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1, MARCH 2010 3
Abstract—Portable electronic products demand multifunc- as reduced wire length between block-to-block, high-density
tional module comprising of digital, radio frequency and memory interconnection. The TSV allows integrating multiple chips
functions. Through silicon via (TSV) technology provides a
with a physical packing density many times better than the
means of implementing complex, multifunctional integration
with a higher packing density for a system in package. A multichip module.
3-D silicon module with TSV has been developed in this pa- The conventional substrate technologies have a large via
per. Thermo-mechanical analysis has been performed and TSV size and wider line width/line spacing. It may not meet the
interconnect design is optimized. Multiple chips representing future requirements of line width <10 µm and thousands of
different functional circuits are assembled using wirebond and
input—output (I/O) pads per square centimeter [3]. Silicon
flip chip interconnection methods. Silicon carrier is fabricated
using via-first approach, the barrier copper via is exposed by the carrier based substrate technology provides dense wiring using
backgrinding process. A two-stack silicon module is developed back-end of-line processing. Matched thermal expansion of
and module fabrication details are given in this paper. The the carrier and the chip allows the use of micro bumps and
module reliability has been evaluated under temperature cycling improves solder interconnects reliability [4]. The 3-D package
(−40/125 °C) and drop test.
construction results in a large thermal resistance, which makes
Index Terms—3-D packaging, system in packaging, through difficult to cool the chip mounted in the inner layers of the
silicon via. package. But the silicon carrier has better thermal conductivity
I. Introduction compared to conventional substrate material, which helps to
reduce the 3-D package thermal resistance [5]. Development of
formation. In the via-last approach, the TSV is formed after Fig. 6. Wafer images after TSV formation.
the circuit/RDL formation on the wafer. The via–first approach
is preferred for the silicon carrier technology, because most A thick layer of copper overburden (30–40 µm) was ob-
of TSV fabrication processes are carried out with the full served on the TSV wafer surface because of the long plating
wafer thickness, then the wafer is thinned to required thickness time required for filling the 200 µm deep via. The wafer
for via exposure. The thinned wafer is processed further to warpage/bow observed to be lager (>500 µm) due to the thick
form the necessary back side metallization/UBM. The carrier copper overburden, it was measured using an optical probe.
fabrication process flow is shown in Fig. 4. The silicon wafer Different methods were considered for the removal of the
is etched using the deep reactive ion etch process forming copper overburden. Chemical etching took long time to remove
blind via of 50 µm diameter and 200 µm deep. Via tapering the thick copper overburden and observed non-uniform etch
is accomplished by a controlled isotropic etch chemistry rate across the wafer. CMP was evaluated using aggressive
consisting of SF6 , Argon (Ar), and O2 plasma after the straight Cu polishing slurry from Rohm and Hass. We developed two-
etch process. The via formation process is split into three steps step polishing to remove the thick copper: step 1 to remove
viz.: 1) straight via formation; 2) via tapering process by a the bulk of the copper with high down force (320 g/cm2 ), and
controlled isotropic etch; and 3) corner rounding by a global step 2 to remove a thin layer of copper with lower down force
isotropic etch process. Tapered via of size 50 µm at the base (100 g/cm2 ). The wafer images before and after the CMP are
and 100 µm at the top is achieved after via tapering steps. shown in Fig. 6. After CMP, an RDL has been deposited for
A dielectric layer of 1 µm SiO2 has been deposited by electrical re-distribution on the carrier wafer. We evaluated
the plasma enhanced chemical vapor deposition (PECVD) BCB and SiO2 as dielectric layer and both the materials were
process. Barrier and seed layers of Ti and Cu are deposited found suitable for our application. A low-temperature (250 °C)
using the physical vapor deposition process. The sidewall PECVD process was used for the SiO2 dielectric deposition.
deposition uniformity is characterized by cross section Exposing the buried copper via in the carrier TSV wafer
analysis. The oxide thickness varied from 0.8 µm at the top is a challenge, because it requires grinding brittle silicon
of the via to 0.4 µm at the bottom of the via as shown in and ductile copper simultaneously. Conventional backgrinding
Fig. 5. Damascene copper plating is used for the via filling. wheel is found not suitable for the ductile copper and observed
Typical composition of copper plating electrolyte includes wheel clogging. We used a rough grinding step followed by a
CuSO4 , H2 SO4 , Cl− , with additives such as Suppressor, fine grinding step and CMP to relieve the stress. The carrier
Accelerator, and Leveler. The plating solution used is wafer was thinned to 250 µm thickness by course grinding,
Everplate-Cu200 from Atotech. We developed the pulse remaining 50 µm was removed with the vitrified bond wheel.
reverse plating process recipe and demonstrated void free via Then the wafer was polished by the wet method to remove
filling. The plating current has been optimized and complete the sub-surface damages. The wafer surface roughness (Ra)
via plating is achieved in three steps viz.: 1) step 1—low is 17 nm and 0.45 nm after grinding and wet polishing,
forward current plating; 2) step 2—medium forward current respectively. The wafer surface was analyzed by energy-
plating; and 3) step 3—high forward current plating. dispersive X-ray spectroscopy and AUGERE and found no
6 IEEE TRANSACTIONS ON COMPONENTS AND PACKAGING TECHNOLOGIES, VOL. 33, NO. 1, MARCH 2010
Fig. 8. Images of carrier wafer after debonding. (a) Polymer residue without
sacrificial layer. (b) No residue with sacrificial layer.
Fig. 12. Drop test setup and results. Fig. 14. SEM micro graph failed sample for TC test.
TABLE II
and there is no need for a spacer die. This method gives small
Chip Solder Interconnect TC Results
stand-off for the stacked wire bond chips. The bond parameters
like top/bottom heater temperature and bond speed have been
Daisy Chain Resistance ()
optimized. Carrier 2 is assembled with flip-chip and wire bond
Time 0 500 1000 2000
chip. Therefore, the pad finish should be suitable for both the cycles cycles cycles
chip attachment methods. Pads on the carrier top and bottom Chip 1 24.3 24.3 24.3 34.3
side are plated with electroless NiPdAu. Wire bondability and Chip 2 17.3 18 18.9 20.5
wire pull strength are found good on the NiPdAu pads. Two
chips have been stacked and demonstrated low loop height The failed samples were cross-sectioned and failure anal-
(<50 µm) for the chip stacking. Fig. 10 show the stacked ysis was performed. The failed samples show detachment
wire bond die assembled for this paper. of RDL/UBM metal layer form the copper via as shown in
Carrier 1 is mounted on a FR4 PCB using SAC305 solder Fig. 14. During the carrier fabrication, the 1 µm thick SiO2
of 250 µm diameter. Carrier 1 assembly is underfilled and layer was used as the dielectric layer after the via exposure and
cured at 165 °C for 3 h. Carrier 2 is over molded using the the contact opening on the via was patterned. Then the barrier
transfer molding process. Then Carrier 2 is assembled on the layer of 1 KA Ti and the seed layer of 2 KA Cu were sputtered
Carrier 1 and underfilled. Fig. 11 shows the images of the 3-D for copper RDL formation. Poor adhesion of the sputtered
silicon module. We prepared samples having Carrier 2 with metal layers on the TSV and stress due to thermal expansion
and without overmold for reliability assessment. of TSV are potential cause for the above failure.
Chip 1 and chip 2 are assembled with the carrier using
solder. The solder height is ∼50 µm, which helps to reduce
VII. Module Reliability Assessment the stack height. The carrier and chip are silicon, therefore no
The 3-D silicon module is assembled onto a two-layer PCB. thermal mismatch between them. Both the chips showed good
The PCB design is based on JESD22-B111 in terms of package interconnect reliability, no failure in solder interconnection
layout, metal traces, and pad opening design. Separate daisy was observed even after 2000 TC cycles. The chip 1 and 2
chain for the three chip interconnections, Carrier 1 to PCB solder joint reliability is measured by electrical continuity of
and Carrier 1 to Carrier 2 has been designed. The 3-D silicon the daisy chain and electrical resistances are given Table II.
module was tested for drop and thermal cycle reliability test
condition. Preliminary drop test of the 3-D module without
VIII. Conclusion
underfill showed complete detachment of the carrier from the
PCB. Samples with underfill and overmold passed the 30 drops A 3-D silicon module platform technology using silicon
at 1500 G, 0.5 ms pulse duration. The drop test setup and carrier technology has been developed and demonstrated for
results are shown in Fig. 12. system in packaging application. Silicon carrier (substrate)
The reliability of the 3-D silicon module has been assessed with TSV interconnection is developed for chip attachment
for thermal cycle reliability conditions (−40 °C to 125 °C, and embedded passives integrations. The module thermo-
ramp 15 C/min, dwell 15 min). Fig. 13 shows the cross section mechanical and reliability performances have been reported
of solder and TSV of Carrier 1 and Carrier 2. Electrical con- in the paper. Chip interconnection methods, such as flip-
tinuity of the TSV and solder joint was monitored by separate chip, wirebond, and gold stud bump have been evaluated and
daisy chains. The daisy chain resistance was monitored every interconnections reliability is reported. Some important results
250 cycles. The solder interconnects and TSV joints showed and recommendations are summarized as follows.
no crack or detachment at time zero. However some of TSV 1) A tapered via structure has been designed and void free
chains showed open, when we measured the resistance after filling has been achieved using damascene pulse-reverse
500 cycles. plating.
8 IEEE TRANSACTIONS ON COMPONENTS AND PACKAGING TECHNOLOGIES, VOL. 33, NO. 1, MARCH 2010
2) Silicon carrier fabrication process based on the via-first Vempati Srinivasa Rao received the B.Tech. degree
in metallurgical engineering from the National In-
approach is established and developed 200 µm thick stitute of Technology, Warangal, India, in 2002, and
carrier with TSV for 3-D module assembly. the M.E. degree in mechanical engineering from the
3) Thin wafer handling technique using spin-on temporary National University of Singapore, Singapore.
Since 2006, he has been a Research Engineer
adhesive is evaluated and found suitable for the silicon with the Microsystems, Modules and Components
carrier fabrication. Laboratory, Institute of Microelectronics, Singapore.
His research interests include wafer level packag-
ing, fine pitch interconnects, Cu/low-k packaging,
Acknowledgment through silicon via technology, 3-D stacked module,
wafer level integration, and package reliability.
This paper is the result of a project initiated by the Micro-
System Packaging Initiative Electronic Packaging Research
Consortium, EPRC VIII Project 2: stacked silicon module Samuel Lim received the B.E. degree in mechanical
with embedded passives for SiP application. The authors and manufacturing engineering from the University
of South Australia, Adelaide, Australia, in 2006.
would like to thank the consortium members and project He has been involved in the process integration of
team for their support and guidance. The consortium members 3-D stacked silicon modules in the Microsystems,
are ASM Technology Singapore Pte Ltd., Freescale Semi- Modules and Components Laboratory, Institute of
Microelectronics, Singapore, as a Lab Officer.
conductor Malaysia Sdn Bhd., Ltd., Infineon Technologies
Asia Pacific Pte Ltd., Microcircuit Technology (2002) Pte
Ltd., STATSChipPAC, Ltd., Ibiden Singapore Pte Ltd., Surface
Technology Systems Pte Ltd., United Test and Assembly
Center Ltd., Institute of Microelectronics, Institute of Ma- Ho Soon We received the B.E. degree in materials
terials Research and Engineering, Institute of High Perfor- engineering from Nanyang Technological University,
mance Computing, and Singapore Institute of Manufacturing Singapore, in 2006.
He is currently a Research Officer with the Mi-
Technology. crosystems, Modules and Components Laboratory,
Institute of Microelectronics, Singapore. His re-
search interests include wafer level packaging, sil-
References icon based 3-D system in packages, through silicon
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Polastre, C. Schuster, A. Sharma, S. M. Sri-Jayantha, C. W. Surovic, of advanced packaging. His fields of expertise are
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T. C. Chai, K. O. Navas, and K. Vaidyanathan, “Reliability studies of a
through via silicon stacked module for 3-D microsystem packaging,” in
Xiaowu Zhang received the B.S. degree in physics
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from the National University of Defense Technol-
[5] N. Khan, S. W. Yoon, A. G. K. Viswanath, V. P. Ganesh, D. W.
ogy, Changsha, China, in 1986, the M.E. degree
Ranganathan, S. Lim, and K. Vaidyanathan, “Development of 3-D stack
in mechanics from the University of Science and
package using silicon interposer for high power application,” in Proc.
Technology of China, Hefei, China, in 1989, and
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the Ph.D. degree in mechanical engineering from the
[6] H. Y. Li, Y. M. Khoo, N. Khan, K. W. Teoh, V. S. Rao, H. B. Li, E.
Hong Kong University of Science and Technology,
B. Liao, S. Mohanraj, V. Kripesh, and K. Rakesh, “High performance
Clear Water Bay, Kowloon, Hong Kong, in 1999.
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He has been with the Institute of Microelectronics
(IME), Singapore, since 1999. Currently, he is a Member of the Technical Staff
at the Microsystems, Modules and Components Laboratory, IME, Singapore.
Navas Khan received the B.E. degree in mechanical His research activities include advanced packaging development and 3-D
engineering from Bangalore University, Bangalore, integrated circuit integration. He has authored or co-authored more than 90
India, in 1993, and the M.E. degree in mechanical technical papers in refereed journals and conference proceedings.
engineering from Nanyang Technological University, Dr. Zhang is the recipient of the 2001 JEP Best Paper Award conferred by
Singapore, in 2006. the ASME Transactions Journal of Electronic Packaging.
He is a Member of the Technical Staff at the
Microsystems, Modules and Components Labora-
tory, Institute of Microelectronics, Singapore. He has
many years of experience in the area of advanced
packaging. He was with C-Dot, India, from 1994
to 2009 in the area of system level packaging of
telecommunication electronics. Currently, he is working on through silicon
via and silicon interposer technology.
KHAN et al.: DEVELOPMENT OF 3-D SILICON MODULE WITH TSV FOR SYSTEM IN PACKAGING 9
E. B. Liao received the B.E. degree in metallurgical V. Kripesh received the Bachelor degree in physics
engineering from the Central South University of from the University of Madras, Chennai, India, in
Technology, Changsha, China, the M.E. degree in 1985, the M.S. degree in physics from the University
materials engineering from the Institute of Metal Re- of Madras in 1987, and the Ph.D. degree in 1995.
search of the Chinese Academy of Sciences, China, He carried out his doctoral work at the Max-Planck
and the M.E. and Ph.D. degrees in mechanical engi- Institute for Metalforschung, Stuttgart, Germany, in
neering from the National University of Singapore, the area of thick and thin film passives for micro-
Singapore. electronics modules.
In 2005, he joined the Microsystems, Modules and He has 16 years of research experience in the area
Components Laboratory, Institute of Microelectron- of advanced packaging, and he has worked as a Vis-
ics, Singapore, and is currently a Senior Research iting Scientist at Infineon Technologies, Corporate
Engineer. His research interests include advanced packaging technologies, Research, Munich, Germany, in the area of 3-D-integrated circuits. Since
microfabrication techniques, and radio frequency passive devices. March 2000, he has been with the Microsystems, Modules and Components
Laboratory, Institute of Microelectronics, Singapore. He has authored more
than 40 journal and conference publications. His research interests include 3-
Ranganathan Nagarajan received the B.E. de- D-silicon stacked modules, Cu/low-k packaging, and wafer level packaging.
gree in electronics and telecommunications from
Osmania University, Hyderabad, India, in 1982, and
the M.Tech degree in integrated electronics and John H. Lau (F’94) received three M.S. degrees
circuits from the Indian Institute of Technology, New in structural engineering, engineering physics, and
Delhi, India, in 1984. management science, and the Ph.D. degree in the-
He has over 24 years of diverse techni- oretical and applied mechanics from the University
cal experience in complementary metal–oxide– of Illinois, Chicago.
semiconductors, micro-electro-mechanical systems, He is the Director of the Microsystems, Modules
and wafer level packaging technologies. He is cur- and Components Laboratory, Institute of Micro-
rently with the Microsystems, Modules and Com- electronics, Singapore. Prior to this, he was with
ponents Laboratory, Institute of Microelectronics, Singapore, as a Mem- HP/Agilent for more than 20 years. With more than
ber of the Technical Staff. His areas of expertise and interest include 30 years of research and development and manufac-
high aspect ratio silicon micro-machining, nano electromechanical systems, turing experience in the electronics and photonics
bio-micro-fluidics, and 3-D wafer level stacking technology. industries, he has authored and co-authored over 250 peer-reviewed technical
publications, authored more than 100 book chapters, and given over 250
workshops and invited presentations.
T. C. Chai received the Bachelor degree in me- Dr. Lau is one of the elected Fellows of the American Society of Mechanical
chanical engineering from Heriot-Watt University, Engineers.
Edinburgh, U.K.
Previously, he was with Texas Instruments,
Singapore, as a Packaging Development Engineer.
He is currently a Member of the Technical Staff at
the Microsystems, Modules and Components Labo-
ratory, Institute of Microelectronics, Singapore. He
has worked on areas of packaging development, re-
liability, and failure analysis for 18 years. Recently,
his focus has been on flip chip packaging for Cu
low-K chip and through silicon via technology.