750°C(1380°F)/ AC.
NIMONIC ® alloy 90
Table 3 - Mean Coefficient of Linear Thermal Expansion Table 6 - Dynamic Young’s Modulus of Extruded Bar
Table 5 - Magnetic Properties Cold rolled sheet from 5 casts given heat treatment 2-3
min/1150°C(2100°F)/FBQ + 20 min/1040°C(1900°F)/AC + 4 h/
Mass susceptibility at 1000 oersted: 2.25 x 10-4 cm3/g 750°C(1380°F)/AC.
2
NIMONIC ® alloy 90
Tensile Properties
Table 8 - Tensile Properties of Extruded Bar
800 40
1600 80
0 0
0 200 400 600 800 1000
Temperature, °C
Tensile Strength
1200 60
Elongation, %
Stress, MPa
800 40
Elongation
400 20
Figure 2. Tensile properties of extruded bar.
Heat treatment 8 h/1080°C(1975°F)/AC +
16 h/700°C(1290°F)/AC.
0 0
98% confidence region calculated on 9 0 200 400 600 800 1000
casts. Temperature, °C
3
NIMONIC ® alloy 90
800 40
0 0
0 200 400 600 800 1000
Temperature, °C
1600 80
Tensile Strength
1200 60
Stress, MPa
Elongation, %
800 Elongation, % 40
Temperature, °C
4
NIMONIC ® alloy 90
R. of A.
800 40
0.2% Proof Stress
Elongation
400 20
0 0
0 200 400 600 800 1000
Temperature, °C
5
NIMONIC ® alloy 90
Elongation, %
Stress, MPa
Elongation
400 20
0 0
0 200 400 600 800 1000
Temperature, °C
6
NIMONIC ® alloy 90
Creep Properties
The creep characteristics of NIMONIC alloy 90 have been the change of slope and the distance between lines being
determined on bar (15 casts) and sheet (1 cast). Total plastic dependent on a time/temperature relationship. A general
strain has been determined on extruded section (1 cast) and description of the Graham and Walles analysis can be found
sheet (1 cast). in ‘Regularities in Creep and Hot Fatigue Data’, Parts 1 and
Creep-rupture properties for NIMONIC alloy 90 2, Aero Research Council T.R. CP379 and 380, 1958,
extruded bar subsequently forged are shown in Table 13 and London H.M.S.O.
Figures 7 and 8 by Larson-Miller presentation and Graham Note: It is implicit in the Larson-Miller presentation
and Walles* technique. that no indication is given regarding test temperatures and
Creep-rupture properties for NIMONIC alloy 90 cold- range of rupture lives covered. Tables 13 and 14 show the
rolled sheet are shown in Table 14 and Figures 7 and 9 also temperature ranges and rupture lives used to establish the
by Larson-Miller presentation and Graham and Walles published curves. These tables should be referred to before
technique. using the curves, since excessive extrapolation in time and
Derived total plastic strain data for extruded section temperature is not recommended.
subsequently cold rolled and cold-rolled sheet are shown in Despite these qualifications, it must be most strongly
Tables 15 and 16. Test specimens were 9.1-11.7 mm emphasized that all data given in this section are typical. No
diameter x 76 mm gauge length. attempt has been made to indicate the scatter that may result
*The Graham and Walles technique assumes that stress- from slight processing or compositional variables. Statistical
time test points fall on the continuous series of straight lines data on the scatter of results for tests on production material
for each temperature, with slopes 1/32, 1/16, 1/8, 1/4, 1/2, can be obtained from Special Metals.
7
NIMONIC ® alloy 90
Figure 7. Creep rupture properties. Before using this curve to derive information, your attention is drawn to the note on
page 7.
MPa x 10
100
90
80
70
60
50
40
30
25
20
15
10
9
°F °C 8
7
20 6
100 5
200 100 4
300 3
400 200
500 3
700
400 1
800
900
500
1000
1100 600
1200
1300 700
1400
800
1500
1600
900
1700
1800
1000
1900
2000 1100
2100
2200 1200
10-1 100 101 102 103 104 105
2300 Time, hours
8
NIMONIC ® alloy 90
1000
900
800
700
700°C
600
500 750°C
400
815°C
300
870°C
200
Stress, MPa
100
90
80
70
60
50
40
30
20
10 100 1000 10 000 100 000
Time, hours
9
NIMONIC ® alloy 90
1000
900
800
700
600
500
400
300
700°C
200
750°C
Stress, MPa
100
90
80
70
800°C
60
50
850°C
40
900°C
30
20
10 100 1000 10 000 100 000
Time, hours
10
NIMONIC ® alloy 90
Table 15 - Total Plastic Strain Data for Extruded Section Subsequently Cold Rolled
11
NIMONIC ® alloy 90
Fatigue Properties
Fatigue properties for NIMONIC alloy 90 have been stressing with varying mean stress. The abscissae represent
determined on extruded bar subsequently hot rolled (tensile- the mean stress and the ordinate fluctuating stress. Thus a
compressive and rotating bend) and cold rolled sheet point on the horizontal axis represents the steady stress
(alternating direct stress). which will produce fracture in a specific time in a normal
creep rupture test. A point on the vertical axis indicates the
fluctuating stress required to produce a pure fatigue failure
Gerber Diagrams
in the same time at the particular testing frequency adopted.
Figures 10 to 12 illustrate the fatigue properties of The lines radiating from the origin correspond to stress
NIMONIC alloy 90 extruded bar subsequently hot rolled conditions of the form P ± CP where P is the steady stress
(heat treatment 8 h/1080°C(1976°F)/AC+16 h/700°C and C is a constant for any line. The full lines join points
(1292°F)/AC) at 600°C(1112°F), 815°C(1499°F) and corresponding to lines of 100, 300 and 1000 hours for
870°C(1598°F) respectively, under conditions of uniaxial varying stress conditions.
12
NIMONIC ® alloy 90
O±P
Semi-range of alternating stress, MPa
600
P
P±
400
½P
P±
200
P±O
0
0 200 400 600 800 1000
Mean tensile stress, MPa
250
150
½P
P±
100
3 P
P± 8
P±¼P
Figure 11. Fatigue properties at 815°C
50 (1499°F) for extruded bar subsequently hot
rolled.
13
NIMONIC ® alloy 90
250
Figure 12. Fatigue properties at 870°C
(1598°F) for extruded bar subsequently hot
O±P
rolled.
100 h, 12 x 106 cycles
Heat treatment 8 h/1080°C(1976°F)/AC+16 300 h, 36 x 106 cycles
h/700°C(1292°F)/AC 200 1000 h, 120 x 106 cycles
½P
100 P±
3 P
P± 8
P±¼P
50
P±O
0
0 50 100 150 200 250
Table 18 - Rotating Bend Fatigue Properties of Extruded Bar Subsequently Hot Rolled
Table 19 - Alternating Direct Stress Fatigue Properties (Mean Stress Zero) for Cold Rolled Sheet
14
NIMONIC ® alloy 90
Impact Data
The room temperature Charpy impact strength for
NIMONIC alloy 90 extruded bar subsequently forged and
given the heat treatment 8 h/1080°C(1976°F)/AC+16
h/700°C (1292°F)/AC is of the order 78J (57 ft•lbf).
Long term embrittlement of this alloy has been
investigated by Charpy impact testing at room and elevated
temperatures and the results of duplicate tests are given in
Tables 20 and 21 respectively.
Charpy test specimens have square cross section of 10
mm, test area of 80 mm2 and V-notch angle of 45°.
Soaking Temperature
Soaking Time,
h 700°C / 1292°F 750°C / 1382°F 800°C / 1472°F 850°C / 1562°F 900°C / 1652°F
J ft•lbf J ft•lbf J ft•lbf J ft•lbf J ft•lbf
30 60:61 / 44:45 49:49 / 36:36 46:47 / 34:35 54:57 / 40:42 76:64 / 56:47
100 60:53 / 44:39 46:45 / 34:33 43:43 / 32:32 54:47 / 40:35 65:64 / 48:47
300 42:39 / 31:29 42:42 / 31:31 45:45 / 33:33 53:47 / 39:35 61:60 / 45:44
1000 34:32 / 25:24 31:34 / 23:25 41:39 / 30:29 50:42 / 37:31 53:50 / 39:37
3000 29:29 / 21:21 32:31 / 24:23 37:41 / 27:30 43:49 / 32:36 43:41 / 32:30
10000 27:52 / 20:38 32:27 / 24:20 37:35 / 27:26 35:27 / 26:20 35:29 / 26:21
15
NIMONIC ® alloy 90
Soaking Temperature
Soaking Time,
h 700°C / 1292°F 750°C / 1382°F 800°C / 1472°F 850°C / 1562°F 900°C / 1652°F
J ft•lbf J ft•lbf J ft•lbf J ft•lbf J ft•lbf
30 62:64 / 46:47 50:57 / 37:42 56:72 / 41:53 57:58 / 42:43 76:75 / 56:55
100 52:58 / 38:43 46:49 / 34:36 53:65 / 39:48 56:60 / 41:44 64:66 / 47:49
300 43:46 / 32:34 46:43 / 34:32 43:43 / 32:32 52:49 / 38:36 54 / 40
1000 38:41 / 28:30 37:38 / 27:28 52:49 / 38:36 48:50 / 35:37 52:43 / 38:32
3000 31:34 / 23:25 27:30 / 20:22 35:37 / 26:27 37:41 / 27:30 37:39 / 27:29
10000 27:26 / 20:20 29:30 / 21:22 30:30 / 22:22 29:29 / 21:21 29:27 / 21:20
16
NIMONIC ® alloy 90
Cold Working
Intermittent Heating (cooling to room
Average mechanical properties pertinent to cold forming
temperature every 24 hours)
operations for 0.6-2.0 mm thick sheet annealed 2-3
Descaled Weight loss (mg/cm2) after 100 hours at min/1150°C(2102°F)/FBQ are:
800°C 900°C 950°C 1000°C 1100°C 0.1% proof stress 434 MPa (63 ksi)
– 3.02 8.12 8.18 17.7 0.2% proof stress 461 MPa (67 ksi)
0.5% proof stress 484 MPa (70 ksi)
Tensile strength 865 MPa (125 ksi)
Elongation on 50 mm 50.0%
Cyclic Heating (15 min in furnace, 5 min
Hardness 243 HV
outside)
Mean grain size ASTM 6.0
Tem- Time to Onset Rate of Weight change Erichsen value* 11.7 mm
perature of spalling spalling in 1000 h Typical plastic anisotrophy 0.95
°C h mg/cm2/h mg/cm2 R value**
890 >1000 – +2.95 Shear strength 613 MPa (89 ksi)
910 >1000 – +5.52 Ratio of shear to 0.71
990 250 0.304 -214 tensile strength
1010 200 0.458 -332 * Tests carried out on a Roell and Korthaus B.P. 512 machine using 0.03
1090 100 1.040 -880 mm polyethylene sheet lubricant (BS 3855:1965).
1110 75 1.268 -1107 ** Mean value of a plastic anisotrophy ratio R for tests at 0°, 45° and 90°
to the final rolling direction using the formula R= ¼ (R0° + 2R45° +
R90°).
17
NIMONIC ® alloy 90
Rod, Bar, Wire and Forging Stock - BS HR2, HR501, HR502 and HR503; SAE AMS 5829; AECMA PrEN 2295, 2296,
2297, 2400, 2401, 2669 and 2670.
The data contained in this publication is for informational purposes only and may be revised at any time without prior notice. The data is believed to be accurate and reliable, but
Special Metals makes no representation or warranty of any kind (express or implied) and assumes no liability with respect to the accuracy or completeness of the information
contained herein. Although the data is believed to be representative of the product, the actual characteristics or performance of the product may vary from what is shown in this
publication. Nothing contained in this publication should be construed as guaranteeing the product for a particular use or application.
18
The Special Metals Corporation
trademarks include:
BRIGHTRAY® NILO®
CORRONEL® NILOMAG®
DEPOLARIZED® NIMONIC®
DURANICKEL® NIOTHERM®
FERRY® NI-ROD®
INCOBAR® NI-SPAN-C®
INCOCLAD® RESISTOHM®
INCO-CORED® UDIMAR®
INCOFLUX® UDIMET®
INCOLOY® 601GC®
INCONEL® 625LCF®
INCOTEST® 718SPF™
INCOTHERM® 725NDUR®
INCO-WELD® 800HT®
KOTHERM® 956HT™
MONEL®
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