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of the Laws of Homogeneous Circuits and Intermediate Metals. The Law of Homogeneous Circuits states that
homogeneous thermocouple conductors are not affected by intermediate temperatures or temperature
differentials along the wires. This allows long thermocouple leads to be used in all temperature environments.
The Law of Intermediate Metals states a third metal can be introduced into the circuit without affecting the
temperature, providing the junctions with the third metal are at the same temperature. This allows the instrument
making the measurement to be a different metal than the thermocouple wires.
Over time, certain metals have been selected for producing standard thermocouples; some are shown in
Table 3.4. The most common type of thermocouple used on extruders is the K thermocouple. Hand-held
pyrometers used in plastic processing are typically either J or K thermocouples. Each thermocouple type has a
unique connector, color, and thermocouple wire. When ordering thermocouple wire, verify that the correct wire
and size is purchased for the thermocouple type and application. It is important to match the thermocouple to
the application.
Three thermocouple junctions, shown in Fig. 3.39, are commercially available, depending on the
application. Grounded junctions are used where electromagnetic induction or radio frequency interference is
present and can interfere with the thermocouple signal or measurement. These
have faster response times than insulated junctions. A second junction is the insulated ungrounded model with
a slower response time due to the insulation. These are typically used in extruders and hand-held pyrometers.
Exposed junction thermocouples have the fastest response time; however, with the exposed junction they are
easily damaged and susceptible to oxidation and temperature deterioration.
Thermocouple response time depends on the sheath diameter and the junction type. Smaller diameters have
a faster response. The advantages of thermocouples are their ruggedness, inexpensive nature, high
responsiveness, broad temperature range, and tip sensitivity. The disadvantages are that their outputs are not
linear and the accuracy depends on the purity of the metal wires used. The output nonlinearity is not a serious
limitation, as the measurement equipment normally takes this into account when correcting the response to
yield the proper reading.
The other temperature measurement device is called aresistance
temperature detector (RTD). RTD operation is based on electrical resistance
increasing or decreasing with temperature in a predictable manner. A probe,
shown in Fig. 3.40, is an assembly containing an element, sheath, lead wires,
and connections. The element that measures the temperature is platinum, copper,
or Figure 3.40. RTD probe. nickel wire wound around
a ceramic or glass core. To specify an RTD it is necessary to know the element
length, element diameter, and resistance in ohms at 0°C. Advantages
of RTDs versus thermocouples are the response is more linear and
the signal stability is better. The main disadvantage is slower response
time compared to a thermocouple.
dimension, assuming the extruder and puller speeds are properly set. Like melt temperature, melt pressure tells
the operator what is going on inside the extruder and die. Die pressure fluctuations correspond with output
fluctuations and dimensional changes. A Dynisco® pressure transducer is shown in Fig. 3.41.
ing and the temperature thermocouple near the end of the extruder controlling the last temperature zone.
Typical melt pressure curves recorded at the end of the barrel, the adapter, and the die are shown in Fig.
3.45. At the end of the screw, the pressure variation is
Figure 3.45. Melt pressure.
quite significant due to the extrudate spiraling action coming off the screw. Pressure fluctuations are caused by
the screw flight and the pressure gradient in the screw channel. Low pressure occurs where there is a break in
the melt stream due to the screw flight. High pressure occurs from the material at the edge of the pushing flight.
For this reason, head pressure measurement should not be taken where the flight will pass over the pressure
transducer. A good place to measure the head pressure is between the last flight and the screen pack. The screens
and breaker plate reorient the extrudate flow, reducing the differences between the peaks and valleys observed
at the end of the extruder. As the extrudate flows through the die, the flow channel capacitance further dampens
the high-frequency pressure fluctuations. If the pressure variations in the die were the same as at the end of the
extruder barrel, the product cross sectional dimensions would be constantly changing, and the final product
tolerances would be very broad.
Output as a function of the low-frequency pressure variation measured in the melt pipe or die is given by
Eq. (3.5):
(3.5)
where
∆Q = Change in volumetric output (percent)
∆P = Change in pressure (percent) n = Power law index
Assume the polymer being processed is polypropylene with a power law index of 0.35 (n = 0.35) and the
die pressure is varying from 1,950 to 2,050 psi for a ∆P of 100 psi.
Assuming the process is running at 200 pounds/hour, the variation in output is 29 pounds/hour. This flow
variation would have a major effect on the final product dimension. Head pressure variation should be kept as
low as possible, preferably 1% or less.