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Materials and Design 32 (2011) 1594–1599

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Materials and Design


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Short Communication

Mechanical and anisotropic behaviors of 7075 aluminum alloy sheets


Mohammad Tajally ⇑, Esmaeil Emadoddin
Dept. of Materials, Faculty of Engineering, Semnan University, Semnan, Iran

a r t i c l e i n f o a b s t r a c t

Article history: Formability of 7075 aluminum alloy sheets was studied after annealing of 71% cold worked (CW) samples
Received 9 June 2010 at different temperatures (270–450 °C). Uniaxial tensile test, deep drawing and Erichsen test were carried
Accepted 1 September 2010 out at room temperature to evaluate formability parameters.
Available online 6 September 2010
Average plastic strain ratio, planar anisotropy, and work hardening exponent of samples were calcu-
lated from the tensile test data. The tensile properties and formability parameters were correlated with
the limit drawing ratio (LDR) and Erichsen test. It was found that the sheets annealed at 400 °C possess
good ductility, high average n-value and the normal anisotropy r-value so that, the formability of 7075
aluminum alloy can be improved by increasing annealing temperatures to the 350–400 °C.
Ó 2010 Elsevier Ltd. All rights reserved.

1. Introduction is also dependent on the material properties such as strain harden-


ing exponent (n), strain rate sensitivity (m), and grain size [11–14].
The 7xxx series aluminum alloys have been widely used as The 7075 aluminum alloy plate, in O temper condition, have
structural materials due to their attractive comprehensive proper- practical and industrial application due to their higher formability
ties, such as low density, high strength, ductility, toughness and in comparison to the other temper conditions. There has been little
resistance to fatigue [1–3]. The 7075 aluminum alloy is one of research on formability and anisotropic behavior of 7075 alumi-
the most important engineering alloys. It has been utilized exten- num alloy. At present study, in order to examine the possibility
sively in aircraft construction due to its high strength-to-density of the practical use of 7075 aluminum alloy, the mechanical prop-
ratio [4]. erties, anisotropic behavior and formability of 7075 aluminum
High strength alloys are desirable to reduce the weight and cost alloy thin sheet at various annealing temperatures were
for constructional applications. In addition, good ductility is also investigated.
required for formability. However, the enhancement of the
strength of a material while maintaining reasonable ductility is a
permanent challenge [5]. By recrystallization, there is a gradual de- 2. Materials and experimental procedures
crease in the tensile strength (UTS), yield strength (YS) and hard-
ness. It also increases the elongation of the rolled material by 2.1. Research material
increasing annealing temperature. The formability of sheet metal
is an important parameter of the manufacturing process design. A7075 O-temper aluminum alloy plate was supplied in 7.2 mm
Thin sheet products are obtained by cold rolling and subsequent thickness for research. The chemical composition of 7075 alumi-
annealing treatment that affects forming behavior. Metals, that num alloy is given in Table 1. For deep drawing test, thickness of
have undergone extensive plastic deformation by rolling or extru- plate was reduced to 3.9 mm by remove material. The 7075 alumi-
sion, exhibit a significant anisotropy of mechanical properties. num alloy plate, in O temper condition, was selected as the starting
Even in the case of untextured metals showing isotropic or almost material (SM) in this investigation.
isotropic yielding behavior, the ductility can be very anisotropic
[6]. Recently, research on aluminum alloy are focused on mechan-
ical properties, texture and anisotropic behavior that give rise from 2.2. Cold rolling and annealing
processing of aluminum alloy sheet especially cold rolling and
annealing [5,7–10]. It was found that the formability of 5052 alu- Cold rolling of the 7075 Al alloy was carried out by rolling plates
minum alloy annealed at 350 °C possessed good formability, opti- with various thicknesses according to mechanical testing: (a)
mal texture and high normal anisotropy value [9]. The formability thickness of 7.2 mm to 2.1 mm equal to 71% CW for tensile proper-
ties; (b) thickness of 3.9 mm to 1.1 mm equal to 71% CW for deep
drawing and Erichsen tests. The cold-rolled samples were annealed
⇑ Corresponding author. at various temperatures in the range of 270–450 °C for 5 min. A
E-mail address: m_tajally@sun.semnan.ac.ir (M. Tajally). programmable Nabertherm furnace was used for annealing; and

0261-3069/$ - see front matter Ó 2010 Elsevier Ltd. All rights reserved.
doi:10.1016/j.matdes.2010.09.001
M. Tajally, E. Emadoddin / Materials and Design 32 (2011) 1594–1599 1595

Table 1 r ¼ ðr 0 þ r 90 þ 2r 45 Þ=4 ð1Þ


Chemical composition (% wt) of the investigated alloy.

Zn Mg Cu Mn Fe Si Cr Ti Al Dr ¼ ðr 0 þ r 90  2r 45 Þ=2 ð2Þ
5.8 2.5 1.6 0.28 0.40 0.35 0.21 0.19 Balance
2.5. Formability testing

2.5.1. Deep drawing


the hot-annealed samples were air-cooled to room temperature by The formability may be expressed as a limiting drawing ratio
natural convection because of very thin thickness of the samples. (LDR) in deep drawing experiment. LDR is defined as the ratio of
the largest diameter of the blank that can be drawn without failure
2.3. Metallographic practice to the smallest diameter of the cup or punch. The 7075-O alumi-
num alloy with a sheet thickness of 1.1 mm that was employed
Metallographic samples were cut from the plates in rolling in deep drawing processes have been used in this study for deter-
direction, ground and polished by 0.25 micron Alumina. The pol- mining LDR. The data of deep drawing process were compared
ished metallographic specimens were anodized by using Barker’s with experimental and numerical values.
reagent (5 ml HBF4 (48%) in 200 ml water) at 30 V direct current
(DC) for 2.5 min by using stainless steel cathode according to ASTM 2.5.2. The Erichsen test
E407 for grain structure observation under polarized light. In the Erichsen test, a hemispherical punch was pressed into the
sheet until fracture occurred. Then at this point the test was
2.4. Mechanical properties stopped immediately and the height of the bulge was measured
[16].
According to standard test procedure E517-92a [15], in order to In several cases the maximal values of the force corresponding
measure r-value of samples uniaxial tension tests were carried out to the necking of the sheet was recorded specimens with thickness
on samples which have been cut in the directions of 0°, 45° and 90° equal to 1.1 mm and 70 mm wide were conducted in accordance
in respect to the rolling direction. The gauge length and width of with ISO 1520, BS 3900: Part E4 and DIN ISO 1520.
the tensile specimens were 50 and 12.5 mm, respectively. The ten-
sile tests were performed at room temperature using INSTRON 3. Results and discussion
4469 universal testing machine equipped by extensometer with
a gauge length of 50 mm. Three specimens for each condition were 3.1. Effect of cold rolling and recrystallization on microstructure
used at a constant crosshead speed of 0.5 mm/min. The parameters
that affect the formability of the sheet metals such as strain hard- The microstructures of starting material and cold-rolled sam-
ening exponent (n) and the plastic strain ratio (r-value), which is ples, for the 7075-O aluminum alloy are shown in Fig. 1. It can
the ratio of the width strain to the thickness strain, (r = ew/et) along be observed that after cold rolling, the aspect ratio of the alumi-
rolling directions (0°), transverse direction (90°) and (45°) with re- num grains for 71% CW increases from 5 to 35 which is consistent
spect to rolling direction were determined. with the macroscopic level of cold reduction.
Grid circles with diameter d0 = 8.0 mm were etched on the ten-
sile samples and used to measure strain in each test. During form- 3.2. Mechanical properties
ing of samples the etched circles were distorted into ellipses and/or
larger circles, and these deformed grid circles were then used to The values of the tensile properties at annealing temperatures
measure strain levels in each case. 270 °C, 350 °C, 400 °C and 450 °C for three directions (0°, 45° and
Three measurements (circles) were made for each specimen 90° to rolling direction) are given in Fig. 2 for 7075 aluminum alloy.
and the mean of the data for r-value tests were obtained. The yield stress and ultimate tensile strength were anisotrop and
The normal anisotropy or mean plastic strain ratio ðr Þ and the vary with respect to the rolling direction.
planer anisotropy (Dr) were calculated from the r values that were The average values of the strengths, elongation, and work hard-
determined along three directions by using the following formulas ening exponent were evaluated as:
[7].

Fig. 1. Microstructure of 7075-O Al alloy for (a) starting material; (b) after 71% CW.
1596 M. Tajally, E. Emadoddin / Materials and Design 32 (2011) 1594–1599

Cold-rolled samples and samples annealed at 270 °C showed


lower elongation in transverse direction, whilst for samples an-
nealed at high temperatures the elongation value was high in
transverse direction. This can be explained in terms of the micro-
structure and mechanical properties. In the cold rolled sheet, the
longer grains restrict the plastic deformation along the transverse
direction, as indicated by the lower elongation. However, cold roll-
ing and subsequent annealing refine the grain size, especially the
grain length, resulting in a greater ductility in the transverse direc-
tion; consequently, the formability along this direction was also
improved.
The (UTS/ry) value which is the ratio of the ultimate tensile
strength to 0.2% proof stress increased from 1.11 for 71% CW sam-
ple to 1.21, 1.23.1.32 and 2.15 by increasing annealing tempera-
tures. The sheets annealed at 400–450 °C had higher (UTS/ry),
which in turn increased the formability. These results were also
consistent with mechanical properties and microstructures.

3.3. Formability parameters

3.3.1. Tensile test


The formability parameters were determined from tensile test
experiment as shown in Fig. 3 and Table 2. The value of normal
anisotropy r or (Lankford value) was high for the sheet annealed
at 400 °C (Fig. 3a) due to fully recrystallized structure (Fig. 4). This
indicates that this sheet possess higher drawability than the sheets
annealed at other temperatures. The planar anisotropy (Dr) was
moderate for all sheets and the tendency to earing during drawing
operations was normal for all annealed sheets (Fig. 3b). This value
of Dr is more than Dr value of 0.14 which has been reported for
aluminum alloy 5052 [17].
Earing is an undesirable phenomenon in metal forming. The
average n-value and nr value also, were high for the sheet annealed
at 400 °C (Fig. 3c). These values indicated that the stretchability of
this sheet was also good. These values were in good agreement
with the evaluated LDR.
To achieve an acceptable average of plastic strain ratio or nor-
mal anisotropy r, it was necessary to anneal the samples at tem-
peratures more than 350 °C.
A comparatively low average n-value of approximately 0.14 re-
vealed that samples annealed at 350 °C did not exhibit good ability
Fig. 2. Variation of tensile properties of AA7075 aluminum alloy with rolling to resist plastic instability during tension. Also, the n-value of these
direction. Ultimate tensile strength (a); 0.2% proof stress (b); elongation. samples was not large enough to give best stretchability. Therefore,
the samples annealed at 400 °C presented better formability than
that of the samples annealed in 350 °C alloy.
X mean ¼ ðX 0 þ 2X 45 þ X 90 Þ=4 ð3Þ Although samples annealed at 450 °C exhibited excellent ductil-
ity at room temperature, the drawability of samples annealed at
where X is yield strength or ultimate tensile strength, or elongation, 450 °C was not much superior to the samples annealed at 400 °C
or working hardening exponent [7]. due to its rather small r-value. The r-value of the samples annealed
By annealing, there was a gradual decrease in the tensile at 450 °C was smaller than that of the samples annealed at 400 °C
strength (UTS) and yield strength (YS), continuation increase in which can relate to the grain orientation at this condition. How-
elongation, average plastic strain ratio or normal anisotropy r ever, the higher elongation resulted in comparatively good draw-
and average strain hardening exponent n  value of the rolled mate- ability. Since, the microstructure of the sheets annealed at 400 °C
rial by increase in annealing temperatures. The sheets annealed at proved a refined and recrystallized grains and better formability
range of 350–400 °C in this study proved a lower value of ultimate in all regions.
tensile strength and yield stress compared to sheets annealed at Thus, the sheets annealed at range of 350–400 °C possessed
other annealing temperatures. more stretchability and drawability than the sheets annealed at
Maximum strengths were observed in the 90° direction at room 270 °C due to the presence of rolled microstructure. The sheet an-
temperature, as shown in Fig. 2. The elongation in the 45° direction nealed at 270 °C showed poor formability due to the presence of
was greater than those in the other directions. The elongation en- cold rolled grains microstructure.
hances by increasing annealing temperatures with a constant
slope. 3.3.2. Deep drawing
Also, the result indicated that sheets annealed at all of anneal- Majority of the surveys have concentrated on the limit drawing
ing temperatures exhibited the maximum strain hardening expo- ratio (LDR) in plastic deformation or problems occurring during the
nent (n) along 45° to the rolling direction and minimum value deep drawing process such as folding, wrinkling and tearing. Figs. 5
along 0° to the rolling direction. and 6 clearly indicated that samples annealed at 400 °C have a
M. Tajally, E. Emadoddin / Materials and Design 32 (2011) 1594–1599 1597

Fig. 4. Microstructure of 7075-O Al alloy after71% CW and annealed at 400 °C.

Fig. 3. Effect of annealing temperatures on formability parameters of 7075


aluminum alloys. Normal anisotropy (a); planar anisotropy (b); strain hardening
exponent (c).

Table 2
Formability parameters of 7075 aluminum alloy.

Annealing Orientation r n nr Dr
temperature respect to RD
270 °C 0 0.49 0.093 0.04557 0.285
45 0.79 0.13 0.1027
90 0.52 0.109 0.05668
Average 0.64 0.102 0.065
350 °C 0 0.62 0.114 0.07068 0.26 Fig. 5. Cups formed with different annealing temperatures: 270 °C (a); 350 °C (b);
45 0.92 0.164 0.15088 400 °C (c) and 450 °C (d).
90 0.70 0.12 0.084
Average 0.79 0.1405 0.11411
400 °C 0 0.77 0.2155 0.165935 0.24 better deep drawing ability than 350 °C and 450 °C annealed sam-
45 1.02 0.257 0.26214 ples. At low temperature ranges (270–350 °C), deep drawability is
90 0.79 0.23 0.1817 poor due to non-fully recrystallized structure. Grains which con-
Average 0.9 0.239875 0.2179 tain dislocations from deformed state cannot further deform in
450 °C 0 0.66 0.2382 0.1572 0.25 deep drawing process and lead to early failure. On the other hand,
45 0.94 0.2381 0.2238 at high annealing temperature grain growth cause non uniform
90 0.72 0.24 0.1728
Average 0.815 0.2386 0.1944
deformation of sheet and reduce formability. At optimum temper-
ature (about 400 °C) fully fine recrystallized microstructure
1598 M. Tajally, E. Emadoddin / Materials and Design 32 (2011) 1594–1599

4. Conclusion

The formability of 7075 aluminum alloy sheets via the limit


drawing ratio (LDR), Erichsen and tensile test after annealing at dif-
ferent temperatures was conducted.

1. The maximum strengths were observed in the 90° direction at


room temperature, and the elongation in the 45° direction
was greater than those in the other directions.
2. It is clear that sheets annealed at higher than 350 °C possess rel-
atively good stretchability and drawability. As a result, the
formability parameters improve by increasing annealing tem-
perature and hence formability of 7075 Al alloy could be
improved by annealing the sheets at temperatures ranges of
Fig. 6. Effect of annealing temperatures on limit drawing ratio (LDR value). 350–400 °C.
3. From the tensile test, it was observed that the sheets annealed
at 400 °C/5 min possess good ductility, the normal anisotropy r-
value, high average n-value. Also, the samples annealed at
400 °C proved a larger LDR value of 2.0 and a higher height of
drawn sheet equal to 7.95 mm at room temperature that indi-
cated the best formability as compared to sheets were annealed
in other temperatures.
4. The results of tensile behavior, the limit drawing ratio (LDR)
and Erichsen test were in agreement with together.

Acknowledgement

The authors are grateful to the Department of Material Engi-


neering of Semnan University for proving laboratory facilities for
Fig. 7. Effect of annealing temperatures on height of drawn sheet (Erichsen test). the research.

achieve best drawability parameters. It can be due to this fact that References
recrystallization is the formation of a new set of fine, strain free
[1] Heinz A, Haszler A, et al. Recent development in aluminum alloys for aerospace
and equaxed grains. Aluminum alloys with a fine and recrystallized applications. Mater Sci Eng A 2000;280(1):102–7.
microstructure deform by grain boundary sliding at low strain [2] Williams JC, Starke Jr EA. Progress in structural materials for aerospace
rates that lead to an enhanced formability [18,19]. systems. Acta Mater 2003;51(19):5775–99.
[3] Li JF, Peng ZW, et al. Mechanical properties, corrosion behaviors and
The LDR value was computed by using the ratio of D0/D1, where microstructures of 7075 aluminium alloy with various aging treatments.
D0 is the initial diameter of blank which can be drawn without cup Trans Nonferr Metal Soc China 2008;18(4):755–62.
rupture of diameter of D1 (punch diameter). The LDR values were [4] Woei-Shyan LS, Wu-Chung S, et al. The strain rate and temperature
dependence of the dynamic impact properties of 7075 aluminum alloy. J
measured equal to 1.8, 2 and 2 for annealing temperatures
Mater Process Technol 2000;100:116–22.
350 °C, 400 °C and 450 °C, respectively. Also, for annealing temper- [5] Lee NS, Chen JH, et al. Anisotropic tensile ductility of cold-rolled and annealed
ature 270 °C, the samples with the initial diameter of circle (D0) aluminum alloy sheet and the beneficial effect of post-anneal rolling. Scripta
equal to 57 mm and 60 mm failed that indicated poor deep draw- Mater 2009;60(5):340–3.
[6] Steglich D, Brocks W, et al. Anisotropic ductile fracture of Al 2024 alloys. Eng
ability. The samples annealed in 400 °C showed a larger LDR value Fract Mech 2008;75(12):3692–706.
of 2.0 and a higher r-value of 0.9 at room temperature that indi- [7] Narayanasamy R, Sathiya Narayanan C. Forming limit diagram for interstitial
cated the best drawability among other annealing temperatures. free steels: part I. Mater Sci Eng A 2005;399(1–2):292–307.
[8] Li Chunfeng, Liu Dahai, Yu Haiping, Ji Zhengbo. Research on formability of 5052
This value of LDR can be comparison with LDR value of 2.03 which aluminum alloy sheet in a quasi-static–dynamic tensile process. Int J Mach
has been reported for aluminum alloy 1050 [20]. Tool Manuf 2009;49:117–24.
[9] Narayanasamy R, Ravindran R, Manonmani K, Satheesh J. A crystallographic
texture perspective formability investigation of aluminum 5052 alloy sheets at
3.3.3. The Erichsen cupping test various annealing temperatures. Mater Des 2009;30:1804–17.
[10] Narayanasamy R, Ravi Chandran M, Parthasarathi NL. Effect of annealing on
The graph of the Erichsen test results are shown in Fig. 6. The formability of aluminum grade 19000. Mater Des 2008(8):1633–53.
height of drawn sheet for samples annealed at 270 °C, 350 °C, [11] Sowerby R, Duncan JL. Failure in sheet metal in biaxial tension. Int J Mech Sci
400 °C and 450 °C was equal to 4.4 mm, 7.0 mm, 7.95 mm and 1971;13:217–29.
[12] Ghosh AK. Strain localization in the diffuse neck in sheet metal. Metall Mater
7.2 mm, respectively (Fig. 7). The results showed that the sheets Trans 1974;B5:1607–16.
annealed at 400 °C have more formability. The sheet annealed [13] Stachwicz F. Effects of microstructure on the mechanical properties and limit
at 400 °C with fine recrystallized grain possessed more stretch- strains in uniaxial and biaxial stretching. J Mech Work Technol
1989;19:305–17.
ability than the sheets annealed at 270 °C which specified by cold
[14] Wu HY, Zhou GZ, et al. Mechanical properties and formability of an Mg-6%Li-
rolled microstructure. At high annealing temperature by coarsen- 1%Zn alloy thin sheet at elevated temperatures. J Mater Process Technol
ing of the grain size, the formability of material decreases [21]. 2008;206(1–3):419–24.
Refinement of grain size significantly improves the formability [15] ASTM standards, designation: E517-92a. Standard test method for plastic
strain ratio r for sheet metal. Annual book of ASTM standards; 2000.
primarily through increasing strain rate sensitivity of flow stress [16] Gavrus A, Banu M, et al. An inverse analysis approach of the Erichsen test
[22]. starting from a finite element model. Int J Mater Forum 2008(Suppl. 1):5–8.
M. Tajally, E. Emadoddin / Materials and Design 32 (2011) 1594–1599 1599

[17] Sakai T, Hamada S, Saito Y. Improvement of the r-value in 5052 aluminum [20] Ambrogio G, Filice L, Palumbo G, Pinto S. Prediction of formability extension in
alloy sheets having through-thickness shear texture by 2-pass single-roll drive deep drawing when superimposing a thermal gradient. J Mater Process
unidirectional shear rolling. Scripta Mater 2001;44:2569–73. Technol 2005;162–163:454–60.
[18] Edington JW, Melton KN, Cutler CP. Superplasticity. Prog Mater Sci [21] Furu T, Pedersen KO. The influence of grain structure and texture on
1976;21:63–170. formability and toughness of extruded aluminium alloys. Mater Sci Forum
[19] Del Valle JA, Pérez-Prado MT, Ruano OA. Symbiosis between grain boundary 2006;519–521:1421–8.
sliding and slip creep to obtain high-strain-rate superplasticity in aluminum [22] Yang Q, Ghosh AK. Formability of ultrafine-grain Mg alloy AZ31B at warm
alloys. J Euro Ceram Soc 2007;27(11):3385–90. temperatures. Metall Mater Trans A 2008;39(11):2781–96.

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