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for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Standard Classification of
Coals by Rank1
This standard is issued under the fixed designation D388; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
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D388 − 19a
3. Terminology basis) that lies between two other rock layers whose compo-
3.1 Definitions: sitions differ significantly from that of coal.
3.1.1 For additional definitions of terms used in this 3.1.6 group, n—a subdivision within a coal rank class
classification, refer to Terminology D121. indicating a coal’s designated rank; for example, subbitumi-
3.1.2 agglomerating, adj—as applied to coal, the property nous A rank coal is a group within the subbituminous class.
of softening when heated to above about 400 °C in a nonoxi- 3.1.7 high rank coal, n—denotes a range of coal classes with
dizing atmosphere and appearing as a coherent mass when a greater degree of metamorphism or alteration, including
cooled to room temperature. bituminous and anthracitic coals.
3.1.3 apparent rank, n—of a coal seam, the estimated rank 3.1.7.1 Discussion—These coals are generally characterized
designation obtained using samples other than face channel by lower inherent moisture and higher calorific value. Rank
samples or core samples with 100 % recovery of the seam, but alone is not a sufficient indicator of whether a coal is suitable
otherwise conforming to procedures of Classification D388. for a specific end use.
3.1.4 class, n—a designation of coal rank indicating the 3.1.8 low rank coal, n—denotes a range of coal classes with
degree of metamorphism, or progressive alteration. a lesser degree of metamorphism or alteration, including
3.1.4.1 Discussion—In order of increasing metamorphism, lignitic and subbituminous coals.
these classes range from lignitic through subbituminous and 3.1.8.1 Discussion—These coals are generally characterized
bituminous to anthracitic coals. Refer to Table 1 of Classifica- by higher inherent moisture and lower calorific value. Rank
tion D388. alone is not a sufficient indicator of whether a coal is suitable
3.1.5 coal seam, n—the stratum, layer, or bed of coal for a specific end use.
(containing less than a 50 % mass fraction of ash on the dry 3.2 Abbreviations:
SemianthraciteD
92
86
98
92
2
8
8
14
...
...
...
...
...
...
...
...
J non-
agglomerating
Bituminous:
Low volatile bituminous coal 78 86 14 22 ... ... ... ...
Medium volatile bituminous 69 78 22 31 ... ... ... ...
6
coal
commonly
High volatile A bituminous ... 69 31 ... 14 000 ... 32.557 ...
agglomeratingE
coal
High volatile B bituminous ... ... ... ... 13 000 14 000 30.232 32.557
coal
High volatile C bituminous ... ... ... ... 11 500 13 000 26.743 30.232
coal H 10 500 11 500 24.418 26.743 agglomerating
Subbituminous:
Subbituminous A coal ... ... ... ... 10 500 11 500 24.418 26.743
Subbituminous B coal ... ... ... ... 9 500 10 500 22.09 24.418
6
Subbituminous C coal ... ... ... ... 8 300 9 500 19.30 22.09
non-
agglomerating
Lignitic:
Lignite A ... ... ... ... 6 300 8 300 14.65 19.30
Lignite B ... ... ... ... ... 6 300 ... 14.65
A
This classification does not apply to certain coals, as discussed in Section 1.
B
Refers to coal containing its natural inherent moisture but not including visible water on the surface of the coal.
C
Megajoules per kilogram. To convert British thermal units per pound to megajoules per kilogram, multiply by 0.0023255.
D
If agglomerating, classify in low volatile group of the bituminous class.
E
It is recognized that there may be nonagglomerating varieties in these groups of the bituminous class, and that there are notable exceptions in the high volatile C
bituminous group.
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D388 − 19a
3.2.1 Where it is desired to abbreviate the designation of the %
ranks of coal, the following abbreviations shall be used: VMim—volatile matter, inherent moisture basis, %
ma—meta-anthracite
an—anthracite 4. Significance and Use
sa—semianthracite
lvb—low volatile bituminous 4.1 This classification establishes categories of coal based
mvb—medium volatile bituminous on gradational properties that depend principally on the degree
hvAb—high volatile A bituminous
hvBb—high volatile B bituminous
of metamorphism to which the coal was subjected while
hvCb—high volatile C bituminous buried. These categories indicate ranges of physical and
subA—subbituminous A chemical characteristics that are useful in making broad
subB—subbituminous B
subC—subbituminous C
estimates of the behavior of coal in mining, preparation, and
ligA—lignite A use.
ligB—lignite B
3.3 Symbols: 5. Basis of Classification
3.3.1 Descriptive Symbols (symbols used for describing 5.1 Classification is according to fixed carbon and gross
quantities, all in lowercase, roman) calorific value (expressed in British thermal units per pound,
d—dry basis Btu/lb) calculated to the mineral-matter-free basis. The higher-
f—free basis (for example, mineral-matter-free and sulfur- rank coals are classified according to fixed carbon on the dry
trioxide-free) basis; the lower-rank coals are classified according to gross
im—inherent moisture basis calorific value on the moist basis. Agglomerating character is
3.3.2 Simple Quantity Symbols (calculated quantities with used to differentiate between certain adjacent groups.
units, all in upper case, italicized)
A—ash, % 6. Classification by Rank
FC—fixed carbon, % 6.1 Fixed Carbon and Gross Calorific Value—Coals shall be
FSI—free swelling index classified by rank in accordance with Table 1.
GCV—gross calorific value, Btu/lb 6.1.1 Coals having 69 % or more fixed carbon on the dry,
IM—inherent moisture, % mineral-matter-free basis shall be classified according to fixed
MM—mineral matter, % carbon, regardless of gross calorific value.
S—total sulfur, % 6.1.2 Coals having less than 69 % fixed carbon on the dry,
SO3:A—sulfur trioxide in the ash, % mineral-matter-free basis shall be classified according to gross
SO3:C—sulfur trioxide in the ash, expressed as a percentage of calorific value on the moist, mineral-matter-free basis.
the coal, %
6.2 Agglomerating Character—Classify coals having 86 %
VM—volatile matter, %
or more fixed carbon on the dry, mineral-matter-free basis, if
3.3.3 Complex Quantity Symbols (simple quantity symbols agglomerating, in the low volatile group of the bituminous
with roman subscripts) class. Classify coals having gross calorific values in the range
Ad—ash, dry basis (possibly sulfate-bearing), % from 10 500 Btu/lb to 11 500 Btu/lb on the inherent-moisture,
Aim—ash, inherent-moisture basis, % mineral-matter-free basis according to their agglomerating
Aim,SO3f—ash, inherent-moisture basis, sulfur-trioxide-free character (Table 1).
basis, %
FCd—fixed carbon, dry basis, % 6.3 Supplemental Information—A correlation of the ranking
FCd,MMf—fixed carbon, dry basis, mineral-matter-free basis, % property, volatile matter (100–fixed carbon), with the mean-
FCim—fixed carbon, inherent-moisture basis, % maximum reflectance of the vitrinite group macerals in coals
FCim,SO3f—fixed carbon, inherent-moisture basis, sulfur- tested in one laboratory over a period of several years is shown
trioxide-free basis, % in Appendix X1.
GCVd—gross calorific value, dry basis, Btu/lb
GCVim—gross calorific value, inherent-moisture basis, Btu/lb 7. Sampling
GCVim,MMf—gross calorific value, inherent-moisture basis, 7.1 Samples—Classify a coal seam, or part of a coal seam,
mineral-matter-free basis, Btu/lb in any locality based on the average analysis and gross calorific
MMd,SO3f—mineral matter, dry basis, sulfur-trioxide-free basis, value (and agglomerating character where required) of not less
% than three and preferably five or more whole seam samples,
MMim,SO3f—mineral matter, inherent-moisture basis, sulfur- either face channels or cores, taken in different and uniformly
trioxide-free basis, % distributed localities, either within the same mine or closely
Sd—total sulfur, dry basis, % adjacent mines representing a continuous and compact area not
Sim—total sulfur, inherent-moisture basis, % greater than approximately 10 km2 (4 square miles) in regions
SO3: Ad—sulfur trioxide in the ash, dry basis, % of geological uniformity. In regions in which conditions
SO3:Cim—sulfur trioxide in the ash, expressed as a percentage indicate that the coal probably varies rapidly in short distances,
of the coal, inherent moisture basis, % the spacing of sampling points and grouping of analyses to
VMd—volatile matter, dry basis, % provide average values shall not be such that coals of obviously
VMd,MMf—volatile matter, dry basis, mineral-matter-free basis, different rank will be used in calculating average values.
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D388 − 19a
7.1.1 Take channel samples by excluding mineral partings moisture or somewhat less than that amount. In Appendix X1
more than 1 cm (3⁄8 in.) and lenses or concretions (such as of Test Method D1412/D1412M, the section titled Character-
sulfur balls) more than 1.25 cm (1⁄2 in.) thick and 5 cm (2 in.) istics and Conditions of Sampling Locality describes a simple
wide, as specified in Practice D4596. field test that can help determine which case is at hand.
7.1.2 A drill core sample may be used provided it was NOTE 2—ASTM Manual 113 provides additional useful information
collected as specified in Practice D5192 and meets the follow- regarding the sampling and handling of core samples.
ing provisions: core recovery is 100 % of the seam, the major
7.2 Other Types of Samples—A standard rank determination
mineral partings and concretions are excluded as specified in
cannot be made unless samples have been obtained in accor-
7.1.1, and drilling mud is removed from the core (see also
dance with 7.1. However, the relation to standard determina-
7.1.6).
tions may be usefully given for other types of samples taken
7.1.3 Place all samples in metal or plastic cans with airtight under unspecified conditions, providing the same standards of
lids, or heavy vapor impervious bags, properly sealed to analysis and computation are followed. Designate these com-
preserve inherent moisture. parative indications as apparent rank, which indicates the
7.1.4 Analyses of samples from outcrops or from weathered correct relative position for the sample analyzed but does not
or oxidized coal shall not be used for classification by rank. imply any standards of sampling. Whenever apparent rank is
7.1.5 In case the coal is likely to be classified on the moist stated, give additional information as to the nature of the
basis, that is, inclusive of its natural complement of inherent sample.
moisture, take samples in a manner most likely to preserve 7.2.1 The apparent rank of the coal product from a mine
inherent moisture for purposes of analysis. Because some of shall be based on representative samples taken in accordance
the moisture in a freshly collected sample condenses on the with the Organization and Planning of Sampling Operations
inside of the sample container, weigh both the container and section (Section 7) of Practice D2234/D2234M.
the coal before and after air drying, and report the total loss in 7.2.2 In case the coal is likely to be classed on the moist
mass as air-drying loss. basis, take samples at the tipple or preparation plant and seal
7.1.6 It is often difficult to obtain samples without including the sample to prevent loss of moisture.
visible surface moisture, such as in typical coring situations
where injected water or drilling mud is used or when the coal 8. Methods of Analysis and Testing
seam is an aquifer. When the as-received basis moisture in 8.1 Laboratory Sampling and Analysis—Prepare coal in
samples is questionable in terms of representing inherent accordance with Practice D2013/D2013M and analyze it in
moisture, and the coal is likely to be classified on the moist accordance with Test Methods D3173/D3173M, D3174,
basis, the sampler shall include the following statement in the D3175, D4239, D3302/D3302M, and Practice D3172. Deter-
description: Moisture questionable. Samples so marked shall mine its gross calorific value in accordance with Test Method
not be used for classification on a moist basis unless brought to D5865. Determine the sulfur trioxide (SO3) retained in the ash
a standard condition of moisture equilibrium as specified in in accordance with Test Method D5016 and express the result
Test Method D1412/D1412M. Analyses of such samples that on a dry basis. Inherent moisture is reported as as-received
have been treated in this manner shall be designated as samples (AR) moisture if the sample was collected according to 7.1.1 or
equilibrated per Test Method D1412/D1412M. as equilibrium moisture if 7.1.6 (Test Method D1412/D1412M)
7.1.7 Equilibrium moisture results for suspected lignite and applies.
subbituminous coals shall be adjusted utilizing the procedure
8.2 Adjust the ash value determined in accordance with Test
outlined in Test Method D1412/D1412M, Appendix X1 to
Method D3174 to be free of sulfur trioxide as follows:4
estimate inherent moisture content.
7.1.8 The assessment of whether the as-received basis
moisture in a sample is equivalent to inherent moisture is a key
S
A im,SO 3 f 5 A d 1 2
SO3 :A d
100 DS 12
IM
100 D (1)
criterion when classifying coal on the moist basis. Samples Add to the value of fixed carbon that is determined in
may be at their inherent moisture level, or may be above or accordance with Practice D3172 the value of the SO3 deter-
below. mined in the ash to obtain the value fixed carbon to be used in
7.1.8.1 If the surfaces of sample pieces appear wet, the total Eq 2.
moisture present is in excess of inherent moisture. Possible 8.3 Agglomerating Character—The test carried out by the
sources of that moisture may include groundwater examination of the residue in the platinum crucible incident to
contamination, precipitation on the coal, contamination of coal
drill core samples by drilling fluids and additives, and fresh
water used to clean the core. Make note of any visible water on 3
Luppens, J. A., Wilson, S. E., and Stanton, R.W., Eds., Manual on Drilling,
the surface of the coal. Break all larger sample pieces into Sampling, and Analysis of Coal, Compiled by ASTM Subcommittees D05.18 and
D05.23, West Conshohocken, PA: ASTM International, 1992, https://doi.org/
smaller fragments (particularly if obtained from core) to 10.1520/MNL11-EB.
inspect for visible water occurring in internal cleats, fractures, 4
To perform the calculations in this standard, the percentage values (rather than
voids, etc. Any visible water indicates a total moisture content their decimal equivalent) should be entered in the equations. The result is the value
in excess of inherent moisture. expressed as a percentage (except for calculations of gross calorific value, which is
expressed as Btu/lb). For example, a value of 40 % should be entered into the
7.1.8.2 If the surfaces of sample fragments appear dry, the calculation as “40” and a result of 90 should be expressed as 90 %. The use of the
total moisture present may be the full complement of inherent factor “100” allows the conversion to %.
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D388 − 19a
the volatile matter determination shall be used.5 Coals which, with the Parr formulas,5,6 Eq 2-4. Background information
in the volatile matter determination, produce either an agglom- concerning the development of the Parr formulas, including
erate button that will support a 500 g mass without pulverizing, explanations of the embedded factors, as well as other ranking
or a button showing swelling or cell structure, shall be considerations and examples of the calculations (Table 1), are
considered agglomerating from the standpoint of classification. provided in Appendix X2.
In addition, a result of 1.0 or more on the Free Swelling Index 9.2 Calculate to mineral-matter-free basis as follows:
test (Test Method D720/D720M) may also be used to indicate 9.2.1 Parr Formulas:
the coal is agglomerating; a result of 0.5 or 0 indicates the coal
is nonagglomerating. 100~ FCim,SO f 2 0.15S im !
3
FCd,MMf 5 (2)
~ 100 2 ~ IM11.08A im,SO f 10.55S im !!
3
9. Calculation to Mineral-Matter-Free Basis
VMd,MMf 5 100 2 FCd,MMf (3)
9.1 Calculation of Fixed Carbon and Calorific Value—For 100~ GCV im 2 50S im !
classification of coal according to rank, calculate fixed carbon GCV im,MMf 5 (4)
to the dry, mineral-matter-free basis and gross calorific value to
~ 100 2 ~ 1.08A im,SO f 10.55S im !!
3
APPENDIXES
(Nonmandatory Information)
X1.1 The reflectance of vitrinite in a sample of coal, as several different analysts over a period of several years. The
determined by Test Method D2798, provides a useful guide to plot shows a range of reflectances for three important rank
the rank of the coal. The correlation of the mean-maximum groups:
reflectance of all varieties of vitrinite with volatile matter, Reflectance Range in
expressed on a dry and mineral-matter-free basis, is given in Oil, Distribution Midpoints Rank
Mean-Max, %
Fig. X1.1. Data are plotted for 807 coal samples that contained
less than 8 % ash from many different coal fields in North <1.15 <1.1 hvb
America. All data were determined by a single laboratory, with 1.02 to 1.55 1.10 to 1.45 mvb
1.35 to 2.0 (?) 1.45 to 2.0 (?) lvb
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D388 − 19a
X2. BACKGROUND INFORMATION ON THE PARR EQUATIONS AND OTHER RANKING CONSIDERATIONS
X2.1 Introduction—Coals are ranked according to Classifi- dioxide, which also is lost; and (3) pyrite decomposes to iron
cation D388 on a mineral matter-free, dry or inherent-moisture oxide and iron is retained in the ash. The Parr formula attempts
basis, depending on the parameter that applies. The rank to correct the measured ash and sulfur for these reactions by
parameters—either volatile matter (or fixed carbon) or gross adjusting their mass back to that of the original minerals in the
calorific values—are commonly reported by laboratories on the coal. By using this formula, the varying amounts of mineral
as-received (AR), dry, and ash-free basis. These reported matter can be factored out of the ranking of coals. For example,
values must be converted to the mineral-matter-free basis for Samples A and B in Table X2.1 are both ranked as Lignite A
ranking purposes. Thus converted, the properties of the mac- because they have similar gross calorific values, when calcu-
eral (carbonaceous) material are used as ranking criteria, and lated to an inherent-moisture, mineral-matter-free basis, in
the effects of variable mineral matter contents, which are contrast to their gross calorific values, which are quite different
unrelated to rank, are eliminated. In essence, only the “pure on an as-received (AR) basis. In this example, differing mineral
coal” fraction of a given sample is being ranked. The Parr
contents are thus factored out for the purposes of ranking.
formula is used to estimate the original mineral matter (on the
inherent-moisture and sulfur-trioxide-free basis) in the coal by X2.3 provides useful equations that enable the ranking
using the ash content (on the inherent-moisture and sulfur- parameters to be calculated from laboratory results on the dry
trioxide-free basis) and total sulfur content (on the inherent- basis for volatile matter, ash, and sulfur.
moisture basis) determined on that coal as follows:
X2.2 Explanation of Analytical Bases for Ranking Proper-
MM im,SO 3 f 5 1.08A im,SO 3 10.55S im ties:
This formula assumes that clay minerals, with an average X2.2.1 Dry, Mineral-Matter-Free Basis—The basis to
water of hydration content of 8 %, and pyrite, which contains which chemical properties are to be calculated for samples of
essentially all the sulfur, are the only mineral groups present. coal of ranks medium volatile bituminous and higher. Mineral
Furthermore, the following reactions are assumed to occur matter (noncoal) in North American coals is best approximated
during ashing: (1) the hydroxyl groups from the clay minerals by the Parr formula:5,6
are lost to the atmosphere; (2) the sulfur converts to sulfur
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D388 − 19a
MMd,SO 3 f 5 A d 1 SD
5
S S D D
S 10.08 A d 2
8 d
10
8
Sd (X2.1)
and sulfur contents are given, the ranking equation (Eq 4,
9.2.1) gross calorific value on the inherent-moisture, mineral-
matter-free basis is equivalent to:
Quoting Parr5,6 (except for the subscriptd and parentheses
around the fractions, added for clarity):
“(5/8)Sd restores the Fe2O3 as weighed in the ash to FeS2, as
100~ GCV d 2 50S d !
GCV im,MMf 5
weighed in the coal, 3 oxygens or 48 in the ash having been
originally 4 sulfurs or 128 in the coal;
(10/8)Sd represents the equivalent of Fe2O3 as weighed in the ash,
100 S 100
100 2 IM D
2 1.08A d 1 2 S
SO3 :A d
100 D
2 0.55S d
that is, the Fe2O3 molecule, 160, is 10/8 of the sulfur present in the (X2.3)
coal; Table X2.1 provides helpful example calculations for
(Ad − (10/8)Sd) is the ash as weighed minus the Fe2O3;
0.08 is a constant applied to the iron free ash to restore the water of
samples with widely different ranks to demonstrate some of the
hydration to the earthy matter less iron pyrites, thus representing the important considerations for classifying coals. These examples
true amount of earthy constituent as weighed in the original coal.” also demonstrate the effects of the correction factor for sulfur
The above reduces to: MMd,SO3f = 1.08Ad + 0.525Sd retained in the ash during the ashing process in accordance
with 8.2 and its importance to rank determination.
and simplifies to: MMd,SO3f = 1.08Ad + 0.55Sd Samples A and B are both ranked as Lignite A because they
where the coefficient of sulfur is arbitrarily adjusted up by have similar gross calorific values when calculated to an
the value 0.025 (to give results that do not statistically differ inherent-moisture, mineral-matter-free basis, in contrast to
from those of other proposed formulas).7 their quite different gross calorific values, when calculated on
X2.2.2 Inherent Moisture, Mineral-Matter-Free Basis—The an as-received (AR) basis. In this example, differing mineral
basis to which calorific value is calculated for determining coal contents are thus factored out for the purposes of ranking.
rank for samples of coal of ranks high volatile A bituminous Samples C and D have essentially the same gross calorific
and lower.7 This is the mineral-matter-free, inherent-moisture value on an inherent-moisture, mineral-matter-free basis, but
basis, which is equivalent to the as-received (AR) basis for are not ranked the same because of their differing agglomer-
samples collected and preserved as described in Section 7. In ating properties. An important, but sometimes unclear consid-
Eq 4, the calorific value is corrected for the estimated heat of eration with higher rank coals is their agglomerating character.
combustion of pyrite (–50S), expressed as units of (Btu/lb)/% Since 1934, the agglomerating character of the sample has
sulfur, and then calculated to the inherent-moisture, mineral- been used to distinguish subbituminous A from high volatile C
matter-free basis by the factor (100 – MMim,SO3f), equivalent to bituminous coals. It was recognized that the calorific value of
(100 − (1.08Aim,SO3f + 0.55Sim)). All data are on the inherent- the two ranks overlapped. In earlier versions of the standard,
moisture basis. “examination of the residue in the platinum crucibles incident
to the volatile matter determination...” was the required proce-
X2.3 Useful Equations—The ranking equation (Eq 3 of dure to determine agglomerating character. These versions go
9.2.1) can be simplified for cases when data are available on on to read “Coals which, the volatile matter determination,
the dry basis: ash, volatile matter, sulfur, and the sulfur trioxide produce either an agglomerate button that will support a 500-g
content of the ash.8 In such cases, Eq 3 of 9.2.1 can be weight without pulverizing, or a button showing swelling or
expressed so as to yield the ranking parameter directly, the cell structure, shall be considered agglomerating... .” However,
volatile matter on the dry, mineral-matter-free basis: for over 25 years, the standard test for the Free-Swelling Index
(Test Method D720/D720M) has included the provision to test
the pulverizing nature of the button under a “500-g weight.” It
VMdMMf 5
VMd 2 0.08A d 1 2 S SO3 :A d
100 D
2 0.4S d
(X2.2)
has been the practice for many years to use the results of the
Free-Swelling test to determine the agglomerating character of
1 2 0.0108A d S 12
SO3 :A d
100 D 2 0.0055S d a coal as outlined in 8.3 of this standard.
Sample F demonstrates the need to use fixed carbon and
For a coal of rank high volatile A bituminous or lower and volatile matter contents (on a dry, mineral-matter-free basis)
for which the inherent moisture (or equivalent as-received since the fixed carbon exceeds 69 % irrespective of the gross
moisture) and dry values for gross calorific value, and the ash calorific value on an inherent-moisture, mineral-matter-free
basis. In Samples E and F, gross calorific values on a dry,
mineral-free basis are very similar, but, because Sample F
7
Fieldner, A. C., Selvig, W. A., and Gibson, F. H., “Application of Ash contains greater than 69 % fixed carbon on a dry, mineral-
Corrections to Analyses of Various Coals,” Transactions, American Institute of
Mining and Metallurgical Engineers, Coal Division, Vol 101, 1932, pp. 223–246.
matter-free basis, these two samples are not given the same
8
Hoeft, A. P., Harvey, R. D., and Luppens, J. A., “Notes on the Determination of rank. Sample E is a high volatile B bituminous coal and
ASTM Coal Rank,” Journal of Coal Quality, Vol 12, No. 1, 1993, pp. 8–13. Sample F is ranked as a medium volatile bituminous coal.
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D388 − 19a
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