Chem 28.
1
Special Schedule of Laboratory Activities
Second Semester AY 2019-2020
Date Activity
Check form 5 and Chem 17 grade
Getting to know each other
Course orientation and locker
check-out
Review: significant figures and
reaction stoichiometry
I. Introduction to Analytical
Chemistry Laboratory
A. Ways of expressing
Jan 16 (Th)
concentration
B. Dilution and Aliquot Factors
C. Selecting an analytical
method and sampling
D. Discussion on scientific
writing and the rules on
plagiarism
II. Application of Statistics to
Analytical Chemistry
A. Introduction to statistics
Jan 21 (T)
B. Error propagation
E1. COINS
Prepare crucibles for E2
III. Classical Methods in
Analytical Chemistry
A. Gravimetry
Jan 23 (Th) 1. Introduction to
gravimetric analysis
E2. GRAVIMETRY
Jan 28 (T) E2. GRAVIMETRY
Jan 30 (Th) E2. GRAVIMETRY
Feb 4 (T) E2. GRAVIMETRY
Chem 28.1 Schedule –2nd Semester 2019-2020
Objectives/Learning Outcomes
Things to
At the end of the activity, the
Bring
students should be able to:
• Be oriented about the course and
policies
• Get to know each other
• Check-out lockers
• Review significant figures and
reaction stoichiometry
Form 5;
• List and define different ways of
Index
expressing concentration
cards; 4
• Solve exercises on dilution/aliquot
bluebooks
factors ; lab
• Identify the considerations in materials;
selecting an analytical method
• Differentiate between types of
sampling
• Be familiar with rules on scientific
writing and plagiarism
• Calculate various statistical
parameters of a data set
• Perform various statistical
1-peso or
techniques for a data set
25-
• Apply the formulas for error
centavo
propagation
coins;
• Calculate various statistical forceps
parameters for the weight of coins
• Prepare the crucibles for the next
experiments (E2 & E3)
• Solve practice exercises using
gravimetric factors
• Perform gravimetric analysis of
E1 AtQ
fertilizer sample
• Obtain the constant weight of the
crucible
• Perform gravimetric analysis of
fertilizer sample
Obtain the constant weight of the
fertilizer
• Perform gravimetric analysis of
fertilizer sample
• Calculate the % moisture of the Face
fertilizer sample masks;
• Obtain a filterable precipitate from gloves
the dried fertilizer sample (finish
until digestion step only)
• Perform gravimetric analysis of
fertilizer sample
• Filter and dry the precipitate
• Calculate the % phosphorus for the
sample
Page 1 of 3
 • Perform gravimetric analysis of
fertilizer sample
Feb 6 (Th) E2. GRAVIMETRY • Filter and dry the precipitate
• Calculate the % phosphorus for
the sample
Feb 11 (T)
NO CLASS MEETINGS
Feb 13 (Th)

Titrimetry
1. Review: titrimetric analysis • Recall the principles of
2-L boiled
titrimetric analysis
2. Pre-lab discussion: E3, E4, distilled
• Discuss the principles of double-
Feb 18 (T) E5 indicator, back-, and
water (per
pair);
complexometric titration.
Solution preparation for E3, E4, & E2 Mock
• Prepare solutions for E3, E4, & FR
E5
E5
Consultation for Mock FR

Feb 20 (Th) Post-lab discussion: E1 to E2

Feb 25 (T) QUIZ 1 (E1 TO E2)
• Perform double-indicator titration
method
Feb 27 (Th) E3. SODA ASH • Determine the composition of a
soda ash sample by double-
indicator titration
• Perform back titration method
• Calculate the % acetylsalicylic acid
Mar 3 (T) E4. BACK TITRATION E3 AtQ
(ASA) in an aspirin sample by back
titration
• Perform complexometric titration Mineral
• Determine the water hardness of a water
mineral water sample using EDTA sample
Mar 5 (Th) E5. EDTA TITRATION
titration (Viva);
Qualitatively assess the hardness of E4 AtQ
the sample
Mar 10 (T) Post-lab discussion: E3 to E5 E5 AtQ
1. Pre-lab discussion: E6 and
E7 (principles of
Mar 12 (Th) permanganometry and
• Prepare solutions for E6
iodometry)
Solution preparation for E6
Mar 17 (T) QUIZ 2 (E3 TO E5)
Mar 19 (Th) ACLE (No classes)
• Perform redox titration
Carbon
• Determine the oxalate content of
E6. PERMANGANOMETRY paper/
Mar 24 (T) an oxalate sample using
Aluminum
permanganometry
foil
Mar 25 (Th)
E7. WINKLER TITRATION Prepare solutions for E7 E6 AtQ

Mar 31 (T) E7. WINKLER TITRATION • Perform a modified Winkler Clear glass
titration bottle;
• Perform water sampling Aluminum
• Determine the dissolved oxygen foil; 0.5-
content of a freshwater sample mL
using an iodometric method syringes

Chem 28.1 Schedule –2nd Semester 2019-2020 Page 2 of 3

 • (3 per
pair)

Apr 2 (Th) Post-lab discussion: E6 to E7

Apr 7-10 NO CLASSES

(LENTEN BREAK)

Pre-lab discussion: E8 & E9 • Recall the principles of

Solution preparation for E8 & E9 spectrophotometry. Describe UV- E7 FR
Apr 14 (T) Vis instrumentation. State and
apply Beer’s law.

QUIZ 3 (E6 TO E7) Commented [RTV1]: Ask students if they prefer na sabay
Apr 16 (Th) quiz and FR submission or as is yung sched

Determine the Ka of methyl red using

Apr 21 (T) E9: METHYL RED double-component
spectrophotometry.
Obtain the % purity and Ka of the
E10: POTENTIOMETRIC
Apr 23 (Th) KHP sample using potentiometric E8 AtQ
TITRATION
titration.
E8: Fe-PHENANTHROLINE Obtain the calibration curve for the
Fe-phen complex. Perform analysis
Apr 28 (T) E9 AtQ
of unknown Fe sample using UV-Vis
spectrophotometry.
Post-lab discussion: E8 to E10 E10 AtQ
Apr 30 (Th)
QUIZ (E8 to E10)
May 5 (T)
May 7 (Th) Locker Check-in
May 11
PRACTICAL EXAM (1-3)
(M)

Dates to Remember:
• Deadline of dropping: Apr 13 (M)
• Deadline for filing LOA: Apr 28 (T)
• End of classes: May 13 (W)

Chem 28.1 Schedule –2nd Semester 2019-2020 Page 3 of 3