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Abstract
Changes in the velocity, amplitude and attenuation of ultrasonic waves are accompanied by
physical changes during rock failure. A large number of triaxial compression tests were
performed to study the progressive failure of shale rock according to these physical properties.
The tested shale samples had different bedding planes and were subjected to different confining
pressures. During the experiments, ultrasonic wave testing was used to monitor the progressive
failure process and to evaluate different characteristic points. Variations were interpreted by
analyzing the ultrasonic velocity and amplitude. Failure points cause velocity drops that are
greater in the P than in the S waves. The percentage wave amplitude decrease at dilatancy point
was determined and that of the P wave is double that of the S wave, which indicates that the P
wave is more sensitive. The shale sample attenuation was analyzed, and the results show that
samples with high density and high homogeneity tend to have a higher attenuation coefficient.
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Figure 3. P-waveform of sample sz-30-0-1. (a) A single waveform curve; (b) all the P-waveforms in the loading process.
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Figure 4. Relationships between wave–velocity curve and stress–strain curve from tests. Dots are ultrasonic measurement points.
Differential stress is the difference between maximum prin- through sample, tp¢ is the time of preliminary wave of P wave
cipal stress σ1 and minimum principal stress σ3. which received by the receiving probe, ts¢ is the time of pre-
The P and S wave velocities are defined as: liminary wave of S wave which received by the receiving
vp = l t p = l (t p¢ - t p0) (1 ) probe, tp0 is the time of P wave produces by the emission probe,
ts0 is the time of S wave produces by the emission probe and l is
vs = l ts = l (ts¢ - ts0) , (2 )
the shale sample length.
where tp is the time for the P wave to be transmitted through Rock failure process can be divided into five stages (see
the sample, ts is the time for the S wave to be transmitted figure 5): crack closure (OA), elastic deformation (AB), crack
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Figure 4. (Continued.)
initiation and stable crack growth (BC), crack damage and can be identified from the inflection of the volumetric strain
unstable crack growth (CD) and post-peak behavior (DE) curve because the volumetric strain of the rock will reach a
(Brace et al 1966, Bieniawski 1967, Martin and Chandler maximum. The stress at point C is termed as dilatancy point
1994, Qin et al 2010, Sun et al 2014, Xue et al 2014a, 2014b, stress. The velocity and magnitude of the P and S waves will
Xue 2015, Xue et al 2015). Point C is the demarcation point exhibit sharp changes at this point.
of the stable crack growth phase and unstable crack growth From the experimental results, it is obvious that in the
phase and represents the dilatancy point. The dilatancy point crack closure stage, microcracks such as pores and joints
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Table 1. Ultrasonic wave–velocity change at failure. illustrates that discontinuities such as microvoids or micro-
Specimen No. −1
Δvp (m s ) −1
Δvs (m s )
cracks in shale samples did not grow into a large scale before
failure.
sz-0-20-1 −205 −114 Many studies have indicated (Shao et al 1987, Chen
sz-0-40-2 −44 −12 1989, Chen et al 1990, Zhao et al 1996, Li et al 2006, Liu
sz-0-70-2 −57 / et al 2008, Zheng et al 2009) that the ultrasonic wave velocity
sz-0-100-1 −222 −100
exhibits an abrupt change around the dilatancy point. Clear
sz-30-20-1 −498 /
sz-30-40-1 −182 −31 differences exist between our experimental results and those
sz-30-70-3 −77 −67 of other scholars. Several reasons may account for this
sz-30-100-1 −65 −21 behavior. Firstly, shale is a typical brittle rock with a dense
sz-60-40-1 −68 −23 lithology, and plastic deformation is not easy to observe. The
sz-60-70-1 −141 −37 average density of the Longmaxi marine shale samples in our
sz-60-100-1 −60 −4 tests is relatively high at 2.62 g cm−3. Therefore, the variation
sz-90-20-2 −167 −76 in wave velocity is insensitive to crack evolution. Secondly,
sz-90-40-2 −111 −12 the damage forms present splitting or shear failure under
sz-90-70-2 −65 −21
different confining levels and different bedding orientations
sz-90-100-2 −197 −125
(He and Huang 2003, Li et al 2012, Jia et al 2013, Chen
Note. The backslash ‘/’ means the missing data et al 2014). The different damage forms in axial and radial
that is not detected. direction may lead to different wave velocity variations.
The decreases in P wave (Δvp) and S wave (Δvs) at the
close under compression, which leads to a decrease in por- failure point are shown in table 1. A comparison of Δvp and
osity. The velocity of the ultrasonic wave has increased. Δvs during the damage process shows that vp changes sig-
During elastic deformation, stable crack growth and unstable nificantly compared with vs in all four bedding orientations
crack growth, the ultrasonic velocity tends to increase slightly θ=0°, 30°, 60° and 90°, which indicates that the P wave is a
and then it stabilizes. At the dilatancy point, the P and S more sensitive indicator to stress response and can better
waves do not show an apparent change. This behavior reflect damage conditions.
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Figure 6. Wave amplitude and stress–strain relationships for shale samples with inclination θ=0°, 30°, 60° and 90°. Dots are ultrasonic
measurement points.
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Figure 6. (Continued.)
Here, σ3 is confining stress, σf is failure point stress, σd is The sharper decrease in P wave amplitude is visible at the
dilatancy point stress, εf is failure point strain, and E is flexure of the volumetric strain curve (dilatancy point). We
elastic modulus. The value of elastic modulus E listed in select the inflection points on volumetric strain curves and
table 2 are calculated by stress–strain curves and may make red dashed lines. The inflection point is the dilatancy
contain errors. point which indicates microcrack coalescence and sample
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Table 4. Wave attenuation, density and shape parameter m for the pressure of 0 and 70 MPa has a high density at 2.73 g cm−3,
tested samples. whereas the others have an average value of 2.61 g cm−3. The
Attenuation Attenuation points circled in figures 7(b) and (c) have an average density
(P) (S) of 2.73 g cm−3. It can be seen from experimental results
Specimen no. (dB mm−1) (dB mm−1) ρ (g cm−3) m (table 4) that among the set with the same θ and confining
pressure σ3, samples with a relatively high attenuation have
sz-0-0-1 0.22 0.17 2.62 6.59
high density and larger m values.
sz-0-0-2* 0.27 0.23 2.73 11.6
sz-0-0-3 0.20 0.04 2.62 7.26
sz-0-70-1* 0.13 0.18 2.73 4.98
sz-0-70-2 / / 2.61 2.25
sz-0-70-3 / / 2.61 2.68
4. Conclusions
sz-30-20-1* 0.34 / 2.73 7.37
sz-30-20-2 0.02 / 2.62 6.19 Sixty Longmaxi shale samples were tested under different
inclinations and confining pressures with triaxial compression
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