Basic Distillation Equipment and Operation

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Equipment

A distillation column is an essential item used in the distillation of liquid mixtures to

separate the mixture into its component parts, or fractions, based on the differences in
volatilities. Fractionating columns are used in small scale laboratory distillations as well
as large scale industrial distillations.

Types of Distillation Columns

There are many types of distillation columns, each designed to perform specific types of
separations, and each design differs in terms of complexity.

Batch Columns

In batch operation, the feed to the column is introduced batch-wise. That is, the column
is charged with a 'batch' and then the distillation process is carried out. When the
desired task is achieved, a next batch of feed is introduced.

Continuous Columns

In contrast, continuous columns process a continuous feed stream. No interruptions

occur unless there is a problem with the column or surrounding process units. They are
capable of handling high throughputs and are the most common of the two types. We
shall concentrate only on this class of columns.

Types of Continuous Columns

Continuous columns can be further classified according to:

the nature of the feed that they are processing

binary column - feed contains only two components

multi-component column - feed contains more than two components

the number of product streams they have

multi-product column - column has more than two product streams

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where the extra feed exits when it is used to help with the separation

extractive distillation - where the extra feed appears in the bottom product stream
azeotropic distillation - where the extra feed appears at the top product stream

the type of column internals

tray column - where trays of various designs are used to hold up the liquid to
provide better contact between vapour and liquid, hence better separation
packed column - where instead of trays, 'packings' are used to enhance contact
between vapour and liquid

Main Components of Distillation Columns

Distillation columns are made up of several components, each of which is used either to
tranfer heat energy or enhance materail transfer.
A typical distillation contains several major components:

a vertical shell where the separation of liquid components is carried out

column internals such as trays/plates and/or packings which are used to enhance
component separations
a reboiler to provide the necessary vaporisation for the distillation process
a condenser to cool and condense the vapour leaving the top of the column
a reflux drum to hold the condensed vapour from the top of the column so that
liquid (reflux) can be recycled back to the column

The vertical shell houses the column internals and together with the condenser and
reboiler, constitute a distillation column. A schematic of a typical distillation unit with a
single feed and two product streams is shown below:

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Basic Operation and Terminology
The liquid mixture that is to be processed is known as the feed and this is introduced
usually somewhere near the middle of the column to a tray known as the feed tray. The
feed tray divides the column into a top (enriching or rectification) section and a bottom
(stripping) section. The feed flows down the column where it is collected at the bottom
in the reboiler.

Heat is supplied to the reboiler to generate vapour. The source of heat input can be any
suitable fluid, although in most chemical plants this is normally steam. In refineries, the
heating source may be the output streams of other columns. The vapour raised in the

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reboiler is re-introduced into the unit at the bottom of the column. The liquid removed
from the reboiler is known as the bottoms product or simply, bottoms.

The vapour moves up the column, and as it exits the top of the unit, it is cooled by a
condenser. The condensed liquid is stored in a holding vessel known as the reflux drum.
Some of this liquid is recycled back to the top of the column and this is called the reflux.
The condensed liquid that is removed from the system is known as the distillate or top
product.

Thus, there are internal flows of vapour and liquid within the column as well as external
flows of feeds and product streams, into and out of the column.

Part 1:
What are Distillation Columns?

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Part 2:
Column Internals

Graphic courtesy of Bismarck State College National Energy Center of Excellence

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