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College Physical Experiments: EXP: Adjusting The Prism Spectrometer and Measuring The Refractive Index of Prism
College Physical Experiments: EXP: Adjusting The Prism Spectrometer and Measuring The Refractive Index of Prism
张凯(Kai Zhang)
西安工业大学理学院
School of science, Xi’an Technological University
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
Outline
1 Introduction
2 Experimental objectives
3 Experimental equipments
4 Experimental principle
5 Experimental instrument
6 Experimental procedures
7 Data processing
8 Questions . . . . . . . . . . . . . . . . . . . .
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
1 Introduction
2 Experimental objectives
3 Experimental equipments
4 Experimental principle
5 Experimental instrument
6 Experimental procedures
7 Data processing
8 Questions
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
Introduction
Spectrometer is a broad term often used to describe instruments that measure
a continuous variable of a phenomenon where the spectral components are
somehow mixed.
An optical spectrometer (spectrophotometer, spectrograph or spectroscope)
is an instrument used to measure properties of light over a specific portion of
the electromagnetic spectrum, typically used in spectroscopic analysis to
identify materials.
Spectrometer goniometer are designed for precise determination of angular
position, particularly for the optical spectra applications,
It can be used as a spectroscope for the observation and measurement of
emission and absorption spectra. Other applications include measurement
and determination of optical angles of prisms, thin film characterization
through the measurement of reflection and transmission, Brewster’s angle
spectroscopy etc.
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
1 Introduction
2 Experimental objectives
3 Experimental equipments
4 Experimental principle
5 Experimental instrument
6 Experimental procedures
7 Data processing
8 Questions
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
Objectives
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
1 Introduction
2 Experimental objectives
3 Experimental equipments
4 Experimental principle
5 Experimental instrument
6 Experimental procedures
7 Data processing
8 Questions
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
Equipments
Spectrometer goniometer
Flat glass plate
Prism
Sodium lamp
Levelling-meter
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
1 Introduction
2 Experimental objectives
3 Experimental equipments
4 Experimental principle
5 Experimental instrument
6 Experimental procedures
7 Data processing
8 Questions
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
Index of refraction
A
When a beam of light is transmitted α
P
where the angles are measured from the P’
surface normal and n is the index of B C
refraction of the glass. When a ray of light is refracted
The n is a dimension-less number and is by a prism, the angle between
a measure of how strongly the medium the incoming and outgoing rays
bends light. The n of air is 1. For glass, n is called the angle of deviation δ,
varies from 1.3 to 1.8, depending on the which can be expressed as
type of glass and on the wavelength of
the light. δ = (i1 − i2 ) + (i4 − i3 ) (2)
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
sin i1
Using the relation n = sin i2 , we obtain the relation
α+δmin
sin 2
n= (6)
sin α2
where δmin is the angle of minimum deviation and α is apex angle of prism.
The prisms that we will use all have α = 60◦ (exactly, we assume).
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
1 Introduction
2 Experimental objectives
3 Experimental equipments
4 Experimental principle
5 Experimental instrument
6 Experimental procedures
7 Data processing
8 Questions
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– Align the telescope so that the vertical cross-hair coincides
Introduction
with one of Objectives Equipments
the outer spectral Theory
lines (in this measurement Instrument Procedures Processing Questions
Complete
–
experiment setup
Turn the graduated circle (f7) to the 08 and 1808 lines of the
verniers (f5) and lock the graduated circle using the corre-
sponding arresting screws (f2).
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
1 Introduction
2 Experimental objectives
3 Experimental equipments
4 Experimental principle
5 Experimental instrument
6 Experimental procedures
7 Data processing
8 Questions
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
additionally usable:
The slit and the prism surfaces must
1 Spectral lamp Ne, pin contact . . . . . . .
be
451 011
1 Spectral lamp Hg/Cd, pin contact . . . . . 451 071
aligned parallel to the rotary axis of451
1 Spectral lamp Ti, pin contact . . . . . . . .
the
081
1 Spectral lamp Na, pin contact . . . . . . . 451 111
telescope.
Some of the adjustment steps, as well as the Fig. 2 Spectrometer
a Telescope
measurements
Adjustingof line
the spectra, are more easily
spectrometer
b Adjusting screw for laterally displacing the collimator
c Prism table
d Adjusting screw for laterally displacing the telescope
carried out when
In order theprecise
to conduct
be carefully adjusted.
room is darkened
measurements, the apparatus must
e Collimator
f Spectrometer base unit
somewhat.
The slit and the crosshairs must be positioned exactly in the
focal plane of the respective objective lens (telescopic beam
path).
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The slit and the prism surfaces must be aligned parallel to the . . . . . . . . . . . . . . . . . . . .
rotary axis
K. Zhang of the telescope.
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
Preliminary
P5.7.1.1 adjustment (see Fig. 2) LD Physics Leaflets
The inclination of (c) can be varied only to a
limited extent. To ensure that enough play is
Apparatus
1 Spectrometer and goniometer . . . . . . . 467 23
left for adjustment, align (c) as horizontally as
1 Spectral lamp He, pin contact . . . . . . . 451 031
possible (by eye)lamp
1 Spectral during this step.
Cd, pin contact . . . . . . . 451 041
1 Housing for spectral lamps with pin contact 451 16
1 Universal choke, 230 V, 50 Hz . . . . . . . 451 30
Align (a), (c) and (e) horizontally by eye.
1 Transformer, 6 V AC, 12 V AC . . . . . . . 562 73
1 Stand base, small, V-shape . . . . . . . . 300 02
Center (a) and (e) using (b), (d) and then
additionally usable:
screw them tight. Do not loosen (b), (d)
1 Spectral lamp Ne, pin contact . . . . . . . 451 011
too much on
1 Spectral one
lamp Hg/Cd,side, as these
pin contact . . . . support
.
1 Spectral lamp Ti, pin contact . . . . . . . .
451 071
451 081
1 Spectral lamp Na, pin contact . . . . . . . 451 111
(a) and (e).
Fig 2’ Prism table Fig. 2 Spectrometer
c23
c2 Leveling screws a Telescope
for prism table b Adjusting screw for laterally displacing the collimator
Adjusting the spectrometer c Prism table
i Levelling-meter d Adjusting screw for laterally displacing the telescope
In
i1 order to conduct precise measurements, the apparatus must
be carefully adjusted.
i
i1 Level bubble e Collimator
f Spectrometer base unit
The slit and the crosshairs must be positioned exactly in the
focal plane of the respective objective lens (telescopic beam
c22
path).
c21
Put i on c (see Fig 2’), screw c2
i’
The slit and the prism surfaces must be aligned parallel to the
rotary axis of the telescope.
to make
.
c horizontal.
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Some of the adjustment steps, as well as the measurements of
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
prism table
. .at an
. angle
. . . .of .458
. .to. the
. .collimator
. . . . (e) so
. that
. .
K. Zhang (XATU) Physical Experiments the (imaginary) line between two of the adjusting
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– Place the flat glass plate in its holder (g) in the center of the – Set the slit
. .to a
. suitable,
. . . . observable
. . . . . . slit
. . height
. . using
. .the
.
K. Zhang (XATU)
prism Physical
table at an angle of 458 to the collimator (e) Experiments
so that slide (e5). September 20, 2019 19 / 32
Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
Repeat the following two steps until the horizontal crosshair and its mirror
image coincide on both sides of the flat glass plate:
Turn the telescope 180◦ as shown in Fig. 4 so that the cross-hairs are reflected on
the opposite side of the flat glass plate.
Check whether the cross-hair and its mirror image coincide. If not, correct half
the difference using the height-adjustment screw of the telescope (a6) (see Fig. 3)
and the other half using the leveling screw (c1) of the prism table, as described
above.
Secure the height-adjustment screw of the telescope (a6) using a lock nut.
Remove the flat glass plate with holder from the prism table.
Disconnect the illumination source from its voltage supply.
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using the micrometer screw for slit width (e1).
e – Set the
Introduction slit toObjectives
a suitable, observable slit height Theory
Equipments using the Instrument Procedures Processing Questions
at slide (e5).
of – With the height adjustment screw of the collimator (e4),
at Adjusting the collimator
align the middle of the slit with the horizontal cross-hair and
lock the slit in position.
e
e
Illuminate the slit using Na lamp. Aim the telescope at (e) and open the
h
e Fig. 5 Collimator
- e1 Micrometer screw slit slightly using (e1). Set the slit to a
g e2 Collimator tube
e3 Arresting screw for collimator tube suitable, observable height using (e5).
- e4 Height adjustment screw for collimator
e5 Slide for adjusting slit height
at With (e4), align the middle of the slit
e with the horizontal cross-hair and
at
-
lock the slit in position.
-
e Loosen (e3) and slide (e2) in the
e,
direction of the arrow (see Fig. 5) until
6)
a sharp image is obtained.
m
By turning the tube, align the slit
y.
vertically so that it is parallel to the
vertical cross-hair, and then tighten
or
the arresting screw for (e3).
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
0206-Wit
width (e1), set the slit to a suitable width.
Slowly turn the prism table and observe
the shift of the spectral lines with the
telescope until the spectral line (yellow,
λ = 589.3nm) just passes through a Remove prism, align the 1
between two lines, use the smaller value. 155° + 15' = 155° 15'
Record data
Fill the data recorded before in the following table and copy it onto the original
data record in the lab report.
Table: Data record form for angle of minimum deviation measurements. In the above table,
SN refers to sequence number, the angle of outgoing and incoming light rays are represented
by θ1 and θ2 respectively. The wavelength of light used in this experiment is λ = 589.3nm.
Note: When you finish your experiment and intend to leave laboratory, your
original experimental data need to be checked by teacher and get his/her signature
below your data to ensure they are free of serious errors.
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
1 Introduction
2 Experimental objectives
3 Experimental equipments
4 Experimental principle
5 Experimental instrument
6 Experimental procedures
7 Data processing
8 Questions
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θ1 θ2 Min. Ind.
SN
θ1l θ1r θ2l θ2r dev. δmin ref. n
1 32◦ 46′ 212◦ 44′ n=
◦ ′
2 33 2 212◦ 57′ 329◦ 42′ 149◦ 45′ δmin u(n) =
3 32◦ 52′ 212◦ 59′ En =
◦ ′
Mean 32 53 212◦ 47′ 329◦ 42′ 149◦ 45′ Result
u(δmin )
Unc. u(θ1l ) = 5′ u(θ1l ) = 7′ u(θ2l ) = 1′ u(θ2l ) = 1′ n = n ± u(n)
( ) ( )
θ 1l = 32◦ 46′ + 33◦ 2′ + 32◦ 52′ /3 = 32◦ 53′ θ 1r = 212◦ 44′ + 212◦ 57′ + 212◦ 59′ /3 = 212◦ 47′ (15)
√
1( ◦ ′ )
u(θ1l ) = (32 46 − 32◦ 53′ )2 + (33◦ 2′ − 32◦ 53′ )2 + (32◦ 52′ − 32◦ 53′ )2 + (1′ )2
6
√
1( ′ 2 )
= (7 ) + (9′ )2 + (1′ )2 + (1′ )2 = 5′ (16)
6
√
1( )
u(θ1r ) = (212◦ 42′ − 212◦ 47′ )2 + (212◦ 57′ − 212◦ 47′ )2 + (212◦ 59′ − 212◦ 47′ )2 + (1′ )2
6
√
1( ′ 2 )
= (5 ) + (10′ )2 + (12′ )2 + (1′ )2 = 7′ (17)
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
θ1 θ2 Min. Ind.
SN
θ1l θ1r θ2l θ2r dev. δmin ref. n
1 32◦ 46′ 212◦ 44′ n = 1.759
2 33◦ 2′ 212◦ 57′ 329◦ 42′ 149◦ 45′ 63◦ 12′ u(n) = 0.001
◦ ′ ◦ ′
3 32 52 212 59 En = 0.06%
◦ ′ ◦ ′ ◦ ′ ◦ ′
Mean 32 53 212 47 329 42 149 45 Result
u(δmin ) = 4′
Unc. u(θ1l ) = 5′ u(θ1l ) = 7′ u(θ2l ) = 1′ u(θ2l ) = 1′ n = 1.759 ± 0.001
¯ ¯ Note:
δmin = ¯(32◦ 53′ − 329◦ 42′ ) + (212◦ 47′ − 149◦ 45)+360◦ ¯ /2 = 63◦ 12′ (18)
√ Unit
1
u(δmin ) = (5′ )2 + (7′ )2 + (1′ )2 + (1′ )2 = 4′ (19)
2
Significant figure
60◦ + 63◦ 12′ 60◦
n = sin sin−1 = 2 sin 61◦ 36′ = 1.759 (20)
2 2 Presentation of the
1 4′ × 2π
u(n) = cos 61◦ 36′ sin−1 30◦ = 0.001 (21) result
2 60′ × 360◦
0.001 Only for reference!!!
En = = 0.06% (22)
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1.759 . . . . . . . . . . . . . . . . . . . .
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
1 Introduction
2 Experimental objectives
3 Experimental equipments
4 Experimental principle
5 Experimental instrument
6 Experimental procedures
7 Data processing
8 Questions
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Introduction Objectives Equipments Theory Instrument Procedures Processing Questions
Questions
Preview questions
1 How to find the angle of the minimum deviation? Why?
2 Why do telescopes focus to infinity when the cross-hair reflected by the flat glass
plate is sharp?
3 What conditions should be satisfied for prism spectrometer adjustment?
Review Questions
1 Why does a spectrometer use two vernier scales? If one vernier cross the 0◦ (or
360◦ ) mark line when telescope rotate from the position of the minimum
deviation of light rays to the direction of incoming light rays, what features do the
prism spectrometer readings show and how to process the corresponding data?
2 What are the physical meanings of type A and B evaluations of uncertainty? How
to calculate them?
3 What is error transfer formula? Try to obtain the formula
α+δmin
sin−1 α
u(δmin )
u(n) = 2 cos 2 2 by using the error propagation formula when
u(α) = 0.
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