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1
This test method is under the jurisdiction of Committee D-2 on Petroleum A 5 weight of the evaporating dish, g
Products and Lubricants and is the direct responsibility of Subcommittee D0.04 on B 5 weight of the evaporating dish plus residue, g,
C4 Hydrocarbons. S 5 volume of the liquid butadiene sample, mL, and
Current edition approved Nov. 10, 1996. Published January 1997. Originally d 5 density of the sample at the temperature of
published as D 1025 – 49 T. Last previous edition D 1025 – 91.
2
This test method is an adaptation of one developed and cooperatively tested by measurement, g/mL, found by using Table 1.
the Butadiene Producer’s Committee on Specifications and Methods of Analysis of 8. Precision and Bias
the Office of Rubber Reserve. It appears in the Butadiene Laboratory Manual, Office
of Rubber Reserve, as Method No. 2.1.56.2. 8.1 Precision—The precision of this test method as
1
D 1025
TABLE 1 Density of Butadiene at Various Temperatures the test method, exceed the following values in only one case
NOTE 1—These data may be used in a graphical manner for better in twenty:
interpolation between data points. 0.02 % (2)
Temperature, °C Density, g/mL
8.1.2 Reproducibility—The difference between two single
−45 0.6958
−40 0.6903 and independent results obtained by different operators
−35 0.6848 working in different laboratories on identical test material
−30 0.6793
−25 0.6737
would, in the long run, in the normal and correct operation of
−20 0.6681 the test method, exceed the following values in only 1 case in
−15 0.6625 twenty:
−10 0.6568
−5 0.6510 0.04 % (3)
0 0.6452
8.1.3 Bias—Since there is no accepted reference material
suitable for determining the bias for the procedure in this test
determined by statistical examination of interlaboratory results method for measuring non-volatile residue, no statement on
is as follows: bias is being made.
8.1.1 Repeatability—The difference between two test
results obtained by the same operator with the same apparatus
9. Keywords
under constant operating conditions on identical test material
would, in the long run, in the normal and correctoperation of 9.1 butadiene; nonvolatile residue
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