Professional Documents
Culture Documents
Standard Procedures
for Calibrating
Magnetic Instruments
to Measure the Delta
Ferrite Content of
Austenitic and Duplex
Ferritic-Austenitic
Stainless Steel
Weld Metal
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Words-
Key Instrument calibration, delta ferrite, ANSIIAWS
A4.2M/A4.2:1997
stainless steel weld
metal, austenitic An American
National
Standard
stainless weld metal, duplex stainless
weld by Approved
American National Standards Institute
November 6,1997
Prepared by
AWS Committee on Filler Metals
and The Welding Research Council
Subcommittee on Welding Stainless Steels
Approved by
AWS Board of Directors
Abstract
Calibration procedures are specified for a number of commercial instrumentsthat can thenprovide reproduciblernea-
surements of the ferrite content of austenitic stainless steel weld metals. Certain of these instruments can be further cali-
brated for measurements of the ferrite content of duplex ferritic-austenitic stainless steel weld metals. Calibration with
primary standards (nonmagnetic coating thickness standards from the U.S. National Institute of Standards and Technol-
ogy) is the preferred method for appropriate instruments. Alternatively, these and other instruments can be calibrated
with weld-metal-like secondarystandards.
Reproducibility of measurement after calibration is specified. Problems associated with accurate determination of
ferrite content are described.
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Personnel
AWS Committee on Filler Metals
R. A. LaFave, Chair ElliottCompany
J. I! Hunr, Ist Vice Chair Consultant
D. A. Fink, 2ndVice Chair The Lincoln Electric Company
H. M. Woodward,Secretary AmericanWelding Society
B. E. Anderson AlcoTec Wire Company
*R. L. Barernun ElectromanufacturasS A
R. S. Brown CarpenterTechnologyCorporation
R.A. Bushey ESAB Weldingand CuttingProducts
J. Caprurola, Jr. Consultant
*L. J. Chrisrensen Consultant
R. J. Christoffel Consultant
D.J. Crement Precision Components Corporation
D. D.Crockerr The Lincoln Electric Company
R. A. Daemen Consultant
D. A. DelSignore Consultant
R. L. Drury III Caterpillar, Incorporated
H. M! Ebert Exxon Research and Engineering Company
J. G.Feldstein Foster Wheeler Energy International
S.E. Ferree ESAB Welding and Cutting Products
L. Flasche Haynes International, lncorporated
C. E. Fuerstenau Alloy Ring Service
G.A. Hallstrom, JI: Hallstrom Consultants
R. B. Kadiyala TechalloyCompany
D.J. Kotecki The Lincoln Electric Company
D.Y Ku American Bureau of Shipping
N. E. Larson Compressed Gas Industries
A. S.Laurenson Consultant
J . S.Lee Chicago BridgeandIron Company,Incorporated
G. H. MacShane MAC Associates
U! A. Marttila Chrysler Corporation
R. Menon Stoody Company
M. T Merlo Select Arc, Incorporated
A. R. Merres Ampco Metal, Incorporated
M.D.Morin ABB Power Generation
C.L. Null Naval SeaSystemsCommand
*Y Ogata Kobe Steel Limited - WeldingDivision
J. J.Payne Consultant
R. L. Peaslee Wall Colmonoy Corporation
E. W Pickering, Jr. Consultant
M. A. Quintana T h e Lincoln Electric Company
*H. E Reid Consultant
*S.D.Reynolds, Jr. Consultant
L. E Roberts Canadian Welding Bureau
Z? K. Salvesen Det Norske Veritas (DNV)
*Advisor
...
111
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AWS Committee on Filler Metals (Continued)
J. M. Suwhill, Jr. Newport News Shipbuilding
A. F? Serdler Armco Steel Company
U! S. Severance ESAB Welding and Cutting Products
*W A. Shopp Editorial Consultant
M.S. Sierdzinski ESAB Welding and Cutting Products
*R. G. Sim The Lincoln Electric Company (Australia)
E. R. Stevens Fisher Controls International, Incorporated
*R. U! Straiton Bechtel Corporation
R. A. Sulit Digital Systems Research
R. A. Swain Euroweld, Limited
R. D. Thomas, JK R. D. Thomas and Company
K. I? Thornberry J. W. Harris Company, Incorporated
*R. limerman Conarco SA
*S. Tsutsumi Kobe Steel, Limited-Welding Division
G. J. Qtanovych Mobil Technology Company
T.R. Warren lngalls Shipbuilding, Incorporated
H. D. Wehr Arcos Alloys
* E J. Winsor Consultant
K. G. Wold Siemens Power Corporation .
iv
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S T D = A W S A'4.2M/A4-2-ENGL L997 E 07842b5 05137b5 7 9 0 111
Foreword
(This Foreword is nota part of ANSIIAWS A4.2M/A4.2:1997,Standard Proceduresfor Calibrating Magnetic Instru-
ments to Measure theDelta Ferrite Content of Austenitic and DuplexFerritic-Austenitic Stainless Steel Weld Metal, but
is included for information purposesonly.)
This document is a revision of the Standard Procedures for Calibrating Magnetic Instruments to Measure the Delta
Ferrite Content of Austenitic Stainless Steel Weld Metal, first published in 1974 and revised in 1986 and again in 1991.
This revision was by the Subcommittee on Welding Stainless Steel of the Welding Research Council and by the AWS
Committee on Filler Metals. Thecurrent revision is the first to use the SI system of measurement as the primary system,
and updates the standard in the light of new information.
A certain minimum ferrite content in most austenitic stainless steel weld metals is useful in assuring freedom from
microfissures and hot cracks. Upper limits on ferrite content in austenitic stainless steel weld metals can be imposed to
limit corrosion in certain media or to limit embrittlement due to transformation of ferrite to sigma phase during heat
treatment or elevated temperature service. Upper limits on ferrite content in duplex ferritic-austenitic stainless steel weld
metals can be imposed to help assure ductility, toughness, and corrosion resistance in the as-welded condition.
Reproducible quantitative ferrite measurements in stainless steel weld metals are therefore of interest to filler metal
producers, fabricators of weldments, weldment end users, regulatory authorities, and insurance companies.
Comments and suggestions for the improvement of this standard are welcome.They should be sent to the Secretary,
Committee on Filler Metals, American Welding Society, 550 N.W. LeJeune Road, Miami, FL 33126.
Official interpretations of any of the technical requirements of this standard may be obtained by sending a request, in
writing, to the Managing Director, Technical Services Division, American Welding Society. A formal reply will be
issued after i t has been reviewed by the appropriate personnel following established procedures.
V
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S T D - A W S A4*2M/A4*2-ENGL L777 07842b5 05137bb b27 m
Table of Contents
Page No .
...
Personnel .................................................................................................................................................................... 111
Foreword ................................................................................................................................................................... V
List of Tables ..............................................................................................................................................................
..
v11
List of Figures ............................................................................................................................................................ vii
I . scope ..................................................................................................................................................................... 1
2. Definitions ............................................................................................................................................................. 1
2.1 Delta Ferrite .................................................................................................................................................. 1
2.2 Draw Filing ................................................................................................................................................... 1
2.3 Ferrite Number (FN) ..................................................................................................................................... 3
2.4 Primary Standards......................................................................................................................................... 3
2.5 Weld-Metal-Like Secondary Standards........................................................................................................ 3
3. Calibration Methods ............................................................................................................................................. 3
3.1 Primary Standards......................................................................................................................................... 3
3.2 Secondary Standards..................................................................................................................................... 4
3.3 Range of Calibration for All Calibration Methods ....................................................................................... 4
4. Calibration of Magne-Gage-Type Instruments ..................................................................................................... 4
4.1 Calibration by Means of Primary Standards................................................................................................. 4
4.2 Calibration by Means of Weld-Metal-Like Secondary Standards................................................................ 8
5. Calibration of FeritscopeslFerritescopes............................................................................................................. 8
5.1 Calibration of Ferritescopes Model FE8-KF by Means of Primary Standards............................................. 8
5.2 Calibration by Means of Weld-Metal-Like Secondary Standards................................................................ 9
6. Calibration of Inspector Gages............................................................................................................................. 9
6.1 Calibration by Means of Primary Standards................................................................................................. 9
6.2 Calibration by Means of Weld-Metal-Like Secondary Standards................................................................ 9
7. Calibration of Other Instruments........................................................................................................................ 10
7.1 Calibration by Means of Primary Standards............................................................................................... 10
7.2 Calibration by Means of Weld-Metal-Like Secondary Standards.............................................................. 10
8. Use of Calibrated Instruments ............................................................................................................................ 11
8.1 Maintaining Calibration ............................................................................................................................... 11
8.2 Variations in Measurements........................................................................................................................ 11
9. Significant Figuresin Reporting Measurement Results ...................................................................................... 12
9.1 Calibration Data ........................................................................................................................................... 12
9.2 Measurement Data ...................................................................................................................................... 12
Annex
A l . Acknowledgment.............................................................................................................................................. 13
.
A2 Ways of Expressing Ferrite Content ................................................................................................................. 13
A3 . Cautions on the Use of Ferrite Number ............................................................................................................ 14
A4 . Standards for Instrument Calibration ................................................................................................................ 15
A5 . Effect of Ferrite Size, Shape and Orientation ................................................................................................... 15
.
A6 Instruments........................................................................................................................................................ 16
.
A7 Use of Calibrated Instruments......................................................................................................................... 20
AWS Filler Metal Specifications by Material and WeldingProcess .......................................................................... 23
A WS Filler Metal Specifications and Related Documents ......................................................................................... 25
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vi
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List of Tables
Table Page No .
1 Ferrite Numbers (FN) for Primary Standards Calibration of Instruments Using a Magne-Gage
No . 3 Magnet or Equivalent ........................................................................................................................... 2
2 Ferrite Numbers (FN) for Primary Standards for Ferritescope Model FE8-KF Calibration ......................... 3
3 Ferrite Numbers (FN) forPrimary Standards for Inspector Gage Calibration .............................................. 4
4 Maximum Allowable Deviation, Calibration Point to Calibration Curve, for Instruments
being Calibrated with Weld-Metal-Like Secondary Standards...................................................................... 5
5 Tolerance' on the Position of Calibration Points Using Primary Standards ................................................... 8
6 Maximum Allowable Deviation of the Periodic Ferrite Number (FN) Check for Feritscoped
Ferritescopes .................................................................................................................................................. 9
7 Maximum Allowable Deviation of the Periodic Ferrite Number (FN) Check for Inspector Gages............10
8 Maximum Allowable Deviation of the Periodic Ferrite Number (FN) Check for Magne-Gage-Type
Instruments................................................................................................................................................... 11
9 Expected Range of Variation in Measurements with Calibrated Magne-Gage-Type Instruments ..............11
10 Expected Range of Variation in Measurements with Calibrated FeritscopesFerritesopes ........................ 12
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List of Figures
Figure Page No.
Example of Calibration Lines for Two Magne-Gage Instruments. Each with a No . 3 Magnet
for Measuring the Delta Ferrite Content of Weld Metals up to 26 FN .......................................................... 6
2 Example of Calibration Lines for a Magne-Gage Instrument with a No . 3 Magnet for Measuring
the Delta Ferrite Content of Weld Metals up to 77 FN .................................................................................. 7
Al Magne-Gage-Type Instruments.................................................................................................................... 17
A2 Ferritescope Model FES-KF ........................................................................................................................ 19
A3 Inspector Gage ............................................................................................................................................. 19
A4 Ferrite Indicator (Severn Gage) ................................................................................................................... 20
A5 Foerster Ferrite Content Meter ..................................................................................................................... 21
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Standard Proceduresfor Calibrating
Magnetic Instruments to Measure the
Delta Ferrite Contentof Austenitic and Duplex
Ferritic-Austenitic Stainless Steel Weld Metal
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S T D - A W S A q - Z H / ? A 4 = 2 - E N G L 1 9 9077 8 4 2 6055 1 3 7 b393 b
A4.2WA4.2:I 997
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2
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Table 2
Ferrite Numbers (FN) for Primary Standards for
Ferritescope Model FE8-KF Calibration (See
5.1 .i)
Coating Thickness Coating Thickness Coating Thickness
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0.80 31.50 6.6 0.42 16.54 12.0 0.19 7.48 24.4
0.78 30.71 6.8 0.41 16.14 12.3 0.18 7.09 25.6
0.76 29.92 7.0 0.40 15.75 12.5
0.74 29.13 7.1 0.39 15.35 12.8
3
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S T D = A W S A4*2M/A4-2-ENGL 3997
07842b5
0533773 T94
Table 3
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Ferrite Numbers (FN) for Primary Standards for Inspector Gage Calibration*
Coating Thickness Coating Thickness Coating Thickness
3.2 Secondary Standards dards can only be calibrated using secondary standards.
Refer to Section 7, Calibration of Other Instruments, for
33.1 Calibration by means of primary standards is the proper calibration instructions.
preferred method of maintaining calibration of appropri-
ate instruments. But the need for frequent in-process 3.3 Range of Calibration for All Calibration Meth-
checks is recognized along with the fact that primary ods. For all calibration methods and instruments, the
standards are not necessarily “durable” for frequent use range of calibration is defined by the interval of FNs be-
outside of a laboratory environment. Therefore,it is rec- tween and including the lowest F N standard and the
ommended that a set of secondary standards be used for highest F N standard used in developing the calibration
frequent in-process checks (see Annex 4.2). according to the corresponding procedure.
4
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S T D * A W S A v - Z f l / A q = Z - E N G L L917 = 07842b5 05L3772 9 2 0 A4.2M/A4.2:1997
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STD-AWS A'I=Zt'l/Aq=Z-ENGL L977 0 7 B W b 5 0533773 Bb7
A4.2M/A4.2:1997
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4
s
U
12 8 O 4 20 24
FERRITE NUMBER
NOTE: A different setof coating thickness standardswas used for each instrument, although thesets included the
same standard numbers.
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STD-AWS Aq*2M/A4*2-ENGL1797 E 07842b5 0513774 7T3 M
A4.2M/A4.2:1997
Coating Thickness
NlST SRM 0.001 in. I mm Counterweight, g FN White Dial
117.5
1362a 0.141 5.55 7.001 34.0 82.5
16.5
3.10 0.079 50.7
142.5
1359 1.W 15.002 0.048 68.9 74.5
1362a 1.58 0.040 76.8 37.0
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S T D O A W SA 4 * 2 M / A 4 - 2 - E N G L 3997 0 7 8 4 2 b 5 0533775 b 3 T
If the calibration lines are not essentially parallel, the tion utilizing secondary standards is acceptable? Four or
data shallbe restudied for errors. more such standards are required for calibration Lurves
for O to 15 FN; and four or more are required for any
4.1.6 A “best fit” straight line shallbe drawn through range of approximately 30 FN above 15 FN. In all cases,
the points plotted in accordance with 4.1.5. Alternatively, the Ferrite Numbers of the standards shall be well dis-
a regression equation shallbe fit to the data collected as tributed over the range of interest (see Annex A4.2).
described in 4.1.4. Magne-Gages tested to date have pro-
duced a straight line up to at least 10 FN. Most yield a 4.2.2 It should be recognized that weld-metal-like
straight line through all points, but some have shown a secondary standards are unlikely to provide readings
slight bend. An example of each is shown in Figure 1. from point to point that are as uniform as those from pri-
For acceptable calibration,all points must fall within the mary standards. Care must therefore be exercised to take
maximum allowable deviations shown in Table 5. If any readings on secondary standards in precisely those loca-
of the calibration points fall outsideof the allowed varia- tions used in assigning the original FNs to the standards.
tions, the data shallbe restudied, or the manufacturer of In case of doubt, the producer of the secondary standards
the instrument shallbe consulted, or both. should be consulted.
4.2.3 Other than the departures noted in 4.2.1 and
4.1.7 Two common sources of discrepant readings 4.2.2, the remainder of the calibration procedure with
during calibration (as well as during measurement) are secondary standards shall be the same as that used with
mechanical vibrations and dirt (usually magnetic parti- primary standards asgiven in 4.1.2 through 4.1.8.
cles) clinging to the magnet. Either factor tends to pro-
duce premature detachment of the magnet from the
sample, with a correspondingly low FN determination 5. Calibration of Feritscopes6/
(high white dial reading). A vibration-free environment Ferritescopes
is essential for accurate FN determination, especially
above 15 FN. Wiping the magnet end with a clean lint- 5.1 Calibrationof Ferritescopes Model FES-KF by
free cloth is suggested when dirt is encountered. In case Means of Primary Standards
of doubt, examination of the magnet end under a micro- 5.1.1This instrument is calibrated to the FN scale by the
scope is appropriate. manufacturer, but calibrationshould be verified by the user.
The only Ferritescope which can be calibrated with pri-
4.1.8 The graph plotted as in 4.1.6, or a regression mary standards according to Table2 is the pre-1980 Model
equation fit to it, may now be used to determine the FNs FE8-KF with analog readout and dual-contact “normal-
of stainless steel weld metals from the white dial read- ized” probe. No tables for calibrationwith primary stan-
ings of the instrument obtained on those weld metals dards are available for post-1980 instruments (thosewith
with the same No. 3 magnet and counterweight, if used. digital readouts orsingle-pole probes). Other Ferritescopes
and the current models identified as Ferritescope may be
4.2 Calibration by Means of Weld-Metal-Like Sec-
calibrated by weld-metal-like secondary standards as de-
ondary Standards
scribed in Section 7, Calibration of Other Instruments.
4.2.1 Calibration by primary standards is the recom- 5.1.2 The manufacturer’s instructions with regard to
mended method, as previously mentioned, but calibra- the use of the instrument and the adjustments of the scale
shall be followed.
5.13 The FNs shall be assigned from Table 2 to each
of the available primary standards as defined in 2.3. For
thicknesses between those given in the table, the FNs
Table 5 shall be interpolated as closely aspossible. Eight or more
Tolerance on the Positionof thickness standards shallbe used, with nominal thickness
Calibration Points Using Primary Standards corresponding to Ferrite Numbers well distributed in the
range O to 25 FN (see Annex A4.1). The instrument read-
Maximum Allowable ing for each of the available primary standards shallthen
Range
Number
Ferrite Deviation
be determined.
o to 5 *Oo.40
over 5 to 10 ?OS0
over 10 to 15 *.70 5. Weld-metal-like secondary standards are commercially sold
over 15 to 20 20.90 byTheWeldingInstitute,Abington Hall, Abington, Cam-
over 20 to 30 21 .o0 bridge, CBl 6AL, UK.
over 30 to 90 55% of assigned FN 6. Trademark of Helmut Fischer GmbH and Company
8
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W 078q2b5 051377b 5 7 5 E
A4.2MlA4.2:1997
5.1.4 The instrument readings shall be plottedon Carte- scale. The latter is preferable becausL it has smaller divi-
sian coordinates paper versus the FN assigned from Table sions (see Annex A6.3).
2 for each primary standard. A “best fit” line shall be
6.1.2 The manufacturer’s instructions with regard to
drawn through the data. Alternatively, a regression equa-
the use of the instrument and adjustments of the scale
tion shall befit to the data collected as described in 5.1.3.
shall be followed.
5.1.5 For approved calibration, all readings shall fall
6.13 The FNs shall be assigned from Table 3 to each
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Table 6
Maximum Allowable Deviationof the Periodic
Ferrite Number (FN) Check for Feritscopes/Ferritescopes
Maximum Allowable Deviation of the Periodic Ferrite Number Check
From the Ferrite Number From the Ferrite Number From the Ferrite Number
Value Assigned to the Value Assigned to the Value First Assigned to the
Primary Standard Secondary Standard Secondary Standard
Table in Range
Number
Ferrite User the 2 by Seller the by
o to 5 20.40 20.40 20.20
over 5 to 10 20.40 20.40 20.20
over 10 to 15 20.70 20.70 20.20
over 15 21.0 21.0 20.30
9
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~
Table 7
Maximum Allowable Deviationof the Periodic
Ferrite Number (FN) Check for Inspector Gages
Maximum Allowable Deviation of the Periodic FerriteNumber Check
From the Ferrite Number From the Ferrite Number From the Ferrite Number
Value Assigned to the Value Assigned to the Value First Assigned to the
Primary Standard Secondary Standard Secondary Standard
Range
Number
Ferrite in Table 3 Seller the by by the User
--`,,,`,`,``,,,,`,``,,`,,``,-`-`,,`,,`,`,,`---
o to 5 20.40 S.40 20.20
over 5 to 10 20.40 50.40 50.20
over 10 to 15 20.70 50.70 50.20
over 15 21.0 fl.O 20.30
6.2.2 Section 7.2 should be referred to for instructions ibration over any given range, while four calibration
to calibrate the Inspector Gage to weld-metal-like sec- ranges are possible. Then for checking the calibration
ondary standards. over a given range againstthe requirements of Table 4,
there must be at least four secondary standards, as re-
quired above, within the given calibration range, and
check measurements on all of them must satisfy the
7. Calibration of Other Instruments requirements of Table 4 for acceptable calibration over
7.1 Calibration by Means of Primary Standards. As that range. In all cases, the Ferrite Numbers of the sec-
of this revision of this standard (see 3.1) only Magne- ondary standards shall be well distributed over the range
Gage-type instruments, Ferritescopes Model FE8-KF of interest.
with normalized probes, and Inspector Gages,can be cal-
7.2.3 Instrument readings shall be determined for
ibrated to this standard by means of primary standards.
each of the available secondary standards and, if possi-
All other instruments must be calibrated by means of
ble, for a zero point. When taking readings on secondary
weld-metal-like secondary standards(see Annex A6.4).
standards, the same precaution noted in 4.2.2 should be
7.2 Calibration by Means of Weld-Metal-Like Sec- taken.
ondary Standards
7.2.4 Instrument readings shall be plotted against as-
7.2.1 Other instruments can be calibrated by weld- signed secondary standardFN values on Cartesiancoor-
metal-like secondary standards to produce a satisfactory dinate paper, and the zero point can be included if
correlation between the instrument readout and weld applicable.
metal FN. While it may be desirable that the instrument 7.2.5 A “best fit” smooth line, or a regression equa-
readout be precisely the calibrated value of FN it is not tion line, shall be drawn through the points plotted in
essential, provided a unique correlation between the in- 7.2.4. For acceptable calibration, no data pointmay vary
strument readout and weld metal FN, can be determined. from the curve any more than the allowable deviations
Such instruments may be used if they have been cali- shown in Table 4. If any point falls outside of the appro-
brated using secondary weld metal standards to which
priate allowed deviation, the data shall be restudied, or
FNs were assigned by an instrument with primary stan-
the manufacturer of the instrument shall be consulted, or
dard calibration. both.
7.2.2 Four or more such secondary standards are re- 7.2.6 The graph plotted as in 7.2.4, o r a regression
quired for calibration curves covering O to 15 FN; eight equation fit to it, may now be used to determine the FNs
or more such secondary standards are required for cali- of stainless steel weld metals overthe calibration range.
bration from O to 30 FN; and four or more such second-
ary standards are required for calibration of any interval 7.2.7 It is the responsibility of the user to ensure that
of approximately 30 FN above 15 FN. Some Feritscopes the instrument is properly calibrate& ¡.e., such that the
accept only a smaller numberof secondary standards in results obtained with weld-metal-like secondary stan-
setting a calibration. For example, the Model MP-3 can dards in the FN range(s) of use are within the expected
only acceptthree secondary standardsfor setting the cal- range of variations shown in Table 4.
10
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S T D - A U S A'I=ZM/Aq.2-ENGL 3797 E 078'Y2b50533778 349 I
I
8. Use of Calibrated Instruments this curve within the maximum deviations of Tables 4,5,
6 , 7, or 8, it must be :ecalibrated in accordance with this
document.
8.1 Maintaining Calibration. Instruments must be
checked periodically on a regular basis against primary 8.2 Variations in Measurements. Based upon round-
or secondary standards to ensure and verify the mainte- robin tests within the Welding Research Council Sub-
nance of the original calibration. Records of such checks committee on Welding Stainless Steels, the FNs deter-
shall be maintained. It is the responsibility of the user to mined by these instruments are expected to fall within
check at a frequency which is adequate to maintain cali- the limits shown in Table 9, 10, or 11 as compared to the
bration. For frequently used instruments, a weekly cali- overall average FN values of stainless steel weld metals
bration check is recommended. For infrequently used checked on other instrumentsof the same type calibrated
instruments, a calibration check before each use is rec- to this standard. When measurements are made with a
ommended. Two standards, one near each extremeof the variety of calibrated instrument types, somewhat larger
calibration range being checked,shall be used for each of variation in measurements than those indicated in Table
the ranges shown in Tables 4, 6, 7, or 8, as appropriate, 9, 10, or 11 might be expected, but the magnitude of the
for which the instrument is used. When the instrument no variation has not been determined.
longer produces values within the maximum deviation Weld ripples and other surface perturbations must be
specified in the relevant table, it shall be removed from removed because surface finish affects measurement ac-
service and the manufacturer shall be consulted (see curacy. Up to about 20 FN,the practice known as draw
Annex A3.2). filing produces acceptable accuracy (see 2.2). For accu-
A calibration curve may be made for an individual in- rate and reproducible ferrite measurements, above 20
strument using reference material other than the stan- FN, a Magne-Gage No. 3 magnet or equivalent requires a
dards used for the original calibration. This calibration flat surface at least 3 mm [1/8-in.] in diameter finished
curve may be used for verifying the original calibration. no coarser than with a 600-grit abrasive (about 0.2 mi-
When the instrument can no longer produce readings on crons/8 microinches RMS). Rougher surfaces or convex
Table 8
Maximum Allowable Deviationof the Periodic
Ferrite Number (FN)Check for Magne-Gage-Type Instruments
Maximum Allowable Deviation of the Periodic Ferrite Number Check
Fromthe
Ferrite
Number From
the
Ferrite
NumberFromthe
Ferrite
Number
ValueAssigned
the
to
Value
Assigned to the
Value
First
Assigned to the
Secondary
Standard
Standard
Primary
Range
Number
Ferrite in Table 1 Seller the by Userby the
Table 9
Expected Range of Variation in Measurements
with Calibrated Magne-Gage-Type Instruments*
Number
Ferrite
Range Instruments
67% of the Instruments
95% of the
o to 10 20.30 FN 20.60 FN
over 10 to 18 20.35 FN 20.70 FN
over 18 to 25 20.45 FN 20.90 FN
over 25 to 90 value
55% of FN
mean 210% of mean FN value
*Based upon WRC round-robin tests.
11
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-.
Table 10
Expected Rangeof Variation in Measurements with CalibratedFeritscopes/Ferritescopes*
Ferrite Number Range 67%of the Instruments 95% of the lnstruments
o to 10 20.20 FN S.40FN
over 10 to 18 k0.40 FN S.80 FN
--`,,,`,`,``,,,,`,``,,`,,``,-`-`,,`,,`,`,,`---
Table 11
Expected Rangeof Variation in Measurements with Calibrated Inspector Gages*
Number
Ferrite
Range 67%Instruments
of the 95% of the Instruments
o to 10 20.20 FN 20.40 FN
over 10 to 18 20.40FN *.80 FN
over 18 to 30 +OS0 FN 21 .O FN
'Based upon WRC round-robin tests.
surfaces will result in artificially low FN values and shall significant figures shown in the relevant table herein
be avoided. Other instruments may respond differently to shall be used.
rough, convex, or narrow surfaces and should be evalu-
ated fully before use. At all ferrite levels, surface prepa- 9.2 Measurement Data. For purposes of reporting mea-
ration must be accomplished without contamination by surement data on weld metal test samples or demonstrat-
ferromagnetic materials. ing compliance with the requirements of a specification
other than this specification, the precision implied by the
number of significant figures in the tables herein is gen-
erally inappropriate. For ferrite measurements of 25 FN
9. Significant Figures in Reporting or higher, rounding-off to the nearest whole number con-
Measurement Results veys appropriateprecision. For ferrite measurement of 5
to 25 FN, rounding-off to the nearest 0.5 FN conveys ap-
9.1 Calibration Data. For purposes of developing cali- propriate precision. For ferrite measurements less than5
bration data or demonstrating compliance of an instru- FN, rounding-off to the nearest0.1 FN conveys appropri-
ment with calibration requirements, the number of ate precision.
12
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S T D - A W S A q - Z H / A q = Z - E N G L 1777 = 078‘42b5 0513780 TT7 W A4.2M/A4.2:1997
Annex
(This Annex is not a part of ANSIIAWS A4.2M/4.2:1997, Standard Procedures for Calibrating Magnetic Instru-
ments to Measure the Delta Ferrite Content of Austenitic and DuplexFerritic-Austenitic Stainless Steel Weld Metal, but
is included for information purposesonly.)
austenitic stainless steel weld metals in the past has too laboratory A might rate the percent ferrite at as low as 3
often been regarded as a firm fixed value. Extensive percent, laboratory B at 5 percent, and laboratory C at as
round-robins have been run on sets of weld metal speci- high as 8 percent, the WRC Subcommittee decided to
mens, containing up to a nominal 25 percent ferrite, in use the new term Ferrite Number (FN) to define the fer-
the U.S. under the sponsorship of the WRC and on simi- rite quantity as measured by instruments calibrated with
its recommended procedure. Thus, FN is an arbitrary,
standardized value related to the ferrite content of an
8. Welding Research Council, 345 East 47thSt., New York, NY equivalently magnetic weld metal. It is not necessarily
10017 the true absolute ferrite percentage of the weld. FNs
13
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A4.2MlA4.2:1997
below 10 do represent an excellent averageof the “per- The American Welding Institute developed the per-
cent ferrite” as determined by U.S. and world methods of sonal computer software package, FERRITEPREDIC-
measuring delta ferrite, based upon the previously dis- TOR, to assist in Ferrite Number estimation. The
cussed round-robins conductedby the WRC Subcommit- software is available from the American Welding Soci-
tee and the IIW Subcommission II-C. FNs above 10 ety. This software permits estimationof weld metal fer-
clearly exceed the true volume percent. Magnetic satura- rite by the WRC-1992 Diagram, as well as by the WRC-
tion measurements on castingsof known-percent ferrite 1988 Diagram, the Schaeffler Diagram and the DeLong
have shown that the magnetic response of a given per- Diagram.
cent ferrite depends upon its composition. So, any rela-
tion between ferrite and FN will be influenced somewhat
by composition of the ferrite. For common duplex fer-
ritic-austenitic weld metals, it is not unreasonable to esti-
A3.Cautions on the Use of Ferrite
mate that the percent ferriteis on the order of 0.7 times Number
the FN as measured herein, but this should not be consid- A3.1 Instrument Calibration
ered as exact.
A3.1.1 Various thicknesses of nonmagnetic material
A2.4 Ferrite Content Calculatedfrom Constitution
over carbon steel represent avery convenient method of
Diagrams. The several committees that have investi-
calibrating instruments for the measurement of ferrite in
gated and reviewed this subject recommend for most ap-
stainless steel weld metals. Useful general information
plications the use of measured ferrite as opposed to the
on the subject can be obtained from the latest edition
use of ferrite calculated from the weld metal analysis.
of The American Society for Testing and Materials
The basic reason for this is that the variables involved in
(ASTM) B 499, Standard Method for Measurement of
determining the chemical composition, and other vari-
Coating Thicknesses by Magnetic Method: Nonmagnetic
ables involved in the diagrams themselves, are very
Coatings on Magnetic Base Metakg The responseof the
likely to have substantially greater effectsthan those as-
instrument when a nonmagnetic “skin” is between the
sociated with the direct determination of ferrite content
measuring probe and the plate, versus its response to fer-
using instruments calibratedin accordance with this stan-
rite in stainless steel weld metal at several levels, canbe
dard. Nevertheless, constitution diagramsare very useful
plotted and the relationship between them established. A
tools, even though they are less exact, because they per-
change in the magnet size or strength, or in the probe
mit anticipation orprediction of ferrite content for a vari-
characteristics, changes the relationship. Thus, a calibra-
ety of situations (see WRC Bulletin 342, Stainless Steel
tion curve or table for FN versus nonmagnetic coating
Weld Metal: Prediction of Ferrite Content, April 1989).
thickness for a Magne-Gage-type instrument (Figure A l )
By taking into account dilution effects, such diagrams
will be different for each of the magnets (Nos. 1, 2, 3,
can also be useful for anticipating or predicting the fer-
and 4) because the strengths of the magnets are different.
rite content of weld overlays and dissimilar metal joints.
The Schaeffler diagram, developed in the late 1940s. A3.1.2 With Magne-Gage-type instruments, only cali-
presents its values as percent ferrite. The DeLong dia- bration using a No. 3 magnet is considered in this stan-
gram, January 1973 version, was the first diagram pre- dard. A weaker magnet (Nos. 1 or 2), if used with the
sented i n terms of FN. Espy, in 1982, proposed a calibration points of Table 1, will on weld metal yield
modification of the Schaeffler Diagram to take into ac- falsely high FN values. Conversely, a stronger magnet
--`,,,`,`,``,,,,`,``,,`,,``,-`-`,,`,,`,`,,`---
count high-nitrogen, high-manganese stainless steel weld (No. 4), if used with the calibration points of Table 1,
metals. More recently, Siewert, McCowan and Olson will on weld metalyield falsely low FN values. If the No.
prepared the WRC-1988 Diagram, under WRC sponsor- 3 magnet of a Magne-Gage is damaged, such as by rough
ship (see WeldingJournaf,December 1988, pp. 289-s to handling or exposure to an alternating current field
298-s, or WRC Bulletin 342, April 1989). Thiswas mod- which weakened it, it will also yield false readings. Work
ified slightly by Kotecki and Siewert toinclude the effect within the WRC Subcommittee on Welding Stainless
of copper in the nickel equivalent, as originally proposed Steel, on behalf of the International Institute of Welding,
by Lake, to produce the WRC-1992 Diagram (see Weld- Subcommission WC, has demonstrated that accurate
ingJourna1, May 1992, pp. 171-s to 17th). The WRC- readings on weld metal are obtained via calibration from
1992 Diagram is considered, at the time of this writing, Table 1 when the magnet strength is such that it provides
to be the best estimation tool available for most austen-
itic and duplex ferritic-austenitic stainless steel weld
metals, and has replaced the DeLong Diagram in Section 9. ASTM standards can be obtained from the American SoCi-
III of the ASME Code with publication of the 1994 etyforTesting and Materials, 100 Barr HarborDrive,West
Addenda. Conshohocken, PA 19428-2959.
14
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A4.2MlA4.2:1997
a tearing-off force as a function of FN of 5 FN/gram 5 thickness standards available from NIST at the t i m of
0.5 FN/gram. With a torsion balance other than a Magne- this writing, and corresponding Ferrite Numbers for cali-
Gage, compliance with this requirement is determined braiion of various instruments. It should bc recognized
directly from the slope of the calibration line. With a that the exactcoating thickness value of a particular stan-
Magne-Gage, this can be evaluated simply by suspend- dard from NIST may not beexactly as given in Table Al,
ing a 5-gram iron weight from the No. 3 magnet. When and the corresponding FN may therefore be slightly dif-
the white dial of the Magne-Gage is turned to just barely ferent. The sets can be ordered from the NIST office
lift the weight past the balance point of the instrument, listed in Footnote 10.
the reading should correspond to 25 2 2.5 FN using the
calibration line of white dial readings versusFN.
A4.2 Secondary Standards
A4.2.1 Weld-Metal-Like Secondary Standards.
A3.1.3 It is strongly recommended that reference Magnetic instruments may also be calibrated by using
weld-metal-like secondary standardsbe used along with weld-metal-like secondary standards rated by two or
the calibration curves obtained from primary standards more instruments carefully calibrated through the use of
when using a Ferritescope Model FES-KFto check for these standard procedures.Each such standard shouldbe
compliance with Table 6, when using an Inspector Gage provided with FN values at specific points on its test sur-
to check for compliance with Table7, or when using a face. These secondary standardscan be used for the cali-
Magne-Gage-type instrument to check for compliance bration of a suitable instrument or for maintaining
with Table 8, I f compliance cannot be obtained as re- calibration. They can also be used to establish the rela-
quired by the appropriate table, the instrument is in need tionship between other instruments and Magne-Gage-
of recalibration or servicing by the manufacturer, or it is type instruments.
not suitable for calibration with primary standards.
A4.2.2 Other mpes of Secondary Standards. The
A3.2 Instrument Malfunction. Recalibration or re- use of cast specimens or powder compacts is risky be-
checking of each instrument at periodic and sometimes cause the size, shape, and orientation of the magnetic
frequent intervals is necessary to ensure that the instru- particles may influence the response of the magnetic or
ment is operating properly(see 8.1). Permanent magnets other type probes to varying degrees, However, cast
may be partially demagnetized by exposure to any signif- specimens or powder compacts calibrated with one in-
icant alternating-current field such as that generated by a strument traceable to this procedure canbe used for cali-
strong alternating current in a wire or by a weaker alter- brating instruments of the same type and manufacture or
nating current in a coil. The tips of such permanent mag- for day-to-day verification of such instruments.
nets, or of the probes which are used to establish a
magnetic field in the specimen, may become worn and
the response of the system may change for this reason.
Bearings may become fouled with dirt and thus fail to
A5. Effect of Ferrite Size, Shape, and
operate freely. Orientation
It has been established that the ferrite size, shape, and
orientation can influence the relative response of the
A4. Standards for Instrument low-field-strength magnets and probes used with the
measuring instruments. For this reason, a measuring in-
Calibration
A4.1 Primary Standards. NIST'O coating thickness
. strument may respond differently to a given volume-per-
cent ferrite in a stainless steel weld metal as compared to
standards were developed many years ago to calibrate in- the same volume-percent ferrite in a cast stainless steel,
struments for the determination of coating thickness. The or even in a solution heat-treated stainless steel weld
standards useful for the determination of delta ferrite metal. The ferrite in as-welded weld metal up to about
consist of varying thicknessesof copper electroplated on 15 FN is very fine and i n the form of lacy, dendritic
a carbon steel base and protected with a hard chromium stringers generally perpendicular to the fusion line, and
flash. NIST certifies the thickness of the total coating to often extensively interconnected at ferrite contents over
within 55% of the stated thickness, but the majority will 3 or 4 FN. Above about 15 FN in as-welded weld metal,
be within t2% or even 51%. Table A l lists the coating the ferrite and austenite generally form laths which are
also very fine. The ferrite in castings is usually much
larger and tends to be lesser in volume and more sphe-
10. Office of StandardReference Materials, Room B311, roidized than in an as-welded weld metal of the same
Chemistry Building, National Institute of Standards and Tech- composition because heat treatment tends to transform
nology (NIST), Gaithersburg, M D 20899. some ferrite to austenite and spheroidize the balance.
15
--`,,,`,`,``,,,,`,``,,`,,``,-`-`,,`,,`,`,,`---
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A4.2MlA4.2:1997
STD.AWS A4.2M/A'I.Z-ENGL 1997 = 078'42b5O513783 7Db =
Table A l
Current NIST Coating Thickness Standards (Nominal Thicknesses)
with Approximate Corresponding Ferrite Numbers
NumberFerrite
Approximate
Thickness
Nominal
1.935 1364a
6.0 1.525 3.1 60.04 3.7
5.3 6.1 1.ooO 39.37
31.50 0.800
0.635 1363a 15.4 8.2 25.00 9.8
19.88 0.505
15.16 0.385
.7 10.04 0.255
0.205 1362a
off-scale off-scale 34.2
0.140 5.51
50.2 3.15 0.080
off-scale off-scale 77.0
0.040 1.57
0.048 1361a off-scale
99.2
0.025 0.98 off-scale off-scale
off-scale off-scale
0.012off-scale 0.47
0.24 0.006 off-sale off-scale off-scale
0.800 1359 31S O 7.7 6.6 12.3
12.20.505 19.88 10.2 18.8
--`,,,`,`,``,,,,`,``,,`,,``,-`-`,,`,,`,`,,`---
0.140 5.5 1 34.2 off-scale off-scale
69.10.048 1.89 off-scale off-scale
8 5.3 1358 6.1
1.o00 39.37
8.86 0.225 20.9 24.0 off-scale
3.15 0.080 off-scale 50.2 off-scale
0.048 1357 69.1 1.89 off-scale off-scale
110.5
0.020 0.79 off-scale off-sale
0.006 0.24 off-scale off-scale off-scale
Since the volume-percent of ferrite in castings is in close probe is a long, thin magnet hung on a spiral spring. The
agreement when measured by either magnetic response spring is wound by means of turning a knob with a corre-
or by metallographic point count, the ferrite content of sponding reading on a dial. When the magnet is pulled
castings is expressed as a percentage and not by the arbi- free of a specimen, the white dial readingused in con-
trary FN, as noted in ASTM Practice A800. junction with the calibration curve establishes theFN of
the specimen.
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(A) STANDARD MAGNE-GAGE
(B) MAGNE-GAGE FROM REAR, COUNTERWEIGHT ADDEDTO LEFT SIDE OF BALANCE BEAM
17
--`,,,`,`,``,,,,`,``,,`,,``,-`-`,,`,,`,`,,`---
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S T D - A W S A’4.2H/Aq.Z-ENGL 1777 0781.12b5 0513785 587 W
A4.2M/A4.2:199?
--`,,,`,`,``,,,,`,``,,`,,``,-`-`,,`,,`,`,,`---
System, referenced in Section A l . Numerous other con- ment with thumb-actuatedspring tension. The instrument
figurations could alsobe conceived. This is outside the gives direct readings in FN if it is a new model designed
scope of this standard. to do so. Older models canbe rebuilt by the manufacturer
to give acceptable readings on weld metal in terms of FN.
A6.2 Feritscope/“Ferritescope”-.”These instruments,
At the timeof this printing, the ability of Inspector Gages
which consist of a probe connected by a cableto an elec-
to determine ferrite above 30 FN is unknown.
tronics package (Figure A2), are usable in any position.
Several models and a variety of probes are available. A6.4 Other Instruments
Only one model and probe (Model FE8-KF) has been A6.4.1 The following instruments at the time of the
shown to be able to be calibrated with primary standards writing of this revision are not capable of being cali-
as given in Table 2 (see 5.1.1). All others must be cali- brated to primary standards. They can, however, be cali-
brated with weld-metal-like secondary standards as no brated to weld-metal-like secondary standards and
standard tables have been developed for calibration with produce acceptableconsistent results. Again, it is the re-
primary standards. Models are available in either battery- sponsibility of the user to ensure that instrument calibra-
powered or alternating current versions. At least one tion is maintained and to have the instrument repairedby
model can be calibrated with secondary standards up to the manufacturer if consistent readings on the weld-
80 FN or more. metal-like secondary standards cannot be obtained. At
the time of this printing, the ability of these instruments
A63 Inspector Gage.13This instrument (FigureA3), is
to determine ferrite above 30 FN is unknown.
usable in any position. It is a hand-held magnetic instru-
A6.4.1.1 Ferrite Indicator (more commonly
called a Severn Guge).14 This instrument (Figure A4) is
12. Manufactured by Fischer Technology, 750 Marshall Phelps
Road, Windsor, CT 06095.
13.Manufactured by Elcorneter, Inc., 1893 Rochester Industrial 14. Manufactured by Severn Engineering Co., Inc., 98 Edge-
Drive, Rochester Hills,MI 48309. wood Street, Annapolis,MD 21401.
18
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Figure A.2-Ferritescope Model FE&KF
--`,,,`,`,``,,,,`,``,,`,,``,-`-`,,`,,`,`,,`---
usable in any position. It is a go-no-go-type gage which converted to the FN scale by the manufacturer. Calibra-
determines whether the ferrite content of the weld under tion of a Severn gagewith secondary standards can only
test is above or below that of each of a number of inserts be approximate because the Severn gage does not pro-
of various magnetic strengths which come with the in- vide a discreteFN test value, only a range of possible FN
strument. At least one unthreaded test insert must be values for the sample under test.
available for use in conjunction with one of the threaded
A6.4.1.2 Foerster Ferrite Content Meter.” This
inserts with specified FN values. The purpose of the un-
is a light, portable, battery-powered instrument (Figure
threaded inserts is to assure that the magnet has not lost
strength. Details may be obtained from the manufacturer
for conversion of percent-ferrite values on earlier model
Severn gages to FN. Severn gages calibrated directly in 15. Marketed by Foerstet Instrument, Inc., 140 Industry Drive,
terms of FN are now available. Oldermodel gages can be RIOC Park West, Pittsburgh, PA 15275.
19
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STD*AWS A4*2M/A4.2-ENGL 1997 07842b5 0513787 351 M
A4.2MlA4.2:1997
--`,,,`,`,``,,,,`,``,,`,,``,-`-`,,`,,`,`,,`---
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Policy Group at 1-800-451-1584.
STD-AWS A4.2M/A4=2-ENGL L777 07842b5 0533789 124
A4.2MIA4.2:1997
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COPYRIGHT 2003; American Welding Society, Inc. Document provided by IHS Licensee=Aramco HQ/9980755100, User=, 12/27/2003
22:07:32 MST Questions or comments about this message: please call the Document
Policy Group at 1-800-451-1584.
STDeAWS A4=ZH/Aq.Z-ENGL L997 0784Zb5 0533770 7 4 b W
A4.2MlA4.2:1997
A5.3 Specificationfor Aluminum and Aluminum Alloy Electrodes for Shielded Metal Arc Welding
A5.4
Specification
for
Stainless
Steel
Welding
Electrodes
for
Shielded
Metal
ArcWelding
A5.5 Soecification
for
Low-Allov
Steel
Electrodes
for
Shielded
Metal
Arc
Weldine
A5.6
Specification for Covered
Copper
and
Copper
Alloy
Arc
Welding
Electrodes
A5.7 Specification for Copper
andCopper
Alloy
Bare
Welding Rods and
Electrodes
A5.8 Specification
for
Filler
Metals
for
Brazing
and
Braze
Welding
--`,,,`,`,``,,,,`,``,,`,,``,-`-`,,`,,`,`,,`---
~~ ~~ ~
A5.9 Specification
for
Bare
Stainless
Steel
Welding
Electrodes
and
Rods
A5.10
Specification
for
Bare
Aluminum
and
AluminumAlloy
Welding
Electrodes
and
Rods
A5.11/A5.11MSpecificationforNickelandNickel-AlloyWeldingElectrodesforShieldedMetalArcWelding
A5.12/A5.12M Specification for Tungsten and Tungsten Alloy Electrodes for Arc Welding and Cutting
A513 Specification
for
Solid
Surfacing
Welding
Rods
and
Electrodes
A5.14/A5.14MSpecificationforNickelandNickel-AlloyBareWeldingElectrodesandRods
A5.15
Specification
for
Welding
Electrodes
and
Rods
for
Cast
Iron
~~
A5.16
Specification
for
Titanium
and
Titanium
Alloy
Welding
Electrodes
andRods
~
A5.17/A5.17MSpecificationforCarbonSteelElectrodesandFluxesforSubmergedArcWelding
A5.18
Specification
for
Carbon
Steel
Electrodes
and
Rods
for
Gas
Shielded
Arc
Welding
A5.19
Specification
for
Magnesium
Alloy
Welding
Electrodes
and
Rods
A5.20
Soecification
for
Carbon
Steel
Electrodes
for
Flux
Cored
Arc
Weldine
A5.21
Specification
for
Composite
Surfacing
Welding
Rods
and
Electrodes
A5.22SpecificationforStainlessSteelElectrodes for FluxCoredArcWeldingandStainlessSteelFluxCoredRodsfor
Gas Tungsten Arc Welding
A5.23/A5.23MSDecificationforLow-AllovSteelElectrodesandFluxesforSubmereedArcWeldine
AS.24
Specification
for
Zirconium
and
Zirconium
Alloy
Welding
Electrodes
and
Rods
A5.25/A5.25MSpecificationforCarbonandLow-AlloySteelElectrodesandFluxesforElectroslagWelding
Ph5.26/A5.26MSpecificationforCarbonandLow-AlloySteelElectrodesforElectrogasWelding
A5.28
Specification
for
Low-Alloy
Steel
Electrodes
and
Rods
for
Gas
Shielded
Arc
Welding
A5.29
Specification
for
Low-Alloy
Steel
Electrodes
for
Flux
Cored
Arc
Welding
A530 Specification
Consumable
for Inserts
~ _ _ _ _ _
A5.3
Specification
1 for
Fluxes for Brazing
and
Braze
Welding
~~ ~
For ordering information, contact the AWS OrderDepartment, American Welding Society, 550 N.W. LeJeune Road,
Miami, FL 33126. Telephones: (800) 334-9353, (305) 443-9353, ext. 280; FAX (305) 443-7559.