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Materials and Manufacturing Processes


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Influence of Heat Treatment on the Machinability of


Titanium Alloys
a b a a b a
M. Armendia , P. Osborne , A. Garay , J. Belloso , S. Turner & P.-J. Arrazola
a
Mondragon Unibertsitatea – Faculty of Engineering , Mondragón , Gipuzkoa , Spain
b
Advanced Manufacturing Research Centre , Rotherham , England , UK
Accepted author version posted online: 26 Jul 2011.Published online: 14 Mar 2012.

To cite this article: M. Armendia , P. Osborne , A. Garay , J. Belloso , S. Turner & P.-J. Arrazola (2012) Influence of
Heat Treatment on the Machinability of Titanium Alloys, Materials and Manufacturing Processes, 27:4, 457-461, DOI:
10.1080/10426914.2011.585499

To link to this article: http://dx.doi.org/10.1080/10426914.2011.585499

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Materials and Manufacturing Processes, 27: 457–461, 2012
Copyright # Taylor & Francis Group, LLC
ISSN: 1042-6914 print=1532-2475 online
DOI: 10.1080/10426914.2011.585499

Influence of Heat Treatment on the Machinability of Titanium Alloys


M. Armendia1, P. Osborne2, A. Garay1, J. Belloso1, S. Turner2, and P.-J. Arrazola1
1
Mondragon Unibertsitatea – Faculty of Engineering, Mondragón, Gipuzkoa, Spain
2
Advanced Manufacturing Research Centre, Rotherham, England, UK

Orthogonal cutting force measurements and single-point tool life tests were conducted in order to analyze the sensitivity to heat treatment
on the machinability of three titanium alloys: Ti6Al4V, Ti-5Al-4V-0.6Mo-0.4Fe (TIMETAL1 54M), and Ti6246. The Ti6246 alloy showed
the highest tool wear rates and the higher cutting forces in all the heat treatment conditions which could be related to its higher mechanical
properties. TIMETAL1 54M alloy, a newly developed alloy with similar mechanical properties to the more commonly used Ti6Al4V,
showed the lowest wear rates. Microstructural changes due to heat treatment have some influence in the machinability of the alloys. The
b annealed samples of the Ti6Al4V and TIMETAL1 54M alloys, with a very coarse lamellar microstructure, showed considerably shorter
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tool life and higher cutting forces. The rest of the heat treatments showed no significant influence in the machining behavior of the analyzed
alloys as they do not cause important microstructural changes.

Keywords Annealing; Machinability; Microstructure; Productivity; Ti54M; Ti6246; Ti6Al4V; Titanium.

INTRODUCTION cut) with uncoated carbide tools. Hughes et al. [4]


Titanium alloys are now increasingly popular in the machined this material with round carbide inserts at
aerospace sector due to their excellent corrosion resist- 60 m  min1 (0.25 mm  rev1 feed rate and 2 mm depth
ance, high strength-to-weight ratio, and high strength of cut) and obtained a tool life of over 50 minutes.
at elevated temperatures. In addition, titanium is replac- Ramesh et al. [5] obtained a tool life of around 20 minutes
ing aluminium in many aircraft applications as the latter machining this alloy using PCD inserts in dry cutting
forms a galvanic pair with the increasingly used Carbon conditions with a cutting speed of 70 m  min1,
Fibre Reinforced Plastic (CFRP) components [1]. How- 0.22 mm  rev1 feed rate, and 1 mm depth of cut.
ever, it is well known that titanium alloys are difficult Ti-5Al-4V-0.6Mo-0.4Fe (TIMETAL1 54 M, it will be
to machine when compared with other structural materi- referred as Ti54M through the text) alloy is an a þb alloy
als like aluminium and most steels. Their low thermal with similar mechanical properties to the Ti6Al4V alloy.
conductivity, high strength even at high temperatures, Ti54M alloy has been shown to provide cost savings
high chemical reactivity with tool materials, and their due to its better machinability when compared to the
low elastic modulus are the reasons for this poor machin- Ti6Al4V alloy [6]. Arrazola et al. [7] confirmed the
ability [2]. To overcome these machining difficulties and expected better machinability of this alloy when com-
improve the productivity of titanium alloy components, pared to Ti6Al4V, with a maximum cutting speed of
a big effort is being performed in the different areas that 90 m  min1 for 15 minutes of machining time. They
affect machinability: workpiece material, tool material attributed this better behavior to the different micro-
and geometry, cutting conditions, etc. The aim of this structure of the studied samples. Similarly, Kosaka
research work is to understand how the machining per- et al. [8] conducted drilling tests in both Ti6Al4V and
formance can be improved by modifying the workpiece Ti54M alloys in different heat treatment conditions. In
material, specifically, its microstructure. To do that, the their tests the Ti54M alloy showed better machinability
machinability of 3 different a þb titanium alloys than the Ti6Al4V in all the heat treatment conditions.
(Ti6Al4V, TIMETAL1 54M and Ti6246) is analyzed. When the different heat treatments are compared the b
Ti6Al4V is the most commonly used of the titanium and recrystallization annealed workpieces were the most
alloys, accounting for approximately 50% of the titanium difficult to drill.
alloy consumption in the aerospace sector. Arrazola et al. Ti6246 is another a þ b alloy which can be heat treated
[3] reported that a maximum cutting speed of 80 m  min1 to high strengths (yield stress in excess to 1200 MPa) and
was established for 15 minutes of tool life in roughing higher sections than Ti6Al4V. This good response to heat
conditions (0.1 mm  rev1 feed rate and 2 mm depth of treatment and the lack of martensite transformation after
rapid cooling indicate that it should be classified as a b
alloy [1]. The machinability of the Ti6246 alloy is poorer
Received February 7, 2011; Accepted April 14, 2011 than that of the Ti6Al4V alloy. Jawaid et al. [9] carried
Address correspondence to M. Armendia, Mechanical and out turning tests on Ti6246 alloy with two uncoated
Manufacturing Department, Mondragon Unibertsitatea – Faculty of cemented carbides with different grain sizes. A tool life
Engineering, Loramendi Kalea 4 20500, Gipuzkoa, Spain; E-mail: of 12 minutes was achieved with the small grain sized tool
marmendia@eps.mondragon.edu;, mikelarmendia@hotmail.com

457
458 M. ARMENDIA ET AL.

with a cutting speed of 60 m  min1 and a feed rate of TABLE 2.—Details of the heat treatments applied to each of
0.25 mm  rev1. the alloys tested
These three alloys will be heat treated with different Annealing Annealing
annealing techniques to study the influence of the conse- temperature ( C) time (h) Cooling
quent microstructural changes. The effect of these
changes in the machining behavior will allow establishing Ti6Al4V
Mill annealed 700 5 Air
the best heat treatment condition to machine each alloy
b annealed 1050 1 Air
and to define the microstructural features to obtain Duplex annealed
new alloys with better machinability. Single point turn- 1st step 954 1 Air
ing tests will be performed to compare the machining 2nd step 677 5 Air
performance of each alloy=heat treatment pair. In Ti54M
addition, forces will be measured during orthogonal cut- Mill annealed 700 8 Air
ting of the different samples to apply the Cutting Force b annealed 1025 1 Air
Coefficient (CFC) theory and gain a better understand- Duplex annealed
ing of the machining performance of each alloy=heat 1st step 935 1 Air
treatment pair. 2nd step 677 8 Air
Ti6246
Mill annealed 700 8 Air
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EXPERIMENTAL SETUP
Workpiece Materials and Heat Treatments
Table 1 shows the composition and the b transus tem- Tool Life Tests
perature of the Ti6Al4V, Ti54M, and Ti6246 alloys. For Single-point turning tests were carried out on a CIN-
each alloy, 1 meter long and 250 mm diameter as forged CINNATI HAWK lathe to perform tool life tests. A feed
bars were received. The forging step consisted in a b rate of 0.1 mm  rev1 and a depth of cut of 2 mm were
ingot breakdown, followed by a=b processing to final selected and conventional cooling was used. For each
size. alloy, preliminary tool wear tests were performed to
For the Ti6Al4V and Ti54M alloys, three samples were obtain the maximum cutting speed at which a cutting time
cut from the as forged bar and sent to receive different of at least 15 minutes is achieved [3, 7]. The correspondent
heat treatments (mill annealing, b annealing and duplex maximum cutting speed of each alloy is applied in the tool
annealing) at Timet while the last one remained life tests to analyze the influence of heat treatment.
untreated. In the case of the Ti6246 alloy, only a mill SANDVIK CNMG 120408-23 H13A uncoated car-
annealing heat treatment has been followed. Table 2 bide inserts were mounted in a SANDVIK C5-DCLNL-
summarizes the details of the performed heat treatments. 35060-12 tool holder, which provided an effective
A Leica DM IRM optical microscope has been used to
study the microstructure of the three alloys in the corre-
spondent heat treatment conditions (Fig. 1). In the as
forged state, they show a bi-modal microstructure com-
posed by a primary (white grains) and transformed b with
acicular a (dark zones). Comparing to the Ti6Al4V alloy,
big a grains (20 mm) taking most of the volume, Ti54M
presents smaller a primary grains (10–15 mm) that lead
to smaller general grain size. In the case of the Ti6246
alloy, the a primary grain size is even smaller (5–10 mm).
When applying the mill annealing and duplex annealing
(only Ti54M and Ti6Al4V alloys) no significant micro-
structure variation has been noticed comparing to the
as forged samples. However, totally lamellar microstruc-
tures with very big grain size (  1 mm) were formed after
b annealing of the Ti6Al4V and Ti54M alloy.

TABLE 1.—Composition and b transus temperature


for the tested titanium alloys.

Composition
Titanium Transus
alloy Al V Mo Fe St Zr b ( C)

Ti6Al4 V 6 4 – – – – 996
Ti54 M 5 4 0.6 0.4 – – 950
Ti6246 6 – 6 – 2 4 935
FIGURE 1.—Microstructure of the studied samples.
INFLUENCE OF HEAT TREATMENT ON TITANIUM ALLOYS 459

clearance angle of 6 and a rake angle of 7 . A fresh


cutting edge was used for each test. Due to the impor-
tance of cutting edge radius in cutting forces [10], this
parameter has been controlled using a white light inter-
ferometer and only the cutting edges with a value within
35  5 mm have been used. The tool rejection criterion
was 0.25 mm for the average flank wear (VB) and
0.5 mm for the maximum flank wear (VBmax).

CFC
A KISTLER 9121 dynamometer was installed on the
lathe to measure the cutting forces. In this case, orthog-
onal cutting tests were performed by machining a 5 mm
thickness and 120 mm diameter tube that was previously FIGURE 2.—Average flank wear after 15 minutes of machining time for the
three alloys in the as forged condition (f ¼ 0.1 mm  rev1; aP ¼ 2 mm).
prepared on each workpiece. SANDVIK TCMT
16T308-KM H13A carbide inserts were used and
mounted in a modified holder which was ground such RESULTS AND DISCUSSION
that they were presented to the work-piece with a 90
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entering angle. These inserts provide a geometry with a Tool Life


clearance and rake angle of 7 , almost equal to the one Comparison between the three alloys. Figure 2 shows
used previously in the tool life tests. Again, a fresh cut- the results of the preliminary cutting tests performed to
ting edge was used for each test. In this stage, the feed obtain the maximum cutting speed for the studied alloys
rate was varied (0.1, 0.15, 0.2, and 0.25 mm  rev1) and in the as forged condition.
cutting speed was maintained constant at 40 m  min1 The data shows that the Ti6246 has the poorest machin-
to avoid premature wear with the higher feed rates. Each ability, with a maximum cutting speed of 60 m  min1.
test was repeated, at least, twice (uncertainty: 3%). For the other two alloys, Ti54M shows a better perfor-
CFCs contain information about the material hard- mance with a maximum cutting speed of 90 m  min1,
ness, tool rake angle, and friction between chip and while the Ti6Al4V alloy can only be machined at
the tool and are used in the prediction of cutting forces, 80 m  min1 for 15 minutes. It implies an improvement
torque, power, and chatter stability limits. Oxley estab- of about 20% in the machinability rate of the Ti54M alloy
lished a model by which the cutting forces measured in when compared to the Ti6Al4V. These results confirm
orthogonal cutting can be divided into the shear or those reported by Arrazola et al. [7].
cutting and edge components [11]:
Influence of the heat treatment. Figure 3 shows the
Tangentialforce : Ft ¼ Ftc þ Fte ¼ Ktc bf þ Kte b ð1Þ measured average flank wear from tool life tests for each
of the studied alloys at the different heat treatment con-
Feedforce : Ff ¼ Ffc þ Ffe ¼ Kfc bf þ Kfe b ð2Þ ditions and at the correspondent maximum cutting
speed. For the Ti6Al4V and Ti54M alloys, tool life in
where b is the depth of cut, f the feed rate, Ktc and Kfc the b annealed condition was considerably lower. The
the tangential and feed cutting coefficients, and Kte same conclusion was achieved by Kosaka and Fox [8]
and Kfe are the tangential and feed edge coefficients, who stated that the higher b grain size of the laminar
respectively. microstructure created after b annealing is more difficult

FIGURE 3.—Average flank wear from the tool life tests for the studied alloys at its correspondent cutting speed (f ¼ 0.1 mm  rev1, aP ¼ 2 mm).
460 M. ARMENDIA ET AL.

FIGURE 4.—Cutting (a) and feed (b) forces for Ti6Al4V, Ti54M and Ti6246 alloys in the as forged condition (vc ¼ 40 m  min1, aP ¼ 5 mm).
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to shear, leading to higher cutting forces and decreasing its expected improved machinability and the results
tool life. obtained previously by the authors [7] at 0.1 mm  rev1
The machining of the mill and duplex annealed sam- of feed rate. However, when increasing feed rate, the
ples of each alloy do not show variations with respect raise in cutting and feed force is bigger for the Ti54M
to the as forged condition. This observation is in line with alloy (larger slope in Fig. 4(a,b)) and for the higher feed
the unappreciable microstructural differences of both rates cutting forces exceed those of the Ti6Al4V. This
Ti6Al4V and Ti54M alloys in these three heat treatment behavior is consistent across all the heat treatments, only
conditions. In the machining of the Ti6246 alloy, the heat changing the intersection position of the lines of best fit.
treatment does not seem to have a significant influence. The larger gradient of the line (cutting coefficients -
Ktc, Kfc) for the Ti54M alloy is an indicator of the higher
shear stress required to machine this alloy. However, a
Cutting Forces comparison of the edge coefficients (Kte, Kfe) shows con-
Comparison between the studied alloys. Figure 4 shows siderably lower values for the Ti54M alloy. As the edge
the measured cutting forces for the tested alloys in the as coefficients are related to flank contact and friction, it
forged condition. For each alloy, the trend lines and its seems that there may be a smaller friction component
equation have been plotted. The behavior of the three in the machining of the Ti54M alloy, leading to reduced
alloys is repeated in the rest of heat treatment conditions. cutting temperatures. The high temperatures and the
The Ti6246 alloy recorded the highest cutting forces. unfavorable distributions in the contact zone are the
This agrees with the higher mechanical properties of this main problem in the machining of titanium alloys, mak-
alloy when compared with Ti6Al4V and Ti54M. ing diffusion the main wear mechanism [12]. In this case,
The Ti54M alloy shows lower cutting and feed forces it seems that tool wear is reduced in the Ti54M alloy due
than Ti6Al4V at the lower feed rates, which agrees with to the lower friction and rubbing effects and, hence,

FIGURE 5.—Cutting forces for Ti6Al4 V, Ti54 M, and Ti6246 in the four heat-treatment conditions (vc ¼ 40 m  min1, aP ¼ 5 mm).
INFLUENCE OF HEAT TREATMENT ON TITANIUM ALLOYS 461

lower temperatures. In fact, this phenomenon is alloy, a higher edge effect can lead to higher cutting
confirmed with the lower wear rates obtained in the temperatures, and hence, tool wear can be accelerated.
machining of this alloy in the tool life analysis tests.
ACKNOWLEDGMENTS
Influence of heat treatment. Figure 5 shows the vari- The authors would like to thank Roger Thomas from
ation of the cutting and feed forces with feed rate for the Timet UK and Steve Weston from Sandvik UK for their
studied alloys in the 4 different heat treatment con- help providing technical, material, and tooling support
ditions. For the Ti6Al4V and Ti54M alloys, the b to this study.
annealing samples showed the highest force values with The authors would also like to thank the Basque
a bigger influence in the feed forces. The rest of heat Government for the Research Grant BFI07.91.
treatment conditions (as-forged, and mill and duplex
annealing) do not show significant differences. These REFERENCES
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