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  • E. Hasil Praktikum: 2. 0,6 Ml/menit

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    dindha pristika aulia
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    The document summarizes the results of an experiment measuring the retention times (R) of caffeine, phenol red, and a mixture of the two compounds using different flow rates (0.4, 0.6, 0.8, 1.0, 1.2 ml/min) of a 30:70 water:methanol solvent system in column chromatography. Retention times decreased with increasing flow rate for all compounds. The retention time also decreased in the order of caffeine, phenol red, and the mixture for each flow rate. Calculations were shown for determining R values from the retention times at different flow rates.

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    HASIL VARIASI LAJU ALIR

    Original Title

    HASIL VARIASI LAJU ALIR

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    The document summarizes the results of an experiment measuring the retention times (R) of caffeine, phenol red, and a mixture of the two compounds using different flow rates (0.4, 0.6, 0.8, 1.0, 1.2 ml/min) of a 30:70 water:methanol solvent system in column chromatography. Retention times decreased with increasing flow rate for all compounds. The retention time also decreased in the order of caffeine, phenol red, and the mixture for each flow rate. Calculations were shown for determining R values from the retention times at different flow rates.

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    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
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    9 views3 pages

    E. Hasil Praktikum: 2. 0,6 Ml/menit

    Uploaded by

    dindha pristika aulia
    The document summarizes the results of an experiment measuring the retention times (R) of caffeine, phenol red, and a mixture of the two compounds using different flow rates (0.4, 0.6, 0.8, 1.0, 1.2 ml/min) of a 30:70 water:methanol solvent system in column chromatography. Retention times decreased with increasing flow rate for all compounds. The retention time also decreased in the order of caffeine, phenol red, and the mixture for each flow rate. Calculations were shown for determining R values from the retention times at different flow rates.

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    of 3

    E.

    Hasil Praktikum
     Tabel Hasil Resolusi variasi laju alir pada perbandingan pelarut ( Air :
    Metanol ) 30 : 70

    R Kafein R PCT R Campuran


    0,4 24.8570 1.2083 1.3574
    0,6 1.1809 2.4724 1.1940
    0,8 1.1319 0.8732 1.1280
    1,0 1.0601 0.8470 0.6660
    1,2 1.0100 7.9260 1.0290
    2. 0,6 ml/menit
    a. Kafein
     Perhitungan :
    ( tR 2−tR 1 )
    1. 0,4 ml/menit R= R=
    W 1+W 2
    a. Kafein
    ( tR 2−tR 1 ) ( 2.802 – 2.569 )
    R= R= R=
    W 1+W 2 (0.1049+ 0.0924)

    ( 3.848−0 ) 3.848 0.233


    R= R R = 1.1809
    (0.1548+ 0) 0.1548 0.1973

    = 24. 857 b. PCT

    b. PCT ( tR 2−tR 1 )
    R= R=
    W 1+W 2
    ( tR 2−tR 1 )
    R= R=
    W 1+W 2 ( 2.571 – 0 ) 2.571
    R=
    (0.0986+ 0) 0.0986
    ( 4.189 – 3.848 )
    R= R = 2.4724
    (0.1518+ 0.1304)
    c. Campuran
    0.341
    ( tR 2−tR 1 )
    0.2822 R= R=
    W 1+W 2
    R = 1.2083
    c. Campuran ( 2.803 – 2.573 )
    R=
    ( tR 2−tR 1 ) (0.0924 +0.1002)
    R= R=
    W 1+W 2
    0.23
    0.1926
    ( 4.189 – 3.848 )
    R= R = 1.194
    (0.1278+ 0.1234)
    3. 0,8 ml/menit
    0.341 a. Kafein
    0.2512
    R = 1.3574
    ( tR 2−tR 1 ) ( tR 2−tR 1 )
    R= R= R= R=
    W 1+W 2 W 1+W 2

    ( 2.106 – 1.931 ) ( 1.545 – 1.435 )


    R= R=
    (0.0798+ 0.0748) (0.0627+ 0.0671)

    0.175 0.11
    R = 1.1319
    0.1546 0.1298
    b. PCT R = 0.847
    ( tR 2−tR 1 ) c. Campuran
    R= R=
    W 1+W 2 ( tR 2−tR 1 )
    R= R=
    W 1+W 2
    (1.932 – 1.797 )
    R=
    (0.0769+ 0.0777) ( 1.630 – 1.492 )
    R=
    (0.1341+0.0728)
    0.135
    0.1546 0.138
    R = 0.8732 0.2069
    c. Campuran R = 0.666
    ( tR 2−tR 1 )
    R= R=
    W 1+W 2 5. 1,2 ml/menit
    a. Kafein
    ( 2.107 – 1.933 )
    R= ( tR 2−tR 1 )
    (0.0719+ 0.0823) R= R=
    W 1+W 2
    0.174
    0.1542 ( 1.404 – 1.285 )
    R=
    R = 1.128 (0.0599+ 0.0579)

    0.119
    R = 1.010
    4. 1,0 ml/menit 0.1178
    a. Kafein b. PCT
    ( tR 2−tR 1 ) ( tR 2−tR 1 )
    R= R= R= R=
    W 1+W 2 W 1+W 2

    ( 1.684 – 1.543 ) ( 1.288 – 1.197 )


    R= R=
    (0.0680+ 0.0650) (0.0548+ 0.0600)

    0.141 0.091
    R = 1.0601
    0.133 0.1148
    R = 0.7926

    b. PCT
    c. Campuran
    ( tR 2−tR 1 )
    R= R=
    W 1+W 2

    ( 1.404 – 1.289 )
    R=
    (0.0547+ 0.0570)

    0.115
    0.1117
    R = 1.029

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