Laboratory Analysis

Rev 1

Date 02.04.2017

Services S.R.L
Services S.R.L Laboratory Report

Introduction
On 17.03.2017 the sample was taken from the flare pit and from the BHA on well 123
Yefremivska and brought to the Tacrom Services laboratory in Poltava, Ukraine.
Pictured on the left is the liquid sample and on the right, a dried sample.

One of the first things that we noticed was that the dried sample displayed magnetic properties

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Services S.R.L Laboratory Report

Analyzed properties
SG = 1.000 @ 20°C ;

pH = 7;

Iron concentration = >5 mg/l;

The liquid sample was filtered and dried in order to separate the solid part. On the resulted solids, we
performed a series of solubility tests with the below mentioned acid recipe:

Description Total / m3 Unit

Water 506 l

32% Hydrochloric Acid 434 l

85% Formic Acid 50 l

Surfactant + Clay stabilizer 5 l

Iron Control 20 kg

Corrosion Inhibitor 5 l

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 Services S.R.L Laboratory Report

The acid recipe was mixed with the dried sample and introduced at bottom hole temperature for various amounts of time.

Acid Recipe Dried Sample Mixture

All the samples were weighed before mixing and after being kept at temperature.

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Services S.R.L Laboratory Report

Sample no. 1 after 30 min @ 70 degrees C

After filtering and drying, solubility was calculated at 6.93% by comparing the initial and final
mass.

TACROM SERVICES 2017. 04. 02.

Services S.R.L Laboratory Report

Sample no. 2 after 60 min @ 70 degrees C

After filtering and drying, solubility was calculated at 10.62% by comparing the initial and
final mass.

TACROM SERVICES 2017. 04. 02.

Services S.R.L Laboratory Report

Sample no.3 after 120 min @ 70 degrees C

After filtering and drying, solubility was calculated at 13.02% by comparing the initial and
final mass.

TACROM SERVICES 2017. 04. 02.

Services S.R.L Laboratory Report

Sample no.4 after 240 min @ 70 degrees C

After filtering and drying, solubility was calculated at 13.05% by comparing the initial and
final mass.
3

TACROM SERVICES 2017. 04. 02.

Services S.R.L Laboratory Report

From the above chart, we can conclude that the optimum reaction time with this recipe is 120
minutes.

After the reaction had occurred, none of the samples were attracted to the magnet.

Testing is going to be continued in our Romanian laboratory with a mud acid recipe.

TACROM SERVICES 2017. 04. 02.