1. No signal output to external
Refer to operation and refer-
data handling device (Le.,
integrator, etc.).
2. Strange chromatograph out-
put. Test chromatogram is
ok.
3. Strange chromatograph out-
put. Test chromatogram is
not ok.
4. Instrument has two detec-
tors installed but only rec-
ognizes one.
5. FID will not ignite.
a. Improper keyboard or exter- 1.
nal device operation, or im- ence manuals as well as
proper cabling. the manuals for the external
device.
a. Faulty detector PCB. 1. Replace detector PCB.
2. If problem persists, install
original detector PCB and
refer to probable cause b.
b. Faulty main PCB. 1. Replace main PCB.
a. Faulty signal cable. 1. Disconnect signal cable
and run the instrument self-
test.
2. If "FAULT: DAC 1 TEST" is
indicated, suspect faUlty
main PCB. Otherwise, sus-
pect a faulty cable or exter-
nal device.
a. FaUlty detector PCB. 1. Swap detector PCBs.
2. If problem persists, swap
back original detector PCBs
to starting configuration and
refer to probable cause b.
3. If problem follows the
swapped PCB, replace the
suspect PCB with a known
good PCB.
b. FaUlty main PCB. 1. Replace main PCB.
a. Improper operation. 1. Refer to operation and refer-
ence manuals to ensure
that proper type, quality,
and flow of gases are being
used.
b. FaUlty ignitor switch on flow 1. Replace ignitor switch on
manifold. flow manifold (refer to Sec-
tion 3 of this document).
c. FaUlty ignitor. 1. Replace ignitor (refer to
Section 4 of this document).
THERMAL CONDUCTIVITY DETECTOR (TCD)
The main portion of the TCD detector is a heated block into which a heater cartridge and two sensor car-
tridges are installed. In addition to the standard heater and sensor cartridges, a second sensor cartridge
(referred to as the delta-t cartridge) is employed which is connected to the TCD detector PCB. If the de-
tector requires replacement, the entire assembly is replaced as a unit.

WARNING

HAZARDOUS VOLTAGES ARE PRESENT IN THE INSTRUMENT WHEN THE POWER

CORD IS CONNECTED. AVOID A POTENTIALLY DANGEROUS SHOCK HAZARD BY
DISCONNECTING THE POWER CORD BEFORE WORKING ON THE INSTRUMENT.
1. Set the main power line switch to the off position.
~~uuuuuuu

4. When the heated zones are cool, turn off all gas
supplies.
,,
5. At the bottom of the detector(s) to be removed, ,
inside the column oven, remove the column and ,,
hardware associated with the detector(s) (liner,
column/liner nuts, ferrules, makeup gas adapt-
er,etc.).

6. If the detector is not going to be replaced with a

new detector, cap the detector base.
7. Lift the hinged top cover at its front edge,

9. If the detector is not going to be replaced with a

new detector, cap the TCD vent port on the top of
the detector. (This will not be required on a se-
ries connected TCD.)
10. Remove the electronics carrier top cover
(above the signal cable plugs and receptacles
to expose the top edge of the TCD detector
PCB).

ELECTRONICS
CARRIER TOP
COVER

11. Disconnect the detector filament and delta-t

temperature sensor leads at their connector
block on the detector PCB. Use a small flat-
blade screwdriver to press each wire lead
release (located adjacent to each connection). STRIPPED END
OFTCD
12. Remove the preformed thermal insulation from FILAMENT LEAD
around the detector to expose the two screws
securing the detector to the instrument main-
frame.

13. On a series-connected TCD, disconnect the TCD

to FID jumper tube from the TCD oven-retum ex-
haust vent port.

14. Remove the two screws securing the detector to

the instrument and then lift the block up enough
to expose the heater and sensor cartridge wires.

15. Carefully slide the three cartridges out of the

block. The two smaller cartridges are the sen-
sors and must be handled gently in order to pre-
vent breakage.

16. Trace the reference gas inlet tubes attached to the base of the detector to their connections at the
TCD solenoid valve. Observe the location on the solenoid valve where each tube is connected.
 I CAUTION I
Use caution when removing and Installing the plastic M8 tubing nuts. Excessive force
can damage them.
17. Disconnect the tubes from the solenoid valve by loosening the plastic fittings securing them. (fhe
fittings should only be finger-tight. If more force is required to loosen them, use a small pair of
pliers to free the fittings.) Note the solenoid valve fitting where each tube is attached. (Corre-
sponding tubes on the new detector must be connected to the same fittings.)

18. If a new detector is being installed, prepare the replacement detector block by pre-bending its
tubes until they are oriented similarly to those on the detector just removed.

19. If a new detector is being installed, ensure that the base and vent port of the new detector are
capped to prevent contamination.

20. Install the heater, temperature sensor, and delta-t sensor cartridges into the heated block.

21. Carefully install the detector, securing it to the instrument with two screws.

I CAUTION I
When Installing tUbing at the solenoid valve,
ensure that all O-rings are positioned properly.
NOTE
When Installing a series-connected TCD, make
sure Its oven-return exhaust vent tube extends
Into the oven.
22. Connect and tighten tUbing from the detector to
the solenoid switching valve, finger-tight. En-
sure that the tUbing is installed at their
proper fittings on the TCD solenoid valve.
23. Connect the TCD filament and "delta- T" temper-
FIlAMENT GAS
ature sensor leads at the connector block on the LEADS TYPE
detector PCB, making sure the filament leads are DELTA-T
connected properly per the illustration at the SENSOR • N2, Ar
right. LEADS He, H2 •
24. Restore supply pressure and check for leakage
at all installed fittings.

26. Remove the caps from the detector base and the
vent port.

I CAUTION I
When Installing Insulation, use care not to plug the vent port. If flow Is Interrupted while
the TCD Is on, It will shorten Its life dramatically.
27. Taking care not to block the vent port, install insulation around the detector block.
28. Install the electronics carrier top cover.

I CAUTION I
Use caution not to crimp the filament and delta-t sensor leads when Installing the TCD
detector cover.
29. Install the TCD detector cover and secure using
two screws.

30. Install column and any other hardware removed

in step 5 of this procedure.

33. Run a TCD Test Sample Chromatogram (refer to

HP 5890 Series II Reference Manual) to ensure
that the system is operating properly. (If re-
versed peaks are experienced, the most likely
cause is reversed gas tubes connected to the
TCD solenoid valve.)
 WARNING

HAZARDOUS VOLTAGES ARE PRESENT IN THE INSTRUMENT WHEN THE POWER

CORD IS CONNECTED. AVOID A POTENTIALLY DANGEROUS SHOCK HAZARD BY
DISCONNECTING THE POWER CORD BEFORE WORKING ON THE INSTRUMENT.
1. Set the main power line switch to the off position.

~~uuuuuuu

4. When the heated zones are cool, turn off all gas
supplies.
,,
,
,,
5. Lift the hinged top cover at its front edge,
exposing the detector area.
TOP COVER

6. Remove the electronics carrier top cover

(above the signal cable plugs and receptacles
to expose the top edge of the
TCD detector PCB).
~
7. Remove the right side panel by
removing four screws: two each ~ 'SCREWS
along its top and bottom edges.
RIGHT SIDE
8. Locate the solenoid valve to PANEL
ELECTRONICS
be replaced. CARRIER TOP
COVER
9. Trace the electrical leads from the solenoid valve
to the ':.124"connector on the TCD detector PCB
(lower right edge).

10. Disconnect the lead connector from its recep-

tacle (J24) on the detector PCB by pulling it
straight out.

11. Note the solenoid valve fitting where each tube

is attached to ensure that the new valve will be
connected correctly.

t CAUTION t
Use caution when removing and Installing the
plastic M8 tUbing nuts. Excessive force can
damage them.
12. Disconnect the tubes from the solenoid valve by loosening the plastic fittings securing them. (The
fittings should only be finger-tight. If more force is required to loosen them, use a small pair of
pliers to free the fittings.) Note the solenoid valve fitting where each tube is attached. (Corre-
sponding tubes on the new detector must be connected to the same fittings.)

13. Remove the solenoid valve and bracket, as a

unit, by removing the two screws securing the
solenoid valve bracket to the instrument.

14. Remove the solenoid valve body from the brack-

et by removing the two screws securing it to the
mounting bracket.

15. Route the leads for the new solenoid valve along
the same path as the leads of the solenoid valve
just removed.

16. Insert the connector for the leads of the new so-
lenoid valve into receptacle J24 by pressing it
straight in until it bottoms.
9. Trace the electrical leads from the solenoid valve
to the '~24" connector on the TCD detector PCB
(lower right edge).

10. Disconnect the lead connector from its recep-

tacle (J24) on the detector PCB by pUlling it
straight out.

11. Note the solenoid valve fitting where each tube

is attached to ensure that the new valve will be
connected correctly.

J CAUTION I
Use caution when removing and Installing the
plastic M8 tUbing nuts. Excessive force can
damage them.
12. Disconnect the tubes from the solenoid valve by loosening the plastic fittings securing them. (The
fittings should only be finger-tight. If more force is required to loosen them, use a small pair of
pliers to free the fittings.) Note the solenoid valve fitting where each tube is attached. (Corre-
sponding tubes on the new detector must be connected to the same fittings.)

13. Remove the solenoid valve and bracket, as a

unit, by removing the two screws securing the
solenoid valve bracket to the instrument.

14. Remove the solenoid valve body from the brack-

et by removing the two screws securing it to the
mounting bracket.

15. Route the leads for the new solenoid valve along
the same path as the leads of the solenoid valve
just removed.

16. Insert the connector for the leads of the new so-
lenoid valve into receptacle J24 by pressing it
straight in until it bottoms.