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Abstract: This paper presents detailed microscopic analyses of the surface roughness, roundness, and sphericity of sands. The surface
roughness of three silica sands was studied using the optical interferometry approach. It was statistically characterized by a set of
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parameters. Optical interferometry yielded very accurate measurements of surface roughness of the three sands. It was found that, as the
surface roughness increases, the friction and dilatancy angles of the sand increase. In addition, two new indices for particle roundness and
sphericity are introduced, compared with the Powers classification, and used to classify the investigated sands.
DOI: 10.1061/共ASCE兲0887-3801共2004兲18:1共36兲
CE Database subject headings: Surface roughness; Shape; Sand; Granular materials; Friction; Microscopy; Digital techniques.
Surface Roughness Measurements specific coordination is measured based on the phase data 共i.e.,
pixel value兲 and the wavelength of the source light. Based on the
white light reflection at the surface and on the reflected wave-
Materials and Methods
length, the height of every single point 共pixel兲 on the sand particle
The surface roughness of three different sizes of silica sand was surface can be measured using the WOI in the VSI mode. The
measured using an optical surface profiler called the Wyko optical resolution of the system in the VSI mode was 3 nm; the system
interferometer 共WOI兲 manufactured by the Veeco Metrology was calibrated using known standards traceable by the National
Group 共1999兲. It is a noncontact optical profiler that uses two Institute of Standards and Technology 共NIST兲.
technologies to measure a wide range of surface heights 共rough- Three sands were used in this study to represent fine-,
ness兲. Figs. 2 and 3 show a schematic and digital photographs of medium-, and coarse-grained silica sands with different surface
the WOI, respectively. It has two operating phases: the phase roughness and shapes. The fine-grained sand is uniform silica
shifting interferometry 共PSI兲 mode allows measurements of 共quartz兲 sand with mean particle size (d 50) of 0.22 mm. It was
smooth surfaces and steps, while the vertical scanning interferom- obtained from the Ottawa Industrial Silica Company and is com-
etry 共VSI兲 mode measures rough surfaces and steps up to milli- monly denoted as F-75 Ottawa sand 共banding sand, herein labeled
meters high. In this study, the VSI mode was used since it gives as F sand兲. The medium-grained sand 共herein labeled as M sand兲
better resolution for the three sands used in the investigation. In was obtained from Unimin Corporation. It is industrial uniform
the VSI mode, a white light source is used since it works best for white quartz sand termed grade no. 30 with 0.55 mm mean par-
vertical scanning interferometry. The height of the surface at a ticle size. The third sand is crushed silica sand obtained from the
Connecticut Silica Company 共herein labeled as C sand兲 with
mean particle size of 1.6 mm.
Table 1. Roundness Grades According to Russell and Taylor and
Pettijohn Classifications 共Powers 1953兲
Russell and Taylor Pettijohn Table 2. Powers Roundness Classification 共Powers 1953兲
Arithmetic Class Geometric Classification Class intervals Geometric mean
Classification Class limit midpoint limit midpoint
Very angular 0.12–0.17 0.14
Angular 0–0.15 0.075 0.0–0.15 0.15 Angular 0.17–0.25 0.21
Subangular 0.15–0.3 0.225 0.15–0.25 0.20 Snbangular 0.25–0.35 0.30
Subrounded 0.30–0.50 0.40 0.25–0.40 0.315 Subrounded 0.35–0.49 0.41
Rounded 0.50–0.70 0.60 0.40–0.60 0.50 Rounded 0.49–0.70 0.59
Well rounded 0.70–1.0 0.85 0.60–1.0 0.80 Well rounded 0.70–1.0 0.84
Samples of the three sands were randomly mounted on thin as illustrated in Fig. 4共a兲. The WOI is supplemented with com-
glass slides and then gold coated. Particle gold coating is essential puter software called Vision 32 关Fig. 4共b兲兴, in which a series of
in scanning electron microscopy 共SEM兲 and VSI because it mathematical algorithms are executed for each scan to estimate
causes electron beam and light reflection for better image viewing different roughness indices. The reference mean line is taken au-
in both systems. A total of 120 particles for each of the sands tomatically, and the overall roughness is given according to the
were scanned. They were arbitrarily selected from each slide. To image taken for each particle. This approach was not used in our
avoid errors due to the particles’ surface curvature and edges only, study since particle edges are included in the calculations, and
the center part of each particle is used in roughness calculations thus sharp edges will show up, causing a sudden drop or rise in
Fig. 4. 共a兲 Illustrative image of sand particle captured using Wyko optical interferometer method; 共b兲 particle surface roughness measurements
acquired using Vision 32 software
Fig. 6. Scanning electron microscopy images of the three sands at different magnification levels
Rq⫽ 冑 1
M N i⫽1
M
兺 j⫽1
兺 Z 2i j
N
(3) Fig. 7. Typical optical microscope profiler images for the sands used
in the investigation
This index represents the standard deviation of the surface
heights. R q has the same disadvantage as R a . The only advan- • In addition, SEM images were taken of the same sands to look
tage of R q compared to R a is due to the fact that the heights at the surface at high magnification and see the roughness of
are squared here, and thus the valleys and peaks have more the grain surface 共Fig. 6兲. To some extent, the SEM images
significance in R q . showed good uniformity in the surface roughness for each of
• The maximum profile peak height (R p ) is the distance be- the three sands.
tween the highest point of the surface and the mean surface for
the entire data set. Therefore, it represents the peak value for
the surface. Results
• The maximum profile valley depth (R v ) is the distance be- As mentioned earlier, 120 particles were randomly selected and
tween the lowest point of the surface and the mean surface for analyzed to quantify surface roughness. The ASCII files that con-
the entire data set 共i.e., it measures the depth of the valley of a tain the scan results were exported to MathCad software for fur-
given surface兲. ther analysis and calculations, including calculating the roughness
• The maximum height of the surface (R t ) is the vertical dis- indices defined in the previous subsection and generating 3D ren-
tance between the lowest and highest points on the surface derings of the particles’ surface profiles 共Fig. 7兲. Tables 3–5 give
a statistical summary of the analyses conducted on F, M, and C
Rt⫽Rp⫹Rv (4) sands, respectively. Furthermore, Fig. 8 shows the frequency dis-
• Skewness (R sk) measures the asymmetry of the surface about tribution of the average surface roughness (R a ) and the root mean
the mean plane; it is the mean-cubed roughness square roughness (R q ) for the three sands used in the investiga-
M N tion. Comparing the statistical summaries of the three sands, one
1
Rsk⫽ 兺 j⫽1
兺 Z 3i j
M NR 3q i⫽1
(5)
can see that the statistical parameters for R q are slightly higher
than those for R a for each of the three sands. Furthermore, the
mean values for R a and R q are 0.8487 and 0.9815 m for the F
The advantage of this index is that, if two different surfaces sand, respectively, compared to 0.9460 and 1.0822 m for the M
have the same R a and R q values, one can distinguish between sand, and 1.1169 and 1.2383 m for the C sand. Fig. 8 shows that
them using the skewness. Valleys in the surface will yield the frequency distributions for R a and R q differ slightly from each
negative R sk whereas peaks will give positive ones. other for the same sand and their standard deviations are ⬃0.55–
• Kurtosis (R ku) measures the peakedness of the surface about 0.61 m for the F sand, ⬃0.61–0.67 m for the M sand, and
the mean plane. R ku is calculated using the following expres- ⬃0.50–0.52 m for the C sand.
sion: A series of biaxial 共plane strain兲 experiments were performed
on the three sands using prismatic specimens that measure 83.3
1
M N wide⫻80.8 long⫻152.4 high. Loose 共relative density D r
Rku⫽ 兺兺
M NR 4q i⫽1 j⫽1
Z 4i j (6) ⫽39– 66%) and dense specimens (D r ⫽88– 100%) were tested
under 15 and 100 kPa confining-pressure conditions 关see Alshibli
It is mostly used for machined surfaces. R ku will register high and Sture 共2000兲 for more details about the experiments兴. Fig. 9
values when a high proportion of the surface falls within a shows the relation between surface roughness 共represented by the
narrow range of heights. mean R a value兲 and peak friction angle ( p ) and dilatancy angle
共兲. Some of the specimens did not reach the critical state, which ness increases for all cases. Furthermore, dense specimens have
made it difficult to calculate the critical state friction angle; there- higher p and values compared to loose specimens tested under
fore, peak friction angles were used in the analysis. It is well the same confining pressure. p and values are also higher for
known that the frictional resistance of granular materials is specimens tested at low confining pressure 共15 kPa兲 compared to
mainly attributed to interparticle sliding resistance and particle those with similar densities tested at high confining pressures
rearrangements/interlocking 共dilatancy effects兲. Higher peak fric- 共100 kPa兲. Finally, it seems there is a consistency in the trend of
tion angles are expected when sand specimens are tested under the rate of increase of p with surface roughness 共i.e., the slope
biaxial loading conditions compared to conventional triaxial com- and shape of the curve兲 for specimens tested at the same confining
pression. Fig. 9 shows that p and increase as surface rough- pressure value.
Fig. 8. Frequency distribution of R a and R q for the sands used in the investigation
SP⫽ 冑
3
d L2
d sd I
(8)
355
Fig. 9. Effect of surface roughness on friction and dilatancy angles 兩 R ⫺R EE 兩
AI⫽ 兺
⫽5 R EE
(11)
Mean 275,247.6 454.52 753.56 2,076.52 661.31 3.5608 1.0239 0.6902 1.0878 0.6565
Median 239,205 430.00 727.00 1,973.00 628.34 0.7573 0.8999 0.6376 1.1207 0.6038
Root mean square 291,080.7 473.61 766.74 2,140.23 681.60 14.235 1.1984 0.7398 1.107 0.8645
Standard deviation 96,645.44 135.86 144.48 529.005 168.47 14.067 0.6356 0.2717 0.212 0.5741
et al. 共2001兲 proposed correlations for the rutting resistance of polygon, circle, cross hair, etc.兲 and performing the measurement
asphalt using the FI, AI, and TI. The rutting resistance was mea- on the selected particles. Then I sph and I R values were calculated
sured using the Purdue wheel-tracking device 共PURWheel兲, and and the results of the analysis are shown in Fig. 1, which shows
strong correlation was found between these indices and the resis- that I R ranges from 1.0 for well-rounded particles to greater than
tance. Matsushima and Konagai 共2001兲 studied the grain-shape 1.5 for very angular particles, and I sph ranges from 0.0 for diskoi-
effect on the peak strength of granular materials using the discrete dal particles to greater than 1.0 for prismoidal particles.
element method. In their study they concluded that the shape does Scion Image Analysis Software was also used to measure the
not affect the strength at the same void ratio where the surface areas, perimeters, and the shortest and longest axes of 25 particles
roughness is dominant here; they verified the result using real of each of the three sands. High-resolution SEM images were
sands. Brezezicki and Kasperkiewicz 共1999兲 proposed a method used to make the measurements. The equivalent circular diameter
for automatic characterization of the shape of coarse particles for each particle was then calculated. The equivalent diameter
based on an image analysis technique. Ghalib and was considered to be the mean axis length as well. Due to the fact
Hryciw 共1999兲 proposed an imaging and watershed analysis that the SEM images were taken for the particles as is 共no flush-
method to determine the soil particle distribution. Yudhbir and ing was done兲, more than five particles were available in the
Abedinzadeh 共1991兲 used an image analyzer to quantify the shape image and it was not easy to separate them. Then a free-hand
of particles. They used Eq. 共8兲 to measure the particle sphericity. drawing tool of SIAS was used to trace the perimeter of each
In this paper, two new indices are introduced to define the particle and the measurements were made based on the features
sphericity and roundness of particles. The sphericity index (I sph) available in this software 共Fig. 10兲. The shape/roundness factors
is defined as discussed and defined above were calculated and Tables 6 – 8 list
兺冏 冏
N statistical summaries of the analysis. Based on the classification
1 D equ共 i 兲 D equ共 i 兲 proposed by the authors (I R and I sph) the F sand mainly consists
I sph⫽ ⫺ (12)
N i⫽1 d s 共 i 兲 d L共 i 兲 of spherical well-rounded particles whereas the M and C sands
consist of subprismoidal rounded particles.
where D equ⫽equivalent particle diameter 共perimeter/兲; and d s
and d L are as defined before. The roundness index (I R ) is defined
as follows:
Conclusions
N
1 P act共 i 兲
I R⫽ 兺
N i⫽1 关共 d s 共 i 兲 ⫹d L 共 i 兲 兲 /2兴
(13) Surface roughness was accurately quantified for three silica sands
using the optical interferometry approach. Roughness parameters
where P act(i) ⫽actual perimeter of the particle. Particles listed in were defined and calculated for representative samples of the
Powers’ chart 共Fig. 1兲 were scanned and converted to image for- three sands used in the study. It was found that, as the surface
mat. Scion Image Analysis Software (SIAS) has drawing tools roughness increases, the friction and dilatancy angles increase.
that enable one to manually measure the parameters in Eqs. 共12兲 The new roundness and sphericity parameters seem to accurately
and 共13兲 共Fig. 10兲 simply by choosing the proper tool 共i.e., line, classify the shape and sphericity of granular particles.