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International Journal of Pavement Research and Technology 11 (2018) 603–610
www.elsevier.com/locate/IJPRT

Influence of temperature on Jnr values of polymer modified


asphalt binders
Khaleel Al-Adham ⇑, Hamad Al-Abdul Wahhab
Department of Civil Engineering, King Fahd University of Petroleum and Minerals (KFUPM), Dhahran, Saudi Arabia

Received 13 August 2017; received in revised form 21 October 2017; accepted 3 January 2018
Available online 10 January 2018

Abstract

At desert environment, asphalt binders that have performance grades of PG 70-16 or PG 76-16 may show early signs of rutting under
heavy loads due to lack of strain recovery when used in the design of asphalt mixes and structures. Type and amount of polymer in addi-
tion to testing temperature are the major factors that affect the recovery properties of asphalt binders. This study was conducted to eval-
uate Jnr parameters of four different polymers (Styrene–Butadiene–Styrene ‘‘SBS”, Crumb Rubber ‘‘CR”, light density Polyethylene
‘‘PE” and modified Olefin ‘‘OF”) used to modify asphalt binders. Asphalt samples were tested at various temperatures and regression
models were created. These models are useful to properly select the polymer type and amount suitable to the area of concern and to be
used in the design of pavement structures especially in Mechanical–Empirical Design Guide. It is found from this study that power-law
models best described the relationship between Jnr and temperature with signs of shear thickening. The results of Styrene–Butadiene–
Styrene Modified asphalt binders have shown best behavior of recovering the strain at high temperatures with Non-recoverable creep
compliance (Jnr) values less than 0.5 obtained at 76 °C. Polyethylene and Olefin polymers could improve local asphalt binders at areas
where PG 58 and PG 64 are required. The Jnr-temp curves can be considered as master curves for local conditions and material.
Ó 2018 Chinese Society of Pavement Engineering. Production and hosting by Elsevier B.V. This is an open access article under the CC BY-NC-ND
license (http://creativecommons.org/licenses/by-nc-nd/4.0/).

Keywords: Desert environment; Elastomer; Non-recoverable compliance (Jnr); Power law; Jnr master curves; Polymer modified asphalt binders; Multiple
Stress Creep Recovery MSCR

1. Introduction It is suggested that Multiple Stress Creep Recovery


(MSCR) test should be conducted at PG temperature to
In order to resist rutting at high temperatures, the con- measure the recovery parameters including the percent
ventional Superpave design method requires that modified recovery (%R) and Non-recoverable creep compliance
asphalt binder should have high values of G*/sin and hence (Jnr). MSCR test is performed using Dynamic Shear
high performance grades (PG). However, at desert environ- Rheometer (DSR) at PG temperature using a constant stress
ment, asphalt binders that have PG 70 or PG 76 may show creep of 1.0-s duration followed by a zero stress recovery of
early signs of rutting under heavy loads due to lack of elas- 9.0-s duration. The test is performed at two stress levels, 0.1
tic recovery of the binder used in the design of asphalt kPa and 3.2 kPa. Ten cycles are run at each of the two stress
mixes and structures. levels making a total of 20 cycles. The stress and strain shall
be recorded at least every 0.1 s for the creep cycle and at least
⇑ Corresponding author. every 0.45 s for the recovery cycle on an accumulated basis
E-mail addresses: Khaleel.aladham@gmail.com (K. Al-Adham), such that, in addition to other data points, the data points
hawahab@kfupm.edu.sa (H. Al-Abdul Wahhab). at 1.0 s and 10.0 s for each cycle’s local time are explicitly
Peer review under responsibility of Chinese Society of Pavement recorded. There are no rest periods between creep and
Engineering.

https://doi.org/10.1016/j.ijprt.2018.01.001
1996-6814/Ó 2018 Chinese Society of Pavement Engineering. Production and hosting by Elsevier B.V.
This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
604 K. Al-Adham, H. Al-Abdul Wahhab / International Journal of Pavement Research and Technology 11 (2018) 603–610

recovery cycles or changes in stress level. The total time viscosity [10–13], elastic recovery [14], softening point and
required completing the two-step creep and recovery test is complex modulus, and decreases the penetration, ductility
200 s [1]. Two parameters are calculated from this test; per- and phase angle of the CR modified asphalt binders.
cent recovery (R) and Non-recoverable creep compliance A recent research conducted MSCR test on asphalt bin-
(Jnr). Percent recovery is the percent difference between the ders contains different sizes of Crumb Rubber particles
final (e10) and initial (e0) strain of the tenth recovery curve (No. 60, 40 and 28) to characterize their high temperature
while Jnr is the ratio between final strain (e10) and applied performance [15]. They concluded that the accumulated
stress i.e., 3.2. strain significantly decreases when using low asphalt grades
However, at hot climate, pavement service temperature or fine CR particles in producing the modified asphalt
could reach up to 73 °C in summer which could harshly binders.
affect most of asphalt binders’ properties that suppose to AASHTO MP 19 was conducted to evaluate the elas-
resist rutting under very heavy and extremely heavy wheel tomeric properties of the modified binders; all tested sam-
loads [2]. On the other hand, asphalt extracted from heavy ples were compared to a standard curve recommended by
oil in Gulf Countries has PG 64-10 and did not satisfy the FHWA. %R–Jnr data points that lie above the suggest line
requirements at all locations of local and international are considered as elastomer and have high potential to
market for pavement construction projects [3]. To solve resist rutting at high temperatures and extremely heavy
this problem, specific types of polymers are needed to traffic. While AASHTO TP 70 requires classifying the
improve the recovery property that will resist rutting at resulted percent recovery and Jnr values into four different
high temperatures. Several research projects conducted classes of traffic loading at each targeted high service tem-
studies to modify asphalt in order to achieve the PG perature of the binder (‘‘S” for Standard, ‘‘H” for Heavy,
requirements at desert environment. Some researchers ‘‘V” very heavy and ‘‘E” for extremely heavy).
found that polymer modification improves the asphalt bin- The results of this study could help designers of asphalt
der performance by decreasing the high temperature per- mixes during their selection of polymer type and amount
manent deformation [4]. taking into consideration all cost components that may
It is important to evaluate the strain recovery property affect their decision. Moreover, the generated Jnr-temp
termed by percent recovery %R and Non-recoverable creep curves could be utilized in Mechanical–Empirical Design
compliance (Jnr) of polymer modified asphalt binders at methods of pavement structures as they considered as mas-
different temperatures and to create models in order to ter curve of recovery property. This relationship may
properly select the polymer type and amount suitable to enforce or replace the viscosity and G*/sin d criteria of
the area of concern and to be used in the design of pave- asphalt binders. The current parameter G*/sin (delta),
ment structures especially in Mechanical–Empirical Design which is measured by applying an oscillating load to the
Guide. Many researchers conducted studies that consid- asphalt binder at relatively low shear strain, is used to
ered the Non-recoverable compliance Jnr as a new param- determine the existence of elastic and viscous effects of
eter to evaluate the rutting behavior of polymer modified asphalt binders. So, additional tests (called PG-plus tests)
asphalt binders using the Multiple Stress Creep and Recov- have been added to measure the potential of polymer mod-
ery (MSCR) test. This test is suggested to replace the con- ified asphalt binders in recovering the applied stress. One of
ventional Superpave standards for rutting criteria at high- those tests is ‘‘Elastic Recovery” which is conducted to
temperatures (G*/sin) [5,6]. The study includes an investi- evaluate the recovery of the modified binders at 25 °C
gation of the newly suggested parameter to capture the rut- which does not capture the actual performance against rut-
ting behavior and rheological analysis of the MSCR by ting at higher temperature, higher traffic volumes and
conducting the laboratory wheel tracking test of the lower speeds.
asphalt mix and create a correlation between Jnr and rut- On the other hand, MSCR test is using higher levels of
ting for theses mixes. They concluded from their study that stress (3.2 kPa) to capture the effectiveness of polymer net-
the best correlation between Jnr and rut depth was obtained work at high temperature. The resulted MSCR Recovery
at high-levels of stress from the MSCR test. provides an indication of the delayed elastic response of
Four groups of polymers that have good reputation in the asphalt binder, while MSCR Non-recoverable creep
international market were selected to be used in this study; compliance (Jnr) is used to classify the modified asphalt
Styrene–Butadiene–Styrene ‘‘SBS”, Crumb Rubber ‘‘CR”, binders into different traffic levels at the targeted service
Polyethylene ‘‘PE” and Olefin ‘‘OF”. These polymers are temperature. Furthermore, Jnr has better correlation with
characterized to basic tests including viscosity and perfor- field rutting than G*/sin d [5,16].
mance grading then subjected to controlled Multiple Stress
Creep Recovery test under the two standards [7,8]. 2. Methodology
The interest in using of crump rubber in asphalt pave-
ments is increasing to improve the performance of the 2.1. Material selection
asphalt binder. Based on the literature, the modification
of the asphalt binder by the Crumb Rubber could reduce Asphalt samples were collected and evaluated in terms
noise [9] when used in high amounts; it also increases the for basic properties including viscosity and ductility in
K. Al-Adham, H. Al-Abdul Wahhab / International Journal of Pavement Research and Technology 11 (2018) 603–610 605

addition to chemical composition. The average values of all Creep Recovery (MSCR) test using the Dynamic Shear
sampled asphalts are shown in Table 1: Rheometer (DSR) at different temperatures. Percent recov-
Four types of polymers that are mostly used in local and ery is the percent difference between the final (e10) and ini-
international projects are selected to modify asphalt bin- tial (e0) strain of the tenth recovery curve while Jnr is the
ders in this study. Styrene–Butadiene–Styrene ‘‘SBS” with ratio between final strain (e10) and applied stress i.e., 3.2.
70/30 Butadiene/Styrene thermoplastic copolymer, poly- Fig. 1 shows typical MSCR results [1].
merized in solution and has a radial structure is used. Each polymer modified asphalt sample was tested for
The second polymer is Crumb Rubber ‘‘CR” which is col- performance grade (PG), then the same sample was condi-
lected from a local factory and is produced from the recy- tioned to be tested for Jnr with 3 °C increments starting
cled rubber obtained from automotive and truck scrap tires from higher to lower temperatures around the PG temper-
and have grain size of passing sieve no. 0.1 mm and ature, ranging from 58 to 79 °C. This temperature range
retained on 0.075 mm. Two Plastomers include low density was selected because most of asphalt binders extracted
Polyethylene ‘‘PE” and modified Olefin ‘‘OF” (also called from crudes have performance grade of PG 64-16 and
Alkenes) were selected in this study. PG 58-16 for heavy and light oil, respectively [2]. Because
rutting is the main concern of pavement distresses at high
2.2. Material testing and evaluation service temperature in arid areas like gulf countries, the tar-
geted grades of modified asphalts in this study are PG 64,
Binders were modified with 2–6% of SBS, PE and OF PG 70 and PG 76.
and 5–10% of CR in order to meet different performance Two samples for each polymer-asphalt combination
grades (PG) suitable for desert environment. These grades were tested and average values of Jnr were reported in
are PG 70, PG 76 and PG 82. Asphalt binder was heated to results section. A third sample for the same combination
reach a specific temperature (165–185 °C) then polymer was prepared, conditioned and tested for model validation
was added gradually and mixed with high shear mixing step. All prepared polymer modified asphalt samples were
for one hour. Each modified sample was stored at 145 °C drawn on the standard curve to differentiate between elas-
overnight to ensure the maturity of the polymer–asphalt tomer and Plastomers.
network. Dynamic viscosity was carried on the modified
samples to measure workability, mixing and compaction 3. Results and analysis
temperatures (AASHTO TP 48). The fifty-two different
modified asphalt binders were subjected to short term In this section, results obtained from binder testing are
aging and then were subjected to Performance Grading discussed in the following sub-sections and full data are
(PG) (AASHTO M320) and Multiple Stress Creep Recov- listed in Table at the end.
ery (MSCR) (AASHTO M332).
3.1. Correlation between stiffness (G*/sin d) and relaxation
(1/Jnr) of polymer modified asphalts
2.2.1. Dynamic Shear Rheometer (DSR) test
The dynamic temperature step measurements for the
Although the difference in testing procedure and applied
samples were performed in CSA II rheometer. All samples
stress levels of both tests and the internal properties of
were tested in a range of 64–82 °C according to the stan-
polymer modifications, the results of stiffness of modified
dard test (AASHTO T315). The results of this test were
samples noted by G*/sin d were correlated to the reciprocal
used to grade the polymer modified asphalt sample accord-
of the Jnr parameter using Pearson Correlation method
ing to their Performance (AASHTO M320) and to find out
which relate to the shear modulus at relaxation condition
the amount of polymer required to meet the targeted PG’s
and both have unit of kPa. A good but not strong correla-
(PG 70, PG76 and PG 82).
tion was resulted with Pearson coefficient of 0.74 and p-
value <0.05. Fig. 2 shows the relationship between the 52
2.2.2. Multiple Stress Creep Recovery (MSCR) test samples. (Full data is presented in Table 2.)
This test method is used to determine the Non-
recoverable creep compliance (Jnr) and percent recovery 3.2. Effect of temperature on the elastomeric property of
(R) of asphalt binders by means of the Multiple Stress polymer modified asphalt binders

Table 1 By plotting percent recovery (%R) and Non-recoverable


Properties of asphalt binders used in the study. strain creep compliance (Jnr) results on the standard curve
Property Average value (%R = 29.4Jnr0.26) recommended by AASHTO TP 70 for
Flash Point, °C 338 each polymer modified asphalt binder tested at 3.2 kPa
Penetration Grade 60/70 stress and at different temperatures, the elastomeric prop-
Rotational viscosity at 135 °C, cP 464 erty of that binder can be evaluated. If the data point of
Ductility at 25 °C, mm 100+ %R–Jnr at specific temperature lies above that line, the elas-
Performance Grade (PG) PG 64-16
tomeric behavior is highly expected at that condition when
606 K. Al-Adham, H. Al-Abdul Wahhab / International Journal of Pavement Research and Technology 11 (2018) 603–610

0.040
εc
0.035

0.030

Recovery
% Strain

0.025

0.020

0.015

0.010
εr
0.005 ε0
0.000
0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0

Time, (s)
Fig. 1. Typical MSCR test result after 10 cycles of creep and recovery.

25.0

20.0
1/Jnr, kPa

15.0

10.0

5.0

0.0
0.0 5.0 10.0 15.0 20.0 25.0 30.0
G*/sinδ, kPa

Fig. 2. Relationship between G*/sin d and Jnr.

used in asphalt mix. Figs. 3 and 4 show the results of SBS at which elastomeric behavior starts can be estimated. Sim-
and CR modified asphalt binders, respectively. ilar behavior could happen for Crumb Rubber (CR) but
Power-law curves parallel to the standard line of elas- the elastomeric behavior could change at very low temper-
tomeric behavior are generated as shown in the Figures. atures which is an undesirable situation at desert
It can be shown from the Figure that 6%-SBS modified environment.
asphalt binder has a remarkable elastomeric behavior at For Polyethylene and Olefin modified asphalt binders,
any temperature. That means a number of polymer’s mole- the resulted curves are not reaching the elastomeric curve
cules are sufficient to improve the elastic recovery for the at high nor moderate temperatures, only the situation at
system, while 4% SBS modified asphalt binders at a lower which the required temperature is less than 58 °C these
temperature might reach a point at which signs of elas- modified binders could have some strain recovery. Fig. 5
tomeric behavior is reduced. By comparing the MSCR shows the results of Olefin modified asphalt binders at dif-
recovery and Jnr values for each tested asphalt binders at ferent temperatures while Fig. 6 presents PE results.
the same temperature, an improvement in recovery was
observed which indicates that there is a significant effect 3.3. Effect of temperature and amount of polymer on Jnr
of polymer type and amount on recovery values. There is values
a sign of superposition of the temperature and number of
molecular interaction points between polymer and asphalt All polymer modified asphalt samples prepared in this
binders that improve the elastic recovery property of the study were tested at 3.2 kPa stress level and at different
system. With simple algebraic calculations the temperature temperatures range from 58 °C to 79 °C in order to find a
K. Al-Adham, H. Al-Abdul Wahhab / International Journal of Pavement Research and Technology 11 (2018) 603–610 607

Table 2
G*/sin d and MSCR results of all tested samples.
Sample PG Temperature, °C G*/sin d Jnr Recovery
kPa 1/kPa %
Unmodified PG 64 58 4.005 1.480 3.602
64 2.598 3.811 0.040
70 1.191 6.141 0.000
Styrene–Butadiene–Styrene PG 70 58 10.678 0.268 34.018
SBS 64 8.009 0.775 18.734
70 3.875 2.036 8.100
76 1.938 2.795 1.342
PG 76 58 17.154 0.079 62.236
64 14.490 0.241 46.549
70 7.519 0.685 29.145
76 4.035 1.703 16.258
82 2.192 2.006 4.435
PG 82 58 31.845 0.014 84.950
64 26.760 0.043 78.043
70 14.860 0.128 67.688
76 8.264 0.363 53.992
82 4.691 0.420 45.360
Crumb Rubber PG 70 58 14.010 0.158 31.048
CR 64 6.751 0.468 16.240
70 3.385 1.247 5.291
76 1.763 2.893 0.643
PG 76 58 8.459 0.135 40.802
64 6.357 0.419 23.320
70 3.160 1.163 8.857
76 1.606 2.830 1.810
PG 82 58 8.658 0.182 39.817
64 6.786 0.550 22.510
70 5.120 1.471 9.776
76 2.631 3.548 2.604
82 1.376 4.193 0.663
Polyethylene PG 70 58 13.141 0.386 9.937
PE 64 9.741 1.048 1.712
70 4.646 2.478 0.969
76 2.093 5.256 0.003
PG 76 58 13.552 0.253 17.830
64 10.423 0.740 5.835
70 7.634 1.843 0.692
76 3.487 4.132 0.044
82 1.377 4.927 0.000
PG 82 58 22.320 0.133 21.453
64 17.202 1.453 8.977
70 12.500 2.222 4.900
76 6.133 2.775 0.823
82 2.264 3.820 0.044
Olefin PG 70 58 6.447 0.825 12.001
OF 64 4.816 2.196 3.109
70 2.234 5.043 0.447
76 1.079 6.906 0.000
PG 76 58 10.803 0.249 18.392
64 9.135 0.675 6.624
70 4.488 1.634 1.140
76 2.225 3.482 0.198
82 1.153 4.174 0.004
PG 82 58 9.911 0.064 52.380
64 7.964 0.270 25.761
70 6.184 1.206 5.624
76 3.737 6.628 0.514
82 2.290 7.199 0.014
608 K. Al-Adham, H. Al-Abdul Wahhab / International Journal of Pavement Research and Technology 11 (2018) 603–610

90 70
2%SBS 2%OF
80 4%SBS 60 4%OF
70 6%SBS 6%OF
Power (Standard Curve)
50
60 Power (Standard Curve)
50 40
%R

%R
40 30
30
20
20
10 10
0 0
0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0
Jnr (1/kPa) Jnr (1/kPa)
Fig. 3. Evaluation of elastomeric behavior of SBS. Fig. 6. Evaluation of elastomeric behavior of PE modified asphalts.

70 results of the four selected polymer modified asphalts that


5%CR
have three levels of polymer amount and performance
60 7.5%CR
grades tested at various temperatures.
10%CR
50 It can be shown from previous analysis that MSCR
Power (Standard Curve) results are affected by testing temperature polymer type
40
and polymer amount. A comparison between all
%R

30 polymer-modified asphalts is included in this study which


is classified into three Performance Grades and tested
20 under different temperature levels. The remarkable behav-
10
ior of SBS polymers in improving the recovery properties
of asphalt binders is due to butadiene content which forms
0 around 70% of its structure and has a rubbery nature which
0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 gives SBS its elasticity at higher contents.
Jnr (1/kPa) The best relationship was found between Jnr and tem-
Fig. 4. Evaluation of elastomeric behavior of CR.
perature follow the power law and has the following
equation:

70 J nr ðT Þ ¼ kT a ð1Þ
2%PE
60 4%PE where
6%PE Jnr is the average of Non-recoverable compliance (e10/s)
50 after 10 cycles tested under 3.2 kPa stress.
Power (Standard Curve)
T is the tested PG temperature in Celsius
40 a is the power law exponent
%R

k is an arbitrary constant that indicates to the scale unit


30
of the equation.
20
The exponent a of the power law curves can gives a sign
10 of rate of change of Jnr values. Table 2 summarizes the
components of the generated regression models a and k.
0 Goodness of fit R2 is excellent for all generated models as
0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 shown in Table 3.
Jnr (1/kPa) The results of this study could help designers of asphalt
Fig. 5. Evaluation of elastomeric behavior of OF modified asphalts. mixes during their selection of polymer type and amount
taking into consideration all cost components that may
affect their decision. Moreover, the generated Jnr–temp
relationship between Jnr parameter and temperature and to curves could be utilized in Mechanical–Empirical Design
create regression models used for proper design of asphalt methods of pavement structures as they considered as mas-
mixes and structures against rutting. Fig. 7 shows the ter curve of recovery property. This relationship may
K. Al-Adham, H. Al-Abdul Wahhab / International Journal of Pavement Research and Technology 11 (2018) 603–610 609

Jnr , 1/kPa 3

0
58 61 64 67 70 73 76 79
Testing Temperature, °C

Fig. 7. Effect of temperature on Jnr values.

Table 3
Components of power-law models generated.
Asphalt binder PG a k R2
Unmodified Asphalt PG 64 8.425 2.00E-15 0.981
Styrene–Butadiene–Styrene PG 70 10.81 2.00E-20 0.999
SBS PG 76 11.62 3.00E-22 0.999
PG 82 12.52 1.00E-24 0.995
Crumb Rubber PG 70 10.98 8.00E-21 0.999
CR PG 76 11.06 5.00E-21 0.999
PG 82 11.27 2.00E-21 0.999
Polyethylene PG 70 9.116 5.00E-17 0.999
PE PG 76 10.4 2.00E-19 0.997
PG 82 12.91 1.00E-24 0.994
Olefin PG 70 8.067 4.00E-15 0.995
OF PG 76 9.402 2.00E-17 0.98
PG 82 10.42 1.00E-19 0.978

enforce or replace the viscosity and G*/sin d criteria of improving the Jnr is low compared to SBS values. It can
asphalt binders which is the material property that is cur- only withstand Heavy traffic (Jnr 1–2 kPa1) at 70 °C and
rently included in the analysis of the dynamic modulus Standard Traffic (Jnr 2–4 kPa1).
|E*| of the mix [17]. Local asphalt binders modified by 6% of Polyethylene
These curves can be used to estimate the required (PG 82-10) are suitable for weather of 70 °C temperature
amount of polymer (as a percent of binder weight) at given and Very Heavy Traffic conditions, while 6% of Olefin
traffic level (Jnr) and targeted service temperatures. Com- modified asphalts are suitable for Heavy Traffic only at
pared to unmodified asphalt binders, all tested samples in same weather conditions. None of the plastomeric modified
this study showed signs of strain recovery improvement asphalt binders show significant improvement at 76 °C
when tested under high stress and different temperatures. temperature compared to SBS modified asphalts.
Furthermore, a comparison between elastomer (SBS and
CR) and Plastomers (PE and OF) modified samples was
conducted to differentiate the effect of polymer type on 4. Conclusions
the rate of change of Jnr when increasing the temperature.
SBS modified asphalt binders can sustain the change of In this study, the effect of temperature on Non-
Jnr value even at high service temperatures (76 °C) which recoverable creep compliance (Jnr) was investigated on dif-
can resist rutting at Extremely Heavy Traffic E (Jnr < 0.5 ferent polymer modified asphalt binders that have various
kPa1) when adding 6% of SBS (PG 82) and Heavy Traffic performance grades (PG). Regression models that predict
H (1 > Jnr > 2) when 4% of SBS (PG 76) is added to local the Jnr values at any temperature were generated and listed.
asphalt binder. The effect of Crumb Rubber (CR) on It is concluded from this research the followings:
610 K. Al-Adham, H. Al-Abdul Wahhab / International Journal of Pavement Research and Technology 11 (2018) 603–610

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 Power-law models are best describing the relationship hot-mix asphalt to generalized dynamic shear moduli of asphalt
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This work was supported by Deanship of Scientific properties of crumb rubber modified bitumen using classic and SHRP
Research at King Fahd University of Petroleum and Min- testing methods, Constr. Build. Mater. 26 (1) (2012) 481–489.
erals (Grant No. SB141009). The authors would like to [15] Z. Lei, X. Chao, G. Fei, L. Tian-shuai, T. Yi-qiu, Using DSR and
MSCR tests to characterize high temperature performance of different
thank the reviewers of this paper for their comments and rubber modified asphalt, Constr. Build. Mater. 127 (2016) 466–474.
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asphalt binder resistance to permanent deformation based on
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