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Article history: Core disciplines in chemical engineering master, like the case of Transport Phenomena, and although
Received 17 April 2018 its content is 100% related to the master, are always hard to understand by the students. We have
Received in revised form 24 July 2018 implemented a new methodology where teams of students should perform the concept, design and
Accepted 19 October 2018
development of practical demonstrations of Mass Transfer Phenomena and Theoretical Background, in
Available online 25 October 2018
order for all of them to be able to really get involved in the thematic, and thus easily assimilate con-
cepts and theoretical development as applied to practical phenomena. After the first application of this
Keywords:
methodology and after a deep analysis of previous results we have made important enhancements on
Pedagogical methodology
Transport phenomena
the innovative work. Among several other modifications, students were able to select the field on which
Innovation each practical demonstration would be developed (among the three usual transport phenomena: mass,
Practical demonstrations fluids and heat) and most particularly encouraged to design and develop practical demonstrations on
Learning improvement the thematics and sub-thematics they had higher difficulties. A total of 6 experiments/demonstrations
were developed by the students of the two academic years. To determine the perception, impact and
improvement made by this methodology, surveys were also made to determine the initial and final sta-
tus of the students concerning their knowledge and difficulties, so as to conclude fairly about the success
of application of this methodology. Final Exam marks have also improved. In this paper we present the
results obtained and describe the application steps of this methodology and discus the evaluation of the
successful rate of the methodology.
© 2018 Institution of Chemical Engineers. Published by Elsevier B.V. All rights reserved.
https://doi.org/10.1016/j.ece.2018.10.002
1749-7728/© 2018 Institution of Chemical Engineers. Published by Elsevier B.V. All rights reserved.
P.A. Augusto et al. / Education for Chemical Engineers 26 (2019) 48–57 49
cal way the theoretical instruction received in classroom lectures To improve this practice − theory link, and specially to reduce
(Stammitti, 2013). It is well known that laboratory experiences are the passivity and stimulate the students in this kind of disci-
not only used in the academic environment for complementing plines, several options have been proposed/implemented. The
and reinforcing in a practical way the theoretical concepts intro- ability to co-operate (team work) to find appropriate informa-
duced to students in lectures, but also, they are used as a means for tion, to solve problems through critical and creative thinking,
developing skills, such as acquiring and processing experimental to make decisions and to communicate effectively (Delgado and
data, comparing such data against theoretical models, developing Fonseca-Mora, 2010) is one of the options and may be developed
critical and analytical thinking, drawing meaningful conclusions, through co-operative learning (Delgado and Fonseca-Mora, 2010),
teamwork and ethics, and the ability to convey experimental find- well-defined comprehensive protocols, rubrics and co-operative
ings and conclusions in the forms of written technical reports and work direct students towards successful learning is another option
oral presentations (Stubington, 1995; Arce and Schreiber, 2004; (Delgado and Fonseca-Mora, 2010); the use of competition has
Feisel and Rosa, 2005; Domingues et al., 2010; Vazquez- Arenas been suggested to improve learning outcomes, motivation, student
and Pritzker, 2010; Patterson, 2011; Narang et al., 2012; Vernengo participation and stimulation (Delgado and Fonseca-Mora, 2010;
and Dahm, 2012) (Stammitti, 2013). It was actually proved that Lefebvre et al., 2009; Zou and Ko, 2012) (Pott et al., 2017); another
students’ perceptions of workload, anxiety and time pressure proved option indicates that the teacher’s involvement in creat-
decreases with well-structured laboratorial work: substantial evi- ing a challenging, integrated teaching unit and students’ effort in
dence of cumulative learning was noted, both during the practical co-operating to create their final written and oral reports led to con-
session, as well as in student responses. It was clear that student’s siderable improvement in understanding unit operations as well as
both critically engage and are enriched by the practice (Pott et al., to very high student motivation (Delgado and Fonseca-Mora, 2010).
2017). Several other alternatives have also been tested: showing
In modern times due to increasing engineering demand, spe- videos with physical examples, technology-based learning plat-
cialization and complexity (UNESCO, 2010), curricula of modern forms (Rooch et al., 2016), providing access to YouTube videos,
and future engineers must show the two valences (Barnett, 2006): recorded class or laboratory demonstrations, and even simula-
towards the theoretical knowledge base and increasingly complex tion software such as that used by Gynnild et al. (2007). These
application contexts. Thus, although the curriculum is already pres- approaches are designed to demonstrate the application of theory
sured to have a large spectrum of valences and skills, one still sees to practical contexts, but often essentially represent passive activi-
more theory and more practice being introduced into it (Pott et al., ties for the student—a learning mode which does not foster deep or
2017). long term learning (Najdanovic-Visak, 2017). Unfortunately, this
Abdel-Salam et al. (2006) centering on fluid mechanics, and robs the student of an important linkage between what is fun-
Chen et al. (2016), in their research, prove that active participa- damentally an applied science and the theory that is rigorously
tion is key in learning experiences. Therefore, laboratory practice covered in class. (Pott et al., 2017).
remains an integral part of university engineering curricula (Pott All the pointed difficulties are transversal to all core disciplines
et al., 2017). like Transport Phenomena. However, almost no specific novel
Nonetheless, the prevalence of assessment-driven learning methodologies have been reported specifically for Transport Phe-
in the practical context often results in the students not nomena. In fact, considering the discipline Transport Phenomena,
critically engaging with the equipment and demonstrated phe- to the best of our knowledge, only one approach was implemented:
nomena, but rather opting for a superficial and targeted learning the use of spreadsheets for time consumption reduction − process-
approach—taking their measurements and samples, with little deep ing experimental data and comparing results against theoretical
understanding being generated (Chin and Brown, 2000; Louw, models can be time consuming due to iterative and complex cal-
2016; Ram, 1999; Young et al., 2006; Pott et al., 2017). culations, which reduce the student’s available time for analysis
In fact, the current status quo fails to enable deep learning, and discussion; in fact, data processing and model evaluation tasks
and is not able to cause the fundamental connection of theory are time consuming and do not add much value to the student’s
to practice and failing to stimulate student interest, engagement learning experience as they reduce available time for result analy-
and motivation. Two examples of this failure are reflected in high sis. (Stubington, 1995; Feisel and Rosa, 2005; Vazquez-Arenas et al.,
failure and dropout rates in some countries (Council for Higher 2009; Vazquez-Arenas and Pritzker, 2010; Stammitti, 2013). How-
Education, 2013), and more specially in some industry complaints ever, this approach is very limited in effect and application.
about graduate inability to ‘apply knowledge’ (Griesel and Parker, In related disciplines (Fluid Mechanics) we have the example of
2009), which clearly suggest that the theory–practice divide needs Pott et al. (2017), that have tried to enable deep learning, improve
attention if we are to improve engineering education. (Pott et al., the fundamental connection of theory to practice and stimulate stu-
2017). dent interest, engagement and motivation through a group-based
One of causes that is pointed for this lack efficiency of labo- competitive, informal, problem solving, interactive learning event.
ratorial work, is that practice are set up in such a way that the In order to succeed the students needed to grapple with, under-
students are very constrained in how they can engage with the stand, and apply the theory of pump curves, pumping networks and
equipment: they have little opportunity to experiment, disman- pressure losses, to achieve a practical solution to the open-ended
tle, reassemble, examine and generally experience the constituent (but constrained) problem. In addition to the importance of bridg-
equipment. Thus, evidence suggest that students practice ‘surface’ ing the divide between the theoretical and the practical, another
and ‘strategic’ learning (Entwistle, 2000). They do not fully engage important parameter that was improved and considered important
with the practical, but rather focus on taking only those readings, to the student success is their attitude: their motivation, anxiety,
measurements and observations which will allow them to fulfill and perception of ability (Jones et al., 2010; Savage et al., 2011)
their report writing task—a task they find onerous and frustrating, (their attitude is linked to success, but also it is often an indicator
partially since they have little deep understanding of the systems of the type of learning they are likely to pursue: deep, strategic or
that they are now writing about. (Pott et al., 2017). In fact, data superficial (Entwistle, 2000)).
processing and model evaluation tasks are time consuming and do Considering analysis methodology of results, more specifically
not add much value to the student’s learning experience as they the elaboration of surveys (as student feedback can facilitate teach-
reduce available time for result analysis, critical thinking and report ing improvements (Wickramasinghe and Timpson, 2006)), and
writing skills development (Stammitti, 2013). most particularly time of elaboration, the most common form of
50 P.A. Augusto et al. / Education for Chemical Engineers 26 (2019) 48–57
Fig. 1. a) Schematic diagram of the followed Enhanced Methodology; b) Implementation in Year 1 and 2.
Fig. 2. a) Experimental setup b) Example of a graph obtained enabling us to determine the influence of the distance in the mass transfer convection coefficient.
P.A. Augusto et al. / Education for Chemical Engineers 26 (2019) 48–57 51
Fig. 3. a) Experimental setup; b) is a graphic example of the evolution of the concentration in the sample point, with time.
student feedback is obtained from end of semester student eval- a course of one semester is given denominated as Transport Phe-
uations. Unfortunately this type of feedback does not benefit the nomena, and were the three topics must be covered (momentum,
students who provided it, because end of semester student evalua- heat, and mass); nonetheless due to the usual previous background
tions are usually standardized at a given institution in order to make of the students on two of these sub-areas (as previously described)
comparisons across disciplines and this often results in question- − heat and momentum − the course is nowadays more focused on
naires that are general and offer limited guidance for improvement mass transfer, although the other subareas are also covered.
in teaching; moreover since they are administered at the end of
the semester they are of little value in providing teaching improve-
ments for the class which gave the feedback (McKeachie, 2002); 2. Hypothesis
the value of end of semester course evaluations that often con-
sist of a series of multiple choice questions and optional student In this work two consecutive academic years have been ana-
comments is further diminished by the fact that academic staff lyzed. In the second year, the method was improved and enlarged.
members are often defensive about low ratings, rejecting the valid- As hypothesis we have assumed that a new methodology should
ity of the student responses. Hence in our particular case, we have be developed and implemented based basically in the concept,
made also a mid-semester student feedback as this has proven to design and development of practical demonstrations, by the stu-
overcome this limitation (Wickramasinghe and Timpson, 2006) − dents, within the frame of Mass Transfer Phenomena, and due to
because the feedback obtained may be used by the instructor to this work, students would be able to get really involved in the the-
make adjustments to the course in progress and also encourages a matic, and would assimilate concepts and theoretical development
more responsible attitude by the students as they reflect upon the easier as applied to practical phenomena.
course. This hypothesis was implemented during the first year of the
Instead of making surveys, other forms could be approached, but application of this innovative plan.
those are very limited. Angelo and Cross (1993) describe methods Another hypothesis was that if we would complement the
such as the use of chain notes, e-mail, teacher designed feed- previous hypothesis by limiting the experiment/demonstration
back forms as opposed to institutionally designed end of semester thematic the students could choose, to the area they felt more diffi-
surveys, group instructional feedback and classroom assessment culties, this would improve even better the effect of this innovative
quality circles). plan.
The study that we present lays the foundation for similar the- This hypothesis was implemented during the second year of the
ory and application-linking practicals based on a non-assessment application of this innovative plan.
paradigm: it is likely to be broadly applicable to other global insti-
tutions and engineering programmes. Indeed, the challenges facing
3. Methodology
many of the world’s engineering educators are similar: need to
teach ever more content, within smaller time-frames, to larger
In Fig. 1 a) it is depicted a schematic diagram of the full followed
classes and with linked practice-theory.
methodology.
In this work we tried to use the majority of the best practice and
The first step (I) consists on the election by the students of the
improved options for pedagogical learning
thematic under the scope of which they will develop and test the
We have aimed our study over the Transport Phenomena course,
experiment/demonstration. This step was only applied for the “sec-
which is a course of the 1st year of the Master in Chemical Engineer-
ond wave” of students (the second academic year). It is important
ing of the University of Salamanca, Spain. In order to have a clear
to notice that the methodology was only started at the middle of
vision of the context, more data is given in the following paragraph
the semester when the students already had enough information to
concerning this course and their insertion in the overall curricula.
evaluate correctly the thematic that was more challenging to them.
Currently in the plan of Chemical Engineering graduation of the
In the second step (II) the students (divided by workgroups)
University of Salamanca the students are lectured with one course
imagined a demonstration/experience that reflected common prac-
of one semester regarding Fluid Mechanics (Transport Phenomena
tical phenomena.
− Momentum) and another course of one semester regarding Heat
In the third step (III) they had setup such experience and
Transfer (Transport Phenomena − Heat). In the Master Graduation
obtained practical results.
52 P.A. Augusto et al. / Education for Chemical Engineers 26 (2019) 48–57
Fig. 4. a) Experimental Setup for VC diffusivity measurement and b) example of curve fitting.
Table 1
Survey made on the students (the most complete − in the second year).
Questionnaire
I − Do you think it is important to have a theoretical-practical/experimental complement for the thematic of the Transport Phenomena discipline?
II − Do you think that developing and performing experiments will help/has helped you to better understand the discipline and its contents?
III − In which Thematic do you have greater difficulties (Mass Transfer, Fluid Mechanics, Heat Transfer)?
IV − To which of these thematic (Mass Transfer, Fluid Mechanics, Heat Transfer) should we allocate the large majority of the time in the Transport Phenomena discipline?
V − In which part of the contents of the discipline Transport Phenomena do you have greater difficulties?
VI − At this moment how much would you grade your difficulty in the selected sub-thematic (question V)?
VII − What kind of experiments/demonstrations do you think we should do to better understand the thematics, specially the one you have higher difficulties?
VIII − At the present time, how would you grade your knowledge about the contents of the discipline?
IX − At the present time, how would you grade your difficulty understanding the contents of the discipline?
X − Was the experimental/demonstration work and development useful for better understanding of the contents of the discipline?
In a fourth step (IV) they compared the obtained results with The challenge was to design and assemble cheap and easy
theoretical development and tuned the experience/demonstration demonstrations. In fact, most of the materials are common and
In a fifth step (V) they have made a full demonstra- used by humankind in a daily basis (plastic recipients, hair dryer,
tion/experience in class, directed to the professors and remaining sponge, etc.). Some cheap and available glass material was also used
students, with the corresponding explanation and discussion. (syringes, support vessels, etc.) and only two scientific instrumen-
In the sixth step (VI) they have elaborated and delivered a report tal techniques were required (weight by analytical balance and use
of the experiment/demonstration. of the spectrophotometer) (in fact, for example, in a determined
In the final step (VII) the students have filled a final survey in experiment the electrode was designed and programmed by the
order to determine and evaluate the improvement on learning; in students by using only a pen and other simple and day-by-day
this stage the exam results and final grades were also compared. materials).
Steps II to VI were applied in both academic years. In the 2nd year of implementation of this innovative plan, the
experiments/demonstrations were directed specifically to the the-
matic where the students had more difficulties.
4. Results The experiments were chosen and developed by the students,
under the supervision of the professors (in class). In what follows
4.1. Practical demonstrations (Augusto et al., 2017; Blanco-Río we detail somehow the experiments, but refer the reader to more
et al., 2017; Arribas-Sanz et al., 2017) detailed publications about them (Augusto et al., 2017). Consider-
ing previous related work (Augusto et al., 2017) its nature is more
Practical demonstrations constitute a result as they may be related to the content of some of the pedagogical experiments set-
applied as a pedagogical method by themselves. up by students, allowing them to be used for future pedagogical
P.A. Augusto et al. / Education for Chemical Engineers 26 (2019) 48–57 53
Fig. 5. a) Experimental Setup for VC diffusivity measurement − uncontrolled release and b) example of results.
learning; therefore the educational improvement and the complete law, Molecular Diffusivity was determined and compared with the-
−C
methodology was not present, neither were the measuring tech- ory (Q = Dm A (C1 l 2 ) , where Q is the total mass flow of NaCl, Dm its
niques to evaluate the success of the implementation of the basic molecular diffusivity coefficient in water, A the area of mass trans-
methodology used at that time. fer, l the length of diffusion transfer, C1 and C2 the concentrations
a) 1st Year of NaCl in water in the bottom of the glass and in the sample point,
a1) Mass Transfer by Forced Convection respectively.
The goals of this experience/demonstration were to show the a3) Determination of Violet Cristal diffusivity in water
difference between natural and forced convection on mass trans- Two experiences/demonstrations were made concerning the
fer, and also analyze the influence of the air flow that generates goal of determination of the diffusivity of Violet Cristal in water.
the forced convection of ethanol contained
in a recipient. The for- The diffusion equation was applied and it was demonstrated that
mula to be applied is: Q = kc A Cai − Ca , being Q the total mass of uncontrol release leads to uncontrol results, as expected, while in
ethanol evaporating, kc the mass transfer coefficient (convection), controlled release we may optimize the system.
A the area of mass transfer, Ca i and Ca the concentration of ethanol a31) Controled release
in the interface and in the bulk of air, respectively. By changing the In this case we have used a controlled release setup (Fig. 4),
airflow and distance from recipient to the air dryer, their influence where we have also inserted a porous media, in order to evaluate
was determined. At the end the overall mass transfer coefficient its influence, according to the equation Def = DCV ε , where Def is the
of convection was determined by applying the equation, and com- effective diffusivity of VC in water, DCV is the molecular diffusivity
pared with theoretical values, obtaining graphs such as the one of VC in water, ε is the porosity of the media and its tortuosity. The
depicted in Fig. 2. final calculated values for the previous variables were compared
a2) Diffusivity of Salt by using conductivity measurements with their theoretical values.
The goal of this experience/demonstration, was to determine the a32) Uncontroled release
diffusivity of NaCl in a solution by using conductivity as the measur- In the second experience Violet Cristal was injected freely in
ing parameter. For such, a home-made conductivimeter was made, the water and we followed the concentration evolution in several
and also a Python program implemented (Fig. 3). By applying Fick’s
54 P.A. Augusto et al. / Education for Chemical Engineers 26 (2019) 48–57
Fig. 6. a) Simulations of the diffusion of VC in water through the porous media, and after uncontrolled release: b) experimental setup; c) some of the obtained results.
(Arribas-Sanz et al., 2017).
Fig. 7. a) Experimental setup; b) some of the obtained results (Blanco-Río et al., 2017).
points of the vessel (Figs. 5 and 6). The final calculated Diffusivity One experience/demonstration was made concerning the goal
was compared with the theoretical value. of determination of the partition coefficient of glycerol in water
b) 2nd Year and oil. The system was also used for determination of the influ-
b1) Determination of Violet Cristal diffusivity in water through ence of some parameters (for example the initial mass of glycerol).
C
an oversized porous media The equation used was K = C1 , where K is the partition coefficient,
2
In this experience/demonstration the goal was the determina- C1 and C2 are the concentration of glycerol in phase 1 and 2, respec-
tion of the diffusivity of Violet Cristal in water, passing through an tively (Fig. 7).
oversized media, with uncontrolled release. The diffusion equation
was applied and values obtained for porosity and tortuosity; later 4.2. Surveys
students have compared with the theoretical values. Simulations
of the diffusion movement were also made and compared (Fig. 6). We have conducted several surveys to the students to evaluate
b2) Determination of Partition Coefficient and Interface Coeffi- the results being obtained by this pedagogical methodology. Here
cients we focus on the surveys made in the 2nd year, as they are much
P.A. Augusto et al. / Education for Chemical Engineers 26 (2019) 48–57 55
Fig. 8. Survey results. Questions: a)I; b)II; c)III; d)IV; e)V; f)VI; g)VII; h)VIII; i)IX; j)X. − Survey results. Questions: a)I; b)II; c)III; d)IV; e)V; f)VI; g)VII; h)VIII; i)IX; j)X.
more complete and focused. The methodology followed was the of the period the same survey was answered by the same students
following: at mid-period, before choosing and starting to develop and results compared. The surveys were all anonymous and secrecy
the experiments/demonstration a survey is performed; at the end and independence was guaranteed. The size of the sample was 10.
56 P.A. Augusto et al. / Education for Chemical Engineers 26 (2019) 48–57
5. Conclusions
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