Anchor Scan Parameters

Dataset Name: 90 C, 25%

File name: D:\SEMEN PADANG 2018\5\JORDY\90 C\90 C, 25%\90 C, 25%.xrdml
Comment: sampel serbuk
Configuration=Reflection-Transmission Spinner, Owner=User-1, Creation
date=9/5/2012 12:30:22 PM
Goniometer=PW3050/60 (Theta/Theta); Minimum step size 2Theta:0.001;
Minimum step size Omega:0.001
Sample stage=Reflection-Transmission Spinner PW3064/60; Minimum step size
Phi:0.1
Diffractometer system=XPERT-PRO
Measurement program=C:\PANalytical\Data Collector\Programs\program
1.xrdmp, Identifier={A5A64079-D6FE-4BDF-87FE-E71B1E14F554}
Gonio (sampel serbuk)
Measurement Date / Time: 9/10/2018 1:35:26 PM
Operator: User
Raw Data Origin: XRD measurement (*.XRDML)
Scan Axis: Gonio
Start Position [°2Th.]: 10.0181
End Position [°2Th.]: 99.9781
Step Size [°2Th.]: 0.0260
Scan Step Time [s]: 7.1400
Scan Type: Continuous
PSD Mode: Scanning
PSD Length [°2Th.]: 3.35
Offset [°2Th.]: 0.0000
Divergence Slit Type: Fixed
Divergence Slit Size [°]: 0.8709
Specimen Length [mm]: 10.00
Measurement Temperature [°C]: 25.00
Anode Material: Cu
K-Alpha1 [Å]: 1.54060
K-Alpha2 [Å]: 1.54443
K-Beta [Å]: 1.39225
K-A2 / K-A1 Ratio: 0.50000
Generator Settings: 30 mA, 40 kV
Diffractometer Type: 0000000011130968
Diffractometer Number: 0
Goniometer Radius [mm]: 240.00
Dist. Focus-Diverg. Slit [mm]: 100.00
Incident Beam Monochromator: No
Spinning: No

Graphics
Peak List

Pos.[°2Th.] Height [cts] FWHMLeft[°2Th.] d-spacing [Å] Rel. Int. [%]

25.8024 185.14 0.3070 3.45292 61.78
31.7135 299.69 0.3582 2.82153 100.00
32.1443 274.60 0.3070 2.78470 91.63
32.9328 136.73 0.3582 2.71981 45.63
33.9377 63.07 0.4093 2.64153 21.04
35.7108 209.19 0.5117 2.51435 69.80
39.6208 55.32 0.6140 2.27476 18.46
43.4508 35.02 0.8187 2.08272 11.69
46.5995 98.05 0.4605 1.94907 32.72
49.4503 95.42 0.3582 1.84318 31.84
53.1790 59.75 0.3070 1.72240 19.94
57.2562 67.64 0.3582 1.60906 22.57
63.1070 95.80 0.7164 1.47324 31.97
78.2664 33.42 0.6140 1.22153 11.15

Pattern List

Visible Ref.Code Score Compound Name Displ.[°2Th] Scale

Fac. Chem. Formula
01-074-0566 24 Calcium Hydroxide .. 0.000
1.062 Ca10 ( P O4 )6 ( O..
01-075-0449 33 Iron Oxide 0.000
0.672 Fe3 O4

Document History
Insert Measurement:
- File name = "90 C, 25%.xrdml"
- Modification time = "9/10/2018 3:22:22 PM"
- Modification editor = "User"

Default properties:
- Measurement step axis = "None"
- Internal wavelengths used from anode material: Copper (Cu)
- Original K-Alpha1 wavelength = "1.54060"
- Used K-Alpha1 wavelength = "1.54060"
- Original K-Alpha2 wavelength = "1.54443"
- Used K-Alpha2 wavelength = "1.54443"
- Original K-Beta wavelength = "1.39225"
- Used K-Beta wavelength = "1.39225"
- Irradiated length = "10.00000"
- Spinner used = "No"
- Receiving slit size = "0.10000"
- Step axis value = "0.00000"
- Offset = "0.00000"
- Sample length = "10.00000"
- Modification time = "9/10/2018 3:22:22 PM"
- Modification editor = "User"

Interpolate Step Size:

- Derived = "Yes"
- Step Size = "0.01"
- Modification time = "9/10/2018 3:22:22 PM"
- Modification editor = "PANalytical"

Smooth:
- Polynomial type = "Quintic"
- Convolution range = "25"
- Degree of smoothing = "10"
- Fast Fourier = "Yes"
- Omit Peaks = "Yes"
- Modification time = "9/10/2018 3:22:31 PM"
- Modification editor = "User"

Smooth:
- Polynomial type = "Quintic"
- Convolution range = "25"
- Degree of smoothing = "10"
- Fast Fourier = "No"
- Omit Peaks = "Yes"
- Modification time = "9/10/2018 3:22:34 PM"
- Modification editor = "User"

Search Peaks:
- Minimum significance = "1"
- Minimum tip width = "0.3"
- Maximum tip width = "1"
- Peak base width = "2"
- Method = "Minimum 2nd derivative"
- Modification time = "8/16/2018 3:51:04 PM"
- Modification editor = "User"

Search & Match:

- Allow pattern shift = "No"
- Auto residue = "Yes"
- Data source = "Profile and peak list"
- Demote unmatched strong = "No"
- Multi phase = "Yes"
- Restriction set = "Untitled"
- Restriction = "Restriction set"
- Subset name = ""
- Match intensity = "Yes"
- Two theta shift = "0"
- Identify = "No"
- Max. no. of accepted patterns = "5"
- Minimum score = "25"
- Min. new lines / total lines = "50"
- Search depth = "10"
- Minimum new lines = "3"
- Minimum scale factor = "0.0001"
- Intensity threshold = "0"
- Use line clustering = "Yes"
- Line cluster range = "1.5"
- Search sensitivity = "1.8"
- Use adaptive smoothing = "Yes"
- Smoothing range = "1.5"
- Threshold factor = "3"
- Modification time = "5/26/2015 8:52:30 AM"
- Modification editor = "User"

Search & Match:

- Allow pattern shift = "No"
- Auto residue = "Yes"
- Data source = "Profile and peak list"
- Demote unmatched strong = "No"
- Multi phase = "Yes"
- Restriction set = "Untitled"
- Restriction = "Restriction set"
- Subset name = ""
- Match intensity = "Yes"
- Two theta shift = "0"
- Identify = "No"
- Max. no. of accepted patterns = "5"
- Minimum score = "25"
- Min. new lines / total lines = "50"
- Search depth = "10"
- Minimum new lines = "3"
- Minimum scale factor = "0.0001"
- Intensity threshold = "0"
- Use line clustering = "Yes"
- Line cluster range = "1.5"
- Search sensitivity = "1.8"
- Use adaptive smoothing = "Yes"
- Smoothing range = "1.5"
- Threshold factor = "3"
- Modification time = "5/26/2015 8:52:30 AM"
- Modification editor = "User"

Subtract Background:
- Add to net scan = "Nothing"
- User defined intensity = "-26"
- Correction method = "Automatic"
- Bending factor = "0"
- Minimum significance = "0.7"
- Minimum tip width = "0"
- Maximum tip width = "1"
- Peak base width = "2"
- Use smoothed input data = "Yes"
- Granularity = "30"
- Modification time = "8/30/2018 11:20:03 AM"
- Modification editor = "User"