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STANDARD
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ICS: 77.140.15
Descriptors: reinforcement of concrete, cold reduced mild steel wire, manufacturing process, chemical,
testing, packaging
© Copyright 2006
the public, protecting the consumers, facilitating domestic and international trade and
furthering international cooperation in relation to standards and standardisation.
http://www.dsm.gov.my http://www.sirim.my
E-mail: central@dsm.gov.my
CONTENTS
Page
Foreword ..…………………………………………………………………………………. iv
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1 Scope ……………………………………………………………….……………………… 1
3 Definitions …………………………………………………………………………………. 1
9 Quality ..……………………………………………………………………………………. 4
Tables
i
MS 144:2006
CONTENTS (continued)
Page
B2 Acceptability index (k) as a function of the number (n) of the test results (for a
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Annexes
ii
MS 144:2006
Committee representation
The Iron and Steel Industry Standards Committee (ISC P) under whose authority this Malaysian Standard was
developed, comprises representatives from the following organisations:
The Technical Committee on Steel Bars, Wire Rods and Wire Products which developed this Malaysian Standard
consists of representatives from the following organisations:
Universiti Malaya
Co-opted member:
iii
MS 144:2006
FOREWORD
This Malaysian Standard was developed by the Technical Committee on Steel Bars, Wire
Rods and Wire Products, under the authority of the Iron and Steel Industry Standards
Committee.
This Malaysian Standard is the third revision of MS 144:2001, Specification for cold reduced
mild steel wire for the reinforcement of concrete.
e) the title of Clause 13 has been replaced with “Routine inspection and testing;
f) in Table 3, the minimum tensile strength for Grade 500 steel has been changed to 525
2
N/mm ;
g) the number of years for the record keeping has been changed from “five years” to “ten
years”; and
Compliance with a Malaysian Standard does not of itself confer immunity from legal
obligations.
iv
MS 144:2006
1. Scope
This Malaysian Standard specifies the requirements for plain and deformed cold reduced mild
steel wires used for the reinforcement of concrete, and for the manufacture of steel fabric in
accordance with MS 145.
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Wire that may be used for the prestressing of concrete and wire used for ties, lifting and other
general engineering or industrial purposes is not included in this standard.
2. Normative references
The following normative references are indispensable for the application of this standard. For
dated references, only the edition cited applies. For undated references, the latest edition of
the normative references (including amendments) applies.
BS 6200, Sampling and analysis of iron, steel and other ferrous metals
MS 146, Hot rolled steel bars for the reinforcement of concrete – Specification
3. Definitions
For the purposes of this standard, the following definitions apply.
3.1 Batch
Any quantity of finished wire of one material type and size, produced by one manufacturer or
supplier, presented for examination at one time.
3.2 Bundle
That value of the yield stress below which fall not more than 5 % of the test results.
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MS 144:2006
3.5 Coil
A wire with surface characteristics designed to increase its bond with concrete.
The diameter of a wire with an area equal to the effective cross-sectional area of the wire.
3.9 Rib
A protrusion on the outside of the wire designed to increase its bond with concrete.
The stress measured during the tensile test when the total extension of the gauge length is that
specified in the grade.
d) the length of wire, if cut lengths are required (see 10.2); and
5. Preferred sizes
The preferred millimetre nominal sizes of wire are 4, 5, 6, 7, 8, 9, 10, 11, 12 and 13.
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MS 144:2006
6.2 The cross-sectional areas and mass of the preferred millimetre nominal sizes shall be
as given in Table 1.
a a
Nominal size Cross-sectional area Mass per metre run
2
(mm) (mm ) (kg)
4 12.6 0.099
5 19.6 0.154
6 28.3 0.222
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7 38.5 0.302
8 50.3 0.395
9 63.6 0.499
10 78.5 0.616
11 95.0 0.746
12 113.1 0.888
13 132.7 1.042
a
Cross-sectional area and mass are subjected to the tolerances specified in Clause 10.
6.3 The effective cross-sectional area and mass shall be determined as follows and be
subjected to the tolerances specified in Clause 10.
For a wire where the configuration is such that, by visual inspection, the cross-sectional area
is substantially uniform along the length of the wire, determine its effective cross-sectional are
by weighing and measuring to an accuracy of ± 0.5 % of a sample of the wire not less than
300 mm long.
2
Calculate the effective cross-sectional area, A (in mm ), using the equation:
M
A=
0.007 85L
where,
NOTE. This term includes both top and bottom-blown oxygen processes.
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MS 144:2006
8. Chemical composition
8.1 The chemical composition of the steel based on cast analysis shall be in accordance
with Table 2. In the case of precast concrete products, the carbon content shall be subjected
to the agreement between the manufacturer or supplier and the purchaser.
Carbon 0.25
Sulphur 0.060
Phosphorus 0.060
8.2 The carbon equivalent value of the steel derived from the following formula shall not
be greater than 0.42 %:
Mn Cr + Mo + V Ni + Cu
C + + +
6 5 15
where,
9. Quality
9.1 The wire shall be free from any defect that can be shown to affect adversely the
mechanical properties of the wire specified in this standard.
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MS 144:2006
For the purpose of checking a wire for compliance with the tolerances specified in this
standard, the nominal density of steel as defined in 3.7 shall be used.
If specified cut lengths are requested in the order, each wire shall be cut to within a tolerance
of ± 25 mm on the specified length.
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The tolerance on mass and cross-sectional dimensions shall be ± 3 % for all sizes.
Deformed wires shall be classified as Type 1 or Type 2. The type shall be determined from
the results of the bond performance tests given in Annex A or, if the shapes are applicable,
from the geometry of the wire as described in 12.3.
a) Type 1: A plain square twisted wire or a plain chamfered square twisted wire, each with
a pitch of twist not greater than 14 times the nominal size of the wire.
b) Type 2: A wire with transverse ribs with a substantially uniform spacing not greater than
0.8ø (and continuous helical ribs where present), having a mean area of ribs (per unit
length) above the core of the wire projected on a plane normal to the axis of the wire
2
not less than 0.15ø mm /mm where ø is the nominal wire size.
Wire described as indented shall comply with geometrical requirements of 12.4 and shall be
classified as Type 1.
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MS 144:2006
Where a wire is described as indented, the indentations shall be spaced along the wire at a
substantially uniform distance and shall be symmetrically disposed around the perimeter of
the section. A minimum of 25 % of the total surface area shall be indented by measurable
indentations and in each line of indentations along the wire, there shall be not less than 3.5
and not more than 5.5 indentations per 25 mm length. The angle between the direction of
indentation and the axis of the wire shall be not less than 40°.
All materials shall be subjected to routine inspection and testing as described in Annex B and
shall include the manufacturer’s inspection (see Clause B1); and either:
a) for material covered by a third party certification scheme, the requirements of Clause
B2; or
b) for material not covered by a certification scheme, the requirements of Clause B3.
The records shall be made available for inspection by the purchaser or his representative for
a period of ten years from the date of delivery.
14.1.1 The minimum tensile properties of the steel obtained from test pieces selected,
prepared and tests in accordance with Annex B shall comply with Table 3.
14.1.2 The specified characteristic strength and elongation shall be as given in Table 3.
a
Min. characteristic strength Min. tensile strength Min. elongation
Grade 2 2
(N/mm ) (N/mm ) (%)
b
485 485 510 12
b
500 500 525 10
a
Gauge length = 5.65√So
b
and at least 5 % greater than yield strength for d > 5 mm or 3 % greater than yield strength for d < 5 mm
recorded in tensile test.
So Denotes original cross-sectional area of the test piece
a) at least 5 % greater than the actual yield stress measured in the tensile test in
accordance with B1.2, B1.3 and B1.4; or
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MS 144:2006
b) between 5 % and 10 % greater than the actual yield stress measured in the tensile test in
accordance with Annex B. In this case the actual yield stress shall not be less than the
2
value determined from the following formula, in N/mm .
A = (2.1 – B)
where,
When the test pieces selected and prepared in accordance with Annex B are subjected to the
tests described in that annex, the test pieces shall withstand the test without fracture.
d) any other markings as may be agreed upon between the wire manufacturer and the
purchaser;
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MS 144:2006
17.2 When one or more of the test results in 17.1 fall below the characteristic strength
specified, ten specimens shall be selected from different wires in the batch.
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If any one test results is less than 93 % of the characteristic strength specified in Table 3,
both the test specimen and the test method shall be carefully examined. If there is a local fault
in the specimen or reason to believe that an error has occurred in the test, the wires from
which the test specimens were taken shall be disregarded and the test result shall be ignored.
If the valid test results have an actual yield stress equal or greater than 93 % of the
characteristic strength specified, the batch shall be deemed to comply with this standard.
If one or more valid test result is less than 93 % of the characteristic strength specified, the
batch shall be deemed not to comply with this standard.
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MS 144:2006
Annex A
(normative)
A1. Principle
The principle of the test is to show that deformed wires claimed to be equal to those satisfying
the classifications, will hold for a given time the specified characteristic strength in a pull-out
test with a free end slip not greater than 0.2 mm.
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fyø
for deformed Type 1 wires; or
21
fyø
for deformed Type 2 wires
28
where,
2
fy is the specified characteristic strength of the steel (in N/mm ); and
ø is the nominal wire size (in mm).
Prepare the prisms using a mortar mix that gives concrete having cube strength of between
2 2
40 N/mm and 45 N/mm at the time of the pullout test.
Support the test wire so that it is rigidly embedded and passes completely through the prism
of concrete along its longitudinal axis. Reinforce the prism along the embedded length with a
helix of 6 mm diameter plain mild steel having a pitch of 25 mm, the outer diameter of the
helix being 5 mm less than the side of the square cross-section. A suitable mould is shown in
Figure A1.
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MS 144:2006
A4. Apparatus
Mount the test piece in a suitable testing device that allows the concrete prism to be held
rigidly while the wire is being pulled axially from the prism. Arrange the test piece such that
the end of the wire at which the pull is applied is that which projects from the top end of the
prism as cast. Place plaster bedding, or rubber or plywood packing, between the top end of
the prism and the surface of the testing device bearing on it.
Mount a suitable dial gauge in such a manner that the gauge records the relative slip between
the unloaded end of the wire and the bottom end of the prism as cast.
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A5. Procedure
During a period of approximately 2 min, steadily increase the axial load in the wire protruding
from the top end of the prism until the tensile stress in the wire attains the specified
characteristic strength fy for the grade of steel from which the wires are made. Maintain this
stress for a further 2 min after which record the free end slip of the wire.
10
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11
Figure A1. Typical mould to be used for bond test
MS 144:2006
MS 144:2006
Annex B
(normative)
a) that the material supplied complies with and has been tested at the frequency specified
in this standard; and
b) the address at which the record of test results is available for inspection.
In the case of material delivered to a supplier, the manufacturer shall issue a certificate
of routine testing stating:
c) the results of the tensile and rebend tests on samples taken from the material. The
tensile test results shall include cross-sectional area.
Samples shall be selected from batches at a frequency of not less than one test sample as
stated in Table B1. If a batch comprises wires from more than one cast, at least one test
sample shall be selected to represent each cast.
< 10 25 25
10 ≥ 35 35
NOTE. At the option of the manufacturer or supplier and in order to simulate natural ageing, test samples may be
subjected to a temperature of up to 100 °C for a period between 30 min to 2 h, provided that rebend test samples are
so treated and the fact is recorded on the test sheets and certificates.
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MS 144:2006
B1.4.1 Determine the tensile strength, yield stress and elongation of the steel by the
methods described in MS ISO 6892, except where otherwise stated below, but using a
recognised extensometer for the tests.
For elongation values, regard the test results as valid, irrespective of the position of the
fracture, provided that the minimum elongation specified has been obtained. Where the
minimum elongation specified is not obtained, discard the results of the test and consider the
test invalid if the distance between the fracture and the nearer gauge mark is less than one-
third of the gauge length, and if the relevant end of the gauge length used for assessing the
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elongation is 2d or closer to the face of the testing machine grips, where d is the size of the
test piece.
NOTE. Elongation values for small size wires are sensitive to testing errors. Where a valid elongation value of 10
% or more is obtained, a retest is recommended. It is recommended that test pieces be slightly scribed at one-
diameter or 5 mm centres, whichever is more convenient, throughout their length, and that a gauge length be
selected that is as nearly symmetrical about the fracture as possible and is clear of the machine grips.
B1.4.2 Calculate the stresses using the effective cross-sectional area of the wire
determined by weighing as described in 6.3.
NOTE. It is not necessary to assess the mean value m of the cast if all individual values of x are equal to or greater
than the characteristic strength cv.
B1.5.2 Each individual value for the tensile strength shall comply with the requirements of
14.1.3 and each individual value of the elongation shall comply with the requirements of
14.1.2.
a) on a bending machine in which the test piece is adequately supported by plain smooth
surfaces or rolls which do not offer resistance to the longitudinal movement of the test
piece; or
Any machine shall be serviceable and capable of imparting constant loading to the specimen
and be without impact effect.
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MS 144:2006
The rate of application of the load shall not exceed three revolutions per minute or equivalent
if method b) is used.
a) Bend the test piece through 45° using one of the methods of bending specified in
B1.6.1 around a former of diameter equal to five times the nominal size of the wire.
c) Allow the test pieces to cool to ambient temperature and bend it back, through at least
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23°, towards its original shape (partially restraighten) by a steadily applied force using
the same machine as in a).
B1.6.3 In the event of failure, if there is any damage to the ribs caused by carrying out the
initial bending, the test shall be invalid.
B1.6.4 Damage to ribs can be avoided by the use of an aluminium insert placed between
the test piece and the former. The maximum thickness of the aluminium insert is to be 6 mm.
For the purpose of determining the consistency of the manufacturer’s production the long
term quality level shall be assessed at regular intervals. No conclusion regarding compliance
with this standard shall be made on the basis of this assessment.
The yield stress results obtained on all casts for each size shall be collated at intervals of 3
months or after at least 200 results have been obtained. These shall be used to determine the
long term quality level.
B2.2.2 Evaluation
m ≥ cv + kσ
where,
k is the acceptability index for which values are given in Table B2.
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MS 144:2006
A certificate of compliance shall be issued by a supplier when requested. This shall state:
a) that the material supplied complies with and has been tested at the frequency specified
in this standard; and
b) the address at which the record of test results is available for inspection.
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The certificate shall include the approval number issued by the recognised certification body.
In the case of material delivered to a supplier, the manufacturer shall issue a certificate of
routine testing stating the following:
a) the cast number and cast analysis. The cast analysis shall include all specified
elements and those used for the calculation of the carbon equivalent value;
c) the individual results of the tensile and rebend test on specimens taken from the
material. The tensile test results shall include the effective cross-sectional area.
The certificate shall include the approval number issued by the recognised certification body.
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MS 144:2006
Table B2. Acceptability index (k) as a function of the number (n) of the test results (for
a reliable failure rate of 5 % (pass = 0.95) at a probability of 90 % (1 – ∞ = 0.90)
n k
5 3.40
6 3.09
7 2.89
8 2.75
9 2.65
10 2.57
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11 2.50
12 2.45
13 2.40
14 2.36
15 2.33
16 2.30
17 2.27
18 2.25
19 2.23
20 2.21
30 2.08
40 2.01
50 1.97
60 1.93
70 1.90
80 1.89
90 1.87
100 1.86
150 1.82
200 1.79
250 1.78
300 1.77
400 1.75
500 1.74
1 000 1.71
∞ 1.64
Material not covered by a third party product certification scheme shall be assessed by
acceptance tests on each batch. Sampling and testing shall be carried out by an organisation
independent of the producer at the producer’s works or in the stockholder’s yard.
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MS 144:2006
For the purpose of testing, the delivery is to be subdivided into test units with a maximum
mass of 100 t each. Each test unit shall consist of products of the same steel grade and the
same nominal diameter from the same cast. The manufacturer or supplier shall confirm in the
certification that all products in the test unit originate from one cast.
a) 15 test specimens (if appropriate 60 test specimens) from different bars for testing in
accordance with B3.3 a) and B3.3 b);
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b) two test specimens from different bars for testing the chemical composition in the
product [see B3.3 c)].
The preparation of test specimens shall be carried out as described in Clause B1.
The following properties are to be determined in testing the test specimens which have been
taken according to B3.2.
a) Inspection by variables:
b) Inspection by attributes:
All elements listed in Clause 8 and the carbon equivalent are to be determined.
a) The following indices are to be determined when testing for the properties listed in B3.3
a).
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MS 144:2006
The test unit shall be deemed to comply with the requirements of this standard if the condition
m15 – 2.33 x S15 ≥ cv is fulfilled by the characteristic strength
where,
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x is as defined in B1.5.1;
m is as defined in B1.5.1;
b) If the condition stated in B3.4.1 a) is not fulfilled, the secondary calculation of the
acceptability index
m15 - cv
k' =
S15
is to be determined from the test results available. Where k’ ≥ 2, testing can be continued. In
this case 45 further test specimens shall be taken and tested from different bars in the test
unit, so that a total of 60 test results are available (n = 60).
The test unit shall be deemed to comply with the requirements of this standard if the condition
is fulfilled for all properties (1.93 is the value for the acceptability index k for n = 60 in
accordance with Table B2).
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MS 144:2006
a) When testing the properties listed in B3.3 b) either all results determined on the 15 test
specimens shall comply with the requirements of this standard; or
b) nominal diameter;
e) cast number;
f) date of testing;
h) the individual test results for all the properties specified in B3.3.
19
Acknowledgements