Techniological Institute of the Philippines Manila

ChE 502 S.Y. 2020-2021

Experiment 2

9 APPENDIX 40 72 72.08 53.44

50 90 90 55.08
9.1. RAW DATA GATHERED
Temperature: 30°C
Initial Molar Ratio: 2
Flowrate Flowrate Actual
Temperature: 30°C Conductivity
of EA of NaOH Vb
Initial Molar Ratio: 1 10 20 20 53.13
Flowrate Flowrate Actual 20 40 40 55.6
Conductivity
of EA of NaOH Vb 30 60 60 57.68
10 10 10 12.25 40 80 80 59.49
20 20 20 16.63 50 100 100 61.09
30 30 30 19.76
40 40 40 22.27 Temperature: 32°C
50 50 50 24.37 Initial Molar Ratio: 1.2
Flowrate Flowrate Actual
Temperature: 30°C Conductivity
of EA of NaOH Vb
Initial Molar Ratio: 1.2 10 12 12.08 20.39
Flowrate Flowrate Actual 20 24 23.96 23.71
Conductivity
of EA of NaOH Vb 30 36 36.04 26.67
10 12 12.08 21.54 40 48 48.13 29.03
20 24 23.96 25.64 50 60 60 31.19
30 36 36.04 28.36
40 48 48.13 30.9 Temperature: 32°C
50 60 60 32.84 Initial Molar Ratio: 1.4
Flowrate Flowrate Actual
Temperature: 30°C Conductivity
of EA of NaOH Vb
Initial Molar Ratio: 1.4 10 14 13.96 29.83
Flowrate Flowrate Actual 20 28 28.13 32.58
Conductivity
of EA of NaOH Vb 30 42 42.08 34.69
10 14 13.96 31.14 40 56 56.04 37
20 28 28.13 34.2 50 70 70 38.46
30 42 42.08 36.8
40 56 56.04 39.02
50 70 70 40.94 Temperature: 32°C
Initial Molar Ratio: 1.6
Temperature: 30°C Flowrate Flowrate Actual
Initial Molar Ratio: 1.6 Conductivity
of EA of NaOH Vb
Flowrate Flowrate Actual 10 16 16.04 37.58
Conductivity
of EA of NaOH Vb 20 32 32.08 40.34
10 16 16.04 39.03 30 48 48.13 41.6
20 32 32.08 42.1 40 64 63.96 44.54
30 48 48.13 44.6 50 80 80 45.21
40 64 63.96 46.7
50 80 80 48.37 Temperature: 32°C
Initial Molar Ratio: 1.8
Flowrate Flowrate Actual
Conductivity
of EA of NaOH Vb
10 18 18.13 43.81
Temperature: 30°C 20 36 36.04 47.34
Initial Molar Ratio: 1.8 30 54 53.96 49.51
Flowrate Flowrate Actual
Conductivity 40 72 72.08 51.33
of EA of NaOH Vb
50 90 90 52.41
10 18 18.13 46.89
20 36 36.04 49.24
Temperature: 32°C
30 54 53.96 51.62
Techniological Institute of the Philippines Manila
ChE 502 S.Y. 2020-2021
Experiment 2

Initial Molar Ratio: 2 10 16 16.04 36.24

Flowrate Flowrate Actual 20 32 32.08 38.72
Conductivity
of EA of NaOH Vb 30 48 48.13 40.54
10 20 20 52.01 40 64 63.96 42.38
20 40 40 53.89 50 80 80 43.97
30 60 60 55.86
40 80 80 57.1 Temperature: 34°C
50 100 100 58.57 Initial Molar Ratio: 1.8
Flowrate Flowrate Actual
Conductivity
of EA of NaOH Vb
Temperature: 34°C 10 18 18.13 43.06
Initial Molar Ratio: 1 20 36 36.04 45.59
Flowrate Flowrate Actual 30 54 53.96 47.34
Conductivity
of EA of NaOH Vb 40 72 72.08 49.06
10 10 10 10.43 50 90 90 50.44
20 20 20 14.20
30 30 30 16.93
40 40 40 19.12
50 50 50 20.97

Temperature: 36°C
Initial Molar Ratio: 1
Temperature: 34°C Flowrate Flowrate Actual
Conductivity
Initial Molar Ratio: 1.2 of EA of NaOH Vb
Flowrate Flowrate Actual 10 10 10 9.64
Conductivity
of EA of NaOH Vb 20 20 20 13.15
10 12 12.08 19.35 30 30 30 15.69
20 24 23.96 22.37 40 40 40 17.74
30 36 36.04 25.12 50 50 50 19.31
40 48 48.13 27.11 Temperature: 34°C
Temperature: 36°C Initial Molar Ratio: 2
Initial Molar Ratio: 1.2 Flowrate Flowrate Actual
Conductivity
Flowrate Flowrate Actual of EA of NaOH Vb
Conductivity 10 20 20 49.74
of EA of NaOH Vb
10 12 12.08 17.5 20 40 40 51.70
20 24 23.96 21.14 30 60 60 53.40
30 36 36.04 23.7 40 80 80 54.90
40 48 48.13 25.76 50 100 100 56.24
50 60 60 27.32
50 60 60 29.01
Temperature: 36°C
Initial Molar Ratio: 1.4
Temperature: 34°C
Initial Molar Ratio: 1.4 Flowrate Flowrate Actual
Conductivity
of EA of NaOH Vb
Flowrate Flowrate Actual
Conductivity 10 14 13.96 29.24
of EA of NaOH Vb
10 14 13.96 27.73 20 28 28.13 30.54
20 28 28.13 30.66 30 42 42.08 31.70
30 42 42.08 33.26 40 56 56.04 33.44
40 56 56.04 35.14 50 70 70 34.97
50 70 70 36.8

Temperature: 34°C
Initial Molar Ratio: 1.6
Temperature: 36°C
Flowrate Flowrate Actual
Conductivity Initial Molar Ratio: 1.6
of EA of NaOH Vb
Flowrate Flowrate Actual Conductivity
Techniological Institute of the Philippines Manila
ChE 502 S.Y. 2020-2021
Experiment 2

of EA of NaOH Vb 10 16 16.04 33.07

10 16 16.04 36.56 20 32 32.08 36.59
20 32 32.08 37.23 30 48 48.13 37.56
30 48 48.13 38.87 40 64 63.96 37.81
40 64 63.96 40.19 50 80 80 41.85
50 80 80 41.74
Temperature: 38°C
Temperature: 36°C Initial Molar Ratio: 1.8
Initial Molar Ratio: 1.8 Flowrate Flowrate Actual
Conductivity
Flowrate Flowrate Actual of EA of NaOH Vb
Conductivity
of EA of NaOH Vb 10 18 18.13 37.57
10 18 18.13 43.04 20 36 36.04 42.47
20 36 36.04 44.64 30 54 53.96 44.52
30 54 53.96 45.76 40 72 72.08 45.33
40 72 72.08 47.28 50 90 90 47.09
50 90 90 48.76

Temperature: 36°C
Initial Molar Ratio: 2
Flowrate Flowrate Actual
Conductivity
of EA of NaOH Vb Temperature: 38°C
10 20 20 48.22 Initial Molar Ratio: 2
20 40 40 49.97 Flowrate Flowrate Actual
Conductivity
30 60 60 51.49 of EA of NaOH Vb
40 80 80 52.08 10 20 20 47.4
50 100 100 53.85 20 40 40 48.06
30 60 60 49.92
Temperature: 38°C
Initial Molar Ratio: 1
Flowrate Flowrate Actual
Conductivity
of EA of NaOH Vb
Temperature: 38°C 10 10 10 8.93
Initial Molar Ratio: 1.2 20 20 20 12.19
Flowrate Flowrate Actual 30 30 30 15.34
Conductivity
of EA of NaOH Vb
40 40 40 16.48
10 12 12.08 17.52
50 50 50 17.64
20 24 23.96 20.02
40 80 80 50.96
30 36 36.04 23.23
50 100 100 51.86
40 48 48.13 24.31
50 60 60 25.61 Temperature: 40°C
Initial Molar Ratio: 1
Temperature: 38°C Flowrate Flowrate Actual
Initial Molar Ratio: 1.4 Conductivity
of EA of NaOH Vb
Flowrate Flowrate Actual 10 10 10 7.56
Conductivity
of EA of NaOH Vb 20 20 20 11.68
10 14 13.96 27.39 30 30 30 13.27
20 28 28.13 29.68 40 40 40 15.5
30 42 42.08 30.01 50 50 50 16.69
40 56 56.04 32.06
50 70 70 33.28

Temperature: 38°C
Initial Molar Ratio: 1.6
Flowrate Flowrate Actual
Conductivity
of EA of NaOH Vb
Techniological Institute of the Philippines Manila
ChE 502 S.Y. 2020-2021
Experiment 2

Temperature: 40°C
Temperature: 40°C Initial Molar Ratio: 1.2
Initial Molar Ratio: 1.4 Flowrate Flowrate Actual
Flowrate Flowrate Actual Conductivity
Conductivity of EA of NaOH Vb
of EA of NaOH Vb 10 12 12.08 18.55
10 14 13.96 23.86 20 24 23.96 19.41
20 28 28.13 27.31 30 36 36.04 21.19
30 42 42.08 29.73 40 48 48.13 23.57
40 56 56.04 30.04 50 60 60 24.49
50 70 70 31.88

Temperature: 42°C
Initial Molar Ratio: 1.2
Flowrate Flowrate Actual
Temperature: 40°C Conductivity
of EA of NaOH Vb
Initial Molar Ratio: 1.6 10 12 12.08 15.99
Flowrate Flowrate Actual 20 24 23.96 18.5
Conductivity
of EA of NaOH Vb
30 36 36.04 20.09
10 16 16.04 32.78
40 48 48.13 21.56
20 32 32.08 34.58
50 60 60 23.17
30 48 48.13 35.89
40 64 63.96 37.31 Temperature: 42°C
50 80 80 38.42 Initial Molar Ratio: 1.4
Flowrate Flowrate Actual
Temperature: 40°C Conductivity
of EA of NaOH Vb
Initial Molar Ratio: 1.8 10 14 13.96 23.88
Flowrate Flowrate Actual 20 28 28.13 25.85
Conductivity
of EA of NaOH Vb
30 42 42.08 27.73
10 18 18.13 40.51
40 56 56.04 29.08
20 36 36.04 41.08
50 70 70 30.29
30 54 53.96 42.56
40 72 72.08 43.67 Temperature: 42°C
50 90 90 44.72 Initial Molar Ratio: 1.6
Flowrate Flowrate Actual
Temperature: 40°C Conductivity
of EA of NaOH Vb
Initial Molar Ratio: 2 10 16 16.04 31.79
Flowrate Flowrate Actual 20 32 32.08 33.4
Conductivity
of EA of NaOH Vb
30 48 48.13 34.81
10 20 20 45.47
40 64 63.96 35.87
20 40 40 46.85
50 80 80 37.02
30 60 60 48.09
40 80 80 49.2 Temperature: 42°C
50 100 100 50.23 Initial Molar Ratio: 1.8
Flowrate Flowrate Actual
Conductivity
Temperature: 42°C of EA of NaOH Vb
Initial Molar Ratio: 1 10 18 18.13 38.09
Flowrate Flowrate Actual 20 36 36.04 39.16
Conductivity
of EA of NaOH Vb 30 54 53.96 40.71
10 10 10 7.67 40 72 72.08 42.13
20 20 20 10.5 50 90 90 43.28
30 30 30 12.57
40 40 40 14.25
50 50 50 15.68

Temperature: 42°C
Techniological Institute of the Philippines Manila
ChE 502 S.Y. 2020-2021
Experiment 2

Initial Molar Ratio: 2 Flowrate Flowrate Actual

Conductivity
Flowrate Flowrate Actual of EA of NaOH Vb
Conductivity
of EA of NaOH Vb 10 18 18.13 37.04
10 20 20 44.22 20 36 36.04 38.58
20 40 40 45.45 30 54 53.96 39.6
30 60 60 46.56 40 72 72.08 40.7
40 80 80 47.57 50 90 90 41.57
50 100 100 48.5
Temperature: 44°C
Temperature: 44°C Initial Molar Ratio: 2
Initial Molar Ratio: 1 Flowrate Flowrate Actual
Flowrate Flowrate Actual Conductivity
Conductivity of EA of NaOH Vb
of EA of NaOH Vb 10 20 20 43.04
10 10 10 7.12 20 40 40 44.14
20 20 20 10.11 30 60 60 45.14
30 30 30 11.93 40 80 80 46.05
40 40 40 13.26 50 100 100 46.9
50 50 50 15.04
Temperature: 46°C
Temperature:
Initial 44°C1
Molar Ratio:
Flowrate Initial Molar Ratio:
Flowrate Actual1.2
Flowrate Flowrate Actual Conductivity
of EA of NaOH Vb Temperature: 46°C
Conductivity
of10
EA of NaOH
10 Vb
10 6.16 Initial Molar Ratio: 1.2
10
20 12
20 12.08
20 15.32
9.08 Flowrate Flowrate Actual
Conductivity
20
30 24
30 23.96
30 17.17
10.89 of EA of NaOH Vb
30
40 36
40 36.04
40 19.07
12.36 10 12 12.08 14.13
40
50 48
50 48.13
50 20.63
13.62 20 24 23.96 16.37
50 60 60 21.79 30 36 36.04 18.14
40 48 48.13 19.58
50 60 60 20.67

Temperature: 46°C
Initial Molar Ratio: 1.4
Flowrate Flowrate Actual
Temperature: 44°C Conductivity
of EA of NaOH Vb
Initial Molar Ratio: 1.4 10 14 13.96 21.68
Flowrate Flowrate Actual 20 28 28.13 23.97
Conductivity
of EA of NaOH Vb 30 42 42.08 25.57
10 14 13.96 23.09 40 56 56.04 26.7
20 28 28.13 24.87 50 70 70 27.73
30 42 42.08 26.61
40 56 56.04 27.84 Temperature: 46°C
50 70 70 28.96 Initial Molar Ratio: 1.6
Flowrate Flowrate Actual
Temperature: 44°C Conductivity
of EA of NaOH Vb
Initial Molar Ratio: 1.6 10 16 16.04 29.18
Flowrate Flowrate Actual 20 32 32.08 31.29
Conductivity
of EA of NaOH Vb 30 48 48.13 32.44
10 16 16.04 30.86 40 64 63.96 33.3
20 32 32.08 32.3 50 80 80 34.27
30 48 48.13 33.35
40 64 63.96 34.54 Temperature: 46°C
50 80 80 35.59 Initial Molar Ratio: 1.8
Flowrate Flowrate Actual
Temperature: 44°C Conductivity
of EA of NaOH Vb
Initial Molar Ratio: 1.8
Techniological Institute of the Philippines Manila
ChE 502 S.Y. 2020-2021
Experiment 2

10 18 18.13 36.33 of EA of NaOH Vb

20 36 36.04 37.46 10 18 18.13 36.33
30 54 53.96 38.36 20 36 36.04 37.46
40 72 72.08 39.37 30 54 53.96 38.36
50 90 90 40.16 40 72 72.08 39.37
50 90 90 40.16

Temperature: 48°C
Initial Molar Ratio: 2
Temperature: 46°C Flowrate Flowrate Actual
Initial Molar Ratio: 2 Conductivity
of EA of NaOH Vb
Flowrate Flowrate Actual 10 20 20 41.94
Conductivity
of EA of NaOH Vb 20 40 40 42.03
10 20 20 41.89 30 60 60 42.57
20 40 40 42.92 40 80 80 43.31
30 60 60 43.81 50 100 100 44.01
40 80 80 44.64
50 100 100 45.4 Temperature: 50°C
Initial Molar Ratio: 1
Temperature: 48°C Flowrate Flowrate Actual
Conductivity
Initial Molar Ratio: 1 of EA of NaOH Vb
Flowrate Flowrate Actual 10 10 10 5.74
Conductivity
of EA of NaOH Vb 20 20 20 7.6
10 10 10 6.62 30 30 30 9.47
20 20 20 8.46 40 40 40 11.09
30 30 30 10.15 50 50 50 11.87
40 40 40 11.53
50 50 50 12.85

Temperature: 48°C
Temperature: 48°C Initial Molar Ratio: 1.2
Initial Molar Ratio: 1.4 Flowrate Flowrate Actual
Conductivity
Flowrate Flowrate Actual of EA of NaOH Vb
Conductivity
of EA of NaOH Vb 10 12 12.08 14.7
10 14 13.96 22.36 20 24 23.96 15.63
20 28 28.13 23.52 30 36 36.04 17.27
30 42 42.08 24.61 40 48 48.13 18.05
40 56 56.04 26.19 50 60 60 19.47
50 70 70 26.17

Temperature: 50°C
Initial Molar Ratio: 1.2
Flowrate Flowrate Actual
Temperature: 48°C Conductivity
of EA of NaOH Vb
Initial Molar Ratio: 1.6 10 12 12.08 12.79
Flowrate Flowrate Actual 20 24 23.96 15.13
Conductivity
of EA of NaOH Vb 30 36 36.04 16.22
10 16 16.04 29.99 40 48 48.13 17.73
20 32 32.08 30.34 50 60 60 18.66
30 48 48.13 31.39
40 64 63.96 32.16 Temperature: 50°C
50 80 80 33.05 Initial Molar Ratio: 1.4
Flowrate Flowrate Actual
Temperature: 48°C Conductivity
of EA of NaOH Vb
Initial Molar Ratio: 1.8 10 14 13.96 20.25
Flowrate Flowrate Actual Conductivity
Techniological Institute of the Philippines Manila
ChE 502 S.Y. 2020-2021
Experiment 2

20 28 28.13 22.36 of EA of NaOH Vb

30 42 42.08 23.73 10 18 18.13 34.68
40 56 56.04 24.67 20 36 36.04 35.84
50 70 70 25.54 30 54 53.96 36.14
40 72 72.08 36.98
Temperature: 50°C 50 90 90 37.62
Initial Molar Ratio: 1.6
Flowrate Flowrate Actual
Conductivity
of EA of NaOH Vb
10 16 16.04 27.72
20 32 32.08 29.13
30 48 48.13 30.18
40 64 63.96 30.93
50 80 80 31.91

Temperature: 50°C
Initial Molar Ratio: 1.8
Flowrate Flowrate Actual Conductivity

Temperature: 50°C
Initial Molar Ratio: 2
Flowrate Flowrate Actual
Conductivity
of EA of NaOH Vb
10 20 20 38.3
20 40 40 40.68
30 60 60 41.4
40 80 80 42.33
50 100 100 42.7

Graphs
30 C AT DIFFERENT MOLAR RATIOS