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Result Batch Reactor

Volume of NaOH = 3 L
Volume of Et(Ac) = 3 L
Temperature = _____ 0C

Time, Temperature Conductivity Concentration of Conversion,


(min) (°C) (mS/cm) NaOH, CNaOH (M) X (%)
(From calibration (Self
curve) calculation)
0 33 5.77 0.0126 0
5 34 5.40 0.01 20.635
10 37 5.39 0.00993 21.190
15 38 5.33 0.0095 24.603
20 39 4.99 0.0071 43.651
25 40 4.87 0.0062 50.794
30 44 4.78 0.0056 55.556

Calculation for Concentration of NaOH (M)


Y =140 X+ 4
A) 5.77 = 140 X + 4

140 X = 5.77– 4

140 X = 1.77

X = 0.0126

Y =140 X+ 4
B) 5.40 = 140 X + 4

140 X = 5.40 – 4

140 X = 1.4

X = 0.01

Y =140 X+ 4
C) 5.39 = 140 X + 4

140 X = 5.39 – 4

140 X = 1.39

X = 0.00993
Y =140 X+ 4
D) 5.33 = 140 X + 4

140 X = 5.33 – 4

140 X = 1.33

X = 0.0095

Y =140 X+ 4
E) 4.99 = 140 X + 4

140 X = 4.99 – 4

140 X = 0.99

X = 0.0071

Y =140 X+ 4
F) 4.87 = 140 X + 4

140 X = 4.87 – 4

140 X = 0.87

X = 0.0062

Y =140 X+ 4
G) 4.78 = 140 X + 4

140 X = 4.78 – 4

140 X = 0.78

X = 0.0056
Calculation for Conversion X (%)

CNaOH ( t=0 ) −CNaOH ( t)


A¿ ×100 %
CNaOH (t=0)
0.0126−0.01 26
¿ × 100 %
0.01 26
=0%

0.01 26−0.01
B¿ ×100 %
0.0126
= 20.635 %

0.0126−0.00 993
C¿ ×100 %
0.0126
= 21.190 %

0.01 26−0.00 95
D¿ × 100 %
0.01 26

= 24.603 %

0.0126−0.007 1
E¿ ×100 %
0.01 26
= 43.651 %

0.0126−0.006 2
F¿ × 100 %
0.0126
= 50.794 %
0.01 26−0.00 56
G¿ ×100 %
0.01 26
= 55.556 %

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