JOURNAL OF EXPERIMENT

Title of Experiment : Determination of Calor Reaction

Day/Date of Experiment : Thursday/May 26th 2016
Name : Risdah Damayanti. N
ID : 1413440021
Class/Group : ICP A of Chemistry/V
Group Members : 1. Aisyah Nurul Wahda
2. Maria Irene Sartika
3. Nur Aliyah Ibrahim
4. Nurul Ilmi
Assistant : Siti Aminah

A. Experiment Purposes
In the end of experiment, apprentice should be understanding and
competent in determination of integral dissolve calor of CuSO 4 and CuSO4.5H2O
by simple calorimeter.
B. Apparatus and Chemicals
1. Apparatus
a. Calorimeter (1 set)
b. Thermometer 110oC (1 unit)
c. Stirrer (1 unit)
d. Measure glass 50 mL (1 unit)
e. Beaker 50 mL (2 units)
f. Stopwatch (1 unit)
g. Analytical Balance (1 unit)
h. Mortar and pestle @(1 unit)
i. Bunsen burner (1 unit)
j. Tripod and gauze @(1 unit)
k. Exicator @(1 set)
l. Spray bottle (1 unit)
 m. Rough and smooth cloth @(1 unit)
2. Chemicals
a. Copper sulphate (CuSO4)
b. Copper sulphate pentahydrate (CuSO4.5H2O)
c. Aquadest (H2O)
d. Tissue
e. Matches

C. Work Procedures
1. Determination of Constanta Calorimeter

50 mL of H2O Note the H2O ± 40oC Add 50 mL of hot

temperature water in the sixth
minutes
 Make the relation curve between Every 1 minute
the time and temperature

2. Determination The Integral Dissolve Calor of CuSO4 and CuSO4.5H2O

10 gr the rough 5 gr the smooth

crystal of crystal of
CuSO4.5H2O CuSO4.5H2O
Every 1 minute 100 mL of H2O + Every 1 minute 100 mL of H2O
until constant 5 gr the smooth during 5 times
crystal of
CuSO4.5H2O

5 gr the smooth crystal of

CuSO4.5H2O in the oven
Every 1 minute 100 mL of H2O + Every 1 minute 100 mL of H2O
until constant the smooth crystal during 5 times
of CuSO4.5H2O

Makassar, May 26th 2016

Assistant Practicant

Siti Aminah Risdah Damayanti N