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h i g h l i g h t s
Marshall Test results show that 4.6% Gilsonite increase Marshall Stability.
The indirect tensile test indicates the performance improvement of mixture made with Gilsonite.
Test result indicates that the addition of Gilsonite to mixtures reduces moisture sensitivity.
The specimens with Gilsonite have better performance to those made with pure bitumen 70–60.
a r t i c l e i n f o a b s t r a c t
Article history: Iran-produced bitumen under the circumstances of severe temperature fluctuation, heavy traffic load and
Received 17 August 2016 raining/freezing conditions show low efficiency; therefore, it is necessary to improve its properties
Received in revised form 11 November 2016 accordingly. Existence of weakness in produced bitumen result in failure occurrence in asphalt pave-
Accepted 14 November 2016
ments during service life of asphalt roads. Given the existence of considerable reserves of Gilsonite in
Iran, its low costs compared with other additives and its remarkable properties, we can study asphalts
modified by Gilsonite. At the present time, little research has been conducted on this modifier in the
Keywords:
world and Iran (which its properties are still not quite evident for researchers). The most important fail-
Hot Mix Asphalt (HMA)
Gilsonite
ure in flexible pavements is permanent deformations which are known as rutting. Rutting is longitudinal
Rutting depression in the wheel path in bituminous pavements. The rate and depth of rutting depend on the
Flow number internal factors such as bitumen properties, aggregate, mixture properties and thickness of pavement lay-
Resilent modulus ers. In this lab study, with regard to the technical and executive issues, common functional performance-
based tests of bitumen were performed on specimens through adding Gilsonite with 0, 2, 4, 6, 8, 10 wt.%
of made bitumen specimens. Then, the optimum percentage was calculated using the AHP. The
specimens containing pure bitumen 60–70 and modified bitumen 60–70 with Gilsonite in two different
aggregations (4 and 5) were made and the effects of adding Gilsonite in Marshall Stability and flow,
indirect tensile strength and moisture sensitivity, as well as dynamic creep, and resilient modulus were
evaluated by the UTM device. The research showed that adding Gilsonite to bitumen in hot asphalt mix-
tures considerably increases Marshall Stability and resilient modulus parameter in asphalt specimens.
However, resilient modulus test indicated a significant reduction in flexibility property of asphalt mix-
tures made of modified bitumens. Moreover, increasing the flow number obtained from the dynamic
creep test indicate the increase of rutting resistance.
Ó 2016 Elsevier Ltd. All rights reserved.
http://dx.doi.org/10.1016/j.conbuildmat.2016.11.069
0950-0618/Ó 2016 Elsevier Ltd. All rights reserved.
H.R. Jahanian et al. / Construction and Building Materials 131 (2017) 156–164 157
heavy vehicles and increase of traffic loads, the growing amount of effect only on high operating temperatures of base bitumen and
asphalt failures are spreading. In low temperature, asphalt pave- has increased rutting resistance. However, Gilsonite failed to
ment suffers many cracks under traffic load, and vice versa, with increase bitumen resistance against fatigue cracking and low tem-
increasing ambient temperature, deformation and rutting be perature cracking. Furthermore, the conducted tests display that
appeared. Major weaknesses of Iran-produced bitumen are high Gilsonite increases the resilient modulus and indirect tensile
sensitivity, low elasticity, the limited range of temperature- strength of the asphalt mixture [8].
Servicing. The modification of bitumen properties increase pave- American Gilsonite Company is one of the greatest Gilsonite
ment service-life and its quality; therefore, pavement repair and producers in the world, the results in 1998 showed that adding Gil-
maintenance costs be reduced significantly. In recent decades, in sonite to the asphalt mixture greatly increases Marshall Stability.
order to achieve pavements with longer service-life and overcome Increasing 8% Gilsonite (relative to the weight of bitumen)
the problems of conventional pure bitumen and asphalts which do increases Marshall Stability rate of asphalt specimen up to
not have sufficient adhesion to aggregates and suitable properties, 25–40%. This variation leads to turning standard surfacing into a
modifiers are used [2]. high-performance one. Another important advantage of using
Gilsonite in asphalt mixture is the decrease moisture sensitivity
of asphalt mixture. The results showed that specimens without
2. Literature review Gilsonite additives have no sufficient moisture resistance level,
while even adding 4% Gilsonite to the asphalt mixture considerably
The mineral now known as ‘‘Gilsonite” was discovered in the increased moisture resistance level. The dynamic modulus tests
early 1860’s, but it was not known until the mid-1880’s that demonstrate that Gilsonite increases the resilient modulus of
Samuel H. Gilson began to promote it as a waterproof coating for asphalt specimens. This result in macroeconomic saving in the
wooden pilings and as insulation for wire cable. It was brittle road construction budget of countries. The results of Wheel Truck
and can be easily turned into a dark brown powder. In 1888, experiment proved resistance against deformation and good per-
Samuel H. Gilson and a partner established the first company to formance of the pavement. Results of Wheel Truck test indicated
mine and market Gilsonite on a commercial-scale [3,4]. Gilsonite that the best results are obtained from mixture with 8% Gilsonite
resembles shiny black obsidian substance. Its color is dark brown and, mixtures with 6% Gilsonite and 2% SBS and 4% SBS are located
in micronized powder. Gilsonite is mined in underground shafts. in the second and third ranks [9].
Since the early 1970s, Norway has used it as additive and modifier In the same year, Swedish Transport research organization car-
of behavioral characteristics of bitumen and asphalt mixtures in ried out a field research on conventional pavement with Gilsonite
areas with heavy passing traffic and cold and wet weather condi- modifier and concluded that the use of Gilsonite is useful for
tions that increase pavement failures such as stripping. Initially, constructing asphalt mixture with harder bitumen in order to have
the bitumen penetration grade 40–50 was used in these and due more rutting resistance and better load distribution within struc-
to the failure of this type of bitumen, Gilsonite was added into ture and as a result less stresses in pavement structure [10].
mixture as a modifier additive. The remarkable point is that the In 2010, Ameri and colleagues in their article concluded that
Gilsonite in the construction of the asphalt mix increased the adding Gilsonite increases the operating temperature of bitumen
expected service-life of pavement up to two fold [5]. In New South (up and down temp), this condition increases with increasing
Wales of Australia, Gilsonite has been used as an additive and Gilsonite. Meanwhile, the average temperature of the pavement
modifier with 0.25% by weight of asphalt mix. Studies and investi- longevity increases with increasing Gilsonite which refers to the
gations conducted on performed surfacing after a period of 6, 12, higher fatigue factor at the same average temp [11]. Transportation
24 months have shown a significant reduction in failures of wheel Research Institute of the Transportation Ministry of the Islamic
rutting and waving compared to previous performed surfacing Republic of Iran in 2012 through a research project concluded that
with no modification of Gilsonite and the positive performance of Gilsonite increases the high operating temperature of pure bitu-
Gilsonite in the asphalt mix caused that the Australian Asphalt men. Therefore, the high operating temperature of pure bitumen
Pavement Association suggested Gilsonite for squares’ surfacing rise can increase the shear strength of pure bitumen, especially
[5]. in the warm seasons, which is a factor itself for increasing the
In the Port of Seattle, located at the North East of the US, rutting resistance of asphalt mixture. Moreover, by adding
Gilsonite was used with the amount of 8% by weight of bitumen, Gilsonite to pure bitumen, stiffness increases and the rate of bitu-
as an additive and modifier of bitumen 60–70 on surfacing areas men stiffness (M value) decreases and, low operating temperature
affected by heavy traffic of trucks. The performed Asphalt after of modified bitumen enhances [12].
one year use showed better resistance than previous ones without
Gilsonite modifier compared to rutting resistance and stripping. In
addition, Gilsonite has been utilized for more than 5 years ago in 3. Research methodology
New Jersey and the region in which trucks are included 20% of
daily passing traffic of 500,000 vehicles. First low penetration Although the application of different materials as filler has
bitumen was used for decreasing wheel rutting and waving, but become increasingly popular in the recent few decades, most
it failed. After performing asphalt made with Gilsonite, it was spec- studies in this field were concentrated on the experimental inves-
ified that the problem of rutting and waving has been solved [5]. In tigations and quantitative effect of filler on mechanical behavior
2008, ‘‘Sou” and ‘‘Wong” concluded that repeated loads of vehicle and volume ratio of asphalt concrete.
wheels be resulted in the accumulation and growth of micro and Filler is of the most important component of asphalt mixture
macro cracks, deformation and wearing of aggregates in asphalt that by filling the voids due to softness and surface properties
pavements [6]. In 2004, Pretorius and colleagues in their paper and chemical composition plays the role of an active ingredient
concluded that Gilsonite in addition to the technical benefits in and influences the adhesion between bitumen and aggregates.
improving asphalt properties has many economic advantages in Gilsonite as an active filler has been able to improve the mechan-
the optimum design of asphalt surfacing [7]. ical behavior of asphalt mixtures. Gilsonite is utilized as a preser-
In the research project carried out in Pennsylvania in 1999 by vative agent in Hot Mix Asphalt mixtures of pavement.
Anderson et al., the results of sharp experiments on the base bitu- The main objective of this study is to determine the perfor-
men and modified bitumen indicated that Gilsonite has a positive mance of HMA containing mineral bitumen powder (Gilsonite) in
158 H.R. Jahanian et al. / Construction and Building Materials 131 (2017) 156–164
Table 1 Table 2
Gradations of the used aggregate mixture. The allowed value of Los Angeles Abrasion Tests.
Sieve Size Percent Passing Type of asphalt layer Maximum allowed value (%)
(mm)
Gradation Gradation Gradation Gradation Gradation Topka 30
1 2 3 4 5 Binder 40
25 – – – – –
19 – 100 100 100 100
12.5 100 90 92 92 92 Elongation index ¼ ðInitial weight of specimenÞ=
9.5 – – 82 85 82
4.75 74 44 58 66 51 ðWeight of elongated grainsÞ ð1Þ
2.36 58 28 41 50 32
1.18 – – 31 38 24 To conduct Flakiness test, selected grains is tried to be passed
0.6 – – 22 27 17 from flaky side through the Flakiness test screen rut. The weight
0.3 21 5 13 18 10 of the grains which passed the groove due to Flakiness is deter-
0.15 – – 8 12 7 mined and Flakiness index is calculated according to Eq. (2).
0.075 10 2 5 8 5
Flakiness index ¼ ðInitial weight of specimenÞ=ðWeight of flaky grainsÞ
ð2Þ
different tests such as Marshall Test, resilient modulus test, To perform fracture percentage test, we separate the grains
dynamic creep test, and indirect tensile strength test (ITS). which are more fractured in a crusher and determine their weight.
To achieve these goals, First, Marshall’s specimens were Fracture percentage is calculated according to Eq. (3) [16].
constructed by performing Marshall Tests to determine optimum
bitumen content. Then, asphalt mixtures were made for above dif-
fracture percentage ¼ ðInitial weight of specimenÞ=
ferent tests with the optimum bitumen content and Gilsonite per- ðweight of fractured grainsÞ ð3Þ
centage. In this step, different content of Gilsonite (0%, 2%, 4%, 6%,
The aggregates tests results; Los Angeles abrasion test, fracture
8% and 10% of total used bitumen) were added to the mixtures and
percentage, Elongation and Flakiness, the sand value, specific grav-
be evaluated the effects of this different contents on behavior of
ity, density and water absorption are show in Table 4.
asphalt mixtures in tests.
The used bitumen properties (PG 64 (AC 60-70)) are presented
in Table 5. Also the physical and chemical properties of the used
3.1. Materials preparation Gilsonite are presented in Tables 6 and 7.
The aggregates gradation is one of the most important factors 3.2. Mixing bitumen and Gilsonite
affecting the strength and capacity of asphalt. The asphalt aggre-
gates grading are chosen considering several factors such as type According to the World Road Association (PIARC) suggestion,
of pavement, type and location of the target layer in the surfacing Gilsonite powder used for the modification of bitumen should
system, the asphalt layer thickness and the largest grain size avail- completely pass through sieve No. 50. Gilsonite powder used in
able in aggregates. In this study, continuous gradation No. 4 and 5, the research is passed through sieve No.200 which is added with
(for application of Topeka and binder layer) based on the Iran High- different% amounts relative to bitumen weight to the bitumen
way Asphalt Paving Code (No. 234) in the allowed range offered in 60–70 which is heated at the temperature of 140 °C. This mixture
it has been used (according to Table 1) [13]. be mixed for 150 min at 150 rpm. Then, it is heated to 180 °C, mix-
In the stage of compression and operation of asphalt mixtures, ing for 30 min, at 4500 rpm by high shear mixer. In this way, the
due to loads induced by roller weight and passing vehicles, aggre- homogenous mixture of pure bitumen and Gilsonite is achieved.
gates are exposed to abrasion and fracture. For the prevention of It is in accordance with the suggestion of (PIARC) [18].
this type of damage or to reduce it, the used aggregates should
be hard, tough and durable and have sufficient strength. This test 3.3. Construction of asphalt specimens
method is described in the standard ASTM C131 [14]. The allowed
values are provided based on the layer type in Tables 2 and 3 [15]. The mix design methods of asphalt concrete try to balance the
To conduct Elongation test, a certain weight of sandy materials combination of aggregates and bitumen in order to achieve the
(retained on the sieve No. 4 and 5) is tried to be passed from the appropriate performance of mixture in long term (high durability)
length side through the bars of Elongation test screen. The weight in a pavement structure. It is evident that the main components of
of grains which cannot pass due to the Elongation is determined asphalt mixtures are aggregates, bitumen and air. The main goal of
and Elongation index is calculated according to Eq. (1). each mix design method is to produce mixtures with high
Table 3
Categorization of test specimens in Los Angeles abrasion test.
Table 4 Table 7
Physical Specifications of the Materials used in research. Test Gilsonite physical properties [15].
strength ratio of saturated specimens to dry specimens should not According to the results, the indirect tensile strength of asphalt
be less than 0.8. The results of this test are show in Figs. 9–13. mixtures with gradation No. 4 and 5 increases in the dry state by
162 H.R. Jahanian et al. / Construction and Building Materials 131 (2017) 156–164
Table 8
Percentage of optimum bitumen in HMA.
Gradation No. 5 5 4 4
Gilsonite % 4.6 0 4.6 0
Optimal bitumen % 5.7 4.9 5.5 4.6
Fig. 10. Indirect tensile strength of asphalt mixture with gradation No. 4 and
modified bitumen.
Fig. 9. Indirect tensile strength of asphalt mixture with gradation No. 4 and control
bitumen.
4.3. Resilient modulus test results Fig. 11. Indirect tensile strength of asphalt mixture with gradation No. 5 and
control bitumen.
Fig. 15. Diagram of permanent cumulative strain areas vs. the cycle.
Fig. 12. Indirect tensile strength of asphalt mixture with gradation No. 5 and
modified bitumen.
5. Conclusion
against applied forces. This matter is more seen in mixtures that [6] Zhi Sou, Wing Gun Wong, Analysis of fatigue crack growth behavior in asphalt
concrete material in wearing course, J. Constr. Build. Mater. (2008).
their load bearing is from aggregate resistance on aggregate.
[7] F. Pretorius, J. Grobler, J. Onreat, Development of a fit-for-propose product
However, it can be concluded that adding Gilsonite can increase performance specification system for asphalt mixes, J. Assoc. Asphalt Paving
resistance against rutting of mixture. Technol. (2004).
Gilsonite is cheaper than other modifiers such as SBS or EVA. [8] David A. Anderson, Donald W. Christensen, Mihai O. Marasteanu, Yusuf Mehta,
Field performance of modified asphalt binders evaluated with super pave test
The increase of traffic load bearing potential, lower costs of methods: 1-80 test project, TRB, 1999.
Gilsonite compared to other modifiers and the above described [9] Gilsonite in paving application, <www.americangilsonite.com>.
cases are the advantages of using these modifiers in asphalt [10] Safwat F. Said, Hassan Hakim, Performance Evaluation of Fatigue Cracking in
Flexible Pavement, Swedish National Road and Transport Research Institute
mixtures. Highway Engineering, 2008.
[11] M. Ameri, A. Mansourian, S. Salehi, G. Yadollahi, Technical study on the Iranian
Gilsonite as additive for modification of asphalt binders use in pavement
construction, Constr. Build. Mater. Iran (2010).
Acknowledgement [12] Department of Transportation, New Methods of Asphalt Mix Design Based on
Performance and Proposing Appropriate Methods Across Country, first ed.,
Transportation Research Institute, Iran, 2012.
The authors wish to thank the personnel of Bitumen and [13] Iran Highway Asphalt Paving Code, No. 234, Deputy of Regulatory Technical
Asphalt Laboratory in Semnan University Iran and Asphalt Standards, Organization of Management and Planning, Iran, 2011.
and Bitumen Research Center (ABRC) in University of Science and [14] ASTM C131/C131M-14, Standard Test Method for Resistance to Degradation
of Small-Size Coarse Aggregate by Abrasion and Impact in the Los Angeles
Technology for their cooperation and support in conducting Machine, ASTM International, West Conshohocken, PA, 2006.
experiments. [15] Standard Test Method for Density, Relative Density (specific gravity), and
Absorption of Fine Aggregate, Annual Book of ASTM Standards: Concrete and
Aggregates, vol. 4, C. ASTM, 01-128-2001.
References [16] Standard Test Method for Sand Equivalent Value of Soils and Fine Aggregate,
ASTM D2413.
[1] Seyed Ali Ziaee, Morteza Jalili Ghazizadeh, Amir Kavoosi, Abolfazl [17] Gholamali Shafabakhsh, Hassan Divandari, Hamidreza Jahanian,
Mohammadzadeh Moghaddam, Evaluating moisture susceptibility of asphalt Determination of Optimum Gilsonite additive content in pure bitumen using
mixtures containing electric arc furnace (EAF) steel slag, in: The Eighth Analytic Hierarchical Process (AHP), J. Road Transp. Res. Inst. (2013).
National Congress of Civil Engineering, University of Babol, Iran, 2014. [18] Use of Modified Bituminous Binders, Special Bituminous and Bituminous and
[2] Ali Khodaei, Saeid Tolabi, Mohammad Ali Dehshiri, The effects of using soil RAP Bitumen’s with Additives in Road Pavements, World Road Association (PIARC),
and Gilsonite on the safety of intracity and countryside roads, in: The 14 th 1999.
International Conference on Traffic and Transportation Engineering, Tehran, [19] ASTM D4867/D4867M-09(2014), Standard Test Method for Effect of Moisture
Iran, 2014. on Asphalt Concrete Paving Mixtures, ASTM International, West
[3] Sasan Aflaki, Nader Tabatabaee, Proposals for modification of Iranian bitumen Conshohocken, PA, 2014.
to meet the climatic requirements of Iran, J. Constr. Build. Mater. Iran (2008). [20] ASTM D4123-82(1995), Standard Test Method for Indirect Tension Test for
[4] Susana Man Sze Ho, Ludo Zsnzotta, Impact of Different Types of Modification Resilient Modulus of Bituminous Mixtures (Withdrawn 2003), ASTM
on Low Temperature Tensile Strength at Critical of Asphalt Binders, International, West Conshohocken, PA, 1995.
Transportation Research Board, 2002. [21] Determination of the Resilient Modulus of Asphalt-indirect Tensile Test,
[5] Ghaffar Afshari, Hassan Imami, Mohammad Gholipour, Bitumen modified by Methods of Sampling and Testing Asphalt, Australian Standard 2891.12, vol. 1,
Gylsunite, furfural extract and polymers, J. Polym. Sci. Technol. Iran (2006). 1995.