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COMPOSITES

SCIENCE AND
TECHNOLOGY
Composites Science and Technology 65 (2005) 1022–1031
www.elsevier.com/locate/compscitech

Bearing strength and failure behavior of bolted composite joints


(part I: Experimental investigation)
Yi Xiao *, Takashi Ishikawa
Advanced Composites Evaluation Technology Center, Japan Aerospace Exploration Agency (JAXA), 6-13-1, Osawa,
Mitaka-shi, Tokyo 181-0015, Japan

Received 27 January 2004; received in revised form 31 January 2005; accepted 14 February 2005
Available online 19 April 2005

Abstract

The experimental investigations described in this paper were conducted in order to study the strength and failure of mechanically
fastened composite joints. Two different types of polymer–matrix-based Carbon Fiber Reinforced Plastic laminates were selected to
evaluate the effect of resin properties on bearing response. A special measurement system using a non-contact electro–optical exten-
someter to measure hole elongation is proposed. During static tensile testing, the response of bearing damage was monitored by
acoustic emission measurement. Several specimens were observed by means of soft X-ray radiography and SEM at different loading
levels to assess internal damage. The observations indicate that the bearing failure can be outlined as a process of compressive dam-
age accumulation, and can be divided into the following four stages: damage onset; damage growth; local fracture; structural frac-
ture. Major features of bearing failure include fiber micro-buckling, matrix cracking, delamination and out-of-plane shear cracking.
Bearing strength and failure mode should also depend on the lateral constraints and the ‘‘toughness’’ of different polymer–matrix
based laminates.
Ó 2005 Elsevier Ltd. All rights reserved.

Keywords: Composite materials; Bearing strength; Failure mechanisms; Non-destructive testing; Mechanically fastened joint

1. Introduction lems of bolt bending and hole elongation under com-


pressive loading. Several significant research papers [1–
As is well known, degradation and failure of aircraft 4] on fastener joints have been published, examining
structures frequently initiate at the joints; therefore, ade- the dependence on specimen geometry and fiber orienta-
quacy of joint design exerts strong influence on safety, tion. In summary, the joints would be expected to even-
durability and reliability. Next-generation mega-carrier tually fail in a variety of modes; namely, net-tension,
aircraft or supersonic transport (SST) aircraft will make shearing-out, and bearing. In terms of structural design,
extensive use of advanced composite materials in both bearing failure preferably occurs as a combination of
primary and secondary structures, and are likely to use these three modes, in view of stability of the failure pro-
mechanically fastened joints. cess. However, bearing failure is a local compressive fail-
Mechanically fastened joints have generally been ure mode due to contact and frictional forces acting on
used for highly loaded composite components, although the surface of the hole [5]. This fracture process is very
the low bearing stiffness of composites can lead to prob- complicated and is influenced by many parameters,
including washer dimension and lateral clamping force
*
Corresponding author. Tel.: +81 422 40 3000x5433; fax: +81 422
[6–10].
40 3599. Crews [6] conducted static and fatigue tests under
E-mail address: xiaoyi@chofu.jaxa.jp (Y. Xiao). bolt-bearing loads for a range of bolt clamp-up

0266-3538/$ - see front matter Ó 2005 Elsevier Ltd. All rights reserved.
doi:10.1016/j.compscitech.2005.02.011
Y. Xiao, T. Ishikawa / Composites Science and Technology 65 (2005) 1022–1031 1023

torques. He reported that bolt clamp-up force exerts a before the bearing test, which revealed no internal de-
significant effect on both static strength and fatigue fects in the materials attributable to the manufacturing
limit. Eriksson [7] has shown that bearing strength is process. Although, the manufacturing method and pro-
influenced by several important parameters, including cesses have profound effects on the final properties of
lateral constraint conditions and ply orientations. composite materials owing to their effect on the micro-
Wang et al. [8] used bearing response and bearing structure and internal stresses, this paper is not primar-
strength of bolted joints to examine the bearing failure ily concerned with this problem. For reference, the
mechanism as a function of clamping pressure. In basic data of the two composite systems are listed in
their work, a pin-loaded bearing (without lateral Table 1.
clamping) test and a bolted bearing (with lateral Fig. 1 shows the geometrical configuration and test-
clamping) test were conducted to evaluate the bearing ing setup of the double lap joint specimens. The double
damage. Wu and Sun [9] investigated the behavior of lap joining configuration was adopted; the bolt fastener
pin-contact failure of composite laminates and found was attached to the Carbon Fiber Reinforced Plastic
that fiber micro-buckling in the 0-deg plies of the lam- (CFRP) specimen with a chromium molybdenum steel
inate plays an important role in the initiation of bear-
ing damage. Camanho et al. [10] carried out a detailed
Table 1
experimental investigation for three basic failure
Summary of the two composite systems (reference data)
modes of a joint, and their results show that the main
IM-7/ IM600/
mechanism of bearing failure is accumulated delami-
PIXA Q133
nation damage. As the above literature survey indi-
Mechanical properties of unidirectional lamina
cates, the damage phenomena of bearing failure in a
Longitudinal modulus (GPa) 152.4 148.3
bolted composite joint are very complicated. One rea- Transverse modulus (GPa) 8.06 8.1
son for such complication can be ascribed to out-of- Longitudinal tensile strength (MPa) 2293 2700
plane compressive deformation in the vicinity of the Longitudinal compression strength (MPa) 948.2 1037
hole. In other words, fiber micro-buckling, matrix Transverse tensile strength (MPa) 66.2 63.7
Transverse compression strength (MPa) 210 235
cracks, delamination, and other forms of damage fre-
DCB fracture toughness (J/m2) 1400 336.8
quently serve as the 3D failure mode under compres-
sive load in laminated composites. Therefore, an Manufacturing process Hot Autoclave
pressing
understanding of the occurrence and progress of the Temperature (°C) 380 180
microscopic damage is indispensable to the evaluation Fiber volume fractions (%) 56 55
of the parameters of damage tolerance in structural
design.
The primary objectives of this study are to: (a) offer
the basic data for design and strength prediction of
bolted composite joints; (b) clarify the relationship
between bearing strength and damage behavior; (c) eval-
uate the effect of ‘‘toughness’’ of different polymer–
matrix-based laminates on the failure mechanism; (d)
verify the validity of the proposed measurement system
for characterizing bearing strength.

2. Experimental details [11]

2.1. Material and specimen preparation

Two material systems were selected for comparison


of bearing strength in the present work: IM-7/PIXA
graphite–polyimide composite from Mitsui Chemicals
Co. Ltd. [12], and IM600/Q133 toughened graphite–
epoxy from Toho Rayon Co. Ltd. [13]. These com-
posites are 16-layer quasi-isotropic [45/0/-45/90]2S
laminates of identical stacking sequence and unidirec-
tional prepreg, fabricated by hot pressing for IM-7/
PIXA and by autoclave for IM600/Q133. Some speci- Fig. 1. Geometrical configuration and testing setup of bolted joint
mens were subjected to ultrasonic C-scan detection specimens.
1024 Y. Xiao, T. Ishikawa / Composites Science and Technology 65 (2005) 1022–1031

fixture. Tightening torque was adjusted at 12–13 link the two side edges of the specimen with the pinhead
kgf/cm1 by means of a mini-torque wrench. All speci- must be installed [15,16], making fixture design very dif-
mens were made with the same width-to-diameter ratio ficult. In the present method, pin relative displacement
of W/d = 8, edge-distance-to-diameter ratio of e/d = 3, can be measured by merely bonding the black-and-white
and specimen length of 110 mm. Average thickness of target.
the specimen was 2.24 ± 0.03 mm for the IM-7/PIXA Testing was conducted by means of an INSTRON-
composite and 2.30 ± 0.03 mm for the IM600/Q133 8501 machine in tensile mode. Cross-head speed was
composite. 1.0 mm/min. During static tests, load–displacement re-
sponse and acoustic emission (AE) were recorded in or-
2.2. Experimental procedures der to examine the failure process of joint specimens. A
two-channel MISTRAS 2001 system (Physical and
In order to measure hole elongation for the bolted Acoustic Co.) was used in the AE measurement. The
joint specimen, a simple and highly functional measure- employed sensor is a resonant frequency type of
ment system was developed, featuring a non-contact 150 kHz (PAC R15I) and has a threshold of 55 dB.
electro–optical extensometer (product of ZIMMER Some specimens were unloaded at different loading lev-
Co., MODEL-100B). This system does not require spe- els, and damage behavior was observed by soft X-ray
cial fixtures, and has been proposed as a practical test radiography and scanning electron microscopy (SEM).
method [14]. In this study, this technique was also
adopted to evaluate the bearing strength of the bolted
composite joints. System configuration is illustrated in 3. Results and discussion
Fig. 2. The ZIMMER electro–optical extensometer is
able to convert in-plane movement of a black-and-white 3.1. Bearing strength
edge (called a target) into a voltage proportional to its
displacement. In other words, the optical image of the Fig. 3 shows typical load–displacement curves (P–d
target is converted into an electronic signal by means curve) of IM-7/PIXA and IM600/Q133 specimens.
of a special photo cathode. In the conventional measur- Bearing strength is defined as the bearing load at which
ing method by contact form, metal fittings (yokes) that the pin relative displacement is deformed to 4% the pin
diameter (4%d), and the maximum load; i.e., bearing
strength, is expressed as S 4%db ¼ P 4%d =d  t and S Ult
b ¼
P max =d  t. Table 2 provides a summary of the experi-
mental data for bearing strength obtained from all spec-
imens. Note that more data were obtained for the IM-7/
PIXA specimens than for the IM600/Q133 specimens,
because such data include the data for preliminary test-
ing. As shown in the table, as compared with the IM600/
Q133 specimens, the IM-7/PIXA specimens show

Fig. 2. Schematic for measurement system using a non-contact Fig. 3. Typical load–displacement curves for IM-7/PIXA and IM600/
electro–optical extensometer. Q133 specimens.
Y. Xiao, T. Ishikawa / Composites Science and Technology 65 (2005) 1022–1031 1025

Table 2
Bearing strength obtained in bolted composite joint tests
Specimens 4% d Bearing Ultimate bearing Failure mode
strengths (MPa) strengths (MPa)
IM-7/PIXA
IP-01 727.7 1289.1 Bearing
IP-02 842.4 1326.0 Bearing
IP-03 835.1 1314.2 Bearing
IP-04 906.6 1381.1 Bearing
IP-05 853.5 1357.1 Bearing
Average 835 1326
IM600/Q133
IQ-01 809.67 1486.72 Bearing
IQ-02 825.62 1491.74 Bearing
IQ-03 796.46 1473.45 Bearing
Average 808 1485

Table 3
Comparison in ultimate strength of IM-7/PIXA and IM600/Q133,
tested in compression for various specimens
Ultimate strength (MPa) IM-7/PIXA IM600/Q133
Bearing strengths 1326 1485
Unnotched compressive strengths 552 640
Open hole compressive strengths 332.6 *549.2
Lay-up: [+45/0/45/90]2s (16ply); * = 32ply.

similar average bearing strength at 4%d, but lower ulti-


mate failure strength.
Table 3 compares experiment results on bearing Fig. 4. Comparison of load response and AE counts vs. time for IM-7/
strength and compressive strength for two composites PIXA and IM600/Q133 specimens.
of similar stacking sequence. Compressive strength was
tested by means of a laminate specimen without a hole increased to 2 kN, a noise on the AE signal was ob-
and with an open hole. As compared with IM-7/PIXA served in IM-7/PIXA, but AE change was gradual in
composites, IM600/Q133 composites have higher failure the case of IM600/Q133. This noise seems to be the ef-
strength in all tests. The cause can be ascribed to the ef- fect of frictional force between the surface of the washer
fect of resin properties and interface bond strength, if and the CFRP specimen. Afterwards, the load increased
the difference in fiber volume fraction (see Table 1) is almost linearly with time. However, when the applied
disregarded. Because PIXA resin has lower YoungÕs load approached the Knee point (about 10 kN), a sharp
modulus (2.84 GPa), which is only about 60% of Epoxy change in the AE signal record was observed. Simulta-
(Q133) [12], resistance to fiber buckling will be lower neously, significant non-linear behavior appeared in
and may lead to a significant reduction in compressive the load–displacement curve. Following this behavior,
strength. Also, the failure mode is particularly sensitive load response gradually decreased. Furthermore, as
to differences in resin properties. These findings can be can be clearly seen from the AE signal, such progressive
understood from the SEM photograph shown in Section behavior appeared stage-by-stage. This finding can be
3.2.3. considered to correspond to fiber micro-buckling, ma-
trix cracking, and delamination, together with out-of-
3.2. Bearing failure mechanisms plane shear cracking.
Fig. 5 shows AE amplitude distributions of each spec-
3.2.1. AE measurement imen in two higher loading stages. For comparison, the
In order to examine internal damage accumulation data of two materials are shown with piling-up plots.
during the loading process, damage in the joint speci- Within load levels of 10–12 and 12–15 kN, AE signals
mens was monitored by AE measurement; the results of low or middle amplitude less than 80 dB were logged
are shown in Figs. 4–6. Fig. 4 shows the response of for the case of IM-7/PIXA, whereas high amplitudes
loads and AE counts versus testing time in IM-7/PIXA greater than 90 dB dominated in the case of IM600/
and IM600/Q133 specimens. When the applied load was Q133. Observations of the SEM photograph shown in
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of high amplitude correspond to delamination or out-


of-plane shear cracking.
In order to compare the damage accumulation pro-
cesses in the two composites, an accumulated AE event
is assumed to be a measure for representing the relative
extent of damage, as shown in Fig. 6. Here, the relative
accumulated AE event of the IM600/Q133 specimen un-
der the maximum load is taken as 100%, and used as the
basis for normalizing the IM-7/PIXA specimen signals.
Variations in the accumulated AE events can be divided
into the following four stages: damage onset, damage
growth, local fracture and structural fracture. In the
damage onset stage, the two specimens provide AE sig-
nals of almost the same level. In the damage growth
stage, total progressive AE events were detected with
similar frequency in the two specimens, and no remark-
able difference could be recognized until the local frac-
ture stage. Because the clamping pressure of the
washer strongly suppresses out-of-plane deformation
in the CFRP specimens, internal damage was accumu-
lated mainly in the manner of in-plane deformation,
and therefore, almost no difference could be detected.
When the applied load increased to the stage of local
fracture, progressive differences were found in the accu-
mulated AE event curves. This finding is essential evi-
dence for the differences in damage mechanisms
estimated from SEM observations presented later. The
IM600/Q133 specimen shows a rather brittle fracture,
whereas the IM-7/PIXA specimen shows a rather ductile
fracture. Therefore, the accumulated AE events led to a
lower value in IM-7/PIXA than in IM600/Q133. At the
final stage, structural fracture, the two composites
Fig. 5. AE counts vs. amplitudes for two specimens, load range: showed a difference in accumulated AE events of about
(a) 10–12 kN; (b) 12–15 kN.
20%.
Section 3.2.3 suggest the following hypothesis: the AE
3.2.2. X-ray radiography
signals of low or middle amplitude correspond to fiber
Some of the specimens were unloaded after loading to
micro-buckling or matrix cracking, and the AE signals
the setting levels, and then X-ray photographs were ta-
ken. The load levels were defined as 50%, 60%, 75%
and 100% of the maximum load, and are referred to as
Stage 1, Stage 2, Stage 3, and Stage Ult., respectively.
Fig. 7 shows X-ray radiography results for bearing dam-
age under the above four loading stages. Micro-damage
such as fiber micro-buckling and matrix cracks starts to
occur at Stage 1, prior to reaching the P4%D load; this
agrees well with the early AE signals. These damages
had little effect on the response in the load–displacement
curves. Slight local delamination could also be seen in
IM600/Q133 specimens. Meanwhile, in the IM-7/PIXA
specimens, rather than delamination, matrix cracks of
the equivalent length were observed in 45- or 90-deg
plies. When the load was increased to 60% and 75%
the failure load, the regions of micro-damage became
more extensive around the hole, and significant non-lin-
Fig. 6. Accumulated AE events for two specimens: IM-7/PIXA and ear behavior appeared in the load–displacement curve.
IM600/Q133. Both composites exhibited these trends until final
Y. Xiao, T. Ishikawa / Composites Science and Technology 65 (2005) 1022–1031 1027

fracture; damage extent in the IM600/Q133 specimens is the load level of 60%; i.e., near the Knee points, as
relatively serious. shown in Fig. 8(a) and (b). Since they easily develop into
the surrounding plies, they seem to cause shear cracks
3.2.3. SEM photographs and delaminations in ±45-plies. In this stage of loading,
In order to observe the internal damage in detail, some the fiber kink bands in 0-plies observed in Fig. 8(a) are
specimens were cut along the centerline after the X-ray serious in IM-7/PIXA, whereas not only the kink band,
radiography tests described in the previous section. but also local delamination appeared in IM600/Q133 as
SEM micrograph images were taken in the through- indicated in Fig. 8(b).
thickness sections of the specimen; the images are shown When the load is increased to the first peak point
in Figs. 8–10, tested at loading levels of 60%, 75%, and (75%), distinct through-thickness shear cracks expand,
100%, respectively. The features of damage behavior as shown in Fig. 9(a) and (b). According to the assumed
can be examined well by dividing failure process into mechanism for forming through-thickness shear cracks,
three geometrical regions, as follows: (1) cushing damage the fiber kink bands in 0-plies develop to the surround-
at the contact surface; (2) damage at the region inside the ing ±45-plies and induce shear cracks and delamination.
washer (inside-washer region); (3) damage at the region Subsequently, these damages couple with each other.
outside the washer (outside-washer region). The growth of shear cracks in IM-7/PIXA is more
The main damage phenomenon in region (1) is crush- remarkable on the outside surface plies of the laminate
ing or surface damage occurring in the contact region than in internal plies, whereas the damage extent in
between the bolt and hole. The central photographs in IM600/Q133 is more serious in the whole sections than
Figs. 8 and 9 clearly show that the main damage pat- in IM-7/PIXA. As described previously in Section 3.2.1,
terns are fiber compressive failures involving fiber mi- through-thickness shear cracks may correspond to the
cro-buckling, and delamination induced from these AE signal of high amplitude.
failures. Especially, this crushing damage is remarkable The damage occurring in region (3) shows that once
on the surface of the specimens (see the left photograph the bearing load exceeds the first peak point where bear-
of Fig. 8(a),1). The reaction force acting on the hole sur- ing damage in the inside-washer region gradually
face could be increased as a result of bending deforma- reaches the saturation state, large-scale delaminations
tion of the bolt. However, as stated below, the crushing and shear cracks begin to be formed in the outside-
damage is not considered to be the main failure mode washer region (see Fig. 9(a) and (b)). This may corre-
among the overall bearing failure processes. spond with the abrupt decrease in load response shown
The main phenomenon of damage in region (2) is in the P–d curve (see Fig. 2, near the first peak point).
compressive damage accumulated in the inside-washer Fig. 10 shows the damage states at maximum load.
region. Some kink bands in 0-plies can be observed at The damage progress is found to be an intermittently

Fig. 7. X-ray radiographs of bearing damage, tested at four load levels.


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Fig. 8. SEM photographs of through-thickness bearing damage, tested at 60% of maximum load (note: middle photo is general view, side photos are
close-up views of marked areas).

accumulated process by multiple through-thickness (a) Damage occurring on the contact surface between
shear cracks. Such damages are thought to spread rap- the bolt and hole is crushing damage. Although,
idly around the circular hole if no restraint is provided this surface damage is remarkable, it does not
for out-of-plane deformation. Comparison of the two become a leading phenomenon in the overall pro-
materials shows that large-scale delamination and shear gress of bearing failure.
cracks are observed up to the specimen end in IM600/ (b) Damage in the inside-washer region can be charac-
Q133. terized by damage accumulation processes such as
fiber kink bands of 0-plies, which induce shear
3.2.4. Description of damage progress cracks and delamination in the surrounding ±45-
On the basis of the above SEM photograph observa- plies. Since out-of-plane deformation of the lami-
tions and other information, Fig. 11 shows a schematic nate is suppressed by clamping pressure provided
description of the damage progress patterns in each re- by the washers, compressive damage expands
gion. Features of the process of progressive damage mainly along the in-plane direction in a stage-by-
can be summarized as follows: stage manner.
Y. Xiao, T. Ishikawa / Composites Science and Technology 65 (2005) 1022–1031 1029

Fig. 9. SEM photographs of through-thickness bearing damage, tested at 75% of maximum load.

(c) After the damage in the inside-washer region grad- tion in load response appearing in the P–d curve as non-
ually reaches saturation, damage such as large- linear behavior can be explained by only one of the pres-
scale delamination occurs under the washer area, ent observations for various damage modes, such as the
leading to a rapid decrease in joint response. fiber kink bands of 0-plies, shear cracks, delamination,
or their interactions. Notably, from the present SEM
The present experimental investigations clarify the observation, multiple load reduction points appearing
very complicated bearing failure processes in the bolted on the P–d curve can be ascribed to through-thickness
composite joints, whereas the P–d curve alone does not shear cracks occurring and progressing intermittently.
give much information. In other words, the slight reduc- Damage coupling in each ply constitutes the major
1030 Y. Xiao, T. Ishikawa / Composites Science and Technology 65 (2005) 1022–1031

Fig. 10. SEM photographs of through-thickness bearing damage, tested at 100% of maximum load.

Crushing
damage
Contact
surface

(a)

Washer -- Washer --

Loss of
washer
support
Fixture --

(b) (c)

Fig. 11. Schematic descriptions of the bearing failure mechanisms: (a) crushing damage; (b) damage within lateral constraint (inside-washer region);
(c) damage without lateral constraint (outside-washer region).

failure modes of the shear cracks. The washer and bolt ment curve, AE characteristics, and failure mechanism
clamping forces may play important roles in the growth were examined. Correlations between the damage pat-
of shear cracks. Detailed investigation of this factor re- tern and its progress were partially described by the
mains a subject of future work. AE signal activities. Furthermore, X-ray radiography
and SEM photographs provided basic explanations of
the bearing failure mechanisms. Thus, the following
4. Conclusions are concluded:

In this study, a detailed experimental investigation 1. Bearing failure occurs by a process of damage accu-
was performed to evaluate the bearing strength and mulation. The accumulation process can be macro-
damage behavior of mechanically fastened joints of scopically divided into four stages: damage onset,
two composite systems (IM-7/PIXA and IM600/ damage growth, local fracture and final structural
Q133). The relationships between the load–displace- fracture.
Y. Xiao, T. Ishikawa / Composites Science and Technology 65 (2005) 1022–1031 1031

2. The kink band in 0- plies and delamination appears 749. American Society for Testing and Materials; 1981. p.
to be the dominant mode in the onset of damage. 131–44.
[7] Eriksson I. On the bearing strength of bolted graphite/epoxy
Through-thickness shear cracks and the large-scale laminates. J Compos Mater 1990;24:1264–9.
delamination are the major cause of final fracture. [8] Wang HS, Hung CL, Chang FK. Bearing failure of bolted
3. Toughness exerts remarkable influence on control of composite joints. Part I: experiments. J Compos Mater
the damage mechanism. The epoxy–matrix-based 1996;30(12):1284–313.
laminate is more vulnerable to matrix cracking and [9] Wu PS, Sun CT. Bearing failure in pin contact of composite
laminates. AIAA J 1998;36(11):2124–9.
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