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Cementing Handbook-George Suman PDF
Cementing Handbook-George Suman PDF
BY
GEORGE o. SUMAN, JR. .AND RICHARD C. ELLIS
Acknowledgment
This handbook is the result of a comprehensive
study of cementing oil and gas wells including cas-
ing handling procedures. The authors' basic work
was sponsored by AMF Tubescope, Inc.; Bakerline,
a division of Baker International Corp.; Dowell
Schlumberger; Oil Tool Division, PENGO Industries,
Inc.; Lynes, Inc.; Texas Iron Works, Inc., and Varco
International, Inc. The authors wish to express their
appreciation to these companies for their sponsor-
ship and for the complete freedom allowed in
preparation of all material. Thanks are also due
the sponsors and many other manufacturers for
providing information and illustrations, and to those
in industry who reviewed the manuscript and con-
tributed many helpful suggestions.
Copyright@ 1977
All rights reserved
U
CEMENT measured with the test apparatus shown in Fig. 1(A) .
SLURRY
;':'
f;~i;
:::
~}--
::,:';: PRESSURE
In this test where the surface in question is the outer
>':;~: ;\..=~.
periphery of the inside pipe, the ability of cement to
A B ':':\~ "~',::j: support axial casing loads was found to be proportional
'" '_.. n..... . .'
SHEAR BOND HYDRAULIC BOND to the area of contact between cement and the casing.
PRESSURE
Therefore, support coefficient,2 shear bond3 or sliding re-
'.'.. .;
m
".'
.';.
.... ..
,.. . sistance,4 as it is described by various investigators, is the
. ..
,.:..:
.-"
0-' 0
.
I
.'\':
'.',.
load required to break the bond, divided by the surface
".. ."
':j ~~';
. area between cement and pipe.
:";
~:.
"
I
;i~
. '.
Shear bond strength increases with cement tensile or
compressive strength as shown in Fig. 2.2 A fairly narrow
range of shear bond at a given tensile strength resulted
for various cement compostions tested. And a significant
CEMENT reduction in shear bond was caused by mud wetting of
the pipe. Poorest results were obtained when the pipe was
mud-wetted and no attempt was made to remove the mud
film.
/ 1f7
~U'..
-
,,,............
.. ~....
"
. Raw cement characteristics, such as fineness of grind, 0'
m
may also affect shear bond strength ".......................
..
~I
. Cement contamination by mud which lowers shear
wt
J:; '", .
en
bond appreciably, see Fig. 3. ..
. Displacement mechanics and efficiency which affect
thickness and continuity of the cement sheath around
0=,
the casing, and 0.2 0.4 0.6 0.8 5 10 15 20
WATER/CEMENTRATIO VOLUME MUD, %
. Pressure/temperature effects which can contract the
casing diameter after the cement hardens. This factor
will be discussed in a later article. Fig. 3-Water content and mud contamination lower shear
bond strength. Absolute value of shear bond is not shown
but the scale is linear so that percent change can be esti-
ZONE ISOLATION mated (after Becker and Petersen)'.
Although cement with a low compressive strength may
smaller in diameter and "pull away" from the cement,
be adequate to handle axial and rotational casing loads,
forming a micro-annulus which permits leakage.
high ultimate strength may be required for zone isola-
Hydraulic bond strength in the test shown in Fig. 1(B)
tion and to support the borehole. Therefore, cement
ranges from 100 to 1,200 psi for water and from 45 to
compositions should be selected which quickly provide
450+ psi for gas (nitrogen) depending on roughness of
adequate compressive strength for continued drilling
the exterior pipe surface and type of mud wetting, see
operations but which also provide adequate strength,
below. No fixed correlation between cement compressive
ultimately, for production operations.
strength and hydraulic bond was found.
A comprehensive study of factors governing zone isola-
tion under downhole conditions would be very complex. Hydraulic bond YS. casing surface and
Zone isolation depends, in part, on load interactions be- type of fluid wetting3,6
tween formation, cement and casing, some of which are
not well understood. Further difficulty arises in deter- Type
mud -
Hydraulic bond (psi)
mining type and magnitude of loads imposed by fluid Surface finish wetting Water Gas
injection pressures and temperatures, and production pres- New mill-varnished."" , '" " . None 200-250
Varnishremoved(chemical).. . . None 300-400
sure drawdown and depletion. Varnishremoved(sand-blasl).... None 500-700 150
Varnishremoved(sand-blast)... . Fresh water 100 50
For these reasons, only qualitative judgements have Varnishremoved(sand-blast).... Invert oil emulsion 100 50
Varnishremoved (sand-blast).... Oilbase 100 50
been attempted in studies to date and these usually relate
to the "hydraulic bond" which indicates adhesion between Resin-sandcoat (new,sand blast) None 1,100-1,200 450
Resin-sandcoat (new, sand blat) Fresh water 100 55
casing and cement, or between cement and formation. Resin-sandcoat (new, sand biast) Invert oil emulsion 100 45
Resin-sandcoat (new,sand blast) Oilbase ICO 45
The actual relationship between hydraulic bond mea-
sured in the lab, and downhole zone isolation has not Cement: API Class A
Water Content: 5.2 galjsk
been reported, if such a determination has been made. Curing temperature: 80°F
Curing time: 24 hours
Casing size: 2" inside 4"
Bonding test. Various investigators3,5,6 have measured
hydraulic bond. Test arrangements are shown in Fig. Hydraulic bond strength is improved by resin-sand
1(B) .3,6 and Fig. 1(C) 5 Pressure is applied to the exterior coatings, as shown above, only when there is no mud
surface of the casing causing the casing to become wetting. Such coatings consist of graded sand bonded by
~ MUD
ONLY
shoe upwards 200. to 400 feet (or 10.% of casing length) .
Elevate compressive and shear bond strength of the ce-
ment around lower joints by decreasing water-to-cement
ratio (increasing density) of last portion of slurry, Fig. 3.
5. Use two plugs. Without a bottom plug, mud film
from the inside casing wall can accumulate beneath the
top plug and be deposited in and around the shoe joints/a
Fig. 7. Fill-up for various film thicknesses can be signifi-
cant, for example: For 10,000 feet of 5~-inch casing,
1/16, 1/32 and 1/64-inch thick films would fill 510, 260.
and 130 feet, respectively.
FAULT SLIPPAGE Even when a top plug is used, accurate displacement
calculations should be made to avoid over-displacement
and mud or water contamination around the shoe.
Fig. 6-Cement sheath effects with formation loading. Strong, 6. Release surface pressure following cement placement
well centralized cement sheath, top, can prevent flattening
effect of salt flows in washed out holes (Cheatham and to minimize chance for a micro-annulus to form between
McEver)". But In fault slippage zones, bottom, cement sheath casing and cement. However, surface pressure is some-
may cause more damage by holding pipe rigid through shear times used as an aspect of casing landing operation to
zone.
prevent casing instability and buckling conditions.21
7. Do not disturb casing until cement has obtained
initial set-about three times thickening time. Keep drill
TOP PLUG
CEMENT SLURRY pipe out of the hole until after this time. The cement
composition should have minimum 500 psi compressive
MUD FILM strength (some say 1,000 psi) at time of drilling-out.
CASING - - --- 8. Control rotary speed while drilling cement out of
casing, as indicated in Fig. 8. But if the casing joints have
been improperly strengthened, i.e. misapplied thread lock-
1--'
-- - ~MUD CEMENT ing compound or welded J-55 or higher grade casing,
---- I
SLURRY
MUDACCUMULATION permissible rotary speed may be only one-tenth or less
FROMFILM of values shown.
Fig. 10-Defects rolled into the pipe wall at the mill. Photo
Obtaining an effective casing/cement installation re-
A shows pits left by mill slugs that penetrate 0.210 inch quires proper inspection, care and handling, and make-up
into a 0.337-inch wall. Photo B shows the hole left by a of the casing itself. Without such treatment, even prop-
broken-out metal fold (lamination) that was rolled into the wall erly designed casing may fail. Texter30 and Casner,31
but did not fuse. Photo C is another example of pitting caused
by removal of foreign material rolled into the outer surface. and others, have identified a variety of potential casing
failures such mill defects, mishandling, borehole doglegs
,"* ;~,->c."'*.ra;,.:~~~>""""".. and corrosion. From such information, API has developed
recommended practices for the care and use of casing32
and has defined the principal causes of trouble in other-
wise properly designed casing strings, see below.
LITERATURE CITED
'Farrisl R. F. "Method for Determining Minimum Waiting-on-Cement 11Suman, G. O. Jr., "World Oil's Sand Control Handbook," Gulf Publishing
Time,' Trans. AIME (1946), 165, pp. 175-168. Co. (1975).
, Bearden, W. G. and Lane, R. D. "Engineered Cementing Operations 18Suman, G. O. Jr.\.. "CasinR Buckling in ProducinJt Intervals," Petroleum
to Elimmate WOC Time," API Drilling and Production Practice (1961), Engineer, (April 19/4), p. 36.
l' 17. .. Schuh, F. J., "Failures in The Bottom Joints of Surface and Intermediate
, Evans, G. W. and Carter, L. G., "Bonding Studies of Cementing Casing Strings," Journal of Petroleum Technol0y,y, January 1968, PI'. 93-1\)1.
Compositions to Pipe and Formations," API Drilling and Production '0 Owsley, W. D., "Improved Casing Cementing, , The Oil and Gas Journal,
Practice (1962), p. 72. Dec. 15, 1949.
· Becker, iI. and Peterson G., "Bond of Cement Compositionsfor "Dellinger, T. B. and McLean, J. C., "Preventing Instability in Partially-
Cementing Wells," Proc..::,]..
Sixth World Petroleum Congress, Frankfurt, Cementea Intermediate Casing Strings," SPE Paper 4606 !,resented at 48th
Germany, June 10-26, T~3. Annual Fall MeetinJI SPE of AIME, Las Vegas, Sep. 36-Oct. 3, 1973.
· Bearden, W. G., Spurlock", J. W. and Howard, G. C., "Control and " Dalrymple, D. H. Personal Communication.
Prevention of Inter-Zonal ~Iow," Journal of Petroleum Technology (May " Calvey, H. J., "Casing Designs and Programs Considered in the Anadarko
1965), pp. 579-584. Basin," Paper SPE 3909, 1972 Deep Drilling Symposium, Amarillo, Sept.
· Evans
b
G. and Carter, G., "New Technique for Improving Cement Bond," 11-12, 1972.
"Evans, G. W, and Harriman D. W., "Laboratory Tests on Collapse Re-
API rilling and Production Practice (1964), PI'. 33-38.
1 Scott, J. B. and Brace R. L., Coated Casing-A Technique for Improved sistance of Cemented Casing,'! SPE Paper 4088, 47th Annual Fall Meeting,
Cement Bonding," APi DrillinK and Production Practice (1,966). PI'. 43-47. San Antonio, Oct. 8-11, 1972.
8 Ferd W. H., Pilkington P. E. and Scott, J. B., "A Look at Cement soHelmick, W. E. and Longley, A. J., "Pressure Differential Sticking of
Bond Logs," Journal of Petroleum Technology, June 1974, PI'. 607-61'7. Drill Pipe and How It Can Be Avoided or Relieved," API Drilling and
· Oliphant, S C. and Farris, R. F., "A Study of Some Factors Affecting Produc/lon Practice (1957), PI'. 55-61.
Gun Perforating," Trans. AI ME (1947), 170, PI'. 225-242. 26Outmans, H. D., "lVlcchanics of Differential Pressure Sticking of Drill
I. Morgan, B. E. and Dumbald, G. K;, "A Modified Low-Strength Cement," Collars," Trans. AIME (1'958), 213, PI'. 265-274.
Trans. AIME (1951'), 192, PI'. 165-1/0. "Outmans, H. D., "Spot Fluid QUIckly to Free Differentially Stuck Pipe,"
11Godfrey, W. K., "Effect of Jet Perforating on Bond Strength of Cement," The Oil and Gas Journal, July 15, 1974, PI'. 65-68.
Journal of Petroleum Technology (November 1968), PI'. 1301'-1314. ,. Barkis, B., "Primary Cementing, the Critical Period." B&W Publication.
12Ben, W. T. and Shore, J. B., "CasinK Damage from Gun Perforators," 29Annis, lvl. R. and Mona~han, P. H., "Differential Pressure Sticking-
API Drilling and Production Practice (1964), PI'. 7-14. Laboratory Studies of Friction Between Steel and Mud Filter Cake," Journal
"Godfrey, W. K. and Methven, N. E., "Casing Damage Caused by Jet of Petroleum Technology, May 1962, PI'. 537-543.
Perforating," Paper SpE 3043, 45th Annual Fall Meeting, Houston, Oct. 30'texter, H. G., "Oil-Well Casing and Tubing Troubles," API Driling and
4-;, 1970. Production Practice (1955), p. 7.
.. Cheatham, Jr., ". B. and McEver, J. W'l" "Behavior of Casing Subjected " Casner, J. A., "Care and lIandin/( of High-Stren/(th Tuhular Goods," API
to Salt Loading,_' Trans. AIME (1%4), 231, 1'1'. 1069-1075. Drilling and Production Practice (1196'r), PI'. 169-1'76.
ISMcCauley, T. V. "PlanninJI Workovers in Wells witlt Fault-Damaged Cas- ::2API Recommended Practice for Care and U!"c of Casing and Tubing," API
ing_-South Pass i!1ock 27 I"ield," Journal of Petroleum Technology (July RP 5Cl, Tenth Edition, March 1975.
1974), p. 739. "Oxford, W. F., "API Southern District Tubular Goods Committee Summary
I. Roberts, D. L., "Shear Prevention in the Wilmington Field," API Drilling of Inspection for Period Jan. 1, 11963to Jan. I, 1964," Houston, March
and Production Practice (1953), p. 1'i6. 1966.
15-second summary
How electronic inspection at the mill, pipe yard or rig
site finds serious metallurgical defects. Pipe handling dis-
cussion tells why torque cOlitrol alone is inadequate for
thread make-up. Axial load in slips is explained as are
hydrostatic rig floor tests for connection leaks and
landing practices to correct for future load changes.
Descriptionof bodywall,connectionImperfections
Seam Lap Roll-Inslug Pit Gouge Crack,cut Plntt Coupllngtt
Casing
Size Ext Int Ext Int Ext Int Ext Int Ext Int Ext Int Mfg Hdg Mfg Hdg
4!h 71 11 1 23 3 32 1 2
5 3 117 41 24 31 2 11 12 5 7 4 251 4
5!h 86 10 156 4 43 6 51 6 24 3 14 23 41 37 8
7 64 99 4 46 1 6 6 3 5 12 1 57 18 18
70/8 78 1 21 2 14 1 10 5 2 3 6 23 34 1
90/8 162 3 60 2 53 9 1 10 1 10 55 94 49 22
10% 14 2 20 1 2 9 13
11%
130/8 1 1 1 17 5
16 .. .. 1
20 2 .. 1
* Source: AMFTuboscop,ereports to several operators on new casinginspection in various yard and field locations, 1975/1976.
** SeeAPI definitionof 'imperfection"and"defect" in text.
t Includes1-3 lengths of wronggrade or wrongweiht.
tt Analysisof connectiondamage by manufactureror 10handling.
\c ~!:tTW~,,~~RE~D
I TURNS OK
torque. 51 And when API conducted tests that measured
torque required to make up API 8 round threaded con-
nections lubricated with API Modified thread compound,
POWERTIGHT BEARING PRESSURE HANDTlGHT it was found-emperically-that these torque values were
MAKEUP API ROUND THREAD about 1% of the calculated pullout strength.
Therefore, the recommended torque values listed in
MAKE-UP
API RP 5CI are calculated from the following relation:
<J OPPOSITE ANYiPART TRIANGLE STAMP[>
!
I
/ OF STAMP OK , Torque (ft. lbs.) = 0.01 Minimum joint strength (lbs.).
I
I
API RP 5C1 further states that torque W8.'Sselected to
HANDTIGHT give optimum make-up of API 8 round connections under
BUTTRESS THREAD normal conditions and should be considered satisfactory
only if the face of the coupling is within plus or minus
Fig. 19-Thread configuration and basic make-up positions of two thread turns of the last thread scratch (vanishing
API 8 round and Buttress threads (after API Spec 5A)." point), Fig. 19.
When using API RP 5C1 recommended make-up torque
practice of using torque alone as the means for make-up tables, use API Modified thread compound and observe
control was never intended by API. the make-up position of each connection.
The two most important factors that influence leak For Buttress threads, API recommends:
resistance of threaded pipe joints were identified, over 30 1. Determine torque required to make-up each of sev-
years ago, as joint make-up and thread compound.43 eral connections to the proper position, then
The basic sealing principle for API 8 round threaded
2. Use that torque to make-up the balance of the same
connections, Fig. 19,46 is that contact (bearing) pressure
weight and grade pipe in the string, but
between pin and box, produced by make-up, forms sev-
eral metal-to-metal seals, and that solids from thread 3. Continually observe make-up position for verification
compound fiU the void space between the threads. These of proper make-up.
solids are required to transmit bearing pressure from one Buttress thread connections have triangles stamped on
threaded surface to the other. The connection seal is
the pin ends. Proper make-up is achieved when the cou-
maintained only as long as bearing pressure is greater pling face is opposite any portion of the triangle, Fig. 19.
than the internal or external differential pressure.
Sealing ability-as well 8.'Sthe influence on friction-of Effect of thread compounds. Torque required to prop-
different thread compounds varies greatly. Pressure tests erly make-up connections depends primarily on friction
have shown that marked variation in sealing ability exists between pin and box threads. For clean, damage-free
between different brands of API Modified thread com- threads, make-up torque is significantly affected by type
pounds as well as with specialty compounds.46 of thread compound. Use of different compounds can
cause make-up torque variations of up to 500%.52
Non-API connections. Several different types of non- Such large variations indicate that, to establish maxi-
API tubular connections are commonly U'sed. Descriptions mum bearing pressure between pin and box mating sur-
of these have been reported in the literature,48 and latest faces-and not risk overstressing pin or box-a more accu-
data on premium thread designs are available from manu- rate means of measuring make-up (than torque alone) is
facturers or COMPOSITECATALOG. required. Two methods for making such measurements
Such connections employ several different basic types will be discussed.
of thread designs. They can have both shouldering and An API subcommittee is currently reviewing thread
non-shouldering connections with "metal-to-metal" seals, compound standards, attempting to develop more precise
while other connections rely on a 'Supplementary, resilient standards for friction and leak resistance performance.
Teflon seal. Careful selection of compounds for each set of condi-
Obtaining a pressure seal in connections that rely on tions, on the basis of friction and leak resistance charac-
metal-to-metal sealing requires make-up, to force the pin teristics, is encouraged. These characteristics should be
and box mating surfaces together. clarified by discussions with both pipe and Iu b r i can t
Theoretically, the pin should be stressed to about the manufacturers.
yield point to obtain maximum leak resistance. This keeps
the connection in the ela:stic stress range and produces the Make-up control (Torque-Turn). During 1963, the
API Southern District Tubular Goods Committee con-
maximum amount of bearing pressure between mating
surfaces for leak resistance.49.5o A precise make-up pro- ducted a survey of tubular string failures.33 This survey
cedure is required to achieve these maximum leak resis- (still the only comprehensive study published) showed
tance conditions. that 86% of reported casing failures occurred in connec-
tions.
API torque recommendations. Although it was never In 1967, Exxon began licensing its newly developed
intended, development of power tongs made it very con- Torque-Turn make-up control device, 47.49.52 an auto-
venient to use torque as the only guide for make-up mated make-up monitoring system for API type connec-
control. However, variations in thread design, surface tions that cross-checks torque with turns (make-up posi-
finish, thread compounds and the size, weight and grade tion) to determine connection acceptability.
of pipe all interact and influence make-up torque. Make-up control with this system involves pre-setting
A new make-up control system recently developed Fig. 2D-New make-up control system uses controlled-power
unit, left, to run ring and plug gages to "hand-tight" positions
by AMF Tuboscope provides a method to evaluate the to check pin and box thread quality. Reference marks, right,
condition of pin and box threads before casing is run then are applied to pin and box, and make-up position is
into the well, and measure connection make-up. 53 verified on the rig floor using calibrated window in special
card, right (courtesy AMF Tuboscope).
To apply AMF's Torque at Proper Engagement
(TAPE) control system, protectors are removed and
threads are cleaned. Then, API ring and plug gages P,
are run on both threads to the hand-tight plane using I
I
a power driven tool with controlled torque, Fig. 20. The r
location of the gage on the threads is checked per API
Standard 5B.
t
Q.
I
I
I
I
I
I
P (EXTERNAL) CASING OD
.. -c'
ui I
Torque reference marks are inscribed around pipe a: I
::> Ie
en
circumference and coupling if the relative position of the en
w :I) _____
I
hand tight plane agrees with API. Thread compound a: I """;'~"_.
-, ,.. ,-,.-"",
:
I
B(BEARING PRESS.
AT SEAL POINT) . T (PIN)
I P(INTERNAL)
specified torque load and the distance between pipe and
coupling reference marks is checked with a special gage
card on which the mark shows in an "acceptance
window" when proper make-up position is achieved, Fig. Fig. 21-Energizing effect of pressure applied across a con-
20. nection. On the curve representing the thin-pin, thick-box
connection in the drawing, B, is initial bearing pressure from
Torque is recorded on a chart and used to verify make-up in the metal-metal inner seal, PE and p, are theoreti-
proper thread engagement and make-up. This new cal external or internal pressures required to initiate a leak at
the seal, and e is a function of connection geometry. When
development will be available initially in California. thicknesses are nearly equal, as in API connections, e ap-
proaches zero and the energizing effect of pressure in either
RIG FLOOR LEAK TESTS direction is not significant.
Hydrostatic testing of casing connections on the rig
floor is a technique used to prove leak resistance of con- tion of the differential pressure and connection geometry,
nections. Tools are currently available that provide for Fig. 21.
internal testing of up to 8%-inch casing, and external External testing, for example, can be more effective in
testing of up to 16-inch casing. detecting leaks in premium type connections that have
Hydrostatic tests have been proven capable of detect-
a metal-to-metal seal surface at or near the tip of the pin.
ing (on the surface) connections that will leak under
Insufficient make-up (position-wise) due to damaged or
pressure. Such a detectable leak could easily result in a defective threads or seal surfaces can result in low
casing leak downhole.
initial bearing pressure even with apparently adequate
There are advantages and disadvantages of both in-
torque. In such connections, the metal is much thinner
ternal and external testing, for example: The small fluid in the pin than in the collar, at the sealing point. There-
volume used in external testing increases sensitivity and fore, higher internal pressure "energizes" the otherwise
shortens test time; however, visual inspection of a leaking
insufficient seal by expanding the pin into the box, in-
connection is not possible with external testing. Also, the creasing bearing pressure. Conversely, increase in external
internal system can test the entire joint.
pressure has very little energizing effect on the seal, Fig.
Connection geometry has a significant effect on 21. In this thin-pin, thick-collar situation, a lower ex-
whether a connection is more subject to leaking due to ternal pressure would detect the problem.
high internal or high external pressures. To prevent
leakage, connection bearing pressure must exceed pressure Test procedures. For API, non-premium connections,
differential from either direction. But the same pressure in which pin and collar thickness difference is less sig-
differential, in turn, has an "energizing" effect on the nificant, test procedures used may be of more importance
bearing pressure that can alter the true leak resistance of than the test method, internal or external.
the connection. And this effect varies greatly with direc- The length of time that test pressure is held on the
---- - -----------
10 5,'
API CLASS
8 AS NOTED CLASS A
4
00
a:
J: 3
W
:2
2
i=
Q
:E
I-
2
-14QOF
180°F
o I I
40 60 80 140 160 180 o 2 3 4 5
Fig. 23-Effect of temperature and pressure on thickening time of Portland cement. At atmospheric pressure, left, thickening
time is reduced by high temperature. At constant temperature, right, thickening time is reduced by pressure (after Bearden)..'
tions by service companies, if the published API schedules However, as was discussed in Part 1, high cement strength
are not applicable. is not always required.
Note: These measurements are made in metal vessels Bentonite has for years been the most commonly used
which prevent any fluid loss. Thickening time values additive for "filler" type cement.65 In addition to its
determined are therefore higher than they might be oppo- effect on density, yield and cost, bentonite increases vis-
site a permeable zone, after partial dehydration. cosity and gel strength, which reduces settling of high
Slurry density may be reduced with extenders such as density particles (weight material, cement) or floating
bentonite, pozzolan, diatomaceous earth and anhydrous of low density particles (Perlites, pozzolan, gilsonite,
sodium meta-silicate. Gilsonite and crushed coal also crushed coal).
reduce density. And special calcined shale--cement (such Bentonite al:;o reduces API fluid loss. However, cements
as Trinity Lite-Wate or Texas Industries Light Weight) containing bentonite are more permeable and have low-
are used for this purpose. ered sulfate resistance.
Low density is frequently desired, to decrease likelihood Pozzolans increase slurry viscosity and provide low
of breaking-down the formation and causing lost circula- permeability. Sodium meta-silicate provides a very low-
tion. In addition, such slurries cost less per cubic foot, as density slurry with early compressive strength; this mate-
yield per sack is increased. rial and calcined shale-cement are becoming popular,
Density decrease results in large part from increased particularly offshore. The latter is a special cement, not
water content. Extenders permit water addition without an extender, as mentioned earlier.
separation. However, cement strength is reduced approxi- Light-weight cements are listed in the accompanying
mately in proportion to water content increase, Fig. 22. table which separates slurry compositions providing more
25
WORLD OIL 1977
A density of 22 ppg can be obtained with hematite or
:2 25 ~ 1% ORGANICDISP. ADDED ilmenite plus friction reducing additives. Fine barite (325
Il.
(XI
c::::::J WITHOUT DISPERSANT mesh grind used in mud) requires a large amount of
ui
I- water, which reduces compressive strength and retards
«a: thickening time, and therefore is rarely used.
3i: A slurry weighted with solids must have viscosity and
o..J gel strength needed to carry and suspend high specific
U. gravity solids. And it should be noted that some additives
..J tend to significantly thin or thicken a slurry (fluid loss
«
o agents, retarders, water content)_
i=
a:
o
Pretesting of such high density slurries should include
o density, thickening time, compressive strength, settling,
CLASS CLASS 50/50
free water and viscosity measurements.
A E POZ
High density (up to 17.5 ppg) may be obtained by
adding dispersant to the slurry to provide pumpability at
Fig. 24-How dispersants reduce yield point to allow turbulent
flow at reduced pump rates in a 5V2-inch casing by 7\18-inch lower than normal water/cement ratios. This approach is
wellbore annulus."" most expensive, but results in highest compressive
strength. Cement densified in this manner also may need
than, and less than, 500 psi compressive strength.66 The an additive to reduce filtrate loss because further reduc-
lowest-weight slurries providing more than 500 psi com- tion in water content may make the slurry unpumpable.
pressive strength are Class C cement with gel, and Also, densification tends to accelerate curing time.
Class C cement with silicate.
Friction reduction. Dispersants can also be used to reduce
Common light weight cements
the yield point (consistency index) of the slurry, which
Density, ppg, for reduces friction and allows turbulence to occur at reduced
Extender, % by wt. cement compo strength:
1-.-.--.-.-.-
Sodium pump rates, Fig. 24. Common dispersants are: Alkyl aryl
Type cement Gel Salt
-1-1-1--1-1-
meta-
I sll. I
Water I Dlacel
D I Above
500psi SOD
psi I
Below sulfona~e, polyphosphate, lignosulfonate, salt and organic
acid.
Gel
Class H ..... 4 14.1 Turbulent flow additives tend to cause settling and
8 13.1
12 excessive free water. These effects should be tested in the
16
Class C" . .. . . . . . . . . . 4 '13".i lab prior to field use.
8 12.5
12
Prehydrated gel. . . .. . 1.5. 'l,i.2
2.0. 13.7 Fluid 1055 (filtrate). Addition of fluid loss agents has
2.5. 12.8
3.0. 'l'2j important application in: P reven ting gas leakage, in
3.5. 12.1
4.0. 11.8 squeeze cementing and, occasionally, to maintain pump-
4.5. 10.7
Pozzolan and lIy ability in primary casing and liner cement jobs.
ash 50/50. . . 2 14.1
6 13.3 Fluid loss additives may also reduce likelihood of dif-
10 12.8
18 12.4 ferential pressure sticking where stuck pipe has been
Silicate...... 'i.o' '1.1.2 associated with mud cake removal. Fluid loss additives
2.0 12.5
3.0 .... might be considered when there is little or no mud cake
Calcined shale-
cement.. . . . 65 .... 13.7 on the borehole wall-for example, when drilling with
85 I I 12.8
95 water. In normal primary cementing, high fluid loss
115
Pozzolan and cement does not dehyrate significantly in permeable zones
bentonitef because filtration is controlled by the mud cake.
Class H . . . . . 6f 74 I I 13.6
6f 83 13.1 The API fluid loss test on cement is conducted at 100
6f 104 12.4
ClassC... .. .. . .. .. 6f 104 12.0
Dlacel D... ... .. .. .. . io'
20
I '13'.2
12.4
or 1,000 psi differential pressure through a 325 mesh
30 11.7 screen. 1,000 psi is used when the slurry has been elevated
40 11.0 in temperature and pressure in a consistometer in accord-
. Perc ent by weight water
.. Trin ity Lite-Wate data. Similar cement available from Texas Industries.
f 65/ 35 cement and Pozmix A, % gel based on combined weight.
ance with one of the API simulation schedules. Testing
conditions .need to be identified for the true meaning of
the data to be known. In addition, many 100 psi tests
Density may be increased with weight material such are mistakenly run on No. 50 Whatman paper instead of
as sand, barite, hematite or ilmenite, and/or salt dis- 325 mesh screen.
solved in the mix water, as shown in the following table:66 Water dehydrates almost instantly from a neat cement
Weight material for cement tested in the above manner. The 30 minute fluid loss
Max. Extra Elf. on Elf. on (100 psi) of neat Class A cement is about 1,000 ml.
Speci fie Grind density, water compo pumping
"'aterlal needed Early in 1960, significant progress was made in devel-
-- gravity - (mesh) ppg - - strength
- time
oping cement additives that lower fluid loss with a high
Jttawa sand....... 2.63 20-100 18 None None None
3arite.. . ... .. . .. .. 4.25 325 19 20% Reduce Reduce
:oarse barite. . . . . . 4.00 16-80 20 None None None molecular weight, synthetic polymer.68 Such additives
Hematite.. .. .... 5.02 40-200 20 2% None None
Ilmenite..... . 4.45 30-200 20 None None None may provide fluid loss in a low range. These additives
Dispersant..... ... .... ...... 17.5 None Increase Increase
Salt..... ...... ... ...... 18 . .. Reduce Varies usually are affected by temperature, Fig. 25. Generally,
thickening time is retarded and, at low temperature, this
or slurry loss to fractured, permeable formations. Assuming that ATMOS 2,000 4,000 6,600 '8:000
frac pressure exceeds reservoir pressure, high filtrate loss cements
(such as untreated thixotropic or neat) can dehydrate and bridge CURING PRESS., PSI
within such fractures, thus blocking further fluid loss. . -- - --- - - -. ..
2. Neat or low density cements. As discussed above, neat and Fig. 28-Effect of curing pressure and temperature on com-
thixotropic cements have high filtrate loss. However, low density pressive strength. At constant temperature, bottom, 24-hour
cements mayor may not have high filtrate loss. strength changes little above 3,000 psi. Slow set, Class C
3. Mixtures with diesel-oil. Various compositions-diesel and cement, top, shows significant strength retrogression as curing
bentonite; diesel, bentonite and cement; or diesel, bentonite and temperature increases ('curing pressures)."
SILICA
:~I
is that compressive strength changes very little above
that pres'Sure level, Fig: 28, bottom. However, at high tem-
peratures (about 250-3000 F) pressure effect may be
more significant than those of Fig. 28. Tentativp data
indicates, at least, that actual well pressure should be
more closely simulated.
3 1 7 3
Recommended curing periods are 8, 12, 18, 24, 36, 48
230'F 260'F 290"F
and 72 hours, depending on job requirements (such as CURINGTIME(DAYS)I CURINGTEMPERATURE
waiting-on-cement time or strength retrogression). Usu-
ally, com pres'Si ve strength is very close to ultimate
Fig. 29-Silica flour inhibits strength retrogression at high
within three days. Early strength is increased with temperatures as indicated for Class E cement. For example,
calcium chloride, 'Sodium chloride, ammonium chlo- 20% silica increases the 2,000 psi, 7-day compressive strength
of neat cement to 12,000 psi, at 2900 F (after Ostroot).'.
ride, "minimum" water and heat. Early strength is
decreased with lignosulfonate, CMHEC and "maximum"
water. Compressive strength inf orma tion is available Silica flour in high percentages inhibits strength retro-
through service companies. gression and produces compressive strength far in excess
of neat cement, Fig. 29.79 Silica flour also reduces perme-
Strength retrogression. Four variables-composition, ability of set cement; for instance, its addition to cement
temperature, pressure and time-affect compressive cured at 3500 F reduces permeability to less than
strength.77 However, at high temperature, cement com- 0.001 md.
positions may retrogress (lose strength) after reaching a Maximum strength cccurs at 300-4000F when 30-50
high value and never attain the strength reached at lower parts of silica flour are added to 100 parts of cement.80
curing temperature; Fig. 28, top, illustrates one severe Usually 35% silica flour is used. Silica sand ground to
example. 200 mesh reacts with cement in the same way as fine
This strength retrogression is accompanied by increased ground 325 mesh silica flour. Silica sand is used when
cement permeability, i.e. a neat retarded cement with high density is desired and silica flour when low density
0.02+ md permeability at 2900 F after three days may is adequate.
have 8+ md at 3200 F after seven days.78 Compositions containing silica sand or flour can be
Retarded cement for high temperature application, retarded effectively for high temperature wells.79 Class J
and high water content cement, seem particularly subject cement does not require silica flour and can be used to
to strength retrogression (Fig. 28). For cement types about 16,000 feet without retarder-this class should not
used in deep and/or hot wells the phenomenon begins at be used at less than 2300 F.
around 2600 F, and becomes severe at 2900 F. Generally Most nonreactive additives (salt, weight materials,
complete strengt!1 retrogression has taken place within crushed coal, mica and other bulking agents) can be
seven days.78 Although remaining compressive strength admixed with a silica stabilized cement without adversely
may be adequate for many applications, addition of affecting temperature stability.80 Bentonites, diatomace-
silica flour to the slurry provides a way !o maintain ous earth and expanded perlite should not be added to
strength.79 Portland cement for use above about 2500 F in concen-
I-
I
I 50
---I
I
I
(j) 40
0..
0
0
q
'X
I-
(!J
Z
W
a:
}j) 20
w
I-
«
5 10
;:!
5 10 15 0 10
EFFECTIVE CONFINING PRESSURE, 1,000 PSI
- --- -
Fig.30-Under confining pressure, ultimate strength of cement, left, is similar to that of typical reservoir rocks, right (after
Handin).81
.
of salt cement
Osmotic pressure will causewater from sand or shale to migrate to the saltcementcausing
expansion which improves bond log..'
triaxial compression tests on various cement samples with . Clay dispersion is minimized to aid well productivity should cement filtrate loss be signifi-
cant. However, original mud cake normally prevents such filtrate loss.
independently applied external confining pressures and
internal pore pressure such as encountered downhole.81
. Salt is an accelerator in low concentrations and it retards at high concentrations, butthe
effect is neutral throughout a broad range in between, Fig. 32. This tolerance can, in
many cases, permit use of either fresh or seawater for mixing without affecting thick-
These tests show that strength increases, Fig. 30, and is ening time.
more or less comparable to rock for similar conditions.
Large variations in the standard compressive strength,
. Salt in small concentrations tends to increase early compressive strength, Fig. 32, but
has little or no effect on ultimate strength. In high concentrations, it reduces early
strength and can cut ultimate strength in half.
as measured at zero confining pressure, tend to disappear
under load; and oil well cements become very duc-
. Saturated cements minimize solution of formation salt sections.
ECCENTRIC ANNULUS
rheology, annular displacing forces.
How to avoid bypassing mud during
primary cementing DRAG FORCE, MUD
DIFFERENTIAL PRESS.
MOVING CEMENT ALSO ACTS
ON WALL (NEG.)
ON MUD (POS.)
CEMENT SLURRY
1O-second summary BUOYANCY EFFECT
OF DENSER CEMENT
Basic principles of mud and cement slurry behavior in (pOS.)
the annulus, as mud is being displaced, are explained.
Fluid design factors and guidelines for improving the dis- Fig. 33-Various forces acting to displace, and resist displace-
placement process to prevent mud channeling are given. ment, of a by-passed vertical mud column during primary
cementing .,
en
~ of the Bingham model.
A recently proposed yield-pseudoplastic model that
-
C/)
W
II: theoretically improved the above, is not widely used.102
I-
C/) Such models attempt to describe the relationship of
TRANSITION
II: shear rate and shear stress for muds and slurries. Ex-
«
w tremely useful in analyzing the displacement process,
J: LAMINAR
~ they are not precise techniques.
en They should be used to determine flow regime and
D..
ui pressure requirements for displacement. But, results
C/)
W
II:
should be interpreted as more qualitative than quantita-
D.. TRANSITION tive. That is, if the analysis indicates a potential displace-
ment problem, believe it. If it shows acceptable displace-
ment conditions, do all that can be done to enhance the
FLOW BEGINS (G~L STR,ENGTH! NO FLOW dispacement process anyway.
FLOW, BPM (SHEAR RATE) Fluid property measurement. The Fann V-G (vis-
Fig. 35-Non-Newtonian fluids exhibit resistance to flow when cosity-gel) meter is used to measure plastic viscosity,
pressure is applied. Velocity profiles of various types of flow yield point and gel strength of mud, and cement slur-
are shown.
ries.103 Field models have two speeds, to develop shear
rate at 300 and 600 rpm; lab models have six speeds: 3,
6, 100, 200, 300 and 600 rpm. The lab model can
SPRING FACTOR, N = 1
DENSITY = 12.2 PPG SLOPE PROPORTIONAL
measure properties over a range of speeds. However,
TO PLASTIC VISCOSITY the two speeds of the field instrument are enough to
f/) 30 measure plastic viscosity (p.p) . and yield point (ty) used
CJ
z for pressure drop and flow regime determination with
is
i5 :
the Bingham model, as in Fig. 36.100
II: 20
...J
RPM DIAL The Power Law Model requires two different fluid
« READ.
property descriptions. Consistency index (K') and flow
is 600 30
300 25 behavior index (n') are also determined from the Fann
200 23 V-G meter readings. Fann dial readings and rotational
100 19
6 10 speeds are converted to shear stress in lbs./sq. ft. and
3 8 shear rate in sec.-I, respectively.
I
Oil 600 These data then are plotted on log paper and (n') is
the slope of the line through the converted readings at
600 and 300 rpm and (K') is the intercept of the extra-
Fig. 36-Example use of Fann V-G meter to calculate plastic polated straight line at unity rate of shear, Fig. 37. De-
viscosity (/lp) and yield point (t,) for Bingham Plastic Model tails on operation of the Fann V-G meter are available
equations. For data shown, /lp = 600 rpm reading - 300 rpm elsewhere.103 104
reading = 30 - 25 = 5 cpo And t, = 300 rpm reading - /lp = 25
- 5 = 20 Ibs.l100 ft.' Flow analysis calculations. Basic equations for flow
analysis of Newtonian and Bingham/Power Law models
the movement. There are two basic fluid types, New- of non-Newtonian fluids, and relevant nomenclature, are
tonian and non-Newtonian. Newtonian fluids, such as
water, exhibit a straight-line relationship between flow 10
rate (shear rate) and pressure (shear stress) while the
fluid is in laminar flow. A Newtonian fluid begins to flow t:
when pressure is applied. As pressure increases, flow 61
C/)
.....
velocity increases, from laminar, through a transition zone (Jj
SPRING FACTOR, N = 1
(part laminar and part turbulent), to fully developed !XI DENSITY= 12.2PPG (\'
d. S\.O~
turbulent, Fig. 34. ::::::::J. FANNV-GMETER
~.1i
W ' SHEAR DIAL SHEAR
Non-Newtonian fluids are more complex; they may II:
I- RPM RATE READING STRESS
exhibit resistance to flow (gel strength) when pressure C/)
is applied. Fluids with gel strength can flow at very low II: K' 600
300 1022
511 30
25 0.3
0.25
«
W 200 341 23 0.23
rates in a solid or plug-like manner.OO Non-Newtonian J:
f/) 100 170 19 0.19
fluids thus can have three flow regimes-plug, laminar 6 10 10 .01
and turbulent-with transition zones between each, Fig. 3 5 8 .008
35. .011. ~___~I~ I I 11,,1111 , I I I 111_11
1 10 100 1000
Drilling muds and oil well cement slurries are non- SHEAR RATE (SEC.-')
Newtonian. Extensive study has developed mathematical
models that can be used to predict flow properties and Fig. 37-Example use of Fann V-G meter, with readings and
pressure-velocity relationships of such muds and cements. speed, to calculate flow behavior index (K') and fluid consis-
The Bingham Plastic Model and the Power Law Model tency index (n') for use in Power Law Model Equations. For
are most commonly used. The former has been utilized
data shown: n' = 3.32 (Iog,o 600 rpm read.l300 rpm read.) =
3.32 X log,o30/25 = 0.26288. And K' = N (300 rpm read.)
for drilling fluid anaysis since the mid-1940s.100 Power 1.066/100 (511)"'= 1 X 25 X 1.066/100 X 511° 288= 0.05173.
V. = 1.62 I1P+ 1.62 [I1pZ + 8.2 (Dh-Dp)Z typ)I/Z *Y. = [NR.' K'96-'/1.86 (Db-Do)-' p]1/(Z-n')
(Db-Dp) p
PI = 11VL/1,5OO (Db-Dp)Z, PI = I1pVL/1,500(Dh-Dp)2 + ty L/225 (Db-Dp). P = 0.039 L p V2f'/(Dh-Dp)
Where: V < V. Where: V < V.
Pt = fLVZpj25.6 (Db-Do). Where: V ~ V. P, = f L VZp/25.6 (Db-Dp), Where V ~ V.
NR. = 928 (Db-Do) V pill NR. = 2,965 (Dh-Dp) V p/l10
Nomenclature for flow equations used and input data should be comple~ely understood, to
Db = Ho)e diameter, in. avoid misleading results.
.Dp = Casing OD, in. Shown below are some example computer calculations,
f = Friction factor (Bingham-Newtonian, Fig. 38) by various service companies, of critical velocity (Vc)
f' = Friction factor (Power Law, Fig. 39)
K' = Consistency index (Fig. 37) of fluid, described by Fann V-G readings from Fig. 36
L = Length, ft. and 37. Note that they correspond closely to similar data
p.= Viscosity, cp calculated by hand, as shown in the accompanying table.
p.p= Plastic viscosity, cp (Fig. 36)
n'= Flow behavior index (Fi~. 37)
Nn. = Modified Reynolds Number (Bingham and Newtonian) Service Co. Critical velocity in two different
Nne' = Modified Reynolds Number (Power Law) annuli, ft./sec.
P = Pressure drop, psi
P1= Pressure drop, laminar flow, psi 5Y2" x 7%," 5Y2" x 8Y2"
Pt = Pressure drop, turbulent flow, psi BJ Hughes 5.2 5.0 ft./Sec.
Q = Pumping rate, bpm Dowell 5.62* 5.46*
p = Density, ppg Halliburton 5.31 5.14
t7= Yield point, Ibs./l00 {t.' (Fig. 36) Western 6.60* 6.37*
V = Velocity of fluid in annulus, ft./sec.
V. = Critical velocity, min. for full turbo flow, ft./sec. '*Computer output presents critical pump rate. For com-
parison, these data have been converted to critical
shown in accompanying tables. These equations can be velocity.
used to calculate pressure drop, critical flow rates and
to determine flow regimes.105 Flow regimes, pressure drop determinations. Plug,
Complete pressure drop and flow analysis calculations, laminar, turbulent flow and transition zones for any non-
even with electronic calculators, are tedious but accept- Newtonian fluid are functions of velocity and fluid prop-
able results can be obtained. Computer facilities in most erties. Mathematical determinations of veloci~y at which
service companies, and many operating companies, have turbulence is fully established have been based on some
made more detailed flow analyses practical. For example, form of Reynolds Number for both models. In the Bing-
variations of flow area due to borehole irregularities, and ham model, 3,000 was used to derive critical velocity-
presence of more than one type of fluid can be easily the minimum velocity that will maintain full developed
considered. However, with computerized analyses, the turbulent flow.
analytical procedure, the type of mathematical model In the Power Law Model, Reynold's Number has
varied; 2,100 and 3,000 have been used although the
Example flow calculation results latter is more generally accepted. More than one or-
ganization prefers to use a sliding value based on flow
Hand calculated for 12 bpm flow over 1,000 ft. in two different annuli, using behavior index, n', Fig. 39.
fluid data from Figs. 36 and 37. *
Pressure drop determinations with Power Law equa-
Function Bingham Plastic Model Power Law Model tions or the Bingham model for turbulent flow use friction
5 X 7U** 5 X 8** 5 X 7U 5 X8
factors taken from a Stanton-type diagram. The Modi-
V 6.48 4.9 6.48 4.9
V. 6.23 6.17 5.29 fied Reynolds Number (Bingham model) is calculated
6,25 t 5.11+t
6.03 and used to find friction factor (f) as shown in Fig.
PI N.A. 40'" . ...... ......
P, 56.5 N.A. 38.106 The Modified Reynolds Number (Power Law
P 34.5 23"
Na. iii,340 N.A. Model) is used to find friction factor (f'), Fig. 39101
NRe' ...... ...... 4,262 '2,789'
*11= 5 cp; ty = 20 Ibs./100 ft.z; p = 12.2 ppg; n' = 0.26288; k' = 0.0517258. Displacement pressure. A non-Newtonian fluid in
**5~" casing in 7U" and 8~" wellbores. either turbulent or plug flow has a flatter velocity profile,
tReynolds Number = 3,000.
ttReynolds Number = 4,000, selected from Fig. 39. across the area of flow, than when it is in laminar flow.
~Note close correlation of hand calculations to service company computer
calculated results shown in text. Thus, cement in turbulent or plug flow will exert a more
izers, covering specific hole sizes and casing sizes and Example calculation: For: m = 0.847 (10 ppg mud);
weight.132 Starting force, permanent set and restoring W = 40.0 lb/ft, 9% inch casing; L =
45 feet (centralizer
force are defined and specified for individual sets of con- spacing); e = 25 degrees; 916 feet of casing below cen-
ditions. tralizer, and a 2 degree/lOO foot dogleg:
Starting force is the force required to start the cen- Lateral load (additive dogleg) = (0.847) (40.0) (45)
tralizer into previously run casing, as determined by API (0.4226) + 2 [(0.847) = 644 +
(40.0) (916)] 0.00785
test. The maximum starting force permitted is less than 487 = 1,131lb.
the weight of 40 feet of medium weight casing on which Lateral load (Subtractive dogleg) = 644 - 487 = 157
the centralizer is run. lb.
Permanent set is the constant bow height of the bow- Some iteration (trail and error calculation) is required
springs after each bow-spring has been flattened 12 times. in calculating centralizer spacing in this manner because
Maximum starting force is determined before permanent a centralizer spacing must be assumed and then the
set-restoring force after. lateral load on the centralizer calculated. The load then
44 WORLDOIL 1977
must be compared to the centralizer load deflection curve,
Fig. 52, to determine whether the desired stand-off will
be achieved. If not, then a closer spa c i n g must be
assumed.
WIPERS, SCRATCHERS
Wipers and scratchers are used primarily to remove
borehole mud cake. They also aid in breaking-up gelled
mud. Both rotating and reciprocating styles are available,
Fig. 53 (also see Part 4). These devices are rarely used
on liners because of close clearances. Fig. 53-Examples of commonly used rotating and recipro-
cating type wipers and scratchers. Rotating type (A, B, C)
Rotating type wipers or scratchers are run across the are spot welded or clamped. Reciprocating types (0, E, F)
zone of interest plus an additional 20 feet above and move between stop collars or are secured in-place with drive-
set nails.
below the zone. Reciprocating type scratchers are gen-
erally spaced at 5 to I5-foot intervals throughout the
stages, additional stages are possible.
zone plus the additional 20 feet above and below. When
Stage cementing can be used: When a long column
reciprocating, the vertical casing movement should always
of cement is required and weak formations are present
exceed the distance between wipers or scratchers. If re-
which will not support the hydrostatic head; when two
ciprocal movement equals the spacing, removed mud
cake and cuttings can accummulate at the end of each or more widely separated intervals are present which must
stroke. be cemented (for instance, an upper high pressure gas
or water sand), or when special situations exist such as
When wipers or scratchers are used, mud circulation
in the Arctic where casing suspension is desired below
should always be started before pipe is moved. And pipe
the base of the permafrost.
should be moved slowly at first. If no pipe movement is
In deep, hot wells, stage cementing may also be re-
planned, these devices should not be run.
quired to. place slurry with proper temperature char-
MULTIPLE STAGE EQUIPMENT acteristics at the desired level, i.e. retarded cement with
Multiple stage cementing consists of conventional adequate thickening time for hot formations may not
placement of cement slurry around the lower portion of set-up if it is circulated to low temperature, shallow zones.
a casing string followed by placement of successive upper
stages through ports in a stage or port collar, Figs. 54, Stage or port collars may also be used for placing
55.134 Although most stage cementin~ is done in two special fluids in upper portions of the casing string for
't
l I 0
coUar to prevent cement from falling through mud in the
'I annulus. This precaution is particularly appropriate when
weak zones exist below the collar.
One disadvantage to stage cementing is that the casing
{.. ,i. ~bENING
o
6,000-
10-second summary (NORMAL)
Liner running and cementing methods are illustrated
and applications of various types of liners are discussed. 8,000-
Solutions to common problems encountered in conven-
tional and special liner cementing, and basic job design
criteria, are suggested. FRAC PRESSURE
10,000-
,/,
,,
LINER CEMENTINGis one of the most difficult operations
,,
associated with drilling and completion. If a liner is not ,,
effectively cemented, the well's capability to produce will 12,000-
,,
likely be reduced and the advantages of the liner installa- , ,,
tion will not be realized. This article describes liner equip-
ment, cementing applications, some associated problems 14,000-
TIE-BACK
STUB LINER
,,
and solutions. I
In one generally accepted definition, a liner is: A string ......
,
16,000- ...' ,
PRODUCTION LINER
TYPES OF LlNlRS
18,000-
1/ I I I I I I I
Drilling liners are used to permit deeper drilling operations by 8 10 12 14 16 18 20
isolating lost circulation or highly pressured intervals and con- EQUIVALENT MUD WT., PPG
trolling sloughing or plastic formations. And in lieu of a full
length casing string, the drilling liner improves drilling hydrau-
20,000-
lics, i.e. greater cross section above liner top enables use of larger
drill pipe and/or reduces annular pressure drop.
Fig. 58-Example of casing and liner program to seal off high
Production liners are required to provide isolation and support pressure zones in a deep well (after Mahoney and Barrios),'''
functions when casing was landed above the producing interval.
50 WORLDOIL 1977
..
CEMENTING INTERMEDIATE CASING
MANIFOLD
TIE-BACK PACKER
PACKOFF BUSHING
(RETRIEVABLE-OPTIONAL)
HANGER
GAS MIGRATION
WIPER PLUG
(SHEAR TYPE)
STANDOFF
DEVICES
FLOAT
COLLAR
Fig. 60-Schematic of a liner tie-back packer used to repair
a leaking liner top where high pressure gas has penetrated
FLOAT SHOE the cement. Packer is run after liner is cemented and cleaned
out (after Lindsey).1<3
LINER EQUIPMENT
A liner is normally run on drill pipe that extends from
the liner setting tool to surface. Special tools are available
to perform various running, setting and cementing opera-
tions.
The following equipment is discussed from float shoe
(bottom) to cementing manifold (top). Equipment loca-
tions are shown schematically in Fig. 59.
WIPER PLUGS
A float shoe is placed at the bottom of the liner. It
contains a check valve designed to prevent back-flow of FLOAT SHOE
the cement. A float collar can be run above the shoe to INFLATE
DISPLACING
provide a back-up check valve to assure that cement can- CEMENT PACKERS
not re-enter the liner after displacement.143 Automatic fill-
up type float equipment may be selected (Part 5). Fig. 61-External casing packers used to provide positive seal
between open hole intervals behind drilling liner (after Cov-
A landing collar is usually run one joint above the float
lin).'"
collar or two or more joints above the float shoe to pro-
vide space for mud contaminated cement inside the liner. and overlap the existing casing or drilling liner. The
The landing collar's function is to latch and seal the liner length of the overlap varies with operators and applica-
wiper plug. It prevents the liner wiper plug from moving tions. Fifty to five hundred feet of overlap have been used
uphole if a check valve fails and also prevents it from in various applications. The overlap should place the
rotating, which aids the drilling-out operation. hanger above any weakened or suspect lower joints in the
preceding casing string.
Liner length is selected to extend across the open hole Longer overlaps are used when high pressures are
. Plugs
Size, weight of drill pipe operating string
Shear pin rating of liner wiper plug LITERATURE CITED
Displacement to shear wiper plug ". Davis, S. H. "Cementing Liners," Chapter 17, Oil Well Cementing Prac-
Displacement volume to shear liner wiper plug and bump tices in the United States, API, 1959.
141West, E. R., and Lindsey, H. Eo, "How to Run and Cement Liners in
plugs Ultra-deep Wells," World Oil, June 1'966.
"2 Mahoney, B. J., and Barrios, J. R., "Cementing Liners .Through Deep
. Cement recommendations High Pressure Zones," Petroleum Engineer, March 1974.
Weight, viscosity, thickening time, compressive strength, 143Lindsey, H. E., "Running and Cementing Deep Well Liners," Three-part
fluid loss and loss circulation material series, World Oil, November, December 1974 and January 1975.
1« Lindsey, H. E., "Setting Liners in Shallow to Medium Depth Wells,"
Use of bottom-hole temperature subs for information neces- World Oil, May 1977. Also paper to Southwestern Petroleum Short Course,
sary to slurry design Lubbock, Texas, April 11377.
"s Covlin, R. .T., "Cementing Practices-Elk Basin Field," API Drilling and
Production Practices, 1968.
. Procedure "6 API Bulletin D-II')', Running and Cementing Liners in the Delaware Basin,
Pre-cementing conditioning Texas, First Edition, December 1974.
141Tragesser, A., and Parker, F. W., "Using Improved Technology to Obtain
Pump rate Better Cement Jobs on Deep Hot Liners," Preprint SPE 3891, April 1972.
Bottom-hole treating or break-down pressure "0 Shell, F., and Tra~esser, A., "API Is Seeking More Accurate Bottom Hole
Spacers, flushes .Temperatures," 001 & Gas Journal, July 10, 1972.
Displacement efficiency ..9 Lindsey, H. E., and Bateman, S. J., "Improve Cementing o( Drilling
Liners 1U Deep Wells," World Oil, October 1973.
to. Carneu L. C., "Single Stage Spacer (or Deep Liner Cementing," Petro-
. Post-cementing procedures leum l!.ngineer, June 1975.
Clean-out with mill or roller bit '" Crowe, W. L., Griffin, T. J.J and Puntney, A. W., "Cement-Mud Spacer
System Improves minois Welts," Drilline DCW, March 1977, pp. 33-34.
Preparations for completion '.2 Moore, P. L., Drilling Practices Manual, The Petroleum Publtshing Co.,
Tulsa, Okla., 1974, Chapter 16, "Cements and Cementing" by D. K.
*After Lindseyl" Smith.
153Lindsey, H. E., "Techniques for Liner Tie-back Cementing," Petroleum
Engineer, July 1973.
10 second summary
Problems and solutions associated with cement plug
placement, special methods for cementing small di-
ameter, tubingless completions are discussed. Common WIRELlNE
misconceptions about squeeze cementing are corrected
and recommended procedures are presented.
~~,~ iil Drill pipe then is pulled slowly above the cement plug,
additional pressure shears a pin in the plug seat and
circulation or reverse circulation can be established.
This method reduces problems that over or under-dis-
placement can create with the balance method.
CONDITION MUD DISPLACECEMENT SPOT BALANCED PULL PIPE
Recommendations that should reduce probability of
ROTATEPIPE ANb FLUIDS PLUG SLOWLY mud contamination and increase chances for successful
Fig. 55-Schematic of balanced plug method. All fluid volumes plug placement by balance or two plug methods are
are carefully calculated so that hydrostatic pressure on plug listed in the accompanying table.
in final location is identical in drill pipe and annulus.
Sand filler. Some operators use sand to "improve" the
"hardness" or "toughness" of a cement plug. Other
DRILL
PIPE operators specify that sand should not be used.
Unless well temperature exceeds 2300 F, fine sand
does not react with cement (see Part 3-Strength Re-
trogression). And compressive strength of cement at
SEAT lower temperatures will decrease as sand concentrations
SHEARED
increase. Neat cements that are densified with a disper-
sant have the highest compressive strength. Thus, lab
testing does not support use of sand to make slurries
"harder." Yet operators who specify sand use in direc-
tional plugs claim improved "hardness" and higher suc-
CEMENT cess ratios.
PLUG
Sand may improve mud removal by some type of
TOP PLUG scouring action and this could reduce mud contamina-
SEATED
tion. Thus, sand may affect hardness in a manner not
related to a sand-cement reaction.
BOTTOM
PLUG Cement slurries should be densified with dispersants,
and sand (if used) should be angular rather than
DISPLACINGCEMENT CEMENT RAISEPIPE,
AND FLUID IN PLACE CIRCULATE rounded. Some operators prefer mixed sand sizes grading
Fig. 56-Two plug method for deeper wells or where displace- from fine to coarse. Sand concentrations should not
ment is difficult to calculate. Seat stops top plug to indicate exceed 10-20% by weight of cement.160
when slurry is spotted. Pipe then is raised and additional
pressure shears seat to open pipe for circulation, or reverse
circulation. Evaluate plug location, quality. In simple plug backs,
10-second summary 2 3
Basic principles of temperature logging. bond logging
and various tests for proving fluid shut-off by primary CEMENT SHEATH THICK., IN.
cementing are described, along with three new tools for
completion, through-tubing work and whipstock installa- Fig. 76-Lab tests of various cement thicknesses with Insulat-
tion. Ing and non-insulating material simulating surrounding forma-
tion Indicate that temperature rise Inside casing from setting
cement can vary significantly with rock thermal dlffusivity
THIS CONCLUDINGarticle discusses several methods of properties (after Gretener).180
66 WORLDOIL 1977
above the expected top. It is desirable to run the survey
at 50 F per inch sensitivity under normal conditions.
CEMENTTOP And well conditions must remain static from the time
ENLARGED
the plug is bumped until the survey is completed. Cau-
:I:
.) HOLE SECTION tion should be observed when mixed lithologies (sand,
shale, limestone, dolomite, salt, etc.) are present because
.... \
)
n.,
w it is possible to misinterpret.a lithology change as a ce-
0 \
\ ment top. In these areas it is advisable to run a base log
\ prior to running casing, to avoid possible erroneous in-
\ terpretations.
I \
The rate at which temperature changes depends on
\
\ temperature to which the cement is exposed. This is
\ usually a function of depth of the cement job, Fig. 78.181
\ Peak temperatures often occur 4-12 hours after start of
I I II I ,
,,, mixing operations but remain elevated for more than
A B C
24 hours, as shown in Fig. 79. Therefore, temperature
TEMPERATURE - surveys normally should be run between 8 and 24 hours
after cement is mixed. Because these surveys are only
Fig. 77-ldealized temperature log in homogeneous lithology applicable for this short period after cementing, they,
environment. Curve C compared to Curve B illustrates effect of course, have no application in old wells.
of enlarged borehole with corresponding increased cement
thickness (after Folmar).179 There are conditions in some areas where extremely
high well temperatures override the temperature increase
240
of the hydrating cement.182 If the cement top is be-
tween casing strings, the temperature will be greater
than, but parallel to, the geothermal gradient. In wells
200 ,--12,000 FT TEST in which particularly heavy or viscous drilling fluids are
used, special cement displacing fluids may have to be
11. used to permit running of the survey.
o 160
Ii Radioactive surveys. Addition of radioactive tracer
~
W 120 material to the lead portion of the cement slurry pro-
I-
vides a positive indicator of the cement top. Either long
or short half-life material can be used. Carnolite has a
80~ f SLURRY TEMP.
half-life of approximately 1,700 years, and permanently
affects natural gamma-ray emissions near its location in
4,000 FT TEST ___ APPARATUS TEMP. the well. Several radioactive materials that can be used
as tracers have half-lives of 8-80 days.
o 2 3 4 5 6
Principal disadvantages of radioactive survey tech-
TIME, HOURS niques for cement height determination are: Special
health precautions; interference with natural radioactive
surveys, and high costS.178
Fig. 78-Cement temperaturedevelopmentwith time as a
function of well depth is indicated by lab results in a simulated
wellbore apparatus preheated to temperatures of various depth Pressure, inflow tests. Pressure tests are conducted
levels. Tests show 800 F slurry first cools fluid inside casing,
then maximum temperature develops several hours after
placement. Temperature rise is greater in higher temperature
environment (after Farris).'" 210 2,000
to range from 10-40° F, Fig. 76.180 The magnitude of a: 180 1,400 cri
the anomaly will depend on thickness (or mass) of ::?E
W
....
b'" (f)
w
II:
11.
cemen t behind the casing, as well as the thermal 170 . 1,200
PRESS.
diffusivity of surrounding formation. Where lithology is
fairly uniform, the temperature log will indicate relative 160 1,000
thickness of cement behind casing,179 Fig. 77. Caliper
150 800
surveys can be particularly helpful in analyzing the tem- 0 4 8 12 16 20 24
perature survey. If a hot area is noted where there is
no hole enlargement, cement has invaded the formation TIME, HOURSFROM STARTINGTO MIX
through fractures or a thief zone. If the indicated ce-
ment top is higher than calculated, cement channeling Fig. 79-Temperature and pressure effects within fluid
should be suspected. filled casing shut in immediately after cementing. Note
To locate the cement top, the temperature survey maximum temperature buildup 8-12 hours after mixing.
Temperature remains elevated for several hours (after
should begin either at the surface or at least 1,000 feet Farris).'"
SAFETY JOINT
missed with zero-degree gun phasing. The tighter the
..~. j phasing, the lower the chances of missing a channel.
HYDRAULIC VALVE PACKER INFLATION
PUMP Combination of a mechanically fired perforating device
and a testing tool makes it possible to perforate and test
INSIDE RECORDER
CARRIER ;1 SCREEN SUB.
on a single trip with tubing or drill pipe.183 This test
is conducted by perforating an impermeable zone above
TOP PACKER or below the zone of interest, setting the packer and
HYDRAULIC JARS
]
opening the tester valve. A minimum cushion, fluid
TEST PORTS or gas, is placed inside the test string. In some locations
SAFETY JOINT
regulations specify the maximum amount of cushion.
OUTSIDE RECORDER Inside and outside recording pressure instruments are
CARRIER
PACKER
also included as an integral part of most testing tools,
Fig. 80.
The tester is usually left open for a:bout an hour.
SPACING
If strong entry is indicated by a heavy "blow" at the
PERFORATED
surface, the tester may be pulled sooner. The amount
ANCHOR BOTTOM PACKER and type of fluid inside the test string can be checked
by reverse circulating the sample to surface or by re-
OUTSIDE tention in the string and later recovery. Pressure charts
t
RECORDER
CARRIER BELLY SPRING are checked to confirm that the tester was open and
exposed to cushion/formation pressure, to verify a good
ANCHOR SHOE test.
Where there is a need for very accurate location of
SINGLE INFLATABLE
COMPRESSION STRADDLE PACKERS WSO holes, a wireline perforator can be used with a
PACKER collar locator and/or gamma ray log for correlation.
After perforating, a conventional tester is run on tubing
and the test is conducted, as with the combination tool.
Fig. SO-Two types of drill stem test tools used to check pos-
sible fluid entry from a cement job test. Single packer type Stra.ddle packers can be used to test more than one
(left) must be set above single test point. Inflatable straddle set of WSO holes above and below zones of interest.
packer tool (right) can test more than one interval (courtesy With a bottom packer added to the test assembly, each
Lynes Inc.).
set of WSO holes can be isolated and tested, Fig. 80.
Wireline perforating and testing tools are available
to verify integrity of the casing following primary ce- for obtaining small fluid samples following selective
ment jobs. And specific procedures are specified by gov- perforating. These tools are primarily used to perforate
ernment regulations in most locations. The casing pres- through to the zone of interest and obtain a sealed
sure test is conducted after cement has set but prior to reservoir fluid sample that could be suitable for PVT
drilling out the cement shoe. These tests are not an analysis. The size of the sample chamber limits the ap-
indication of cement effectiveness. plication of this type equipment.
In some locations, i.e., California, regulations require
that the casing be perforated and tested by either bailing After drilling out. Where additional drilling is to be
or inflow evaluation tests, called water shut-off (WSO) conducted and when the casing is cemented in an im-
tests. In California the WSO tests provide assurance permeable formation, the casing shoe can be drilled
that a cement seal of the annulus exists, to protect out and the casing seat inflow tested. The amount of
shallower freshwater reservoirs from brine and/or hydro- open hole to be drilled .below casing is specified by law,
carbon contamination. This procedure of perforating and in some locations, but is usually 5-10 feet. Tests can
checking rate and content of inflow, if any, has been be made with a conventional tester set near bottom.
used to verify a cement seal above and/or below hydro- The testing procedures are the same as those used with
carbon producing zones in many areas. The advantage the perforating and testing program.
of this technique is that if a failure is indicated, a ce- A pressure test can also be conducted after drilling
ment squeeze of the WSO holes will be placed opposite out the casing shoe and 5-10 feet of open hole. Two
a non-productive formation, rather than opposite the objectives of this procedure are: To test effectiveness
zone of interest. Also, inflow likely will purge mud from of the cement seal at the casing shoe; and to determine
the perforations, a desired preparation for low pressure formation strength (fracture gradient) at the shoe.
squeeze jobs. One indication of cement seal failure at the casing
Additional measurements frequently included on CBLs Interpretation. Validity of CBL interpretation is a con-
troversial issue. There are no industry standards for
1.5 tools or procedures. Inadequate information on CBL
headings, miscalibration of tools, lack of effective tool
centering in the casing and/or poor running procedures
have resulted in misleading interpretations.
Interpretation of a specific CBL depends on how and
what portion of the acoustic signal is measured and
en recorded. Factors that significantly affect tool response
I-I include: Acoustic frequency of tool; electronic control
o
> that determines the acoustic signal segment measured
ui
c (Gating systems and bias settings); spacing between
::)
I- transmitter and receiver; tool calibration; centralization,
::::;
Q.
::E
and logging speed.
<I:
I
Here are other factors that can introduce errors in
<I:
Z
(!j
CBL interpretation:
en
. Extent of cement set (hardening) affects sonic signal veloc-
ity and amplitude. During the setting process, gel which forms
around the cement particles is apparently an excellent absorber
of acoustical energy. As cement hardens, acoustic transmissibility
increases significantly and the casing signal is dampened out.
Thus it is best to run CBLs at least 24-36 hours after the cement
job is completed or when compressive strength of cement reaches
1,000 psi.
o
o 2 3 . Cement composition also affects acoustic transmission. If a
CEMENT SHEATH THICKNESS, INCHES
high degree of sensitivity is applied where low-density cementing
materials have been used, poor bond may be indicated although
good bonding actually exists. Tests in dril1ed holes with casing
Fig. 83-Effect of cement sheath thickness on pipe amplitude cemented with API Class A cement, indicated that small sections
signal (with pipe bonding only). With less than ~-inch, ampli- void of cement could be located only by using high sensitivity.
tude increase tends to indicate free pipe. Therefore, voids or channels may not always be indicated on
CBLs unless proper sensitivity selection-with respect to cement
composition-is used.1"
100
. Cement sheath thickness may vary, causing changes in
attenuation rate. Lab tests indicate that a thickness of ~-inch
or more is required to achieve full attenuation, Fig. 83. Thus,
casing should be sized to provide a minimum of ~-inch clear-
ance in the drilIed hole, with adequate centralization. Cement
thickness can be critical in certain liner completions where
thickness is less than ~-inch.
> . Cement compressive strength and percent of casing circum-
::!: 10
ui ference bonded affects CBL amplitude, Fig. 84. It is not possible
C to determine the difference between a job in which cement
:J strength is lower than anticipated, and a job in which cement
I-
::i strength is as estimated but small mud channels exist.18OVertical
Q. zone isolation does not exist in the latter case.
::!:
<I:
. A microannulus is a very small gap between casing and
cement. This gap will affect a CBL. However, the presence of a
51,h" CSG., 0.3" THICK. microannulus normally does not prevent isolation between zones
1.0 and it usually tends to "heal" with time.
70 WORLDOIL 1977
10. Radioactive fluid injection and surveys to identify injec-
tion points and possible presence of migration channels behind
casing, and
11. Noise-logging to detect behind-casing fluid movement.
DRILlPIPE
ELEMENTS
CASING
__ DEFLATED INFLATED
STARTING MILL
WITH PilOT
, TOOLaD 2 "/16"
WHIPSTOCK
PERMANENT PACKER
MODIFIED TO
RECEIVE AND lATCH
WHIPSTOCK
Fig. 86-New through-tubing inflatable bridge plug can be run Fig. 87-Schematic of new whipstock anchor offered by Baker
through 3V2-inch tubing, on macaroni string or coiled tubing, Packers. System provides positive seat without danger of dis-
and set in casing as large as 7o/s-inch. Tool holds 700-psi turbing tool when bit is pulled back through casing window.
differential pressure (photo courtesy Lynes, Inc.). Permanent packer is set first in oriented position (if desired)
then whipstock anchor is run on the pilot mill and stabbed
into the packer. Additional set-down weight then shears mill
free to begin sidetrack operation.
wac time, and cement filled ECPs are perforated to support is not provided. Mud channels or pockets left
establish exclusive communication to zones of interest, from conventional cementing can be "drained" when
Fig. 85. the well is perforated and produced. This can remove
The need for remedial squeeze cementing for zone lateral support and cause failure of the formation rock.
isolation should be eliminated. Casing will be centered In unconsolidated sands, lateral support can be a fac-
in the borehole at the ECP and a unifonn cement sheath tor preventing initial sand movement that leads to sand
thickness will exist. control problems. This new support mechanism pro-
Isolation packing, ball sealers, chemical diverters, etc. vides the means to establish stabilized arch sand control-
are frequently used to ensure that each perforation re- a method that could increase productivity at minimum
ceives treating fluids. However, after improper conven- cost.204,205
tional cementing, such fluids may move vertically in the Through-tubing bridge plug. Lynes Inc. has recently
annulus even though they entered individual perfora- introduced a new tool that can supplement, simplify
tions. The Pack/Perf system contacts the formation with or even eliminate certain cement plug back operations
a pressurized rubber seal, backed by non-contaminated in casing (or possibly open hole) below an existing
cement, that positively blocks vertical fluid movement in tubing string, Fig. 86.
the annulus. Acid, hydraulic frac fluid, chemical sand The pennanent through-tubing inflatable bridge plug
consolidation fluid and other treatments will enter the device has a 2 11/16-inch aD. It can be run, on a
fonnations for which they are intended. macaroni string or coiled tubing, through 3~-inch tubing
Increased borehole wall support can be a significant and be expanded with fluid and set inside casing, up to
advantage where wells are completed in weak fonna- 7 5/8 inches. Once set, the plug is capable of with-
tions or where the reservoir is geopressured. Such for- standing up to 700 psi differential pressure.
mations are particularly subject to failure if mechanical The tool can be used to bottom a cement plug or,
LITERATURE CITED
178Teplitz, A.J. and Hasselbrock, W.E., "An Investigation of Oil Wen
Cementing," API 1946 Drillin~ & Production Practices.
119Folmar, L.W., "Methods of Detecting Top of Cement Behind Casing,"
API-Oil Well Cementing Practices in the U.S., 1959 (Chapter 12).
18.Gretener, P.E., "Temperature Anomalies in Wells Due to Cementing of
Casing," ]PT, February 1968.
'8' Farris, R.F., "Method for Determining Minimum Waiting-on-Cement
Time," Petroleum Technology, January 1946.
'8. Kading, H.W. and Hutchins, J.S., "Temperature Surveys: The Art of
Interpretation," API Drilling & Production Practices, 1969.
'83Young, V.R., "Testi!'$ of Primary Cement Jobs, API-Oil Well Cement-
ing Practices in the U.S., 1959, ChaRter 111'.
18.Anderson, W.L. and Walker, T., 'Research Predicts Improved Cement
Bond Evaluations with Acoustic Logs," ]PT. November 19611.
188Winn, R.H., Anderson, ,T.O., Carter, L.G., "A Preliminary Study of
Factors Influencing Cement Bond Logs," ]PT, April 1962.
'86Walker, T., "Case Histories of Bond Logging," O&G], May 7, 1962.
181Riddlo;., G.A., "Acoustic Wave Propogation in Bonded and Unbonded Oil
Well t.<asing," SPE 454, October 1962.
188Pardue, G.H., et ai, "Cement Bond Log-A Study of Cement and Casing
Variables," ]PT, May 11963.
180Flournoy, R.M., and Feaster, J.H.. "Field Observations on the Use of
the Cement Bond LOR and Its Application to the Evaluation of Cement-
ing Problems," SPE 632, 1963.
'90Harcourt G., Walker, T., and Anderson, T., "Use of the Micro-Seismo-
gram and Acoustic Cement Bond Log to Evaluate Cementing 'Techniques,"
SPE 798, '1964.
,., Anderson, T.O., Winn, R.H. and Walker, T., "A Qualitative Cement-
bond Evaluation Method," API Trans. 1964.
19.Walker, T., "A Full-Wave Display of Acoustic Signal in Cased Holes,"
]PT, August 1'968.
... Bade, I.F., "Cement Bond Logging ,Techniques-How They compare and
Some Variables Affecting Interpretation," ]PT, January 1963.
19.Chaney, P.E., Zimmerman, C.W., Anderson, W.L., "Some Effects of
Frequency Upon the Character of Acoustic Logs," ]PT, April 1966.
'96Fertl, W.H., Pilkington, P.E., and Scott, J.B., "A Look at Cement Bond
Logs," SPE 4512, 1973.
'00 Pilkington, P.E., and Scott, J.B.J. "Comparing Cement Bonds After
Ten-Plus Years," Pet. Eng., April 1:176.
,., Wilson, C.L., et ai, "How Good is That Wen Completion?" O&G],
June 26, 1955.
108Wade, R.T., et ai, "Production Logging_The Key to Optimum Wen
Performance," ]PT, February 1965.
,.. Kading, Horace W. and Hutchins, J.S., "Temperature Surveys,: The Art
of Interpretation," API-Drilling and Production Practices 11969.
'00Meunier D., Tixier, M.P., and Bonnet, J.L., ",The Production Combi-
nation Tool-A New System for Production Monitoring," SPE 2957, 1970.
20'Witterholt, E.J., Tixier, M.P., "Temperature Logging in Injection
Wells," SPE 4022, 1972.
... McKinley, R.M., Bower, F.M., Rumble, R.C., "The Structure and
Interpretation of Noise from Flow Behind Cemented Casing," ]PT,
March, 1973.
... Odeh, A.S., Jones, L.G., "Two-Rate Flow Test, Variable-Rate Case-
Application to Gas-Lift and Pumping Wells," ]PT, January 1974.
... Suman, G.O., Jr., "Unconsolidated Sand Stabilization Through Wellbore
Stress State Control," SPE 5717, '1975.
"'" Snyder, Robert E., "What's New in Well Completion," World Oil, May
1977.
End of series