CONFIDENTIAL

**Use caution when handling Sulfide solutions, always wear gloves and protective eye
wear**

**Use caution when handling SAOB (2 M KOH, Highly Caustic) always wear gloves and
protective eye wear**

Part# 2010429 Title: LP2010429 Revision: B

Description: Sulfide Calibration Solution, 100 ppm, in 50% SAOB

1.0 Formulation:

1.1 100 mg/lt Sulfide Ion

1.2 50% volume/volume SAOB solution.

2.0 Materials:

2.1 100 ± 0.1 ml of 1000 ppm Sulfide Stock Solution (PN 2010437)
2.2 500 ± 5 ml SAOB solution (PN 2010438)
2.3 500 ml Distilled water
2.4 100 ml volumetric flask ± 0.2 ml
2.5 500 ml graduated cylinder
2.6 1 liter plastic volumetric flask
2.7 Magnetic stir plate and stir bar
2.8 (2) 500 ml Nalgene Plastic bottles (PN 9520004)
2.9 (2) Avery Labels 5164.

Teledyne Analytical Instruments – PO Box 121744, Z -19 SAIF Zone, Sharjah, UAE. PH# +971506345537
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 3.0 Procedure:

3.1 Open a new Lot # in the Laboratory Logbook, the Lot# will be the SO# or the WO# if no SO# is
available.
3.2 Record the chemical supplier, name, grade, Lot # and amount for each of the chemicals used,
example, Spectrum KCl, AR grade, Lot AE45321, 100.5 gm
3.3 Add 500 ± 5 ml of SAOB to the flask.
3.4 Add 100 ± 0.2 ml of the 1000 ppm Sulfide solution to the flask.
3.5 Add distilled water to the 1000 ml mark on the flask.
3.6 Add stir bar and stir for 5 minutes..

4.0 Verification and Release:

4.1 Using a calibrated Sulfide Ion Sensor, verify that the solution is 100 ± 1 ppm.
4.2 Adjust up with the 1000 ppm stock solution and down with a 50% mixture of SAOB and distilled
water.
4.3 Record the measured value and any adjustments in the logbook.
4.4 Pour the solution into the bottles and seal the bottles.
4.5 Print label with Lot# and expiration date, 1 month from the date of manufacture.
4.6 Place label slightly above the center of the bottle and level.
4.7 Release to manufacturing.

Revision
Revision ECR# Description Approval
Rev.A Rupert Original Document Aug 19, 2013
Rev.B Rupert 50% SAOB from 25% June 22, 2016

Teledyne Analytical Instruments – PO Box 121744, Z -19 SAIF Zone, Sharjah, UAE. PH# +971506345537
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