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    Nanditha A
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    This document describes an experiment to standardize a sodium thiosulfate solution and determine the iodine value of an oil sample. Two trials were performed to standardize the sodium thiosulfate solution against a potassium dichromate solution, obtaining consistent volumes of 19.5 ml of sodium thiosulfate needed. A blank and sample were then titrated against the standardized sodium thiosulfate solution using starch as an indicator. The results will be used to calculate the normality of the sodium thiosulfate solution and the iodine value of the oil sample.

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    This document describes an experiment to standardize a sodium thiosulfate solution and determine the iodine value of an oil sample. Two trials were performed to standardize the sodium thiosulfate solution against a potassium dichromate solution, obtaining consistent volumes of 19.5 ml of sodium thiosulfate needed. A blank and sample were then titrated against the standardized sodium thiosulfate solution using starch as an indicator. The results will be used to calculate the normality of the sodium thiosulfate solution and the iodine value of the oil sample.

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    2 views1 page

    OBSERVATION

    Uploaded by

    Nanditha A
    This document describes an experiment to standardize a sodium thiosulfate solution and determine the iodine value of an oil sample. Two trials were performed to standardize the sodium thiosulfate solution against a potassium dichromate solution, obtaining consistent volumes of 19.5 ml of sodium thiosulfate needed. A blank and sample were then titrated against the standardized sodium thiosulfate solution using starch as an indicator. The results will be used to calculate the normality of the sodium thiosulfate solution and the iodine value of the oil sample.

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    of 1

    OBSERVATION

    SET 2
    Standardization of Sodium thiosulphate

    Indicator: Starch

    Sl Volume of Potassium Burette Reading (ml) Volume of Sodium


    No. Dichromate (ml) thiosuphate (ml)
    Initial Final

    1 20 0 19.5 19.5

    2 20 0 19.5 19.5

    Sample titration: Titration against Na2S2O3

    Indicator: Starch

    Item Initial burette reading Final burette reading Volume of Sodium


    (ml) (ml) thiosuphate (ml)

    Blank 0 16.7 16.7

    Sample 0 2.4 2.4

    Calculation
    Weight of oil sample taken (W1) = 0.5g

    Volume of K2Cr2O7 =

    Normality of K2Cr2O7 (N1) = 0.1N

    Normality of Na2S2O3 (N2) = =

    Iodine Value = =

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