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SPE 14654
Tfsispafw waa prepared forpresentational the Eaet Texse RegionalMeetingof the society of PetroleumEngineersheld in Tyler, Texas, April2!-22, 1966.
This paper wae selected for presentation by an SPE Program Committee following review of information contained in an abstract submittadby the
author(s).Contents oflhepaper, aspreeented, have nolbeen reviewed bythe Metyol Petroleum Engineers andaresubject to:orrWtion by the
author(e). The material, aa presented, does not necessarily reflect any poslllonoi tl{a Society of Petroleum Engineers, its offf~ers,or membere. Papers
presented at SPE meetings are subject to publication review by Editorial Commiffeea of the SOCietyof petroleum En9inR’ >. permisaiofl tOCOPYis
restricted tosn abstract of not more than 3Dff words. lllustratione maynotbe copied. The abstract ehouldcontain conspicuousacknowledgm?ntof
where and by whom the paper is presented. Write Publication Manager, SPE, P.0. Box 8336?6, Richardson, TX 75083-3636. Telax, 730989 SPEDAL.
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2 ST_fM~TING CARBONATE FORMATIONS lJSINGA CI SED FRACTURE ACIDIZING TE~~UE SPE 14654
1
Closed Fracture Acidizing
rested for the necessary frsctuxe flow
apacities. A prncedlJre has been developed to
help overt me some of the proolems of low,
2. The formation is etched in an acid etchec fracture flow cagaclt.ieswhich
,neven or irregular manner as desired, but sometimes result from standard fzacture
he etcl,ad flow channels are crushed ?n acidizing.s This procedure entails pump-
‘losure either because the formation 1s ing acid through a closed or partially
,00 soft, as in a chalk formation, OK be- closed fracture at or just below fracture
:ause excessive acid leakoff softens the opening pressure to prevent opening the
Ivezall fractu:’eface. fracture to any appreciable width. Acid
flows out this closed fracture, possibly
‘3. The formation has a relatively in turbulent flow, rapidly dissolvin.jmush
,OW Hcl volubility (for a carbonate - 85 more ccre face than if it were flowing in
;O 90%) which leaves acid insoluble fines an open fracture. Also, in most ca”bonate
10 to 15%) that c~n remain on the frac- formations there are azeas or stringers
;ure face and restrict additional acid that have different reaction rates
:eacti6n. At times this insoluble primarily due to different HC1 volubility,
~aterial can be extremely sticky or gummyl composition, or permeability. This condi-
~nd actually reduce the fracture floW tion will generally allow one area to dis-
:apacity. solve faster than an adjoining area. AS
the areas cr stringers dissolve they be-
4. The acid reaction time at high come large~, and in a very short period
Jump rates is insufficient for acid to most of the acid is tending to flow
:eact with the fracttireface to obtain the through them, thus creati?g channels or
lneven removal necessary for adequate qrooves. Under some conditions, these
Fracture conductivity.
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:he same rate is also shown. For example, of carbonate formations, and it is dif-
; 0.32 in. LD hole could carry the same 45 ficult to predict these unless actual core
>bl/day as a fracture with” 2,000 md-ft flow studies are conducted (Table 1).
:1OW capacity at 100 psi differential. A
~ole of 1.10 in. ID could carry the same LABORATORY ACID ETCHED FRACTURE FLOW
150 BPD that a fracture with 20,000 md-ft CAP3CITY TESTS
flow capacity at l,C30 psi differential.
Laboratory tests are conducted on a
:losed Technique Advantages routine basis by flowing acid across a
vertically cut core face to determine acid
This closed fracture acidizing pro- etched flow capacities of various acids
?edure has numerous advantages over high and acid systems (Table 1). In many in-
:ate-high pressure treatments. stances adequate flow capaciki?s can be
obtained with conventional fracture
1. Jobs are generally simpler be- acidizing procedures. At times however,
~ause treatment rate and pressure can be the fracture flow capacities obtained are
ouch lower. too low and other techniques are needed,
such xs usictgheated acids if the well is
2. There is much less chance of cold. When these flow capacities are low,
iamage to wellbore equipment, tubing, an additional acid flow period is run with
?ackers, etc since less pressure is the fracture in a closed condition. This
>eeded. forces the acid to flow out this closed
but partially etched fracture, and in most
3. Since the fluid is almost allowed cases dissolves deep grooves or channels
to flow out rather than being forced out in the core face for high flow capacities.
Jnder high pressure, acid will tend to However, there are times when this system
follow the areas with the greatest total does not provide any benefit.
rake of volubility such as high HC1
volubility and high permeability. This These tests are conducted to measure
Mill help keep acid in the normally more the flow capacity under closure pressure
?roductive zones. of a created and acid etched fracture:
The core sample is cut into circular disks
4. Extremely high flow capacities 2.25 to 4 in. OD by 0.75 to 1.0 in. thick,
?an be developed that will be much less such that the surface exposed to acid is
susceptible to drainage plugging from for- in the same plane as a vertical fracture.
nation fines, organic deposits, or scales. These disks are then mounted in lead and
the face of the sample turned flat with a
5. The etched groove or channel will lathe. A hole is drilled through the axis
stay open under severe closure and/or of the sample and the lead mounting. The
zrushing conditions “(Table 1). sample is then placed in the etching test
cell with the turned face of the sample
6. Acid or other aqueous fluid sen- touching an ampcoloy block that acts as
sitive formations can be stimulated with the opposite fracture face. The cell is
less chance of formation closure and cor- brought up to test temperature, and a mi-
responding loss in flow capacities. crometer is attached and set at zero. The
sample is then separated from the ampcoloy
Closed Technique Disadvantages block 0.05 inches. Acid is flowed thraugh
the hole and radially across the sample
There are some disadvantages to this face at 1000 psia (open etching). After a
procedure that should be considered: specific time interval, the acid is
removed and replaced with kerosene. clo-
1. No way has yet been developed to sure pressure is then applied to the sam-
model or predict the number and ext~:nt of pie, and the flow capacity obtained from
etched grooves or channels. the open etched test is measured. Acid
can then be flowed through the “closed”
2. Diverting with ball sealers can fracture with closure pressure applied
be a problem at low rates and low dif- (closed etching). The amount of sample
ferential pressures across perforations; removed or crushed is then measured by
however, this prcblem can generally be micrometer. This process can be repeated
overcome with balanced density or light several times but the common practice is
weight ball sealers, and/or by increasing to perform two to three flow periods. Any
the pump rate when the ball sealers are at specified closure pressure can be used.
the perforations. If none is given, a closure pressure of 1/
3 psi per ft of depth is used with a mini-
3. The closed fracture acidizing mum of 1,000 psi.
treatment will not work on certain types
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4 STIMULATING CARBONATE FORMATIONS USING A CLOSED FRACTURE ACIDIZING TECHNIQUE SPE 14654
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‘D?7 lAf=.KA
!. J-l .L-Z”-T
Sherman
--------- ----- l?. Fredrickson
-- —--- .. ----
c
Treating naturally fractured systems Step 5 - Shut down for 1.5 hr for the
?as one inherent problem thaL should be fracture to close.
:onsidered if a large zone is to be treat-
?d: most naturally fractured reservoirs Step 6 - Pump 2,000 gal 20% ungelled
lave low matrix permeabilities. If the HC1 at 1 bbl/min. Displace
perforations happen to intersect a natural only to formation.
Eracture, the pressure necessary to pump
into it and even widen it are generally Thirty new wells in this field have
lot excessive. However, if these perfora- been treated making 100 BOPD average with
Lions penetrate an interval having no the general overall techniques. No wells
~atural fracture, the pressure needed to were treated with unheated acid or without
Eracture to intersect a natural fracture the closed fracture acidizing procedure.
~an be exceedingly high. In a short in-
terval this may be no problem if there are Case History No. 2
sufficient open perforations for ~dequate
?roduction. However, when a section has Middle East: Chalk Wells at 8,000 ft
several zones that cannot drain vertical- with 2000F l?HT:
ly, each zone must be actually treated in
>rder to produce. If some perforations Well No. 1: Previous standard frac-
:onnect with the natural fracture system ture acidizing using viscous preflushes
and some do not, diverting under suffi- had resulted in 500 BOPD production, de-
:ient pressure to break down the unconnec- creasing to 300 BOPD in five years.
ted ones can be very difficult.
Well was treated with 40,000 gal 28%
The most effective system would be to HC1 alternated every 5,000 gal with a non-
Jse straddle packers of some sort to es- acid fluid loss control and acid extender
tablish that each specific zone is capable phase at 1 to 2 BBL/min. Initial produc-
>f actually taking fluid. Balling off tion was 3,000 BOPD, decreasing to 1,800
~ith ball sealers, followed by an injec- BOPD after one year.
tion survey, could be used to determine if
all the zones are taking fluid. Well No. 2: Previous treatment similar to
Well No. 1 but had been shut in due to low
Once it is determined that the entire production.
interval is capable of taking fluids at a
reasonable pressure, the standard closed Well No. 2 was treated similar to
Eracture acidizing procedure can be run. Well No. 1 with flush resulting in produc-
In a large zoile, several stages of acid tion of 2,000 BOPD, decreasing to 1,200
separated with ball sealers should be con- BOPD after one year.
~idered (Case History No. 3) .
Case History No. 3
case History No. 1
Mississippi: Chalk Wells at 15,000
Texas: San Andres Formation, Yoakum ft witi’ 2’?OoFBHT:
~nd Gaines County, 5,000 ft with 105 to
L15°F BHT: WelLs had been fractured with
proppants ~nd fracture acidized with
All fluid are heated to llOoF with a limited success. These formations are
hot oiler and weighted to 9.0 lb/gal for considered to be naturally fractured.
fiensityplacement control.
Present treatment consisted of 3,00!3
Step 1 - Pump 140 bbl water ccntain- gal 15% chemically retarded acid followed
ing scale inhibitor, then by 1,000 gal 15% HC1, followed by 4,000
shut down for 1 hour. gal 28% HC1, all at 0.5 bbl/min with the
following results:
Step 2 - Pump 6,000 gal crosslinked
gelled preflush at 6 to 8 Well No. 1: Before 25 BOPD at 100 psi
bbl/min.
After 280 BOPD at 3,250 psi
step 3 - Pump 10,000 gal 20% HC1 con-
taining 2.0% gelling agent, Well No. 2: Before 50 BOPD at 100 psi
alternating at 2,000 gal
intervals with gelled fluid After 304 BOPD at 4,200 psi
A7
6 STIMULATING CARBONATE FORMATIONS USING A CLOSED FRACTURE ACIDIZING TECHNIQUE SPE 14654
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Kid East 5,000 Emulsified 28% HC1 Open 18 1,500 204 North Texas 3,000 28.% HC1 @e. 1.000 1,348
Closed 36 1,500 93.020 100 @en I 1,000 24,816
54 1,500 156.188 Closed 54 1,000 280,000+
2.000 153;772
2.500 146.520 GeIled 28% HCI Open 1.000 644
3,000 141,768 Open & 1,000 4,636
3,500 134,484 Closed 54 1,000 191,332
Wchigan 4,000 28% HC1 Open 18 1,340 1,380 Mid Sast 10,800 15% HC1 Open 3,900 3,260
Open 36 1,340 7,412 200 Open H 3,900 1,244
Closed 54 3,900 47,832
Closed 18 1,340 176,188
28% HC1 Closed 36 1,340 280. 000+ 28% IiCl Open 18 3,900 4,232
Open 36 3,900 1.288
West Texas 1O,4OO(CI)* Gelled 28Z HC1 Open 18 3,472 <10 Closed 54 3,900 74.312
200 36 3,472 <10
Mid tiSt 8,000 28% HC1 Open 2,645 <10
1O,4OO(C2)** Open 18 3,472 <10 210 Open & 2,645 <1.I
200 36 3,472 <10 Closed 54 2,645 <10
Closed 54 3,472 <10
mexico 10,800 28% HC1 Open lb 3,594 8,940
West Texas 5,600(CI) 28% HC1 @en 18 1,886 344 180 Open 36 3,594 67,688
125 Cpen 36 1,886 844 Closed 54 3,594 280,000+
Foamed .?8ZHC1 Open 18 1,886 2,360 Gellei 28z HC1 Gpen 18 3,594 1,012
*en 36 1.886 41.568 Open 36 3,594 644
Closed 54 3,594 181,5KI
Foamed ?8% HC1 Closed 1,886 134.400
Germany 4,800 Gelled 28% HC1 Open 18 1.560 4.340
6,000(C2) 28Z NC1 Open 18 2,000 368 170 open 36 1,560 2,248
140 @en 36 2.000 1,888
Clc.sed 54 2;000 111,856
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TASLE I Cent’d TABLE 2
Fracture Flow races of 1.0 cps fluid througha fracture 100 ft high by 500 ft long
Closure Flow
Core Sample Depth (ft) Type Etch PressureCapacity at various flow capacites and pressure drops. The hole sf ze necessary to f lou
Origin Tenm. (“F) Acid Tvpe 2K!ZXL!2?2 (psi ) (md-ft)
the same rate is calculated.
*
(W-many 4,800 Gelled 2RZ NC1 Closed 18 1,560 129,780
170 Closed 36 1,560 280,000+
sasc Texas 10,OOO(C1) HC1-Acetic Open 18 3,360 120,608 FraccureFlow Pressure Flow Equivalent
180 3b 3.360 89,680
Capacity (red-f t) Orop (Psi) Sates (B/D) Hole Size (in. )
tist Texas 10, OOO(C2) HC1-AcetIc @en 18 3,360 2,852
180 Open 36 3,360 2,’236
Closed 54 3,360 186,440
2,000 100 45 0.32
East Texas 16,000(C1) Gelled :82 HC1 @en 4,670 1,060
250 op. E 4,670 29,084 8,000 100 180 0.53
1‘5%HCI Closed 54 4,670 280,000+
20,000 100 450 0.75
M,000(C2) Gelled 28% HC1 Open 18 4,670 124
250 open 36 4,670 88
15% HC1 Closed 54 4,670 <10
2,000 500 225 0.41
*cl - Core No. 1.
8.000 500 901 0.69
**C2 - Core No. 2.
I 20,000 500 2,254 0.98
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