APPENDIX

A. EQUIPMENT

Equipment:
1. Erlenmeyer Flasks
2. Beaker Glass
3. Funnel Glass
4. Propipette
5. Ring stands, Ring, Clamps
6. Graduated Cylinder
7. Balance
8. Stirrer Glass
9. Volumetric Pipette
10. Spoon
11. Wash Bottle
12. Watch Glass
13. Glass Stoper
14. Burette
B. MATERIAL

Materials :
1. Methampyrone powder
2. HCl 0.02 N
3. Iodium 0.1 N
4. Starch solution
5. As2O3 powder (in oven)
6. NaOH 1 N
7. Methyl Orange Indicator
8. HCl 2 M
9. NaHCO3 powder
10. Aquades
C. STEP
I. Standardization of 0.1 N Iodine Solution

150 mg

Weigh carefully 150 mg Dissolve with 20 ml of 1 N Dilute with 40 ml of water

As2O3 which has been NaOH
dried at 105⁰C for 1 hour

Add 2 drops of methyl Add HCl until the yellow Add 2 g of NaHCO3 and
orange, and the solution color turns into pink color dilute it with 50 ml of
will turns into yellow water
color
 Titrate with iodine slowly
Add 3 ml of starch
and close the erlenmeyer
solution and it will turns with plastic and napkin to
into pale yellow cloudy avoid the light
Permanent blue color
appear when it reach end
point of titration

II. Determination of Methampyrone Concentration

200 mg

Weigh carefully 200 mg Dissolve in 5 ml of water Add 5 ml of 0.02 N HCl

of methampyrone

Titrate with 0.1 N iodine The solution will turns into

Add with starch as an immediately
indicator blue color
D. RESULT
I. Standardization of 0.1 N Iodine Solution

II. Determination of Methampyrone Concentration