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S TA N D A R D S

Derivatization Reagents

Recommended Reagents for GC Derivatization


Chemically Modify Your Sample to Improve the Chromatography!
Recommended Reagents for GC Derivatization
COMPOUND TYPE OF DERIVATIVE ECD* POSSIBLE REAGENT CHOICES
Alcohols Acetate Acetic Anhydride/Pyridine
TMS Sil-Prep®, BSTFA/TMCS
t-Butyl Dimethyl Silyl Ether t-Butyl-DMCS/Imidazole, MTBSTFA
Aldehydes Dimethyl Acetal DMF/DMA
Amines TMS Sil-Prep®
Acetate Pyridine-Plus™
Amine (Primary and Secondary) Acetate Acetic Anhydride/Pyridine
TMS MSHFBA
Amino Acids TMS BSTFA
HFB-Isobutyl Ester HFB-IBA Kit
Trifluoroacetate X Trifluoroacetic Anhydride
Bile Acids Acetate Pyridine-Plus™
Carbohydrates Acetate Acetic Anhydride/Pyridine
TMS Power Sil-Prep®
Catecholamines Trifluorocetate X N-(Trifluoroacetyl)imidazole
Dibasic Acids (short chain) Dipropyl Ester BF3/Propanol
Drugs:
Alkaloids Heptafluorobutyrate X Heptafluorobutyric Anhydride
TMS MSTFA, Sil-Prep®
Antibiotics TMS Sil-Prep®, Power Sil-Prep®
Anticonvulsants TMS MSTFA, BSA/TMCS
Barbiturates N-Methyl Barb-Prep®
Dimethyl Ketal DMF/DMA
Cannabinoids Trifluoroacetate X N-Trifluoroacetylimidazole
TMS BSTFA, MSTFA
Estrogens Acetate Pyridine-Plus™
Fatty Acids:
C9 and Longer Methyl Ester BF3/Methanol, Methanolic HCl, Meth-Prep™ I
Short Chain (Up to C8) TMS MSTFA
Methyl Ester BF3/Methanol, Methanolic HCl, Meth-Prep™ I
Glycerides (mono and di) Acetate Acetic Anhydride/Pyridine
Glycerides (mono, di and tri) Methyl Ester Na Methoxide/Methanol, Meth-Prep™ II
Glycolipids, Sphingolipids Methyl Ester Na Methoxide/Methanol, Meth-Prep™ II
Hydroxyamines TMS BSTFA
Hydroxy Groups (Primary/Secondary) Heptafluorobutyrate X Heptafluorobutylimidazole
Trifluoroacetate X N-Trifluoroacetylimidazole
17-Ketosteroids TMS DMF-Sil-Prep®
Krebs Cycle Acids Methyl Ester BF3/Methanol
Phenols Heptafluorobutyrate X Heptafluorobutyric Anhydride
TMS BSTFA
Methyl Esters DMF/DMA
Polyols TMS Sil-Prep®, Power Sil-Prep®
Steroids TMS Sil-Prep®
Acetate Pyridine-Plus™
Trifluoroacetate X Trifluoroacetic Anhydride
*Derivatives suitable for use with Electron Capture Detector (ECD).

When do you use derivatization?


When you need to:
1. Increase or decrease the volatility of the analytes to improve separation
2. Improve peak symmetry by reducing interaction of sample and column
3. Increase detector response (i.e. ECD)
4. Enhance thermal stability
© Copyright 2004 Alltech Associates, Inc. Contact your Alltech office or distributor for current or local prices.

40
S TA N D A R D S
Derivatization Reagents

Ready-To-Use Silylation Mixes


Silylation replaces an active hydrogen atom (-OH, t-Butyldimethylchlorosilyl/Imidazole
-NH2, -NHR, -SH) with a silyl group. Generally it reduces
• Derivatives of alcohols are 10,000 time more stable
the polarity of the compound and decreases possibility
than TMS ethers to hydrolysis
of hydrogen bonding.
T-BUTYLDIMETHYLCHLOROSILYL/IMIDAZOLE
DESCRIPTION QTY. PART NO. PRICE
t-BuDMCS/Imidazole 10 x 1mL 18028

POWER Sil-Prep® (TMSIM:BSA:TMCS)


• Powerful reagent for sterically hindered groups

POWER SIL-PREP®
DESCRIPTION QTY. PART NO. PRICE
POWER Sil-Prep® 10 x 1mL 18012

5421

Sil-Prep® (HMDS:TMCS:pyridine) DMF Sil-Prep® (HMDS:TMCS:DMF)


• General purpose reagent for making TMS derivatives • Prevents enolization of keto groups

SIL-PREP® POWER SIL-PREP®


DESCRIPTION QTY. PART NO. PRICE DESCRIPTION QTY. PART NO. PRICE
Sil-Prep® 10 x 1mL 18013 DMF Sil-Prep® 10 x 1mL 18015

Silylation Reagent Strength What are the requirements for a


HMDS good reagent?
TMCS It will:
Sil-Prep®
1. Not cause any rearrangements or
MSTFA
structural changes in the analyte
MSHFBA
BSA 2. Produce a reaction that is 95-
BSTFA 100% complete
TMSIM 3. Produce a stable derivative
BSTFA + 1% TMCS 4. Not contribute to loss of sample
POWER Sil-Prep® during the reaction
5. Produce a derivative that is inert
to the column and connections
6. Not produce interfering byproducts
Need Ion Chromatography
Standards?
Alltech has the most complete
selection of IC standards and the
ability to manufacture custom
standards. See pages 319-320.

3493

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41
S TA N D A R D S
Derivatization Reagents

Individual Silylation Reagents


BSA [N,O-bis(trimethylsilyl)acetamide] MSTFA (N-Methyl-N-trimethylsilyltrifluoroacetamide)
• Powerful silylating reagent and solvent for polar • Best reagent for drug analysis because excess reagent
compounds and byproducts elute during solvent delay
• May be used directly on HCl salts of compounds
BSA MSTFA
DESCRIPTION QTY. PART NO. PRICE DESCRIPTION QTY. PART NO. PRICE
BSA 10mL 18056 MSTFA 10mL 18061
BSA 25mL 18057 MSTFA 1 x 1mL 18038
BSA 10 x 1mL 18034

BSTFA (N,O-bis(trimethylsilyl)trifluoroacetamide) MTBSTFA [N-(tert-butyldimethylsilyl)-


• More volatile reagent and byproducts compared to BSA N-methyltrifluoroacetamide]
• Powerful silylating reagent; even more effective • Derivatives more stable than common TMS derivatives
combined with TMCS as a catalyst • Produces a distinct M-57 ion in GC/MS analysis
BSTFA • Even more effective when combined with TBDMCS as
DESCRIPTION QTY. PART NO. PRICE
a catalyst
BSTFA 10mL 18085
BSTFA 10 x 1mL 18040 MTBSTFA
BSTFA + 1% TMCS 10mL 18087 DESCRIPTION QTY. PART NO. PRICE
BSTFA + 1% TMCS 10 x 1mL 18089 MTBSTFA 10 x 1mL 18097
MTBSTFA 10mL 18102
MTBSTFA + 1% TBDMCS 10 x 1mL 18155
CMDMCS MTBSTFA + 1% TBDMCS 10mL 18148
• Longer retention times than TMCS derivatives
• Enhanced ECD response
CMDMCS
DESCRIPTION QTY. PART NO. PRICE
TMCS (Trimethylchlorosilane)
CMDMCS 5mL 18031 • Similar to HMDS when used alone
DMCS (Dimethylchlorosilane) • Very effective as a catalyst to other reagents
TMCS
• DMS derivatives are more sensitive to hydrolysis than DESCRIPTION QTY. PART NO. PRICE
TMS derivatives TMCS 3 x 10mL 18091
DMCS TMCS 10 x 1mL 18084
DESCRIPTION QTY. PART NO. PRICE
DMCS 3 x 10mL 18071

HMDS (Hexamethyldisilazane) TMSIM (N-Trimethylsilylimidazole)


• Slow and inefficient used alone • Preferentially silylates hydroxyl groups
• Very effective in combination with TMCS • Best silylation reagent when water is present
HMDS TMSIM
DESCRIPTION QTY. PART NO. PRICE DESCRIPTION QTY. PART NO. PRICE
HMDS 25mL 18069 TMSIM 10 x 1mL 18050
HMDS 10 x 1mL 18003

MSHFBA (N-Methyl- Glass Conditioning Reagent


N-trimethylsilylheptafluorobutyramide) Glass-Prep™ (5% DMDCS in toluene)
• Similar to MSTFA but does not produce harmful • Deactivate any glass surface
deposits in FID
MSHFBA GLASS-PREP™
DESCRIPTION QTY. PART NO. PRICE DESCRIPTION QTY. PART NO. PRICE
MSHFBA 10mL 214610 Glass-Prep™ 100mL 9700
MSHFBA 20 x 1mL 2146201 Glass-Prep™ 400mL 2233
DMDCS, Neat 10 x 5mL 18090
© Copyright 2004 Alltech Associates, Inc. Contact your Alltech office or distributor for current or local prices.

42
S TA N D A R D S
Derivatization Reagents

Alkylation (Esterification) Reagents


Alkylation replaces an acidic hydrogen (carboxylic acids, phenols) with an alkyl group. Alkyl esters are extremely
stable and can be stored for long periods of time.
BF3/Methanol (14%) BF3/n-Butanol (14%)
• Convenient and inexpensive method for forming • n-Butyl esters for short chain mono- and dicarboxylic
esters acids
• Reagent is stable for six months if refrigerated and • Retention times longer than methyl esters
kept dry
BF3/METHANOL (14% W/V) BF3/n-BUTANOL (14% W/V)
DESCRIPTION QTY. PART NO. PRICE DESCRIPTION QTY. PART NO. PRICE
BF3/Methanol 400mL 18002 BF3/n-Butanol 10 x 5mL 18021
BF3/Methanol 100mL 2168100
BF3/Methanol 25 x 5mL 18017
BF3/Methanol 10 x 5mL 18041

BCl3/Methanol (10%) Meth-Prep™ I


• More stable than 14% BF3/Methanol– may be stored • On-column derivatization
for several months at room temperature • Aqueous solution does not give solvent peak
BCl3/METHANOL (10% W/V) METH-PREP™ I
DESCRIPTION QTY. PART NO. PRICE DESCRIPTION QTY. PART NO. PRICE
BCl3/Methanol 25 x 5mL 18032 Meth-Prep™ I 10 x 1mL 18005
BCl3/Methanol 10 x 5mL 18080

BF3/n-Propanol (14%) Instant Methanolic HCl Reagent Kit


• n-Propyl esters for short chain mono- and dicarboxylic • Acid catalyzed esterification of alcohols
acids • Reagent is generated before use and is stable for one
• Retention times longer than methyl esters week at room temperature
BF3/n-PROPANOL (14% W/V) INSTANT METHANOLIC HCl REAGENT KIT
DESCRIPTION QTY. PART NO. PRICE DESCRIPTION QTY. PART NO. PRICE
BF3/n-Propanol 100mL 2172100 Instant Methanolic HCl ea 18053
BF3/n-Propanol 10 x 5mL 18042 Reagent Kit
Anhydrous Acetyl Chloride 5 x 2.8mL 18095
Anhydrous Methanol 10 x 5mL 18157

Transesterification Reagents
Transesterification is the process of converting one type of ester into another. Most commonly this is a very large
ester (i.e. triglycerides, steryl esters, wax esters, phospholipids) converted into a methyl ester that is more easily
analyzed.
Meth-Prep™ II Sap Ester Reagent Kit
• In one step forms fatty acid methyl esters from • Useful for converting lipids to fatty acid methyl esters
triglycerides at room temperature • Reagent prepared fresh before using
• Requires no extraction before injecting into GC SAP-ESTER KIT
• Faster than sodium methoxide reagents DESCRIPTION QTY. PART NO. PRICE
Sap-Ester Kit ea 18026
METH-PREP II™

DESCRIPTION QTY. PART NO. PRICE


Meth-Prep™ II 10 x 1mL 18007 Sodium Methoxide/Methanol
• Converts a wide range of large esters to fatty acid
methyl esters
SODIUM METHOXIDE/METHANOL
DESCRIPTION QTY. PART NO. PRICE
Sodium Methoxide/Methanol 10 x 5mL 18018
Sodium Methoxide/Methanol 25mL 218025
© Copyright 2004 Alltech Associates, Inc. Contact your Alltech office or distributor for current or local prices.

43
S TA N D A R D S
Derivatization Reagents

Acylation Specialty Reagents


Acylation reduces the polarity of amino, hydroxyl Amino Acid Derivatization Kits
and thiol groups on multi-functional molecules such as
• Simple two step procedure
carbohydrates and amino acids.
• Three different reagents available: TFA, PFP and HFB
Acetic Anhydride/Pyridine AMINO ACID DERIVATIZATION KITS
• Used for acetylation of alcoholic and phenolic DESCRIPTION QTY. PART NO. PRICE
hydroxyl groups; and primary and secondary amino TFA-IPA Derivatization Kit ea 18092
PFP-IPA Derivatization Kit ea 18093
groups
HFB-IPA Derivatization Kit ea 18094
ACETIC ANHYDRIDE/PYRIDINE
DESCRIPTION QTY. PART NO. PRICE Barb-Prep™
Acetic Anhydride/Pyridine Kit ea 18100
• On-column methylation of barbiturates
Acetic Anhydride 10 x 1mL 18103
• No byproduct formation
Pyridine-Plus™ BARB-PREP™
• Much more powerful than acetic anhydride/pyridine DESCRIPTION QTY. PART NO. PRICE
Barb-Prep™ 10 x 1mL 18009
• Rapid reaction and fewer byproducts
PYRIDINE-PLUS™ DMF-DMA
DESCRIPTION QTY. PART NO. PRICE • Novel reagent for derivatization of fatty acids, amino
Pyridine-Plus™ Kit ea 18105
acids, amines and barbiturates
Fluorinated Imidazoles DMF-DMA
DESCRIPTION QTY. PART NO. PRICE
• No acidic byproducts compared to anhydride reagents DMF-DMA 10 x 1mL 18051
FLUORINATED IMIDAZOLES
DESCRIPTION QTY. PART NO. PRICE
TFAI (N-Trifluoroacetylimidazole) 10 x 0.2g 18046
HFBI (N-Heptafluorobutyrylimidazole) 10 x 0.2g 18048 LC Reagents
Perfluoroalkyl Anhydrides UV Enhancing
• Produces derivatives suitable to electron capture UV ENHANCING
detection DESCRIPTION QTY. PART NO. PRICE
p-Bromophenacyl Derivatization Kit — 18036
PERFLUOROALKYL ANHYDRIDES p-Nitrobenzoyloxyamine HCl (PNBA) 1g 510113
DESCRIPTION QTY. PART NO. PRICE
Trifluoroacetic Anhydride 5 x 1mL 18083
Pentafluoropropionic Anhydride 25g 65192
Fluorescence Enhancing
Pentafluoropropionic Anhydride 5 x 1mL 18116 FLUORESCENCE ENHANCING
Heptafluorobutyric Anhydride 25g 63163 DESCRIPTION QTY. PART NO. PRICE
Heptafluorobutyric Anhydride 5 x 1mL 18118 o-Phthalaldehyde (OPA) 5g 35606

Get all of the information you need to make the best use of derivatization!

Modern Derivatization Methods for Handbook of Analytical Derivatization


Separation Science Reactions
This book concentrates on synthesis This book describes analytical
of derivatives for HPLC and Capillary derivatization methods organized according
6745 Electrophoresis, techniques of great 6746
to the sample to be derivatized.
interest in the pharmaceutical field.

MODERN DERIVATIZATION METHODS FOR SEPARATION SCIENCE HANDBOOK OF ANALYTICAL DERIVATIZATION REACTIONS
DESCRIPTION PART NO. PRICE DESCRIPTION PART NO. PRICE
Modern Derivatization Methods for 5354 Handbook of Analytical Derivatization 1149
Separation Science Reactions
© Copyright 2004 Alltech Associates, Inc. Contact your Alltech office or distributor for current or local prices.

44
S TA N D A R D S
Ion-Pair Reagents

Alltech IPC™ Reagents


• Equivalent to Waters PIC® Reagents Table 1 - Alltech IPC™ Reagents
• Preformulated at optimum concentration and pH ALLTECH’S DESIGNATION WATERS’ EQUIVALENT
IPC™ A PIC® A
• Convenient – Simply dilute with HPLC grade solvents IPC™ B5 PIC® B5
“A” Series IPC™ B6 PIC® B6
IPC™ B7 PIC® B7
• Used for chromatography of acidic compounds IPC™ B8 PIC® B8
“B” Series Low UV IPC™ A Low UV PIC® A
Low UV IPC™ B5 Low UV PIC® B5
• Used for chromatography of basic compounds Low UV IPC™ B6 Low UV PIC® B6
Low UV IPC™ B7 Low UV PIC® B7
A SERIES AND B SERIES Low UV IPC™ B8 Low UV PIC® B8
DESCRIPTION QTY. PART NO. PRICE
IPC™ A, Tetrabutylammonium 5 x 15mL 185101
Phosphate
IPC™ B5, Sodium 5 x 25mL 185110
Pentanesulfonate Alltech IPC™ B7
IPC™ B6, Sodium 5 x 25mL 185140 5870
Hexanesulfonate 1 2
IPC™ B7, Sodium 5 x 25mL 185103
Heptanesulfonate
1. Niacinamide
IPC™ B8, Sodium Octanesulfonate 5 x 25mL 185142 4 2. Riboflavin
3. Pyridoxine
4. Thiamine
“Low UV”* Series
• Suitable for use at wavelengths down to 200nm 3

LOW UV SERIES
DESCRIPTION QTY. PART NO. PRICE
Low UV IPC™ A, 5 x 20mL 185149
Tetrabutylammonium sulfate
Low UV IPC™ B5, 5 x 20mL 184198
Tetrabutylammonium phosphate
Low UV IPC™ B5, 5 x 20mL 184199 0 2 4 6 8 Min.
Tetrabutylammonium phosphate
Low UV IPC™ B5, 5 x 20mL 184282 Column: Adsorbosphere HS C18, 7µm,
®

Tetrabutylammonium phosphate 250 x 4.6mm HPLC Column


Mobile Phase: Methanol:Water (50:50) both with IPC™ B7
Low UV IPC™ B5, 5 x 20mL 184283
Tetrabutylammonium phosphate Flow rate: 1.0mL/min
Detector: UV at 254nm
*For use at wavelengths below 240nm.

Ion-Pair Salts
Alltech offers high-purity ion-pairing salts for those
wishing to formulate their own mobile phases.
• High purity for HPLC applications
ION-PAIR SALTS
DESCRIPTION QTY. PART NO. PRICE Need Ion Chromatography
1-Pentanesulfonate 25g 403125 Standards?
1-Hexanesulfonate 25g 403126 Alltech has the most complete
1-Heptanesulfonate 25g 403127 selection of IC standards and the
1-Octanesulfonate 25g 403128 ability to manufacture custom
Tetrabutylammonium Phosphate, 10mL 680502 standards. See pages 319-320.
0.5M, pH 7.5)
3493

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45
S TA N D A R D S
Gas Standards

Gas Standards
• Portable, lightweight and easy to use disposable
cylinders
• Each standard comes with a certificate of analysis

6346 6347 6675

MicroMAT™-10 MicroMAT™-14 MicroMAT™-58


10L Disposable Cylinder 14L Disposable Cylinder 58L Disposable Cylinder

Single Component Gas Standards


SINGLE COMPONENT MIXTURES SINGLE COMPONENT MIXTURES
ANALYTE/ ANALYTE/
CONCENTRATION BALANCE CYLINDER SIZE PART NO. PRICE CONCENTRATION BALANCE CYLINDER SIZE PART NO. PRICE
Acetylene Nitrous Oxide
1% Helium MicroMAT™-10 G0413 98.00% — MicroMAT™-14 M7009
1% Nitrogen MicroMAT™-10 G0423 0.1ppm Nitrogen MicroMAT™-14 24042
Argon 1.0ppm Nitrogen MicroMAT™-14 24044
99.995% — MicroMAT™-14 M7003 100ppm Nitrogen MicroMAT™-10 G1721
Carbon Dioxide 1000ppm Nitrogen MicroMAT™-10 G1722
99.80% — MicroMAT™-14 M7006 Methane
100ppm Helium MicroMAT™-10 G1211 99.00% — MicroMAT™-14 M7011
1000ppm Helium MicroMAT™-10 G1212 100ppm Helium MicroMAT™-10 G0111
1% Helium MicroMAT™-10 G1213 1000ppm Helium MicroMAT™-10 G0112
10% Helium MicroMAT™-10 G1214 1% Helium MicroMAT™-10 G0113
Carbon Monoxide 10% Helium MicroMAT™-14 24066
1000ppm Helium MicroMAT™-10 24047 100ppm Nitrogen MicroMAT™-14 M7029
10% Helium MicroMAT™-10 24054 1% Nitrogen MicroMAT™-10 G0123
Ethane 10% Nitrogen MicroMAT™-14 24067
99.00% — MicroMAT™-14 M7012 10ppm Air MicroMAT™-14 19781
Ethylene Oxygen
100ppm Helium MicroMAT™-10 G0311 99.5% — MicroMAT™-14 M7001
100ppm Helium MicroMAT™-14 M7030 100ppm Helium MicroMAT™-14 M7121
1000ppm Helium MicroMAT™-10 G0312 1% Helium MicroMAT™-10 G1613
1000ppm Nitrogen MicroMAT™-14 24022 1% Nitrogen MicroMAT™-10 G1623
8-10ppm Air MicroMAT™-14 24096 2% Nitrogen MicroMAT™-14 24094
Helium 6% Nitrogen MicroMAT™-14 24095
99.995% — MicroMAT™-14 M7005 10% Nitrogen MicroMAT™-10 G1624
Hydrogen Propane
99.99% — MicroMAT™-14 M7004 99.00% — MicroMAT™-14 M7014
100ppm Nitrogen MicroMAT™-14 M7125 Vinyl Chloride (NIST Traceable)
1000ppm Nitrogen MicroMAT™-10 G1522 10ppm Nitrogen MicroMAT™-14 G2001
1% Nitrogen MicroMAT™-10 G1523 1000ppm Nitrogen MicroMAT™-14 G2004
Nitrogen
99.998% — MicroMAT™-14 M7002
© Copyright 2004 Alltech Associates, Inc. Contact your Alltech office or distributor for current or local prices.

46
S TA N D A R D S
Gas Standards

Multi-Component Gas Mixtures


MULTI-COMPONENT GAS MIXTURES
DESCRIPTION CONCENTRATION CYLINDER SIZE PART NO. PRICE
BTEX in Nitrogen
Benzene, Ethylbenzene, Toluene, Xylene 1ppm (mix) MicroMAT™-58 24076
10ppm (mix) MicroMAT™-58 24099
100ppm (mix) MicroMAT™-58 24115
C2 to C4 Alkyne in Nitrogen
Acetylene, 1-Butyne, 2-Butyne, Propyne 15ppm each MicroMAT™-10 19797
C1 to C4 Hydrocarbons in Nitrogen
Methane, Ethane, Ethylene, Acetylene, Propane, Propylene, 15ppm each MicroMAT™-14 24130
Propyne, n-Butane
C4 Hydrocarbons in Nitrogen
n-Butane, Isobutane, 2-Butene (cis and trans), 1-Butene, 15ppm each MicroMAT™-14 24132
Isobutylene, 1,3-Butadiene, Ethyl Acetylene
2-Olefin Mixture in Nitrogen
2-Butene (cis and trans), 2-Pentene (cis and trans), 2-Hexene 15ppm each MicroMAT™-14 19775
(cis and trans)
C2 to C6 Olefin Mixture in Helium
Ethylene, Propylene, 1-Butene, 1-Pentene, 1-Hexene 100ppm each MicroMAT™-14 19784
1000ppm each MicroMAT™-14 M7020
C2 to C6 Olefin Mixture in Nitrogen
Ethylene, Propylene, 1-Butene, 1-Pentene, 1-Hexene 1000ppm each MicroMAT™-14 M7019
C1 to C6 n-Paraffin Mixture in Helium
Methane, Ethane, Propane, Butane, Pentane, Hexane 100ppm each MicroMAT™-14 19782
1000ppm each MicroMAT™-14 M7018
C1 to C6 n-Paraffin Mixture in Nitrogen
Methane, Ethane, Propane, Butane, Pentane, Hexane 15ppm each MicroMAT™-14 19772
100ppm each MicroMAT™-14 19783
1000ppm each MicroMAT™-14 M7017
Branched Paraffin Mixture in Nitrogen
Isobutane, 2-Methylbutane, 2,2-Dimethylpropane, 2- 15ppm each MicroMAT™-14 19774
Methylpentane, 3-Methylpentane, 2,2-Dimethylbutane
CO and CO2 in Nitrogen
Carbon Monoxide, Carbon Dioxide 25ppm (CO), 1000ppm (CO2) MicroMAT™-14 24136
CO, CO2, Methane, Ethane, Ethylene, Acetylene in Nitrogen
1% each MicroMAT™-14 M7035
CO, CO2, Methane, H2, O2 in Nitrogen
1% each MicroMAT™-14 M7036
CO, CO2, CH4, H2, O2, N2 in Helium
Carbon Monoxide, Carbon Dioxide, Methane, Hydrogen, Oxygen, 5% (CO), 5% (CO2), 4% (CH4), 4% MicroMAT™-14 19792
Nitrogen (H2), 5% (O2), 5% (N2)
CO, CO2, O2 in Nitrogen
Carbon Monoxide, Carbon Dioxide, Oxygen 7% (CO), 15% (CO2), 3% (O2) MicroMAT™-14 M7041
CO, CO2, CH4, O2 in Nitrogen
Carbon Monoxide Carbon Dioxide, Methane, Oxygen 7% (CO), 15% (CO2), 4.5% (CH4), MicroMAT™-14 19791
7% (O2)
CO, CO2, H2, O2 in Nitrogen
0.5% each MicroMAT™-14 24138
0.5% each (CO, CO2, O2), 5% H2 MicroMAT™-14 M7037
CO2, O2 in Nitrogen
1% each MicroMAT™-14 24029
1% (CO2), 2% (O2) MicroMAT™-14 M7040
2% (CO2), 24% (O2) MicroMAT™-14 24034
3% (CO2), 17% (O2) MicroMAT™-14 24035

For a complete listing of Matheson Gas Standards


and Accessories, request datasheet 19772D

© Copyright 2004 Alltech Associates, Inc. Contact your Alltech office or distributor for current or local prices.

47
S TA N D A R D S
Gas Standards

Special Gas Standards Hardware for Using Gas


Reactive Gas Standards Cylinders
REACTIVE GAS STANDARDS
DESCRIPTION CONCENTRATION CYLINDER SIZE PART NO. PRICE MicroMAT™-10 Syringe Adapter
Hydrogen Sulfide in 10ppm MicroMAT-58 24102 • Maximum pressure 120psig
Nitrogen
95ppm MicroMAT-58 24105
Nitric Oxide in 20-30ppm MicroMAT-58 24107
Nitrogen

Natural Gas Standards


• Certificate of analysis
5386

MicroMAT™-10 Syringe
• Shelf life one year Adapter
Natural Gas Standards Concentrations MICROMAT™-10 SYRINGE ADAPTER
GPA CALORIMETRIC HIGH ETHANE HELIUM-ENRICHED DESCRIPTION CYLINDER SIZE PART NO. PRICE
HELIUM 0.50 — — 2.00 Aerosol Syringe Adapter MicroMAT-10 8048
NITROGEN 5.00 2.50 9.00 1.60 Replacement Septa, 12/pk — 75801
CARBON DIOXIDE 1.00 3.00 0.50 0.20
ETHANE 9.00 3.50 12.50 3.00
PROPANE 6.00 1.00 7.00 1.70
ISOBUTANE 3.00 0.40 3.00 1.00 MicroMAT™-14 Syringe Adapter
N-BUTANE 3.00 0.40 3.00 1.00
• Maximum pressure 240psig
ISOPENTANE 1.00 0.15 0.50 0.30
N-PENTANE 1.00 0.15 0.50 0.30 • May be used with any 1/8"
NEOPENTANE — 0.10 — — NPT (F) outlet
N-HEXANE — 0.05 — —
N-HEPTANE — 0.02 — —
METHANE Balance Balance Balance Balance

NATURAL GAS STANDARDS


DESCRIPTION CONCENTRATION CYLINDER SIZE PART NO. PRICE
Natural Gas GPA See above MicroMAT™-14 24100 5385

Standard MicroMAT™-14 Syringe


Natural Gas See above MicroMAT™-14 24116 Adapter
Calorimetric Standard MICROMAT™-14 SYRINGE ADAPTER
Natural Gas High See above MicroMAT™-14 24128 DESCRIPTION CYLINDER SIZE PART NO. PRICE
Ethane Standard Syringe Adapter MicroMAT-14 8810
Natural Gas Helium- See above MicroMAT™-14 24131 Replacement Septa, 10/pk — 8812
Enriched Standard

MicroMAT™-58 Regulator
• Stainless steel with hose
barb outlet
Need Ion Chromatography • Push button on/off control
Standards? • Preset 0.3SLPM flow rate
Alltech has the most complete
selection of IC standards and the
ability to manufacture custom
standards. See pages 319-320.

3493
6674

MicroMAT™-58 Regulator
MICROMAT™-10 REGULATOR
DESCRIPTION CYLINDER SIZE PART NO. PRICE
0-30psig, C-10 Valve MicroMAT-58 37201
© Copyright 2004 Alltech Associates, Inc. Contact your Alltech office or distributor for current or local prices.

48
S TA N D A R D S
Drug Standards

Quik-Chek™ Chromatographic Drug Solutions


• Ready to use
• No DEA license required (USA and Canada†)
• Quality certificate supplied
• No administrative fees
These solutions are prepared in a stable solvent
suitable for chromatographic use. The concentration
stated is the amount of base drug per unit volume—no
salts or hydration levels to consider. Standards are
quantitative unless stated otherwise and each unit
comes with a quality certificate.
They are supplied in sealed silanized glass ampules
under an argon blanket for maximum stability. A
silanized glass screw-cap vial with T.O.P. Hat™ closure is
supplied for storage after the ampule has been opened.
†See ordering instructions on page 52 for locations outside the USA and Canada.
6244

Quik-Cheks™ save time and they guarantee quality and easy


use.

QUIK-CHEK™ DRUG STANDARDS QUIK-CHEK™ DRUG STANDARDS


CLASSIFICATION CLASSIFICATION
AMT IN 1ML SOLVENT

AMT IN 1ML SOLVENT


INTERNAL STANDARD

INTERNAL STANDARD
THERAPEUTIC DRUG

THERAPEUTIC DRUG
ABUSED DRUG

ABUSED DRUG
METABOLITE

METABOLITE

DESCRIPTION PART NO. PRICE DESCRIPTION PART NO. PRICE


• • Acetaminophen 1mg 6017253 • 4-Bromo-2,5-dime- 1mg 015703
• Acetazolamide 1mg 016023 thoxyphenethylamine
• 6-Acetylcodeine* 1mg 014803 • Brompheniramine 1mg 013823
• Acyclovir 1mg 016343 • Bumetanide 1mg 016053
• Albuterol 1mg 015833 • Buprenorphine 1mg 016513
• Allobarbital 1mg 6011673 • Bupropion 1mg 6015483
• dl-Alphaprodine 1mg 6017973 • Buspirone 1mg 015933
• Alphenal 1mg 6010323 • Butabarbital 1mg 011033
• Alprazolam 250µg 014273 • Butalbital 1mg 010273
• Amiloride 1mg 016033 • Butethal 1mg 6011043
• 7-Aminoclonazepam* 1mg 015723 • Caffeine 1mg 017283
• 7-Aminoflunitrazepam* 1mg 015733 • Cannabidiol 1mg 013893
• Amitriptyline 1mg 017753 • Cannabinol 1mg 013883
• Amitriptyline-d3 1mg 6019003 • Captopril 1mg 015843
• Amobarbital 1mg 010393 • Carbamazepine 1mg 6017883
• • Amoxapine 1mg 6013923 • Carbamazepine-10,11- 1mg 6013463
• • • d-Amphetamine 1mg 010023 epoxide
• l-Amphetamine 1mg 014923 • l-9-Carboxy-11-nor-Δ- 100µg 01422
• d-Amphetamine-d6 100µg 01914 9-THC (Qualitative)
• Aprobarbital 1mg 010553 • dl-9-Carboxy-11- 100µg 01910
• • Barbital 1mg 010733 nor-Δ-9-THC-d3
• Bendroflumethiazide 1mg 016043 (Qualitative)
• Benzocaine 1mg 6014253 • Carisoprodol 1mg 6013753
• Benzoylecgonine 1mg 018203 • 4-Chlorotestosterone 1mg 6014893
• Benzoylecgonine-d3 100µg 01911 • Chlorpheniramine 1mg 6017033
• d-Benzphetamine 1mg 6017763 • Chlorpromazine 1mg 6017203
• Benzylpiperazine 1mg 015813 • Cimetidine 1mg 6014263
• Boldenone 1mg 6015053 • Ciprofloxacin 1mg 016353
• Bromazepam 1mg 6013563 • Clobazam 1mg 015753

© Copyright
*In 2004 **In
acetonitrile. Alltech Associates,***In
chloroform. Inc. DMF. Contact your Alltech office or distributor for current or local prices.

49
S TA N D A R D S
Drug Standards

QUIK-CHEK™ DRUG STANDARDS QUIK-CHEK™ DRUG STANDARDS


CLASSIFICATION CLASSIFICATION

AMT IN 1ML SOLVENT

AMT IN 1ML SOLVENT


INTERNAL STANDARD

INTERNAL STANDARD
THERAPEUTIC DRUG

THERAPEUTIC DRUG
ABUSED DRUG

ABUSED DRUG
METABOLITE

METABOLITE
DESCRIPTION PART NO. PRICE DESCRIPTION PART NO. PRICE
• Clomipramine 1mg 6014613 • Ethacrynic Acid 1mg 016093
• Clonazepam 1mg 017943 • Ethchlorvynol 1mg 017333
• Clonidine 1mg 6014023 • Ethinamate 1mg 6017063
• Clopamide 1mg 016063 • Ethosuximide 1mg 018453
• Clorazepate 1mg 6015543 • Ethotoin 1mg 6013593
• Clostebol 1mg 6015103 • dl-N- 1mg 014963
• Clozapine 1mg 016213 Ethylamphetamine
• Cocaethylene* 1mg 6015363 • • Ethylmorphine 1mg 018053
• • l-Cocaine 1mg 018003 • Famotidine 1mg 015873
• Codeine 1mg 018013 • Felodipine 1mg 015983
• Codeine-d3 100µg 01913 • Fenfluramine 1mg 6017983
(Qualitative) • • Fentanyl 25µg 013993
• • l-Cotinine 1mg 6014193 • • Flunitrazepam 1mg 6015123
• Cyclobenzaprine 1mg 016073 • Fluoxetine 1mg 015303
• Cyclopentobarbital 1mg 6016273 • Flurazepam 1mg 017953
• Cyheptamide 1mg 012883 • Gabapentin 1mg 015763
• Desalkylflurazepam 1mg 6013423 • Gemfibrozil 1mg 015893
• • Desipramine 1mg 6013613 • GHB 1mg 601563
• Despropionyl fentanyl 100µg 014993 • Glipizide 1mg 016103
• Dexamethasone 1mg 016393 • Glutethimide 1mg 017073
• • Dextromethorphan 1mg 6018373 • Glyburide 1mg 016113
• Diacetylmorphine 1mg 013653 • Halazepam 1mg 014083
• • Diazepam 1mg 017213 • Haloperidol 1mg 6013803
• Diclofenac 1mg 016083 • Hexobarbital 1mg 013303
• Dihydrocodeine 1mg 017773 • Hydrochlorothiazide 1mg 015903
10,11-Dihydro-10-hy- 1mg 016523 • • Hydrocodone 1mg 018063
• droxycarbamazepine** • Hydrocortisone 1mg 016383
N,N-Diisopropyl-5- 1mg 016493 • Hydroflumethiazide 1mg 014343
• methoxytryptamine • • Hydromorphone 1mg 013553
• (+)-cis-Diltiazem 1mg 015853 • α-Hydroxyalprazolam 100µg 01545
• 2,5-Dimethoxy-4- 1mg 016193 (Qualitative)
Bromoamphetamine • α-Hydroxyalprazolam 50µg 01542
2,5-Dimethoxy-4-n- 1mg 016463 Glucuronide
• propylthiophenethyl- (Qualitative)
amine • Hydroxybupropion 1mg 016223
N,N-Dimethyl-5- 1mg 016503 • • N-Hydroxy-MDA 1mg 014973
• methoxytryptamine • 4-Hydroxy-PCP 1mg 6015343
• N,N-Dimethyltryptamine 1mg 6013673 • • p-Hydroxyphenobarbital 1mg 6012213
• Diphenhydramine 1mg 6017053 • l-11-Hydroxy-Δ-9-THC 100µg 01468
• Diphenoxylate 1mg 015973 (Qualitative)
• Doxepin 1mg 6013623 • α-Hydroxytriazolam 100µg 601561
• Doxylamine 1mg 6014183 (Qualitative)
• Drostanolone 1mg 6015263 • Hydroxyzine 1mg 6015013
• Ecgonidine 1mg 016483 • Ibuprofen 1mg 6013813
• Ecgonine 1mg 018213 • Imipramine 1mg 6013483
• Ecgonine Methyl Ester 1mg 014553 • Indapamide 1mg 016123
• Enalapril 1mg 015863 • • Ketamine 1mg 6014143
• l-Ephedrine 1mg 017403 • Ketoprofen 1mg 016423
• Epitestosterone 1mg 6015173 • Lansoprazole 1mg 016133
• Epitestosterone 10µg 601558 • • Levorphanol 500µg 014213
Glucuronide • Lidocaine 1mg 6018423
(Qualitative) • Lisinopril 1mg 015993
Estazolam 100µg 601560 • Lorazepam 1mg 013583
• (Qualitative) • Lorazepam Glucuronide 100µg 01544
(Qualitative)
*In acetonitrile.
© Copyright 2004 **In chloroform.
Alltech Associates,***In
Inc. DMF. Contact your Alltech office or distributor for current or local prices.

50
S TA N D A R D S
Drug Standards

QUIK-CHEK™ DRUG STANDARDS QUIK-CHEK™ DRUG STANDARDS


CLASSIFICATION CLASSIFICATION

AMT IN 1ML SOLVENT

AMT IN 1ML SOLVENT


INTERNAL STANDARD

INTERNAL STANDARD
THERAPEUTIC DRUG

THERAPEUTIC DRUG
ABUSED DRUG

ABUSED DRUG
METABOLITE

METABOLITE
DESCRIPTION PART NO. PRICE DESCRIPTION PART NO. PRICE
• Loxapine 1mg 6014673 • Naproxen 1mg 6015083
• d-LSD 25µg 018093 • • Nicotine 1 mg 017373
• d-LAMPA 25µg 018103 • Nitrazepam 1mg 017933
• 2,3-MDA 1mg 015773 • Norchlordiazepoxide 1mg 6013433
• 3,4-MDA 1mg 014603 • Norclomipramine 1mg 6015003
• 3,4-MDE 1mg 014543 • Norcocaine* 1mg 6015353
• 2,3-MDMA 1mg 015783 • Norcodeine 1mg 013843
• 3,4-MDMA 1mg 014093 • Nordiazepam 1mg 013453
• MDPA 1mg 014713 • Nordoxepin 1mg 6014623
• Medazepam 1mg 013573 • Norethandrolone 1mg 6014883
• Meperidine 1mg 017173 • Norfluoxetine 1mg 015313
• Mephenesin 1mg 016143 • Normeperidine 1mg 014813
• Mephobarbital 1mg 015393 • Normethsuximide 1mg 6010123
• Mepivacaine 1mg 6014233 • Normorphine 1mg 013853
• • Meprobamate 1mg 017083 • l-Norpseudoephedrine 1mg 6013223
• Mescaline 1mg 6017183 • • Nortriptyline 1mg 6013513
• • Mesoridazine 1mg 6014043 • Norverapamil 1mg 6015133
• Mesterolone 1mg 6014903 • Omeprazole 1mg 016163
• Metformin 1mg 016153 • Oxandrolone 1mg 6015183
• • dl-Methadone 1mg 018023 • • Oxazepam 1mg 013703
• • • d-Methamphetamine 1mg 010013 • Oxazepam Glucuronide 100µg 01541
• l-Methamphetamine 1mg 014703 (Qualitative)
• dl-Methamphetamine- 100µg 601926 • Oxcarbazepine** 1mg 016453
d9 (Qualitative) • • Oxycodone 1mg 013543
• Methandriol 1mg 6015253 • Oxymesterone 1mg 6015233
• Methandrostenolone 1mg 6013493 • Oxymetholone** 1mg 6014853
• • Methaqualone 1mg 017313 • • Oxymorphone 1mg 013983
• Metharbital 1mg 6013693 • Paroxetine 1mg 016363
• Methenolone 1mg 6015073 • Pentazocine 1mg 017113
• Methohexital 1mg 6013763 • • Pentobarbital 1mg 016233
• 4-Methoxyamphetamine 1mg 015743 • Phenazopyridine 1mg 015923
• 4-Methoxymeth- 1mg 016203 • • Phencyclidine 1mg 017263
amphetamine • Phen-d5-cyclidine 100µg 01916
• Methsuximide 1mg 6018463 • Phendimetrazine 1mg 6017743
• 4-Methylaminorex 1mg 014913 • Phenethylamine 1mg 013013
• l-N-Methylephedrine 1mg 016443 • Phenmetrazine 1mg 014943
• • Methylphenidate 1mg 014103 • • Phenobarbital 1mg 016263
• Methyltestosterone 1mg 6014833 • Phentermine 1mg 017833
• 4-Methylthio- 1mg 016183 • • Phenylpropanolamine 1mg 6017803
amphetamine • Phenytoin 1mg 6017303
• α-Methyltryptamine 1mg 016473 • Prazepam 1mg 013913
• Methyprylon 1mg 6017963 • Primidone 1mg 6017813
• Metoclopramide 1mg 016003 • Procainamide 1mg 6017853
• Metronidazole 1mg 015803 • Procaine 1mg 6017133
• Midazolam 1mg 015713 • • Promazine 1mg 6013523
• 6-Monoacetylmorphine 1mg 014593 • d-Propoxyphene 1mg 017043
• • • Morphine 1mg 018033 • N-Propylamphetamine 1mg 014573
• Morphine-d3 100µg 01912 • Propylbenzoylecgonine 1mg 014733
(Qualitative) ***
• Nabumetone 1mg 015793 • Propylhexadrine 1mg 6015533
• • Nalorphine 1mg 013633 • Protriptyline 1mg 6013713
• Naloxone 1mg 6013683 • d-Pseudoephedrine 1mg 6013213
• Naltrexone 1mg 6013733 • Psilocybin 100µg 013641
• Nandrolone 1mg 6014843 • • Psilocyn 100µg 013661
*In acetonitrile.
© Copyright 2004 **In chloroform.
Alltech Associates,***In
Inc. DMF. Contact your Alltech office or distributor for current or local prices.

51
S TA N D A R D S
Drug Standards

QUIK-CHEK™ DRUG STANDARDS


CLASSIFICATION Improving Peak Shape in GC
Many drugs are reactive in a GC column.

AMT IN 1ML SOLVENT


INTERNAL STANDARD
THERAPEUTIC DRUG

This can lead to tailing or low response.


To improve the chromatography, many
ABUSED DRUG
METABOLITE

choose to make a derivative of the


material to increase its stability and
DESCRIPTION PART NO. PRICE improve the peak shape. The most
• Ranitidine 1mg 015943 commonly used reagent is MSTFA. It is
• Saquinavir 1mg 016373 co-injected with the sample and forms
• Secobarbital 1mg 016953 the derivative in the GC injector. See the
• Simvastatin 1mg 016013 Reagents Section for more information.
• Spironolactone 1mg 015953
• Stanozolol 1mg 6014863
• Synephrine 1mg 016413
• Talbutal 1mg 014533
• Tamoxifen 1mg 015963
• • Temazepam 1mg 013833
• Temazepam 100µg 01543 Do you want to improve
Glucuronide
(Qualitative) your drug recoveries?
• Terazosin 1mg 016173
Alltech’s Drug-Clean mixed
• Testosterone 1mg 6014873 mode silica-base SPE packing
• Testosterone 100µg 601559 combines reversed-phase and
Glucuronide ion exchange functionalities in a
• Δ-8-THC 100µg 013863 single column. This allows high
• Δ-8-THC 1mg 013866 drug recoveries with minimal
• Δ-9-THC 100µg 013873 impurities compared to single-
• Δ-9-THC 1mg 013877 phase extractions.
• Thebaine 1mg 6018073 See pages 6-7 for more details
• • Theophylline 1mg 6018383 or request Product Support Sheet
• Thiopental 1mg 6014473 #M102
• Thioridazine 1mg 6014073
• Tocainide 1mg 6014563
• Tramadol 1mg 016433
• Trazadone 1mg 6014663
• Triazolam 1mg 014283
• Trichlormethiazide 1mg 014453
• Trifluoromethylphenyl- 1mg 015823
Need help getting rid of
piperazine all of those drug sample
• Trimethadione 1mg 6014493 vials?
• Trimipramine 1mg 6013603 Safely separate the solutions
• Verapamil 1mg 6013773 from the vials using the Alltech
• Warfarin 1mg 016403 Vial Crusher. See page 122 for
*In acetonitrile. **In chloroform. ***In DMF. more info.

For Our International Customers


Prices listed in this catalog are U.S. prices only. Complete line of drug standards including pure
Please request a pro forma quotation for current export materials and pre-weighed ready-to-dilute materials
are available. For complete listing, request Bulletin
prices. Due to the high cost of airfreight and document 469.
preparation, our minimum international order is $500
(excluding freight charges). The solutions listed on these
pages are exempt from licensing only in the USA and
Canada. Most countries require formal import permits.
We will send specific instructions for ordering with our
quotation. For prompt response, please FAX (814-234-
3594) or email (drugs@alltechemail.com) for quotation
requests.
© Copyright 2004 Alltech Associates, Inc. Contact your Alltech office or distributor for current or local prices.

52
S TA N D A R D S
FAME Standards

Fatty Acid and Ester Standards


Save time and money with guaranteed standards
• Quality certificate supplied with every standard and mix
Don’t waste your valuable lab time to verify your calibration and identification of standards. Alltech supplies a
purity certificate for every standard and mix.
FATTY ACID AND METHYL ESTER STANDARDS
FREE FATTY ACIDS FATTY ACID METHYL ESTERS
CARBON # DESCRIPTION QTY. PART NO. PRICE QTY. PART NO. PRICE
11:0 Henedecanoic Acid (Undecylic) 0.5g 622110 0.5g 623110
12:0 Dodecanoic Acid (Lauric) 1g 622120 1g 623120
13:0 Tridecanoic Acid (Tridecylic) 1g 622130 1g 623130
14:0 Tetradecanoic Acid (Myristic) 1g 623140 1g 623140
15:0 Pentadecanoic Acid (Pentadecylic) 0.5g 622150 0.5g 623150
16:0 Hexadecanoic Acid (Palmitic) 1g 622160 1g 623160
16:1 cis-9-Hexadecenoic Acid (Palmitoleic) 0.1g 6221610 0.1g 6231610
17:0 Heptadecanoic Acid (Margaric) 1g 622170 1g 623170
18:0 Octadecanoic Acid (Stearic) 1g 622180 1g 623180
18:1 cis-9-Octadecenoic Acid (Oleic) 1g 6221810 1g 6231810
18:1 trans-9-Octadecenoic Acid (Elaidic) 1g 6221811 0.5g 6231811
18:1 cis-11-Octadecenoic Acid (cis-Vaccenic) — — — 0.1g 62318101
18:1 trans-11-Octadecenoic Acid (trans-Vaccenic) — — — 0.1g 62318121
18:2 cis,cis-9,12-Octadecadienoic Acid (Linoleic) 1g 6221820 1g 6231820
18:2 trans,trans-9,12-Octadecadienoic Acid (Linoelaidic) 0.1g 6221821 0.1g 6231821
18:3 All cis-9,12,15-Octadecatrienoic Acid (Linolenic) 0.1g 62218300 0.1g 6231830
18:3 All cis-6,9,12-Octadecatrienoic Acid (γ-Linolenic) 0.1g 62218301 0.1g 6231831
20:0 Eicosanoic Acid (Arachidic) 1g 6220200 1g 623200
20:1 cis-11-Eicosenoic Acid 0.1g 6220201 0.1g 623201
20:4 All cis-5,8,11,14-Eicosatetraenoic Acid (Arachidonic) 0.1g 6220204 0.1g 623204
20:5 All cis-5,8,11,14,17-Eicosapentaenoic Acid 10mg 6220205 10mg 623205
22:0 Docosanoic Acid (Behenic) 1g 6220220 1g 623220
22:1 cis-13-Docosenoic Acid (Erucic) 1g 62202210 0.1g 6232210
22:5 All cis-7,10,13,16,19-Docosapentaenoic Acid 10mg 6220225 10mg 6232250
23:0 Tricosanoic Acid 0.1g 6220230 0.1g 623230
24:0 Tetracosanoic Acid (Lignoceric) 0.1g 6220240 0.1g 623240

FATTY ACID METHYL ESTER MIXES


DESCRIPTION COMPONENTS QTY. PART NO. PRICE
K101 C8:0, C10:0, C12:0, C14:0, C16:0, C18:0, C20:0 100mg 625001
K103 C12:0, C14:0, C14:1, C16:0, C16:1 cis 50mg 625002
K1000 C13:0, C15:0, C17:0, C19:0, C21:0 50mg 625003
K104 C14:0, C16:0, C18:0, C20:0, C22:0, C24:0 100mg 625004
K110 C16:0, C16:1 cis, C16:1 trans, C18:0, C18:1 cis-9, C18:1 trans-9, C18:2 cis,cis, C18:2 trans, trans 100mg 625005
K108 C16:0, C18:0, C18:1 cis-9, C18:2 cis,cis ,C18:3 all cis 50mg 625006
K2000 C18:0, C18:1 cis-9, C18:2 cis,cis, C18:3 all cis, C20:4 all cis 50mg 625007
K3000 C18:2 cis,cis, C18:3 all cis, C20:4 all cis, C22:6 all cis 50mg 625008
K4000 C20:0, C20:1 cis, C20:2 cis,cis, C20:3 all cis, C20:4 all cis 50mg 625009
K107 C20:0, C20:1 cis, C22:0, C22:1 cis, C24:0, C24:1 cis 50mg 625010
K5000 Mix A C6:0, C8:0, C10:, C12:0 100mg in 625017
5mL
K5000 Mix B C12:0, C14:0, C16:, C18:0 100mg in 625018
5mL
L207 C18:0, C18:1 cis-9, C20:0, C22:0, C22:1 cis, C24:0, C24:1 cis 50mg 625021
L205 C18:0, C18:1 cis-9, C18:2 cis,cis, C18:3 all cis, C20:4 all cis 100mg 625022
L209 C20:0, C20:1 cis, C20:4 all cis, C22:1 cis, C22:6 all cis 25mg 625023
AOCS Mix 1 C16:0, C18:0, C18:1 cis-9, C18:2 cis,cis, C18:3 all cis, C20:0 50mg 625024
AOCS Mix 3 C16:0, C18:0, C18:1 cis-9, C18:2 cis,cis, C18:3 all cis, C20:0, C22:0, C22:1 cis, C24:0 50mg 625026
AOCS Mix 3A C16:0, C18:0, C18:1 cis-9, C18:2 cis,cis, C18:3 all cis, C20:0, C20:1 cis, C22:0, C22:1 cis, C24:0 25mg 625027
AOCS Mix 5 C8:0, C10:0, C12:0, C14:0, C16:0, C18:0, C18:1 cis-9, C18:2 cis,cis 50mg 625029
AOCS Mix 6 C14:0, C16:0, C16:1 cis, C18:0, C18:1 cis-9, C18:2 cis,cis, C18:3 all cis 50mg 625030
Contact your Alltech office or distributor for current or local prices.
© Copyright 2004 Alltech Associates, Inc.

53
S TA N D A R D S
Hydrocarbon Standards

Hydrocarbons and Miscellaneous Standards and Kits


• Quality certificate supplied with every standard & mix HYDROCARBONS (N-PARAFFINS)
CARBON NO. DESCRIPTION QTY. PART NO. PRICE
Use Alltech Standards and Mixes with complete
C5 n-Pentane 1g 620050
confidence in purity and quality. Don’t waste your C6 n-Hexane 1g 620060
valuable lab time to verify the standards you need. To C7 n-Heptane 1g 620070
satisfy your documentation needs, Alltech supplies a C8 n-Octane 1g 620080
purity certificate for every standard and mix. C9 n-Nonane 1g 620090
C10 n-Decane 1g 620100
C11 n-Hendecane 1g 620110
C12 n-Dodecane 1g 620120
ALLTECH ORGANIC ACID STANDARDS C13 n-Tridecane 1g 620130
DESCRIPTION QTY. PART NO. PRICE C14 n-Tetradecane 1g 620140
Oxalic Acid, 1000ppm 125mL 37033 C15 n-Pentadecane 1g 620150
Maleic Acid, 1000ppm 125mL 37037 C16 n-Hexadecane 1g 620160
Malic Acid, 1000ppm 125mL 37039 C17 n-Heptadecane 1g 620170
Succinic Acid, 1000ppm 125mL 37043 C18 n-Octadecane 1g 620180
Formic Acid, 1000ppm 125mL 37045 C19 n-Nonadecane 1g 620190
Acetic Acid, 1000ppm 125mL 37047 C20 n-Eicosane 1g 620200
Citric Acid, 1000ppm 125mL 37049 C21 n-Heneicosane 1g 620210
Tartaric Acid, 1000ppm 125mL 37051 C22 n-Docosane 1g 620220
Lactic Acid, 1000ppm 125mL 37053 C23 n-Tricosane 1g 620230
Abietic Acid, 1000ppm 125mL 37055 C24 n-Tetracosane 1g 620240
Methane Sulfonic Acid, 1000ppm 125mL 37057 C25 n-Pentacosane 0.1g 620250
C26 n-Hexaconsane 0.1g 620260
C27 n-Heptacosane 0.1g 620270
N-PARAFFIN MIXTURES C28 n-Octacosane 1g 620280
DESCRIPTION QTY. PART NO. PRICE C29 n-Nonacosane 0.1g 620290
Neat Mixtures (No Solvent - Equal Weights of Components) C30 n-Triacontane 0.1g 620300
C5, C6, C7, C8 2mL 628001 C32 n-Dotriacontane 0.1g 620320
C7, C8, C9, C10 2mL 628002 C34 n-Tetratriacontane 0.1g 620340
C9, C10, C11, C12 2mL 628003 C36 n-Hexatriacontane 0.1g 620360
C11, C12, C13, C14 2mL 628004 C38 n-Octatriacontane 0.1g 620380
C12, C14, C16, C18 2mL 628005 C40 n-Tetracontane 0.1g 620400
Mixtures (In 5mL Hexane - Equal Weight of Components) C44 n-Tetratetracontane 0.1g 620440
C16, C18, C20, C22 0.5g 628006
C20, C22, C24, C26 0.1g 628007
C24, C26, C28, C30 50mg 628008
C28, C30, C32, C34 50mg 628009 AROMATIC HYDROCARBON MIX
C32, C34, C36, C38 50mg 628010 DESCRIPTION QTY. PART NO. PRICE
C32, C36, C40, C44 50mg 628011 BETX Mix 2g 629001
Contains equal amounts of benzene, toluene, ethylbenzene, o-xylene, m-xylene
and p-xylene.

STANDARDS KITS
DESCRIPTION KIT CONTAINS 100MG EACH COMPONENT PART NO. PRICE
Free Fatty Acid Kits
Short Chain C2, C3, C4, C5, C6, C7, C8 18600
Even Carbon C10, C12, C14, C16, C18, C20, C22 186021
Odd Carbon C9, C11, C13, C15, C17, C19, C21, C23 18608
Fatty Acid Ester Kits
Methyl Esters, Even Carbon C10, C12, C14, C16, C18, C20, C22 18603
Methyl Esters, Odd Carbon C9, C11, C13, C15, C17, C19, C21 18609
Ethyl Esters, Even Carbon C6, C8, C10, C12, C14, C16, C18, C20, C22, C24 18610
Ethyl Esters, Odd Carbon C7, C9, C11, C13, C15, C17, C19, C21, C23 18611
Hydrocarbon Kits
Saturated, Even Carbon C10, C12, C14, C16, C18, C20, C22, C24, C28, C32, C36 18484
Saturated, Odd Carbon C9, C11, C13, C15, C17, C19, C21, C23, C25 18485

© Copyright 2004 Alltech Associates, Inc. Contact your Alltech office or distributor for current or local prices.

54

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