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60 mL H2NO3
Watertown For carbon and stainless steels, 50 mL H2O Use at 71–82 °C (160–180 °F) for
arsenal general structure 10–60 min. Use with cut or ground
12 mL H2SO4 surfaces.
38 mL HCl
Dilute aqua For high-alloy steels and iron- 25 mL H2O Time: 10–15 min at room
regia cobalt high-temperature alloys temperature
25 ml HNO3
50 mL HCl
Piearcy and co- Maraging steel macrostructure 60 mL lactic Use at room temperature.
workers acid
20 mL HNO3
10 mL HCl
Burg and Weiss Nitriding steels macrostructure 85 mL H2O Use at 71 °C (160°F) for 10 min.
15 mL
ammonium
persulfate
Marble's General etch for austenitic stainless 50 mL H2O Solution can be heated.
reagent steel
10 g CuSO4
50 mL HCl
Miller and Welds and general macrostructure 90 mL H2O Use electrolytically with polished
Houston of austenitic stainless steel surface. Platinum or stainless steel
10 g CrO3 cathode. Use at 16–38 °C (60–100
°F), 6 V, for 2–7 min.
Loria As-cast structure and grain size in 20 mL H2O Use at room temperature.
(nitrosulfuric cast steels
acid etch) 20 mL HNO3
10 mL H2SO4
Nielsen Stress-corrosion cracks in austenitic 95 mL methyl Use at room temperature for
stainless steel alcohol approximately 1 h. Crack pattern
vividly revealed
5 mL bromine
Table 8 Major microstructure etchants for common phases and constituents in ferrous materials