CHM 701 : Modern Instrumentation Method and Technology

Assignment 2
Name: Deeptesh Avikash Lal
ID: 2018002801

Question 1.

Graph of Intensity Vs Concentration

The above graph
30
represents the
25 24.7 Intensity Vs
f(x) = 1.93 x + 1.56
20 R² = 1 20.9 Concentration of
17.4 vanadium in the
intensity

15 Linear ()
12.5 intensity seawater prepared
10 9.2 Linear (intensity) standard solution.
6 7
5 5 4 5 Using the gradient the
2.1 2 3
0 1 concentration at the
0 2 4 6 8 10 12 14 3.1, 9.4 and 11.6
Concentration intensity was
determined.
Y=1.925X + 1.5643
Y represents Intensity
X represents Concentration
Making X subject of the formula, thus
X= (Y – 1.5643) / 1.925
For 3.1 Intensity
(3.1 – 1.5643) / 1.925 = 0.7977

For 9.4 intensity

(9.4 – 1.5543) / 1.925 = 4.07
For 11.6 intensity
(11.6 – 1.5643) / 1.925 = 5.21

Question 2.
Compound Name : Benzene
IR spectrum shows the aromatic functional group
H NMR shows 1 set of chemically equivalent proton present in the compound experiences the
same chemical environment.
C NMR shows the carbon present in the compound experiences the same chemical
environment.
Overall
the signals projected at the values of the graph are crosses checked with the functional group
Reference table.
The best compound that matches with the information provided by the Spectrum is Benzene.
Question 3
Compound Name : 3-methyl-2-butananone
IR spectrum shows the ketone functional group ( carbon oxygen double bond ), carbon
hydrogen group and methyl group
H NMR spectrum shows multiple, singlet and double peaks.
The integral ratio tells the group of the photon present
1:3:6
The ratio tells the approximately the number of photons present.
C NMR spectrum shows four different chemical environment experienced by the carbon
present in the compound.
Overall
The values where the signals are projected can be crossed checked with the Reference group
table to figure out the compound
The best compound which matches the information provided by the spectrum is 3-methl-2-
butanone