Patents JP 2004-162119 A

Corrosion resistant steel with excellent haz toughness

Abstract
JP2004162119A
[PROBLEMS] To provide a corrosion-resistant steel having excellent toughness of a weld heat-
Japan
affected zone in an indoor environment, a dew environment, an air environment, and a salt damage
environment such as a beach area.
SOLUTION: In mass%, C: 0.03% or less, Si: 0.01 to 3.0%, Mn: 0.1 to less than 3%, P: 0.03% or less, S: Download PDF Find Prior Art Similar
0.01 % Or less, Cr: 4 to 9%, Al: 0.1 to 5%, N: 0.02%, and optionally, Cu: 0.05 to 10%, Ni: 0.05 to 0.05%.
10%, Mo: 0.01 to 1%, V: 0.005 to 0.1%, Nb: 0.005 to 0.050%, Ti: 0.005 to less than 0.03%, Ca: 0. Other languages: Japanese
0005-0.05%, Mg: 0.0005-0.05%, REM: 0.001-0.1%, and a Tp value represented by the following
Inventor: Kenji Kato, Naoki Saito, 謙治 加藤, 直樹 斎藤
formula is 1150 or more. Corrosion-resistant steel having excellent weld toughness characterized by
being 1400 or less.
Tp = 1601-(34% Cr + 287% Al) + (33% Mn + 60% Cu + 107% Ni) Worldwide applications
[Selection diagram] Fig. 1
2002 JP

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Application JP2002329327A events

2002-11-13 Application cled by Nippon Steel Corp, 新⽇本製

鐵株式会社

2002-11-13 Priority to JP2002329327A

2004-06-10 Publication of JP2004162119A

2006-11-15 Application granted

2006-11-15 Publication of JP3845366B2

Status Active

2022-11-13 Anticipated expiration

Info: Cited by (5), Legal events, Similar documents, Priority and

Related Applications

External links: Espacenet, Global Dossier, Discuss

Claims (3) Hide Dependent

1. In mass%,
C: 0.03% or less Si: 0.01 to 3.0%
Mn: less than 0.1 to 3% P: 0.03% or less S: 0.01% or less Cr: 4 to 9%
Al: 0.1 to 5%
N: 0.02%
And optionally Cu: 0.05 to 10%
Ni: 0.05 to 10%
Corrosion-resistant steel having excellent toughness in the weld heat-affected zone, characterized by containing one or more of the following, and having a Tp value
represented by the following formula of 1150 or more and 1400 or less.
Tp = 1601- (34% Cr + 287% Al) + (33% Mn + 60% Cu + 107% Ni)

2. In mass%,
Mo: 0.01 to 1%
V: 0.005 to 0.1%
Nb: 0.005 to 0.050%
The corrosion-resistant steel having excellent toughness of a weld heat-affected zone according to claim 1, wherein one or more of Ti: 0.005 to less than 0.03%
are contained.

3. In mass%,
Ca: 0.0005 to 0.05%
Mg: 0.0005 to 0.05%
REM: 0.001-0.1%
The corrosion-resistant steel having excellent toughness of a weld heat-affected zone according to claim 1, wherein the corrosion-resistant steel contains one or
more of the following.

Description

[0001]
TECHNICAL FIELD OF THE INVENTION
The present invention relates to a high corrosion-resistant steel having excellent base metal strength and weld toughness, and more speciccally, various containers used
in a dew condensation corrosion environment or in an indoor environment, a vacuum container, a low-temperature heat exchanger, a bathroom member, and the like.
Bridges, columns, tunnel reinforcements, building interior and exterior materials, roocng materials, cttings, etc. used in corrosive environments in the atmosphere, as well
as concrete corrosion environments such as various reinforced structures and columns, and ships, bridges, piles, and sheet piles The present invention relates to a steel
having excellent corrosion resistance, a good base metal, and a weld heat affected zone toughness in a corrosive environment such as a seawater corrosive environment
such as a marine structure and a use form.
[0002]
[Prior art]
[Patent Document 1] Japanese Patent Application Laid-Open No. Hei 5-279791 [Patent Document 2] Japanese Patent Application Laid-Open No. Hei 6-179949 [Patent
Document 3] Japanese Patent Application Laid-Open No. Hei 6-179950 [Patent Document 4] Japanese Patent Application Laid-Open No. Hei 6-179951 [Patent Document
5] [Patent Document 6] Japanese Patent Application Laid-Open No. 6-212257 [Patent Document 7] Japanese Patent Application Laid-Open No. 7-3388 [Patent Document
8] Japanese Patent Application Laid-Open No. 11-3500082
Steels used in corrosive environments such as high-temperature wet corrosion environments, dew condensation corrosion environments, atmospheric corrosion
environments, tap water corrosion environments, soil corrosion environments, concrete corrosion environments, and seawater corrosion environments often use some
anticorrosion measures. In recent years, the use of Cr-containing steel and stainless steel for the purpose of improving the corrosion resistance of steel substrates has
been increasing from the viewpoint of improving reliability, simplifying the manufacturing and construction processes, making maintenance free, and saving resources. I
have. However, in the conventional technology, the improvement of corrosion resistance leads to an increase in material cost, and in many cases, it is not a practical
measure from the viewpoint of economy, and in the case of austenite, it is applied because the strength is low. Applications may be limited.
[0004]
As can be seen from the above example, in general, steel containing a certain amount of Cr is susceptible to local corrosion when the corrosive environment becomes
severe, and in order to improve the resistance to corrosion as a measure against this, the content of Cr or Mo is further increased. Was a very common technical
measure.
[0005]
In recent years, JP-A-5-279791, JP-A-6-179949, JP-A-6-179950, JP-A-6-179951, JP-A-6-212256, JP-A-6-212257, JP-A-7-3388, JP-A-11-35082 and the like have proposed
steel in which Al is added to Cr for the purpose of improving corrosion resistance or improving corrosion resistance and workability. Although these steels are recognized
to be effective to some extent in improving corrosion resistance or corrosion resistance and workability, they are inferior in the toughness of the base metal part and the
weld heat affected zone, and are a great hindrance to application to welded structures.
[0006]
[Problems to be solved by the invention]
In view of the above situation, the present invention provides a low-cost steel having a large corrosion resistance in a corrosive environment such as a dew condensation
corrosion environment, an atmospheric corrosion environment, a tap water corrosion environment, a seawater corrosion environment, and the like, and having excellent
weld heat affected zone toughness. It is intended to be.
[0007]
[Means for Solving the Problems]
The present inventors have developed various steels having excellent corrosion resistance in corrosive environments such as dew condensation corrosion environment,
atmospheric corrosion environment, tap water corrosion environment, concrete corrosion environment, and seawater corrosion environment in order to achieve the above
object. It was examined from the viewpoint of. First, as a result of studying various means for improving corrosion resistance in the above-mentioned corrosive
environment at the same time as excellent weld toughness, a steel containing 0.1% to 5% of Al was added to a steel containing 4% to 9% of Cr. It has been found that it
exhibits very good corrosion resistance in many of the corrosive environments described above. However, such a steel has a wide ferrite phase transformation region. For
example, when heated to 1200 ° C. or more during welding, coarse ferrite is generated, and there is a concern that toughness is greatly reduced. The inventors have
conducted many experiments and succeeded in quantifying the relationship with the amount of the added alloy element as a means for suppressing the generation of
ferrite phase transformation that occurs during welding. It has been found that when the amount of alloy addition satisces the range of the expression of Tp, the
formation of ferrite in a high temperature range is suppressed.
[0008]
The outline is
(1) In mass%,
C: 0.03% or less Si: 0.01 to 3.0%
Mn: less than 0.1 to 3% P: 0.03% or less S: 0.01% or less Cr: 4 to 9%
Al: 0.1 to 5%
N: 0.02%
And optionally Cu: 0.05 to 10%
Ni: 0.05 to 10%
Corrosion-resistant steel having excellent toughness in the weld heat-affected zone, characterized by containing one or more of the following, and having a Tp value
represented by the following formula of 1150 or more and 1400 or less.
Tp = 1601- (34% Cr + 287% Al) + (33% Mn + 60% Cu + 107% Ni)
[0009]
(2) In mass%,
Mo: 0.01 to 1%
V: 0.005 to 0.1%
Nb: 0.005 to 0.050%
Ti: The corrosion-resistant steel excellent in toughness of a weld heat-affected zone according to (1), characterized by containing one or more kinds of 0.005 to less than
0.03%.
[0010]
(3) In mass%,
Ca: 0.0005 to 0.05%
Mg: 0.0005 to 0.05%
REM: 0.001-0.1%
(1) or (2), wherein the corrosion-resistant steel has excellent toughness in the heat affected zone of welding.
[0011]
BEST MODE FOR CARRYING OUT THE INVENTION
C: C is an element that improves the strength, but the addition of a certain amount or more leads to a decrease in the toughness of the base metal and the weld heat
affected zone, so the upper limit of the amount added was made 0.03%.
[0012]
Si: It is effective to add Si as a deoxidizing agent and a strengthening element to steel containing 2% or more of Cr, but if the content is less than 0.01%, the deoxidizing
effect is not sujcient, and If the content exceeds 0%, the effect is saturated and, on the contrary, the toughness of the weld heat-affected zone is lowered. Therefore, the
content range is limited to 0.01% or more and 3.0% or less.
[0013]
Cr: It is necessary to contain 4% or more of Cr in order to ensure corrosion resistance. However, adding more than 9% not only increases the cost but also increases the
toughness of the base material and the weld heat affected zone. Therefore, the upper limit content is set to 9%.
[0014]
Al: Al is an important element in addition to Cr in order to ensure corrosion resistance in the present invention, and the content of Al is required to be 0.1% or more from
the viewpoint of ensuring corrosion resistance. If added in excess of 5%, the temperature range of ferrite phase transformation becomes extremely wide, so its content is
limited to 0.1% or more and 5% or less.
[0015]
Mn: In the present invention, Mn mainly acts as an element for improving strength and forming austenite, and is added to suppress the formation of coarse ferrite
promoted by Cr and Al added from the viewpoint of corrosion resistance. That is, as is well known, Cr and Al are ferrite-forming elements, and when they are added in a
large amount, they do not undergo transformation from solidiccation to room temperature to form a ferrite single-phase structure. Even in the heat-affected zone, the
toughness may be signiccantly reduced. Then, the inventors systematically conducted experiments for the purpose of improving the base metal and the toughness
without impairing the corrosion resistance, and as a result, they found that the addition of Mn can avoid this. The specicc constraints will be described later. According to
this, it is necessary that the Mn content be 0.1% or more. However, if the content is 3% or more, the curability increases, so that the content is less than 3%. To be added.
[0016]
N: Since N reduces the toughness of the base metal and the heat affected zone when a large amount of steel sheet is added, N is desirably small, and the upper limit
content is 0.02%.
[0017]
P: If P is present in a large amount, the toughness is reduced. Therefore, it is desirable that P is small, and the upper limit content is 0.03%. It is preferable to minimize the
content that is inevitably mixed.
[0018]
S: Since the presence of a large amount of S lowers the pitting corrosion resistance, a smaller amount is desirable, and the upper limit content is 0.01%. As with P, it is
preferable that the inevitable mixing amount of S be as small as possible.
[0019]
Further, in the present invention, the following elements can be selectively added.
Cu, Ni: Both Cu and Ni have the effect of improving the toughness of the base material and the heat-affected zone, as well as the effect of improving the strength and
suppressing the formation of ferrite. All of these effects require addition of 0.05% or more. However, if any addition exceeds 5%, embrittlement occurs. And
[0020]
Mo: Mo is effective in suppressing the generation and growth of pitting corrosion without impairing the toughness of the base material when added in an amount of
0.01% or more in steel to which Cr and Al are added. Even if added in excess of 0%, not only the effect is saturated but also the toughness is reduced, so the range is
made 0.01% to 1.0%.
[0021]
Nb: Nb is an element that improves strength and toughness without impairing corrosion resistance, and its effect is recognized from 0.005%, but when it exceeds 0.05%,
the toughness of the weld heat affected zone is signiccantly reduced. Therefore, the range is set to 0.005% to 0.05%.
[0022]
V: V is an element that improves the strength without impairing the corrosion resistance, and the effect is recognized at 0.005% or more. However, the addition of a large
amount impairs the toughness as is well known, so the upper limit is set to 0. .1%.
[0023]
Ti: Ti is an element that contributes to recnement of the crystal grain size at a high temperature through formation of a nitride, and can improve the toughness of a heat-
affected zone particularly without impairing corrosion resistance. The effect can be recognized from 0.005% or more in both cases. However, when 0.03% or more is
added, a large amount of carbide precipitates, so that the toughness of the base metal and the heat affected zone is rather inhibited. Therefore, the range is set to 0.005%
to less than 0.03%.
[0024]
Ca, Mg: Ca and Mg are elements that can improve corrosion resistance in steel containing Cr and Al. At present, there are many unclear points in the mechanism, but
improvement of corrosion resistance is recognized at 5 ppm or more in any case, but when added in excess of 500 ppm, not only the effect of improving corrosion
resistance is saturated, but also the tendency of toughness to decrease is obvious. And the addition amount is limited to 5 ppm or more and 500 ppm or less.
[0025]
REM: Further, in the present invention, even if a rare earth element (REM) is appropriately added, the properties of the base metal and the welded portion can be improved
without impairing the corrosion resistance. The addition amount needs to be 0.001% or more, but a large amount of addition impairs toughness and the like, so the upper
limit is made 0.1%.
[0026]
Further, in the present invention, the TP method is introduced in order to improve the toughness of the welded portion which forms the essence of the present invention.
FIG. 1 shows that, based on a steel of 0.015% C-0.15% Si-0.0050%, a welding cycle is given to a material added with Mn, Cr, Al, and optionally Cu and Ni, It is the result of
observing the formation behavior of four transformation points and coarse ferrite. That is, it can be seen that when the Tp expression shown on the horizontal axis is
1150 or more, the formation of a coarse ferrite phase is suppressed. However, when an alloy element is excessively added, a hardened structure is likely to be formed.
Therefore, there is naturally an upper limit, and the upper limit is set to 1400 from experiments. Therefore, the range of the Tp equation is set to 1150 or more and 1400 or
less.
[0027]
When the steel of the present invention is used, after being manufactured as a steel ingot by, for example, ingot ingot lump method or continuous casting method and
other methods, after being manufactured as a steel sheet by hot rolling or hot forging, it is directly used as a steel sheet. It may be used, or it may be manufactured as a
product by processing and welding into any shape according to the user's intention, such as steel pipe (electrically welded pipe, seamless pipe, etc.), mold steel, etc. An
optimum product manufacturing process can be selected due to restrictions of existing manufacturing facilities and the like. Regardless of which manufacturing process
is selected, it is sujcient that the steel of the present invention can be manufactured. Furthermore, in order to obtain appropriate strength and further improve
toughness, quenching and tempering and normalizing may be performed after hot rolling. Furthermore, there is no problem even if a thermomechanical method used in
recent years is applied.
[0028]
The steel of the present invention can be applied to various corrosive environments in which these corrosive environments are combined, such as high-temperature wet
corrosive environments, dew-corrosive corrosive environments, atmospheric corrosive environments, tap water corrosive environments, soil corrosive environments,
concrete corrosive environments, seawater corrosive environments. it can.
[0029]
【Example】
After smelting the steels having the components shown in Table 1, hot rolling was performed so as to obtain a steel sheet having a thickness of 15 mm. Some of the
steels were subjected to heat treatment, and the following tests were performed.
(1) Toughness evaluation test of weld heat affected zone Impact test of base metal and after welding heat cycle [maximum heating temperature; 1400 ° C cooling rate:
15 ° C / s] was performed, transition temperatures were determined, and [base metal Transition temperature]-[transition temperature after thermal cycle] (］ vTrs).
(2) Corrosion test test A 5 mm-thick corrosion test was sampled from a steel plate by cutting, and the test was performed under the following conditions.
Indoor environment : Conducted an exposure test for 100 days without painting in a room with air conditioning and heating
Humid environment : After holding at -20 ° C for 2 hours, holding in an environment of 95% humidity and -25 ° C for 4 hours is repeated 1300 times. In each case, the size
of the rust spot is expressed as a score.
Salt damage environment : The test piece is exposed to the shore splash zone for 17 months.
[0030]
Table 2 shows the results of the test. Steels A to K are all in the range of the present invention, and the toughness of the heat affected zone is in the range of ± 15 ° C. in
the evaluation of ΔvTrs, and there is little decrease in toughness. In addition, as for the corrosion resistance, only a small rust of 2 mm or less was observed in some
parts, and all exhibited good characteristics.
[0031]
On the contrary, L steel to R steel are all comparative steels. That is, the L, M, and N steels deviate from the upper limits of the amounts of C, Si, and Mn, respectively,
within the scope of the present invention. Is big. In the O steel, the range of Cr deviated from the lower limit, indicating that the corrosion resistance was signiccantly
reduced. Since the P steel has an Al content exceeding the upper limit and thus has a very low Tp value, the toughness of the weld heat affected zone is reduced. Further,
in each of the Q and R steels, each element is within the scope of the present invention, but the Tp value deviates from the scope of the present invention. Therefore, the
toughness of the heat affected zone is reduced.
[0032]
[Table 1]
[0033]
[Table 2]
[0034]
【The invention's effect】
As described above, the present invention not only has excellent corrosion resistance in various corrosive environments such as indoor environments, atmospheric
corrosive environments, and seawater corrosive environments, such as dew-contaminated corrosive environments, but also has an important welding heat affected zone
in welded structures. It is possible to provide steel with excellent toughness at low cost, and it is extremely large that contributes to industrial development.
[Brief description of the drawings]
1 is a diagram illustrating the presence or absence of a relationship and δ ferrite and A 4 transformation point which is measured and calculated values of A 4
transformation point (Tp value).
Cited By (5)

Publication number Priority date Publication date Assignee Title

WO2005087964A1 * 2004-03-15 2005-09-22 Nippon Steel Corrosion-resistant steel excellent in toughness of base metal and weld and process
Corporation for producing the same

JP2010065301A * 2008-09-12 2010-03-25 Nippon Steel Corp High-strength steel excellent in corrosion resistance at coating in seashore area, and
method of producing the same

CN101376953B * 2007-08-28 2010-08-11 宝⼭钢铁股份有限公 High-corrosion resistant high-strength weather resisting steel and manufacturing
司 method thereof

WO2010113828A1 * 2009-03-30 2010-10-07 新⽇本製鐵株式会社 Corrosion-resistant steel for use in chimney or que of natural gas combustion or
liqueced petroleum gas combustion plant
 Publication number Priority date Publication date Assignee Title

JP2012167305A * 2011-02-10 2012-09-06 Nittetsu Elex Co Ltd Member for vacuum apparatus and method of manufacturing the same

Family To Family Citations

* Cited by examiner, † Cited by third party, ‡ Family to family citation

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