ACUMEN LAB

HACH Analysis Worksheet

Sample ID: nFDS0038/0110 (rep 1)

Parameter: Phosphorus
Date of analysis: 21/1/10
Analysis performed by: Yati

Analyte
Abs
standard / ppm
1 0.337
5 0.646
10 0.977
25 1.955

Intercept: 0.2944
Slope: 0.0668

Analyte in
Sample Final volume Dilution
Sample Abs sample
weight (g) (mL) factor
(mg/kg)
A 1.543 2.0076 100 1 742
B 1.002 2.198 100 1 482
C 1.318 2.0987 100 1 731
D 1.033 2.0659 100 1 535
E 2.132 2.1592 100 1 1275
F 1.989 2.0016 100 1 1268
blank 0.254

Calibration Curve Calibration Curve

2.5 12
Peak area
Peak area

10
2
f(x) = 0.0668 x + 0.2944
R²8= 0.9992
1.5
6

1 4

2
0.5
0
0 f(x)5= 0 10 15 20 25 30
0 R²concentration
= 0.00000 of analyte, ppm
0 5 10 15 20 25 30
concentration of analyte, ppm

Checked by
 HACH Analysis Worksheet

Sample ID: Refer Below

Parameter: Phosphorus

Company : ALPHA INDUSTRIES SDN BHD (JB)

Date of analysis: 9-Dec-15
Performed By: Sofea

Analyte
Abs - Blank Abs
standard / ppm

1 0.099 0.155
5 0.492 0.548
10 0.968 1.024
15 1.453 1.453

Intercept c: 0.0049
Slope x: 0.0965

Calibration Curve
1.600
1.400 f(x) = 0.0965 x + 0.0049
1.200 R² = 1.0000
1.000
0.800
0.600
0.400
0.200
0.000
0 2 4 6
Concentration 8 analyte, ppm
of 10 12 14 16

Conc. Analyte in
Sample Final volume Dilution
Sample Abs calculated sample Average
weight (g)/mL (mL) factor
from curve (mg/kg)
nCML0023/1215 0.080 0.5144 100 1 0.198 38.522 39

nCML0024/1215 0.079 0.5034 100 1 0.188 37.306 37

nCML0025/1215-1 0.122 2.0304 100 1 0.633 31.188

32
nCML0025/1215-2 0.124 2.0512 100 1 0.654 31.882

blank 0.056

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 HACH Analysis Worksheet

Sample ID:
Parameter:

Company :
Date of analysis:
Performed By:

Analyte
Abs - Blank Abs
standard / ppm

0.0 0.000 0.015

5 0.183 0.198
10 0.343 0.358
20.0 0.653 0.668
30.0 0.960 0.975
40.0 1.361 1.376
Intercept c: 0.0154
Slope x: 0.0317

Calibration Curve
1.200

1.000
f(x) = 0.0317 x + 0.0154
0.800 R² = 0.9992

0.600

0.400

0.200

0.000
0.0 5.0 10.0 15.0
Concentration 20.0 ppm
of analyte, 25.0 30.0 35.0

Conc. Analyte in
Sample Final volume Dilution
Sample Abs calculated sample %
weight (g)/mL (mL) factor
from curve (mg/kg)
50-1 0.612 0.1329 100 1000 18.334 137953.785 13.795

50-2 0.542 0.1180 100 1000 16.127 136672.004 13.667

51-1 0.518 0.1286 100 1000 15.371 119523.270 11.952

51-2 0.502 0.1325 100 1000 14.866 112198.414 11.220

52-1 0.425 0.1268 100 1000 12.439 98098.202 9.810

52-2 0.418 0.1299 100 1000 12.218 94058.321 9.406

53-1 0.356 0.1298 100 1000 10.264 79072.539 7.907

53-2 0.354 0.1254 100 1000 10.201 81344.221 8.134

54-1 0.284 0.1220 100 1000 7.994 65522.981 6.552

54-2 0.292 0.1254 100 1000 8.246 65757.616 6.576

55-1 0.203 0.1442 100 1000 5.440 37727.221 3.773

55-2 0.203 0.1342 100 1000 5.440 40538.489 4.054

Blank 0.015 -0.486

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 HACH Analysis Worksheet

Sample ID: Refer Below

Parameter: Phosphorus

Company : TROPICAL CONSOLIDATED CORP. SDN. BHD

Date of analysis: 6-May-15

Analyte
Abs - Blank Abs
standard / ppm

1 0.114 0.180
5 0.491 0.557
10 1.028 1.094
15 1.473 1.473
20 2.009 2.009
30 3.003 3.069

Intercept c: 0.0061
Slope x: 0.0998

Calibration Curve
3.500
3.000
f(x) = 0.0998 x + 0.0061
2.500 R² = 0.9997
2.000
1.500
1.000
0.500
0.000
0 5 10 15
Concentration 20 ppm
of analyte, 25 30 35

Analyte in
Sample Final volume Dilution Conc. calculated
Sample Abs sample Average
weight (g)/mL (mL) factor from curve
(mg/kg)
FDS0224/0415-1 1.039 2.0480 100 1 9.691 473.202
470
FDS0224/0415-2 1.009 2.0074 100 1 9.390 467.794

FDS0225/0415-1 1.062 2.1296 100 1 9.922 465.896

458
FDS0225/0415-2 1.052 2.1858 100 1 9.821 449.332

FDS0226/0415-1 0.849 2.0373 100 1 7.787 382.211

400
FDS0226/0415-2 0.909 2.0086 100 1 8.388 417.613

blank 0.066

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