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International Journal of Mineral Processing 100 (2011) 57–71

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International Journal of Mineral Processing


j o u r n a l h o m e p a g e : w w w. e l s ev i e r. c o m / l o c a t e / i j m i n p r o

A review of froth flotation control


B.J. Shean, J.J. Cilliers ⁎
Rio Tinto Centre for Advanced Mineral Recovery at Imperial College London, Department of Earth Science and Engineering, Imperial College London, SW7 2AZ, United Kingdom

a r t i c l e i n f o a b s t r a c t

Article history: The last few decades have seen major advances in instrumentation and technology, and simplifications and
Received 6 August 2010 modifications of new flotation plant designs. This has allowed for significant developments in process control.
Received in revised form 19 April 2011 In particular, the development of base level process control (control of pulp levels, air flowrates, reagent
Accepted 8 May 2011
dosing, etc.) has seen significant progress. Long-term, automated advanced and optimising flotation control
Available online 14 May 2011
strategies have, however, been more difficult to implement. It is hoped that this will change as a result of the
Keywords:
development of new technologies such as machine vision and the measurement of new control variables, such
Froth flotation as air recovery.
Process control This review looks at each of the four essential levels of process control (instrumentation, base level flotation
control, advanced flotation control and optimising flotation control) and examines current and future trends
within each sub-level.
© 2011 Elsevier B.V. All rights reserved.

Contents

1. Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58
2. Key variables and considerations in the control of flotation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
2.1. Key variables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
2.2. Effects of plant layout and the location of the cell in the circuit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
2.3. Types of process input disturbances . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
2.4. System constraints . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
3. Instrumentation and base level flotation control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
3.1. Pulp levels in cells . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
3.1.1. Instrumentation used for pulp level measurement and control. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
3.1.2. Base level control systems for pulp level control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
3.2. Air flowrates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
3.2.1. Instrumentation used for air flowrate measurement and control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
3.2.2. Base level control systems for air flowrate control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
3.3. Slurry flowrates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
3.3.1. Instrumentation used for slurry flowrate measurement and control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
3.3.2. Implementation of slurry flowrate in control systems . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
3.4. Elemental assaying . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
3.4.1. Instrumentation used for elemental analysis . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
3.4.2. Implementation of elemental assaying in control systems . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
3.5. Density . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
3.5.1. Instrumentation used for density measurement. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
3.5.2. Implementation of density measurement in control systems. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
3.6. Reagent addition . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
3.6.1. Instrumentation used for reagent addition . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
3.6.2. Base level control systems for reagent addition . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
3.7. Eh, pH and conductivity . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
3.7.1. Instrumentation for the measurement of Eh, pH and conductivity . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
3.7.2. Base level control systems for Eh, pH and conductivity control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62

⁎ Corresponding author. Tel.: + 44 20 7594 7360; fax: + 44 20 7594 7403.


E-mail address: j.j.cillifers@imperial.ac.uk (J.J. Cilliers).

0301-7516/$ – see front matter © 2011 Elsevier B.V. All rights reserved.
doi:10.1016/j.minpro.2011.05.002
58 B.J. Shean, J.J. Cilliers / International Journal of Mineral Processing 100 (2011) 57–71

3.8. Gas dispersion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63


3.8.1. Instrumentation used for the measurement of gas dispersion variables . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63
3.8.2. Implementation of gas dispersion variables in control systems . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63
3.9. Machine vision . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63
3.9.1. Instrumentation and methods used for machine vision . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63
3.9.2. Implementation of machine vision in control systems . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64
4. Advanced flotation control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64
4.1. Advanced control of mass pull and re-circulating load . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64
4.1.1. Mass pull control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64
4.1.2. Re-circulating load control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64
4.2. Advanced control of grade and/or recovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65
4.2.1. Model-based methods in advanced flotation control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65
4.2.2. Expert systems in advanced flotation control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66
5. Optimising flotation control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66
5.1. Modelling-based methods in optimising flotation control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 67
5.2. Expert methods in optimising flotation control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 67
6. Examples of approaches found in advanced/optimising flotation control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
7. Commercial advanced/optimising flotation control software . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
8. Conclusions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
Acknowledgements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68

1. Introduction methods are now commonly used in modern control strategies.


Similarly, traditional base level flotation control was applied to single
Froth flotation is one of the most broadly used separation methods cells, although modern control strategies are now regularly applied to
in the mineral processing industry. However, despite being intro- entire banks of cells (e.g. pulp level control).
duced in the early 1900s and numerous years of research and The two higher tiers of flotation control are advanced flotation
development, flotation is still not fully understood and remains control (AFC) and optimising flotation control (OFC). AFC involves the
relatively inefficient. As such, large economic gains stand to be made rejection of the effects from input disturbances to the process (e.g. a
through optimisation of many present processes (McKee, 1991; change in feed grade) and maintaining performance parameters —
Hodouin et al., 2000; Moilanen and Remes, 2008). grade and recovery (although care should be taken when defining
It is important to realise from the outset that process control recovery; in a dynamic situation accumulation of material within the
consists of several interconnected levels. Several authors, e.g. Roesch system and lag times should be considered). OFC, on the other hand,
et al. (1976); McKee (1991); Laurila et al. (2002); and Gupta and Yan aims to maximise overall financial profitability (commonly by
(2006), describe the process control of froth flotation by a hierarchy of maximising grade and recovery). Both AFC and OFC attempt to
3–4 inter-connected layers. The hierarchy described by Laurila et al. achieve their objectives through manipulation of lower level control
(2002) is presented in Fig. 1. setpoints. It thus follows that the efficiency of AFC and OFC systems
The lowest level is the instrumentation itself, which is the basis for are dependent on satisfactory lower level flotation control systems
all process control. As such, the choice/design and maintenance of the being in place. Several cells are generally controlled simultaneously;
instrumentation is of central importance to any process control and advanced control methods (which in control engineering
system. Furthermore, the correct choice of instrumentation can only terminology classically refers to any control strategy more compli-
be achieved if a detailed understanding of the functioning and cated than SISO PID control; and more recently to computer based
application of the required instrument, within a given process, is technologies) are used as PID control is insufficient.
acquired (Laurila et al., 2002). Numerous years of research into the automation of froth flotation
Base level flotation control is focused on maintaining primary control has been conducted to increase process efficiency, with efforts
variables at setpoints. These primary variables include: pulp level, air prior to the 1970s being largely unsuccessful. Several authors, such as
flowrate and reagent addition rate. This is generally achieved through McKee (1991) and Laurila et al. (2002), agree that reasons for this
the usage of conventional SISO PID control; although more advanced include: a lack of appropriate instrumentation and technologies, and

Fig. 1. Process control system level hierarchy for flotation processes (Laurila et al., 2002).
B.J. Shean, J.J. Cilliers / International Journal of Mineral Processing 100 (2011) 57–71 59

the old design of flotation plants; which consisted of numerous simple other simultaneous sub-processes also occur. Examples
smaller cells making process control more complicated and cumber- include: entrainment of gangue into the froth phase, coalescence of
some. As such, operator intervention was the only method of process bubbles, de-attachment of valuable particles from bubbles as they
control (and this is still largely true of many plants today). impact the froth phase, etc. (Ventura-Medina, 2000). The feed
However, the early 1970s saw extensive improvements in composition and upstream grinding stages prior to flotation also
available instrumentation and the research into the development of significantly affect the process. Thus, in reality, the flotation process is
automatic control of flotation began to show increasing promise highly complex with Arbiter and Harris (1962) estimating that there
(McKee, 1991; Thwaites, 2007). Subsequently, there has been major are approximately 100 variables that affect (to varying degrees) the
development in base level flotation control; although the develop- flotation process. Moreover, co-interactions between variables further
ment of robust, long-term, automatic A/OFC systems has proven more complicate control efforts. For example, an increase in air flowrate
challenging. According to McKee (1991) this is partially due to “the may well result in a larger bubble size, which will subsequently affect
inherent complexity and unpredictability of the response of most flotation the bubble rise velocity, rate of attachment, gas holdup, froth depth,
circuits to upset conditions, unclear expectations of what a control etc. — meaning other variables may be affected and need manipulat-
system can achieve, unrealistic objectives for control systems and ing after a given response time. As such, it is the high number of
excessive complexity of the actual control strategies.” Osorio et al. variables and the complex, non-linear, inter-relationships between
(1999) included coupling among control loops, long varying lag times, these variables that make flotation control in specific very
and an “imperfect knowledge of the phenomenology of flotation and the challenging.
lack of appropriate and precise instrumentation” as contributors for
complicating control attempts.
Despite this, Laurila et al. (2002) believe that flotation is currently 2.1. Key variables
facing “a new era in terms of automation and process control”, with
there being three main reasons for this: Laurila et al. (2002) suggest that the following variables –
specifically from an A/OFC viewpoint – are most important:
• Henning et al. (1998), and Moilanen and Remes (2008) noted that
“flotation circuit design is moving away from multiple recycle streams • slurry properties (density, solids content)
and towards simpler circuits.” This simplifies regulation and control • slurry flow rate (retention time)
of the over-all process. • electrochemical parameters/potentials (pH, Eh, conductivity)
• Authors such as Kallionen and Heiskanen (1993), and Carr et al. • chemical reagents and their addition rate (frothers, collectors,
(2009) have noted that the sizes of flotation cells are increasing, the depressants, activators)
main benefits being: a reduction in capital expenditure and • pulp levels in cells
operational costs, lower energy consumption per cubic metre, less • air flowrates into cells
items to maintain and a lower plant footprint. Fewer cells also mean • froth properties (speed, bubble size distribution, froth stability)
less instrumentation is required; allowing for less-intricate process • particle properties (size distribution, shape, degree of mineral
control systems. However, this does mean more accurate instru- liberation)
mentation is required. Fewer, larger cells also increase the incentive • mineralogical composition of the ore
for better base level control on each individual cell. • mineral concentrations in the feed, concentrate and tailings
• Recent developments in instrumentation have seen the develop- (recovery, grade)
ment of tools such as fieldbus technology and image analysis, and • froth wash water rate (especially in flotation columns)
have allowed for the assembly of “smart instruments”; devices that
use self-diagnostics to provide information about the equipment Manipulating/measuring each of these variables simultaneously
status and measurement quality. may well be unnecessary to achieve a good process control result.
Laurila et al. (2002) also highlight that as each flotation process is However, each of these variables and their effects on the flotation
unique (e.g. cell configuration, instrumentation, ore, chemistry, etc.) a process should be considered.
large variety of A/OFC strategies have been developed and imple-
mented, and a single, universal, control approach cannot be given. 2.2. Effects of plant layout and the location of the cell in the circuit
The aim of this literature review is to broadly explore the various
control strategies that have been/are being, developed and utilised The process layout is a key consideration in process control.
from a metallurgist's perspective. This work shall begin with a look at Recycle streams in particular can make process control (e.g. pulp level
the key variables and considerations in the control of flotation. Each of control) more challenging, especially if accumulation and/or sudden
the four levels of flotation control will then be explored in detail. discharges of material are allowed to occur. Additionally, different
Lastly, a description of some available commercial control systems sections of the plant require different process control regimes; the
and conclusions are presented. It should also be noted that although rougher and scavenger sections being operated at comparatively low
this paper focuses primarily on cell flotation devices, as opposed to froth depths and high air flowrates, to achieve high mineral recovery;
column flotation devices, much of the literature and theory is whilst cleaner sections operate with greater froth depths and lower
applicable to both. air flowrates in a bid to increase grade (Laurila et al., 2002).

2. Key variables and considerations in the control of flotation


2.3. Types of process input disturbances
Froth flotation is a three phase separation process for complex ores
based on the manipulation of the difference in hydrophobicity of the It is important to identify the frequency and severity with which
solids. Suspended, hydrophobic metal-rich particles are contacted input disturbances can occur for a given flotation process. Wills and
with, and subsequently combine to, air bubbles — whilst the more Napier-Munn (2006) suggest that if the grinding circuit control
hydrophilic gangue particles sink and are recovered to the tails systems are running efficiently, variations in particle feed rate, pulp
stream. The valuable-mineral loaded bubbles report to a froth phase density and particle size should be minimal — with the flotation
and overflow into a launder, before being recovered to the circuit being responsible for compensating for variations in mineral-
concentrate stream. Although the process may sound relatively ogy and floatability of the ore.
60 B.J. Shean, J.J. Cilliers / International Journal of Mineral Processing 100 (2011) 57–71

2.4. System constraints Laurila et al. (2002) add that accurate level measurement is often
problematic as the slurry–froth transition is not sharp and variations
Existing circuit constraints need to be considered when imple- in slurry density and/or very dense froth layers often exist. This
menting a process control regime. Two types of constraints exist. especially complicates methods using direct ultrasonic or hydrostatic
Firstly a process may be equipment constrained (e.g. a recovery pressure measurements.
cannot be achieved because the required air flowrate rate cannot be Lastly, Carr et al. (2009) highlight that “control valve options are
supplied). Secondly, a process may be constrained by another part of limited due to the eroding conditions and large variations in flowrate.”
the system; an example being the limitation of the maximum Dart and pinch valves are generally used (neither being optimal), and
recovery of a desired species, at a high concentrate grade objective, both being occasionally incorrectly sized. The optimal operating range
within a flotation plant as a result of insufficient liberation by the of these valves is 30–60% open, although these valves are commonly
grinding circuit (McKee, 1991). Bergh and Yianatos (2011) add that seen operating at below 30% open. Operating a valve near the fully
“in practise the plant operating point that satisfies the overall economic closed position causes increased wear, while operating near the fully
goals of the process will lie close to the intersection of constraints.” open position reduces the control range of the valve.

3. Instrumentation and base level flotation control 3.1.2. Base level control systems for pulp level control
Stenlund and Medvedev (2000); Kämpjärvi and Jämsä-Jounela
Information about the input disturbances, process operating (2003); and Carr et al. (2009) report that flotation cells traditionally use
parameters and final product quality is required before optimisation feedback PI control to ensure pulp levels remain at desired set-points;
and control can be performed; with the quality of measured although Wills and Napier-Munn (2006) add that feedforward control is
information largely determining the efficiency of an implemented also regularly integrated to account for flowrate variations upstream. This
control system. However, despite the availability of instrumentation is achieved by manipulating the tailings flow from the cell by adjustment
for the measurement of important parameters such as: ore compo- of the slurry outlet valve. This technique is effective for the control of
sition, flowrates and less ore specific properties (e.g. pulp levels, isolated cells, but is also commonly used to control a bank of cells in series.
density, pH) — essential properties such as liberation degree, surface This approach is problematic, as each individual cell control loop attempts
chemistry, bubble size distribution, bubble loading, etc. remain to independently maintain the pulp level at the set-point. As such, a
difficult to measure and infer (Bergh and Yianatos, 2011). control action for one cell is a disturbance for the next; the net result
Currently, most existing instrumentation on flotation plants makes being that each cell drives the following cell off its set-point.
use of analogue signal technology; with signals requiring conversion As such, sophisticated multivariable model-based control methods
into a digital format before interfacing with automation systems. As have been developed; whereby the whole bank of cells is modelled
such, it is thought that analogue technology is to be replaced by digital and compensations between adjacent cells calculated and/or consid-
fieldbus technology. This will result in completely digital communi- ered. Two examples of multivariable control methods are presented in
cation between instrumentation and base level control systems at Stenlund and Medvedev (2000). The first makes use of a ‘decoupling
source, and has already enabled the decentralisation of pulp level and controller’ model, where ‘compensator’ parameters are introduced
air flowrate base level control systems. This has also allowed for better (representing the dependencies of each cell in a series on prior cells)
integration of base level control during flotation cell design (Laurila to counteract the interactions between cells. The second method
et al., 2002). Continued development of base level control is now introduced is a multivariable model-based feedback controller, which
largely focused “towards operational aspects that facilitate and speed up manipulates flows out of each cell simultaneously so as to continually
the setting of control loops” (Moilanen and Remes, 2008). minimise a defined error function. Kämpjärvi and Jämsä-Jounela
(2003) described an alternative multivariable model whereby a feed-
3.1. Pulp levels in cells forward controller was linked with traditional PI controls on each cell.
Moilanen and Remes (2008) described a similar feed forward control
3.1.1. Instrumentation used for pulp level measurement and control algorithm. Despite this, Carr et al. (2009) reports that these “more
Laurila et al. (2002) and Carr et al. (2009) suggest that the most sophisticated methods… are rarely used in industrial processing plants.”
typical methods of pulp level measurement are: Commercial control packages such as FloatStar Level Stabiliser by
Mintek, or CellStation by Outotec, also aim to control all cell levels
• Float with a target plate and ultrasonic transmitter simultaneously using advanced control techniques. Both have
• Float with angle arms and capacitive angle transmitter reportedly been trialled successfully and installed on industrial plants
• Reflex radar (www.mintek.co.za; www.outotec.com).
From an A/OFC perspective pulp level control is important as it dictates
Other methods mentioned in literature include: the froth depth (defined as the distance from the pulp/froth interface to
the overflow lip). Theoretically, a deeper froth allows for increased
• Hydrostatic pressure measurement. Authors such as Roesch et al. drainage of mechanically entrained gangue, and subsequently, a higher
(1976); Hamilton and Guy (2000); and Maldonado et al. (2008) concentrate stream grade (Wills and Napier-Munn, 2006). As such, A/OFC
describe methods whereby the hydrostatic pressure is measured to systems commonly manipulate the setpoints of pulp-level controllers.
determine the pulp level. Accurate measurement requires that both
the slurry density and air holdup in the pulp be known. 3.2. Air flowrates
• Microwave radar and ultrasonic transmitters. Microwave or ultra-
sonic beams are emitted towards the froth and are reflected at the 3.2.1. Instrumentation used for air flowrate measurement and control
slurry surface before being measured, and the pulp level being Laurila et al. (2002) report that there are three common methods
inferred (Hamilton and Guy, 2000). of measuring air flowrates in flotation processes. Two of the methods
• Conductivity and capacitance Hamilton and Guy (2000) describe two make use of differential pressure metres, which “are popular in
techniques whereby the large difference in dielectric constant industry, including flotation, due to their low price, simple principle and
between gasses and liquids is used to determine the pulp level. fairly low requirement of maintenance.” The three methods are:
Similarly, the difference in electric conductivity, measured using a
conductivity probe, can also be used to locate the froth–pulp • Thermal gas mass flow sensor. The cooling effect of the air as it flows
interface (Wills and Napier-Munn, 2006; Maldonado et al., 2008). past a sensor is measured and correlated to an air flowrate. These
B.J. Shean, J.J. Cilliers / International Journal of Mineral Processing 100 (2011) 57–71 61

instruments are unobtrusive to the air flow, although they are bank air flowrate profile control is also advantageous. If the cell air
expensive and factory calibrated, making changes difficult. flowrates are not controlled individually, and air is fed to a group of
• Differential pressure metre with venturi tube. Green and Perry (2007) cells, butterfly valves are often operated manually to adjust the flow
describe that the narrowed venturi tube acts as a restriction to the to each cell. Lastly, Laurila et al. (2002) add that “flotation cells with
flow, resulting in a pressure drop that is measured and a flow rate self-aspirating aeration mechanisms often do not have automatic airflow
determined. This method is reliable, produces tolerable pressure control. The available range of airflow control is anyhow limited. This
drops and is accurate, although the venturi tube has large space problem is pronounced at high altitude.” This limits the potential for the
requirements and is expensive Laurila et al. (2002) add that “an implementation of advantageous A/OFC strategies.
orifice plate is not a suitable solution due to the significant pressure loss
it causes”. 3.3. Slurry flowrates
• Differential pressure transmitter with Pitot tube or annubar tube. Both
the Pitot tube and annubar element determine the gas flowrate, in a 3.3.1. Instrumentation used for slurry flowrate measurement and control
pipe, by comparison of the internal pipe pressure and the static gas Magnetic flow metres are commonly used to measure slurry
pressure. The difference between the methods is that the Pitot tube flowrates and are based on Faraday's principle of induction, with the
only has one measurement point, while the annubar element has device consisting of an electromagnet coiled around an insulated
several measurement points and thus provides an average air length of pipe. Electrodes are installed at opposite sides of the pipe,
velocity. Both methods are deemed accurate and the observed which enable an electric current to be generated through the flowing
pressure drop is small. Fig. 2 illustrates the instrumentation used for fluid and measuring device. From this measured current a flowrate
air flowrate measurement. can be determined. This method is non-obtrusive and modern
magnetic flowmeters take up to 30 measurements per minute. Slurry
Problems associated with differential pressure metres include
measurement is problematic, however, as solids and air bubbles
large space requirements, with large sections of straight piping being
decrease performance. Moreover, if magnetic solids (e.g. magnetite)
needed to ensure a fully developed flow profile. One solution is to
are present de-magnetisation is required (Laurila et al., 2002). Slurry
decrease the pipe size, as the required straight pipe length is related to
flowrates can also be controlled by variable or fixed speed pumps that
pipe diameter. Butterfly valves are used to control the air flow as they
are capable of handling slurries. Suitable valve options have already
are cheap and sufficient for the task (Laurila et al., 2002).
been discussed in Section 3.1.1.

3.2.2. Base level control systems for air flowrate control


Wills and Napier-Munn (2006) elaborate just how important and 3.3.2. Implementation of slurry flowrate in control systems
useful aeration control is; adding that “flotation generally responds In flotation circuits, slurry flowrates are generally manipulated to
faster to changes in aeration, than to changes in froth depth, and control pulp levels in cells (see Section 3.1.2), and are not controlled
because of this aeration is often a more effective control variable”. to a setpoint. Nevertheless, the measurement of slurry flowrates are
Similarly, they infer (by use of an example) that in comparison to important, as Laurila et al. (2002) point out, for A/OFC, and allow for
reagent addition, air is by far the “cheaper ‘reagent’ and leaves no calculating re-circulating loads and performing mass balance calcu-
residual concentration if used in excess.” As such, air flowrate is lations. Slurry flowrate measurement is also important for reagent
frequently incorporated into A/OFC systems, often in conjunction addition base level flotation control.
with pulp level and/or reagent addition control systems; an example
being the simultaneous manipulation of air-flow rate and pulp level 3.4. Elemental assaying
to control mass pull.
Carr et al. (2009) note that “the control of flotation aeration is easier 3.4.1. Instrumentation used for elemental analysis
than slurry level control”. Luyben and Luyben (1997), Laurila et al. On-line X-ray fluorescence (XRF) analysers provide elemental
(2002), and Carr et al. (2009) agree that a simple, well-tuned, assays from process flow streams and are now considered standard
feedback/feedforward PI/PID control loop is adequate to accurately hardware on large scale flotation plants (Garrido et al., 2008). Several
regulate air flow by manipulation of the control valve setting. Sizing of points of the process can be sampled, with some modern XRF
the control valve is of central importance for effective control. analysers handling up to 24 streams and most machines being capable
Oversized valves are often fitted to infer a smaller pressure drop, of analysing for several elements and solids content. The time to
but in reality result in a limited control response (Luyben and Luyben, analyse a single sample can range from 15 s to a minute, and the
1997); and can significantly, and rapidly, affect flotation performance sampling cycle time is between 10 and 20 min — depending on the
and pulp level control. Smith et al. (2008), suggest that down-the- number of sample points attached to the analyser (Laurila et al., 2002;

Fig. 2. Illustration of (A) thermal gas mass flowmeter, (B) venturi tube with differential pressure metre and (C) Pitot tube.
62 B.J. Shean, J.J. Cilliers / International Journal of Mineral Processing 100 (2011) 57–71

Bergh and Yianatos, 2011). Accuracy ranges from 1 to 6% and • Metering pumps are also used, especially if volumes to be added are
detection limits are as low as 3–30 ppm (Moilanen and Remes, very small or cost is of importance. This method is more accurate,
2008). Moreover, Haavisto et al. (2008) introduce a new method of but the pumps are costly and require regular maintenance.
analysis; “the visual and near-infrared reflectance spectroscopic analysis
of process slurries”. This measurement aims to be “a supplementary
method, which complements the on-line assay information available 3.6.2. Base level control systems for reagent addition
from an XRF analyser.” It is further reported that “spectral information Base level reagent addition control commonly consists of a
can be used to accurately predict element contents in the slurry in feedforward ratio-type control, as mentioned by Hodouin et al.
between successive XRF analyses”, and as these “measurements can be (2000), whereby the reagent addition rate is altered according to the
taken with high frequency as opposed to sparse XRF analysis, a practically feed rate of ore to achieve a reagent (in slurry) concentration setpoint
continuous on-line estimate of the slurry contents is reached.” This (e.g. grammes of reagent per ton of ore). This reagent concentration
would allow for any process disruptions to be rapidly identified. setpoint may then be altered retrospectively by operators in a
Despite the obvious benefits of online XRF analysis Garrido et al. feedback fashion after considering composition results from an XRF
(2008) report that these analysers are generally “under-utilised analyser. Similarly, the setpoint could be manipulated by an A/OFC
because operators do not trust the online information given by estimation system to achieve a required metallurgical result; although Wills and
models”. They further describe a calibration method for estimation Napier-Munn (2006) add that this is more common with collector
models that “minimise the effects of the uncontrollable disturbances control, with frother addition rate setpoints usually being set
during the estimation.” manually.

3.4.2. Implementation of elemental assaying in control systems


Wills and Napier-Munn (2006) report that “the key to effective 3.7. Eh, pH and conductivity
(flotation) control is online chemical analysis, which produces real-time
analysis of the metal composition of process streams”. However, the 3.7.1. Instrumentation for the measurement of Eh, pH and conductivity
relatively long sampling cycle times mean that input disturbances of Measurement of electrochemical potential (Eh), pH and conduc-
high frequency can be missed, making it difficult to capture the tivity provide information on the surface chemistry of the particles in
experimental data required to form dynamic models of the process the slurry and are the only direct, non-intrusive methods of
(Bergh and Yianatos, 2011); and take required control actions. Moreover, determining what is occurring chemically within the flotation cell
Remes et al. (2007) conducted a study into the effect of speed and (Ruonala, 1995). Laurila et al. (2002) report that pH is a commonly
accuracy of on-line elemental analysis on flotation control performance. measured electrochemical property, and is related logarithmically to
The study concluded that an increase in sampling cycle time results in a the hydronium ion activity in solution. Measurement is achieved by
strong decline in controllability, resulting in negative economic impacts. using ion selective electrodes, although this is often problematic as
“the electrodes are easily contaminated by active substances in the
3.5. Density slurry.” As such, sampling systems are often used for pH measure-
ment, where washing of the electrodes and regular maintenance can
3.5.1. Instrumentation used for density measurement be performed.
Roesch et al. (1976) report that nuclear density metres are Conductivity measurement can often be used instead of, or in
commonly used for density measurement on flotation plants. conjunction with, pH measurement — as both provide complimentary/
Gamma radiation is emitted by a radioactive isotope and the similar information. Conductivity metres are generally cheaper and
attenuation of the radiation by the slurry is measured, from which are more suitable for highly alkaline solutions, although their use
the density can be determined from a prior calibration. This method is should be avoided in highly aerated systems. In addition, Wang and
non-obtrusive to the process flow. This is in agreement with Laurila Cilliers (1999), and Bennett et al. (2002) performed studies where
et al. (2002), who add that air bubbles in the slurry often make use of a conductivity measurements were used to determine froth density and
nuclear density metre impossible and choice of location in the process flow regimes.
is an important consideration. Additionally, some on-stream XRF Eh measurement too is problematic, with Woods (2003) adding
analysers are now capable of density measurement. that “maintaining electrode probes so that they respond appropriately in
these plants is difficult to achieve”, and concluding that the choice of
3.5.2. Implementation of density measurement in control systems materials in Eh probes requires further research.
Density measurements are used in mass balance calculations,
which are associated with A/OFC (Laurila et al., 2002). Furthermore,
control/manipulation is normally preformed in the grinding circuit/s 3.7.2. Base level control systems for Eh, pH and conductivity control
(Wills and Napier-Munn, 2006). Base level control of pH involves maintaining the slurry pH at a
desired setpoint, through manipulation of acid or lime addition rates,
3.6. Reagent addition with PID control loops being adequate for the task (Laurila et al.,
2002). Long response times of the system mean a lag time should
3.6.1. Instrumentation used for reagent addition follow any corrective action/s performed to fully appreciate the effects
A variety of alternative equipment for maintaining/setting reagent it has had (Wills and Napier-Munn, 2006). Commercial controllers,
addition rates are used industrially. Laurila et al. (2002) suggest the such as FloatStar pH Controller, are also available and use advanced
main reasons for this are due to the seemingly negligible amounts that control methods.
need to be added (often measured in millimetres per minute) and the Control of Eh usually involves the addition of nitrogen or air to the
large variety of different reagents added, each with their own system to alter the electrochemical potential (Woods, 2003). Much
chemical properties and attributes. Common methods include: research into improving metallurgical results through Eh manipula-
tion (A/OFC) has been published over the last four decades. Ruonala
• A simple on-off type dosing system which periodically opens a valve et al. (1997); and Woods (2003) present thorough reviews of this
and allows reagent to enter the process. Regular checks are required work on both laboratory and industrial scales, for several ore types. A
to ensure the correct amount is added, as this method can be very summary of a brief literature review, listing the ore-type the studies
inaccurate. were conducted on, is listed below in Table 1.
B.J. Shean, J.J. Cilliers / International Journal of Mineral Processing 100 (2011) 57–71 63

Table 1 problems with the design include the requirement of a range of orifice
Summary of literature review for Eh measurement/control in froth flotation. valves to suit all gas velocities and the build up of froth within the
Author and date Mineral type system (Torrealba-Vargas and Finch, 2006; Gomez and Finch, 2007).
Berglund (1991) Pyrite, sphalerite-galena, chalcopyrite
Bruckard et al. (2007) Arsenopyrite, lollingnite and arsenic from 3.8.1.2. Gas holdup measurement sensor. “The sensor is based on
tin bearing ores Maxwell's model that relates the concentration of a non-conducting
Chander and Fuerstenau (1975) Copper and chalcocite dispersed phase to the conductivities of the continuous phase and the
Clark et al. (2000) Chalcocite, chalcopyrite and bornite
dispersion.” This requires two measurements in separate vessels (see
Guo and Yen (2005) Enargite and chalcopyrite
Hayes and Ralston (1988) Galena, chalcopyrite and sphalerite Fig. 3, part B); one vessel measures the conductivity of the aerated pulp;
Hicyilmaz et al. (2004) Pyrite the other measures the conductivity of the air free pulp (achieved using
Hintikka and Leppinen (1995) Complex sulphide ores and gold bearing ores a syphon). The ratio of these measurements is used to solve Maxwell's
Kirjavainen et al. (1992) Copper ores with rich copper–zinc–lead pyrite ores model and estimate the gas holdup. This method ensures continuous
Kocabağ and Güler (2007) Pyrite, galena, chalcopyrite
measurement; although care is required when choosing the opening
Leppinen et al. (1997) Copper and zinc rich complex ores
Qing et al. (2008) Lead–silver–zinc complex ores sizes of the syphon to ensure no bubbles enter the vessel and result in
Roos et al. (1990) Chalcocite and covellite inaccuracies (Gomez et al., 2003; Gomez and Finch, 2007).
Roos et al. (1990) Copper and chalcopyrite
Shen et al. (1997) Sphalerite and pyrite
3.8.1.3. Bubble size measurement sensor. The McGill bubble sizing
Uribe-Salas et al. (2000) Galena, chalcopyrite and pyritic ore
Walker et al. (1984) Chalcocite device (see Fig. 3, part C) is able to measure the full bubble size
Yuan et al. (1996) Complex copper/zinc sulphide ore with distribution found in the pulp phase. A sample is drawn from the pulp
pyrite and pyrrhotite via a tube and directed into a sloped viewing chamber (the sloped
window allows for a near mono-layer of bubbles to form) exposed to a
pre-set light source. The continuous flow of bubbles is then captured
via image analysis. The accuracy of the measurement is difficult to
establish, although the method is widely used and continues to evolve
3.8. Gas dispersion by improvements dictated by field trials (Gomez and Finch, 2007).

3.8.1. Instrumentation used for the measurement of gas dispersion 3.8.2. Implementation of gas dispersion variables in control systems
variables A recent publication by Bartolacci et al. (2008) focused on using
Gomez and Finch (2007) report that “gas dispersion is the collective gas dispersion sensors in conjunction with a Froth Stability Column
term for superficial gas (air) velocity (volumetric air flowrate per unit and machine vision (both still to be discussed). Air flowrate, pulp
cross sectional area of cell, Jg), gas holdup (volumetric fraction of gas in a level, reagent dosage and feed rate were varied whilst dispersion
gas-slurry mix, εg) and bubble size distribution (Db)”. The publication parameters, froth stability, bubble surface area flux and metallurgical
also details the equipment used for the measurement of these results were measured. The results indicated a high dependence of
variables. grade and recovery on dispersion parameters and froth stability; a
clear indication of the potential of these measurements being
3.8.1.1. Superficial gas velocity measurement sensor. The sensor consists integrated into an A/OFC system.
of a vertically positioned tube; the lower end is partially submerged in
the pulp zone to collect bubbles (see Fig. 3, part A). The continuous 3.9. Machine vision
version has an orifice valve mounted on the air outlet. When air is
allowed out of the orifice valve, time is given for a pressure steady- 3.9.1. Instrumentation and methods used for machine vision
state to be reached and measured (i.e. the rate of air into the column is Machine vision makes use of cameras positioned above flotation
equal to that out the orifice valve). The volumetric air flowrate is cells to record digital images of the froth surface. Several froth features
then inferred from a previous calibration and Jg calculated. Current can be extracted from these images and used for control purposes.

Fig. 3. Schematics of (A) gas velocity, (B) gas holdup and (C) bubble size measurement devices (Gomez and Finch, 2007).
64 B.J. Shean, J.J. Cilliers / International Journal of Mineral Processing 100 (2011) 57–71

These features are categorised into three types; namely: physical, for building better predictive flotation A/OFC models, based on visual
statistical and dynamic properties. Within each category several aspects of the froth as opposed to stream grades (Bergh and Yianatos,
methods exist for extracting different variables and/or features. For 2011).
example bubble size, a physical property of a froth, is one feature that
may be extracted through usage of bubble edge or watershed 4. Advanced flotation control
algorithms. An extensive amount of literature has been written
about the methods by which features are extracted from froth; with a AFC, also known as stabilising control, aims to reject the effects of
full, recent, literature review being carried out by Aldrich et al. (2010) input disturbances (e.g. a change of ore type) and maintain the
(see Table 2). flotation process as close to steady state as possible (McKee, 1991;
Aldrich et al. (2010) highlight that the use of physical features Laurila et al., 2002). This is generally achieved by controlling mass
for control purposes remains problematic. Issues associated with pull; recycle load; stream grade and/or recovery to setpoints (usually
physical feature extraction include: set by operators or an optimising controller), with the manipulated
variables being the setpoints of base level controllers (i.e. pulp level,
• It is commonly observed that the surface bubbles of flowing froths
air flowrate, reagent addition rate and pH/conductivity). As such,
are significantly larger than those in the layers immediately below;
effective AFC is only possible if robust, efficient base level flotation
the lower layers forming the predominant portion of the volume
control systems are in place.
overflowing into the launder. This cannot be corrected for readily.
• Neethling et al. (2003) observed that the surface film size
4.1. Advanced control of mass pull and re-circulating load
distribution is not necessarily representative of the bubble size
distribution in the underlying froth layer Wang and Neethling
An effective method of keeping the plant's mass balance at steady
(2009), however, have determined a method to relate surface film
state is to maintain constant mass pulls and/or re-circulating loads at
size to underlying bubble size distribution.
setpoints (often in conjunction with maintaining grade and/or recovery).
• The watershed method often over-segments larger bubbles and
under-segments smaller bubble sizes.
4.1.1. Mass pull control
Mobility feature extraction has been shown to be particularly Mass pull refers to the amount of concentrate collected. A recent
useful within the context of A/OFC. paper by Supomo et al. (2008) describes the successful installation
and operation of VisioFroth, a commercial machine vision based
3.9.2. Implementation of machine vision in control systems control system developed by Metso, at PT Freeport in Indonesia. The
It is common in industry for operators to control and regulate a control system measures the velocity of the overflowing froth, and
flotation plant by visual inspection of the froth surface. Indeed, an then adjusts the froth-depth to achieve the desired mass pull. An
understanding of processes occurring within the froth phase is central alternative commercial package, FloatStar Flow Optimiser by Mintek,
to understanding the overall behaviour of flotation systems (Glembotskii, uses density and flowrate measurements to calculate mass pull. The
1972; Cutting et al., 1986; McKee, 1991; Mathe et al., 1998). The structure required mass pull is then obtained through manipulation of pulp
of froths has a significant effect on grade and recovery; with several level and air flowrate (www.mintek.co.za).
publications (e.g. Supomo et al., 2008; Moilanen and Remes, 2008)
suggesting a link between froth velocity and metallurgical performance. 4.1.2. Re-circulating load control
As such, the development and implementation of machine vision was an Re-circulating material through a flotation plant results in decreased
attempt to refine and automate the control based on the froth appearance. residence time of material per flotation cell, but does allow for the
Currently, numerous commercial machine vision systems are available; valuable material to spend more time in the flotation plant as a whole;
making the on-line measurement of froth velocity possible. This is useful and, subsequently, increases the overall recovery (Wills and Napier-
in the implementation of A/OFC, an example being the measurement and Munn, 2006). However, this re-circulating load may need to be varied to
control of mass pull. Moreover, the faster dynamics of machine vision account for input disturbances (McKee, 1991). FloatStar Flow Optimiser
(1 min) compared to XRF technology (10–20 min), open the possibility is an example of a commercial control package which uses the

Table 2
Overview of methods used for feature extraction by machine vision (Aldrich et al., 2010).

Type Methods Froth variables or features References

Physical Edge Bubble size and shape Banford et al. (1998); Forbes and De Jager (2004b); Forbes et al. (2006); Lin et al.
(2007a,b); Wang et al. (2003); Wang and Stephansson (1999)
Watershed Bubble size and shape Forbes and De Jager (2004a); Sadr-Kazemi and Cilliers (1997); Ventura-Medina and
Cilliers (2000); Yang et al. (2008)
Statistical Spectral RGB Bonifazi et al. (2005a,b); Gebhardt et al. (1993); Hargrave et al. (1996, 1998); Hargrave
and Hall (1997); Morar et al. (2005); Oestreich et al. (1995); Siren (1999);
Vathavooran et al. (2006)
FFT Moolman et al. (1994)
Wavelets Bartolacci et al. (2006); Liu and MacGregor (2007, 2008)
Texture Hargrave and Hall (1997); Holtham and Nguyen (2002)
Co-occurrence matrices Spatial and neighbouring grey level Aldrich et al. (1995, 1997); Bezuidenhout et al. (1997); Moolman et al. (1994, 1995a,b)
Fractals Fractal descriptor Bonifazi et al. (2000); Hargrave and Hall (1997); Hargrave et al. (1998)
Latent variables PCA Bartolacci et al. (2006); Liu et al., (2005); Liu and MacGregor (2007, 2008)
Neural networks Estrada-Ruiz and Perez-Garibay (2009); Hyötyniemi and Ylinen (2000); Jeanmeure
and Zimmerman (1998); Kaartinen and Hyötyniemi (2005); Moolman et al. (1995c);
Niemi et al. (1997)
Dynamic Mobility Bubble tracking Botha (1999)
Block matching Barbian et al. (2007); Forbes and de Jager (2007); Holtham and Nguyen (2002);
Moolman et al. (1994); Supomo et al. (2008)
Pixel tracing Nguyen and Holtham (1997)
Stability Barbian et al. (2003, 2005, 2006); Moolman (1995); Morar et al. (2006)
B.J. Shean, J.J. Cilliers / International Journal of Mineral Processing 100 (2011) 57–71 65

measurement and manipulation of mass pull rates to regulate the collector addition rate based on concentrate grade). Furthermore,
amount of material recycled (www.mintek.co.za). continual analysis of plant data and corrective adjustment of the
predictive (model-based) controller make it adaptive to changing
4.2. Advanced control of grade and/or recovery conditions (i.e. adaptive control). Adaptive control is especially
important within the context of flotation control, which is prone to
AFC commonly refers to strategies that aim to maintain grade non-linear, complex behaviour. As such, many predictive flotation
and/or recovery (Laurila et al., 2002). However, McKee (1991) states control systems often (but not always) include adaptive control
that “A [stabilising] control system which is capable of firstly stabilising aspects. By 1991, Thornton noted that although the amount of
circuit performance, and then driving the circuit to a desired grade or literature devoted to multi-variable model-based control was exten-
recovery operating point, would undoubtedly be considered highly sive, the number of applications in industry was still comparatively
successful.” — highlighting the importance of the stabilising aspect of small; with McKee (1991) noting that 5 control strategies were
AFC. particularly common at the time (and largely remain so). These are:
The review of the successfulness of alternative AFC strategies is
• “Feed back control of collector addition to maintain recovery set points.
made difficult, as follow-up reports of implemented control strategies
• Feed forward control of collector based on the calculated metal content
are uncommon, as noted by McKee (1991); who suggested that this
of the new feed.
was because most control systems do not remain in operation for
• Maintaining concentrate flows within limits, usually by varying
periods of years after installation and are shut down. Furthermore,
aeration rates or pulp levels.
Wills and Napier-Munn (2006) add that few (if any) plants can claim
• Maintaining circulating loads within limits, again by variation of
to have fully automated control systems that can run the plant un-
aeration rates or pulp levels.
supervised for long periods of time. Thus it seems that despite the
• Controlling aeration rates or pulp level to obtain concentrate grade set
large body of literature devoted to the subject, the successful
points.”
application of AFC (and indeed OFC) techniques into industrial
application have been largely unsuccessful. Reasons given for this in Despite the apparent popularity of adaptive multivariable model-
literature include: based controllers, Desbiens et al. (1994), and Gupta and Yan (2006)
note issues with the stability of adaptive control; with the controllers
• Design of control systems are insufficiently thought out during plant
becoming saturated, and un-adaptive, after a period of time.
design stages (Narraway et al., 1991; Thwaites, 2007; Bergh and
Moreover, in spite of the majority of the predictive multivariable
Yianatos, 2011); and major control variables are often only
control strategies being based on empirical correlations, research and
identified once the plant is operational (Wills and Napier-Munn,
development of phenomenological models – whereby relationships
2006). This commonly results in poorly designed, incompetent,
between cause and effect are devised through an understanding of the
control systems being installed on new plants; with later (often
physics of the flotation process – for use in predictive controllers was
inadequate) modifications being required; or additional ad-hoc
also conducted. As such, phenomenological modelling methods can
control systems being added on as ‘after-thoughts’.
broadly be classified into 3 groups; namely: kinetics, population
• A vast knowledge of control systems and jargon is required to
balance and probabilistic based modelling (Polat and Chander, 2000).
develop, install and maintain A/OFC systems; with the majority of
The success of phenomenological modelling, within an AFC context, is
operators/metallurgists/management not having a background in
debatable.
control engineering (Hodouin et al., 2001; Thwaites, 2007; Wills
The use of first-order flotation kinetics modelling is thoroughly
and Napier-Munn, 2006).
covered by Polat and Chander (2000), and has undoubtedly received
• As already discussed, the non-linear, complex behaviour of flotation
the most attention in literature. Kinetics modelling “is based on
systems complicates modelling attempts; making the design of
the assumptions that the rate of the particle–bubble collision process is
robust, effective controllers – that can deal with large ranges of
first-order with respect to the number of particles and that the
operating conditions – difficult.
bubble concentration remains constant”. Numerous batch experiments
It is partially for these reasons (specifically the latter two) that (Imaizumi and Inoue, 1963; Tomlinson and Flemming, 1963; Harris
Wills and Napier-Munn (2006) argue that the best control systems and Chakravarti, 1970; Jameson et al., 1977; Dowling et al., 1985;
are those that interact with the operator (i.e. supervisory control Rastogi and Aplan, 1985) and continuous flotation tests (Jowett and
systems), giving explanations, when alterations to setpoints/variables Safvi, 1960) support the use of the first-order rate equation. This has
of base level flotation control systems are required; and as such, allowed a flotation cell to be modelled using the chemical reactor
experienced, conscientious operators currently remain a competitive analogy; whereby the removal of solids from the pulp phase is defined
alternative towards any automated control system. by a first order rate equation. This means a bank of cells can be
According to Gupta and Yan (2006), there are broadly two types of approximated by perfectly mixed CSTR's in series (Gaudin, 1957;
AFC used in mineral processing (a hybrid between the two is also Niemi and Paakkinen, 1969; Atkins et al., 1986; Yianatos and
possible). These are: Hendrìquez, 2006). Subsequently, efforts have been made to
accurately determine the so called ‘over-all flotation rate constant’
• Use of model-based methods
(or k). This is not trivial, as k is dependent on particle size, degree of
• Use of expert control systems
liberation, air flowrate, agitation, etc. To account for this, various
The evolution and current trends of each of these branches will continuous distribution functions of k have been devised (Polat and
now be discussed. Chander, 2000); although previous reviews by Dowling et al. (1985)
conclude that no single distribution model could sufficiently repre-
4.2.1. Model-based methods in advanced flotation control sent k; and Roesch et al. (1976), suggest that attempts based on the
Model-based methods can be further sub-categorised into two first order kinetics assumption are “approximative and hide secondary
categories, namely: empirical and phenomenological modelling (Polat details”.
and Chander, 2000). Alternatively, a population balance model is presented by Bascar
Empirical models make use of statistical methods to relate (1982), Bascar and Herbst (1982), and Bascur (2000). The three phase
measured input and output plant data, such that multivariable models model represents each mineralogical species and particle size, with
relating between two or more independent and dependant variables each particle species being classed according to state in the slurry (i.e.
can be established and used for predictive control (e.g. controlling free in pulp, attached to bubble in pulp, free in the froth, attached to
66 B.J. Shean, J.J. Cilliers / International Journal of Mineral Processing 100 (2011) 57–71

bubble in froth). Kinetic equations relate transfer of particles between of examples of a specific class. As such, a given system (e.g. a froth
slurry states and hydrodynamic considerations (e.g. power dissipa- surface) can be categorised — and appropriate control action taken if
tion into pulp, gas holdup in pulp, etc.) are incorporated into the required (Aldrich et al., 1997; Filipic and Junkar, 2000).
population balance. This makes it possible to simulate the effects of • Fuzzy logic — reasoning that serves to be approximate rather than
manipulated variables such as air flowrate, pulp level, agitation, etc. precise. Compared with binary logic, where a result is false or true
on a flotation process. (or quantitatively 0 or 1), fuzzy logic caters for a degree of truth
Despite much research into both empirical and phenomenological (anywhere between 0 and 1). Flotation system parameters (e.g.
based modelling, authors such as Bergh and Yianatos (2011) and pulp level) are divided into fuzzy sets (according to defined
McKee (1991) highlight several issues that still exist; the latter membership functions), which can subsequently be combined to
concluding that “Multivariate predictive control is ideally the solution form fuzzy subsets. A response to a fuzzy set/subset is then applied,
for high quality control. However, to be applicable without losing its using IF–THEN rule based strategies (Gupta and Yan, 2006). For
benefits, good measurements, acceptable regulatory control of local example, if froth velocity and air rate are the variables being
objectives (i.e. base level controls), reliable dynamic models, explicitly arranged into fuzzy subsets, the control logic might be something
stated process constraints and new methods to promote robustness are like: IF froth velocity is low AND air rate is high, THEN decrease froth
needed. Flotation processes have weaknesses in most of those aspects.” It depth; ELSE IF froth velocity is low AND air rate is low/medium,
is for reasons such as these that expert control systems (where THEN increase air rate; ELSE do nothing.
decision making by operators is automated by use of artificial
intelligence) are used. One area in which AI has been used extensively is the identification
and categorisation of froth images from machine vision. Aldrich et al.
4.2.2. Expert systems in advanced flotation control (1997) trialled and compared inductive learning techniques with a
The potential of expert systems in the mineral industry was back-propagation neural net method in industry; with all methods
recognised as early as 1983 (Bearman and Milne, 1992); and were being found to be equally capable of classification of various froth
introduced into A/OFC as modelling of flotation systems is difficult, features. Similarly, Cipriano et al. (1998) used rule-based expert
they are suitable for the handling of non-linear systems, and they control, combined with machine vision, to control rougher cells. The
automate (and standardise) decision making by operators. Although supervisory controller was able to identify froth characteristics and
several methods of Artificial Intelligence (AI) based control systems subsequently suggest actions to be taken to the operators. More
exist, three important techniques include: recently, Supomo et al. (2008) reported on the successful use of the
commercial control software VisioFroth on PT Freeport, in Indonesia.
• Artificial neural networks (ANN) — data-driven computing devices, The system combines expert control with machine vision to control
comprising of a large number of neurons, inter-connected by a pre- mass pull, and has reportedly resulted in increased recovery.
determined network of synapses on a large scale. These neurons are Similarly, PlantVision by KnowledgeScape also makes use of expert
arranged in several layers and adjustable numerical weights are control.
associated with the connecting synapse network (see Fig. 3). Neural In a comparison between expert control and multivariable model-
networks are trained by iteratively updating the associated weight based control methods, Zavala et al. (1995) compared a supervisory
matrix, such that a set of outputs can be predicted for a given set of system of multiple SISO PID regulators, a multivariable model-based
inputs. As such, an ANN based controller can be ‘taught’ how to predictive controller and an expert rule-based controller on a
manipulate base level control system's setpoints to maintain a given simulated flotation system. The findings included that: the expert
metallurgical objective; an example being the changing of collector system readily became saturated, the PID controllers were difficult to
addition rate to maintain recovery (Aldrich et al., 1997; Gupta and tune, while the model-based controller required a linear model of the
Yan, 2006) (Fig. 4). system; the suitability of such a model to handle all disturbance types/
• Inductive machine learning — makes use of mathematical models to magnitudes being unlikely. Tighter control was obtained with the
generate rules and form induced decision trees, and is based on the model-based controllers. Subsequent studies by Pérez-correa et al.
concept of information entropy. A set of samples, each with a (1998) and Osorio et al. (1999) altered the model-based controllers to
corresponding vector of classifying attributes (e.g. bubble size, froth become more flexible to varying conditions (although a high degree of
velocity, etc.) is assessed. The vector is then split according to the on-line mathematical manipulation was required); and altered the
most informative attribute (each split forming a branch of the expert controllers to avoid control saturation while achieving high
decision tree); with each newly formed subset subsequently being recoveries — despite severe simulated input disturbances.
re-split (according to a different attribute) until each subset consists The combination of AI and model-based methods is also possible.
Cubillos and Lima (1997, 1998) noted that using ANN to model
flotation systems is problematic (due to the many associated degrees
of freedom and the heavy computational requirements). However,
such issues are averted, and the full advantages of ANN realised, by
implementing neural network systems into predictive model-based
control systems, such that the AI system is responsible for updating/
modifying constants within the model with time; thus allowing the
hybrid controller to remain adaptive. Testing of this hybrid control
strategy offered promising results, with the controller reportedly
being robust and flexible.

5. Optimising flotation control

The upper-most tier of process control in flotation is OFC, which by


definition aims to maximise the financial feasibility of the process.
This is achieved by determining where on the theoretical grade–
recovery curve is most profitable to operate and, subsequently, shifting
Fig. 4. Simplified diagram of a neural network (Gupta and Yan, 2006). the operating point orthogonally to further maximise profit (see Fig. 5).
B.J. Shean, J.J. Cilliers / International Journal of Mineral Processing 100 (2011) 57–71 67

varied to four cells in a rougher bank, and the air rate that yielded the
PAR identified in each of the cells. Moreover it was shown that
operating the cells at their PAR air rates resulted in a higher mineral
recovery being obtained.
The link between operating cells at PAR air rates and improved
flotation performance was also shown in studies presented by Smith
et al. (2010) and Hadler et al. (2010), where it was shown that
optimising air recovery in a bank of cells resulted in either a higher
concentrate grade, a higher mineral recovery, or in many cases both.
This has important implications for control as air recovery is a single
quantitative variable that can be measured and maximised; and the
process optimised in terms of grade and recovery.
Other methods of OFC exist; some using modelling and others
resorting to expert control methods.
Fig. 5. Grade–recovery curve illustrating optimising control objective (Wills and
Napier-Munn, 2006).
5.1. Modelling-based methods in optimising flotation control

This in turn creates recovery and/or concentrate grade setpoints for the Many model-based optimising flotation controllers are algorithms
lower AFC/base level control structures (Laurila et al., 2002). However, that locate the optimal operating point on the grade–recovery curve;
OFC should only affect lower control levels if the process is at steady and then present recovery and grade setpoints to lower control
state (McKee, 1991). systems and/or plant operators/management. Flintoff (1992) presents
Grade–recovery curves vary according to feed grade and can be the principal of iso-economic contours; which are presented as
altered through manipulation of plant operating variables such as air negatively sloped straight lines on a grade–recovery curve that are
rates. In this way, grade–recovery curves can be optimised (Neethling calculated according to the price of final product, smelting costs,
and Cilliers, 2008). An example of this is presented by Hadler and transportation costs, etc. The optimal operating position is then found
Cilliers (2009), whereby the grade–recovery curve for a bank of four by locating the point at which the calculated iso-economic contour is
rougher cells was optimised by maximising the stability of the froth tangent to the grade–recovery curve (generated from plant data).
within each cell. Other modelling-based optimising controllers are more complex,
The use of froth stability as a parameter was first presented by and also consider operating parameter limits and technical details (i.e.
Moys (1984), who published a study whereby the horizontal velocity not solely economical factors). Muñoz and Cipriano (1999) present a
of the froth could be related to the froth stability, α (also defined as model-based control strategy that aims to both regulate and optimise
the air recovered into the launder in the form of unbroken bubbles). a combined primary grinding and flotation circuit. The optimising
Using this quantitative measure of froth stability, Woodburn et al. branch of the controller aims to maximise financial profit using non-
(1994) developed a semi-empirical froth-based flotation model that linear dynamic modelling; encompassing both technical (e.g. mill
combines a conceptual froth structure with the kinetics of flotation; power limits, sump level limits, etc.) and economic criteria (e.g. metal
the latter being based on the flux of bubble surface area overflowing prices, grinding costs, etc.). More recently, Maldonado et al. (2007),
from the cell (see Eq. (1)). proposed a method “considering phenomenological models for each
flotation bank of the circuit, validated using process data obtained from
ΨB = αQ a Sb ≈ðζvf hwÞ Sb ð1Þ several sampling surveys.... The control objective is the minimisation of
the Cu tailing grade in each bank given a final Cu concentrate grade.” This
In this model the flux of bubble surface area (ΨB) is calculated is achieved through dynamic programming methods, such that non-
from the volumetric air flowrate into the cell (Qa), the specific bubble linear behaviour can be accounted for; with promising simulation
area (Sb) and the air recovery, α. This is approximately the same as results being obtained.
relating ΨB to the specific bubble area, froth velocity (vf), froth height
(h), weir length (w) and the volume fraction of the froth that is air (ζ), 5.2. Expert methods in optimising flotation control
usually taken as unity. This relationship was simplified by Barbian
et al. (2003), who suggested the value of α can be calculated by Laurila et al. (2002) suggest “new expert systems are concentrating
Eq. (2). to solve the issue of feed type classification, which is a challenging and
important task.” It has already been mentioned that the grade–
α≈ζ vf h w=Q a ð2Þ recovery curve is a function of the ore type, and hence it is logical that
operating parameters and dosing rates should be altered accordingly
Barbian et al. (2003, 2005, 2006) measured froth stability at if possible. Laine (1995) adds that the performance of such a control
laboratory and industrial scales using two different methods; air strategy is decided by the ability of the system to effectively classify
recovery and the Froth Stability Column. The air recovery was the feed ore, which in turn is dependent on the information received
determined using image analysis to measure the froth velocity, with by the classification algorithm. The on-line measurement technique
the overflowing froth height being measured visually. The Froth must extract adequate useful information; whilst the algorithm must
Stability Column is an alternative measure of froth stability compris- be able to effectively (and readily) classify ore into one of the defined
ing a non-overflowing column in which the froth rises unhindered. ore type classes. This would allow for a feedforward type controller to
The rate of froth growth and maximum froth height achieved are used alter upstream operating parameters so as to optimally process each
to give a quantitative measure of froth stability. A good correlation defined ore type. An example of such an expert system is presented by
was shown between the two froth stability measures, suggesting the Jämsä-Jounela et al. (2000); where Kohonen self organising maps
potential for both as future measures of froth stability at an industrial (a type of ANN) are used for classification of the ore feed information
scale. Of greater interest, however, were the results shown by Barbian gathered from instrumentation. Once the ore is classified, the expert
et al. (2006), where a peak in froth stability was shown as the air control system alters the setpoints of lower control systems and sends
flowrate increased. A peak in air recovery (or ‘PAR’) was also shown in information to operators; with the performance being indicated by an
the study by Hadler and Cilliers (2009), in which air flowrate was “economical success index display”.
68 B.J. Shean, J.J. Cilliers / International Journal of Mineral Processing 100 (2011) 57–71

Table 3
Summary of literature review focusing on various types of control.

Branch Type References

Modelling based Feedback predictive MIMO Hodouin et al. (1993)


Feedback and feedforward predictive MIMO Del Villar et al.(1999); Desbiens et al. (1998b); Ding and Gustafsson
(1999); Hodouin et al. (2000); Hulbert (1995); Zavala et al. (1995)
Non-linear mathematical modelling Benaskeur and Desbiens (1999); Delport (2005); Desbiens et al. (1998a);
Maldonado et al. (2007)
Adaptive control Desbiens et al. (1994); Jämsä-Jounela (1992); Sbarbaro (1999); Thornton
(1991)
Modelling/AI based hybrids Hierarchical combination of expert Bergh et al. (1995); Cubillos and Lima (1997, 1998); Gaulocher et al.
and modelling (2008); Núñez et al. (2010)
AI based Supervisory control Benford and Meech (1992); Bergh et al. (1996, 1998, 1999); Bergh and
Yianatos (1999); Cipriano et al. (1991); McKay and Ynchausti (1996)
Fuzzy logic Carvalho and Durão (1999, 2000, 2002); Cipriano et al. (1998); Hirajima
et al. (1991); Osorio et al. (1999); Suichies et al. (1998, 2000)
Neural networks Aldrich et al. (1997); Cortez and Durão (1995); Durão and Cortez (1995);
Moolman et al. (1995d)
Inductive learning Aldrich et al. (1997)
Integrated flotation and grinding control Modelling and/or AI based Bascur (1991); Muñoz and Cipriano (1999); Pulkkinen et al. (1993); Sosa-
Blanco et al. (2000)

However, despite the various OFC strategies outlined in literature, Optimiser (these first three have already been discussed), FloatStar
many mineral processing plants currently rely on operators and plant Grade–Recovery Optimiser and FloatStar Reagent Optimiser. FloatStar
management to manually select setpoints of lower control systems, Grade–Recovery Optimiser, an OFC, uses online grade analysis to
based on past experience, in order to optimise the process (Laurila ensure that recovery is maximised for a specified grade; through
et al., 2002). manipulation of level, air flowrate, re-circulating load and reagent
addition setpoints across the plant. FloatStar Reagent Optimiser uses a
6. Examples of approaches found in advanced/optimising combination of control approaches (such as fuzzy logic and non-linear
flotation control multivariable predictive control) to automate the manipulation of
reagent addition rates (see Fig. 6; www.mintek.co.za).
Various methods of achieving AFC and OFC have been discussed. A Several commercial systems make use of machine vision; these
summary of examples using some of these different advanced include: VisioFroth by Metso (www.metso.com), FrothMaster by
methods are presented in Table 3 (adapted from (Hodouin et al., Outotec (www.outotec.com) and PlantVision by KnowledgeScape
2001)). It should be noted that although the methods are divided into (www.kscape.com). Measured variables include froth velocity, bubble
groups, some overlap between methods is inevitable (e.g. adaptive size distribution, stability and colour. Expert systems are used to
model-based controllers are inevitably also classed as predictive manipulate variables such as pulp level, air addition rate, reagent
controllers). addition and/or water addition in a bid to increase recovery at a set (or
improved) concentrate grade. Each of these systems has been
successfully trialled and incorporated on plants. For example, VisioFroth
7. Commercial advanced/optimising flotation control software
was successfully implemented on the PT Freeport plant in Indonesia
(Supomo et al., 2008) (Table 4).
Various commercial A/OFC systems are available on the market
and have been trialled and implemented in industry; many of which
have already been mentioned in this communication. 8. Conclusions
One such control package is the FloatStar suite; which consists of
FloatStar Level Stabiliser, FloatStar pH controller, FloatStar Flow Despite several advances in base level controls since the 1970s,
reports of fully automated advanced and optimising flotation control
systems operating successfully (and unassisted) for long periods
remain scarce. It is hoped, however, that through continued
development of new, robust technologies (e.g. machine vision and
air recovery measurement) and the continued simplification/modifi-
cations of plant designs (requiring less-intricate control systems),
long term, automated advanced and optimising flotation control
will be achievable. Such an outcome would indeed be financially
rewarding.

Acknowledgements

The authors would like to thank Prof. Raymond Shaw, Dr. Stephen
Neethling and Dr. Kathryn Hadler of Imperial College London for their
valuable input and advice.

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