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https://doi.org/10.1007/s40194-019-00773-6
RESEARCH PAPER
Received: 29 June 2018 / Accepted: 8 July 2019 / Published online: 20 July 2019
# International Institute of Welding 2019
Abstract
The welding process parameters of dissimilar 2024-T4 and 7075-T6 aluminum alloy friction stir welded (FSWy) joints are
selected by the metallographic microstructure, the mechanical properties, and the hardness distribution. The joints with rotational
speed of 900 rpm and advancing speed of 100 mm/min that have the highest tensile strength are used to carry out the experimental
fatigue research. The short crack growth behavior of dissimilar FSW joints is analyzed through the replica technique. The stage of
the crack initiation and stable growth accounts for about 60~80% of total fatigue life. The short crack grows rapidly once it
reaches the crack size of approximately 350~450 μm. The cracks are prone to initiate at the defects of subsurface in the weld
nugget zone and propagate in a quasi-cleavage fracture mode.
Keywords Friction stir welding . Dissimilar joints . Mechanical property . Short crack
phases [11]. The fatigue crack initiation is affected by the Table 2 Mechanical properties of base metals
material property, microstructure, and stress level [12, 13]. Material UTS (MPa) YS (MPa) Elongation (%)
The crack of dissimilar 6061-7050 FSW joints initiated at
the HAZ/TMAZ region where the secondary intermetallic 2024-T4 458 280 11
particles and voids exist [14]. The intermetallic particles and 7075-T651 543 444 6
grain boundary influence the short crack growth rate [15]. The
interaction of the propagating crack with a grain boundary has
an important effect on fatigue life and fatigue strength [16].
The welding parameters of dissimilar 2024-7075 alumi- cycle interval, and the tensile load of 80% maximum stress
num alloy FSW joints are selected by the mechanical proper- was kept in order to make the fatigue crack in an open position
ties and the microstructure. The behavior of fatigue crack ini- when the cellulose acetate membrane was pasted on the joint
tiation and growth for the dissimilar FSW joints with the op- surface. The cellulose acetate membranes were pasted on four
timized welding parameters are analyzed in this paper. surfaces of the specimen at each cycle interval since the crack
initiation and propagation could happen in any side. The cel-
lulose acetate membranes were carefully pulled away from the
2 Materials and experimental joint surface after they completely dried. The surface crack
traces were permanently recorded in the cellulose acetate
Three-millimeter-thick rolled plates of 2024-T4 and 7075- membranes. Approximately 25–30 dried membranes should
T651 aluminum alloys with the dimensions of 300 mm long be obtained for each surface of the joint during the whole
and 150 mm wide were used to produce the dissimilar FSW fatigue life in order to ensure the effectiveness of the data.
butt joints. The stir tool is composed of a 10-mm diameter The cracks were observed by optical microscope and their
shoulder and a tapered cylinder pin of 4 mm, 3.5 mm in top length was measured by a image software. The fracture mor-
diameter, and 2.85 mm in length. The welding direction was phologies were observed with a JEOLJSM 6500F scanning
perpendicular to the rolling direction of the 2024 and 7075 electron microscope (SEM).
alloy plates with the 2024 plate on the advancing side. The
nominal chemical composition and mechanical properties of
the two alloys are listed in Tables 1 and 2, respectively. The 3 Results and discussion
joint specimens for tensile and fatigue tests were cut with a
wire-cut machine. The transverse section of the joints was 3.1 Parameter selection
ground with carbide abrasive papers of grit sizes from 240 to
3000. The welding parameters and tensile results are listed in 3.1.1 Metallurgical analysis
Table 3.
The metallographic morphologies of the specimens were Figure 1 shows the cross-sectional metallographical morphol-
observed after they were etched using Keller’s reagent (2.5 ml ogy of dissimilar 2024-7075 aluminum alloy FSW joint with
HNO3, 1.5 ml HCL, 1 ml HF, and 95 ml H2O). The Vickers the welding parameter of rotating speed of 900 rpm and tra-
hardness was measured in the transverse sections of the joints verse speed of 100 mm/min. The joint is divided into the
with 0.5-mm spacing between the indentations using the in- following six areas: heat-affected zone of advancing side (A-
denter with 200 gf load for 15 s. HAZ), thermo-mechanically affected zone of advancing side
The tensile tests were performed using electro-hydraulic (A-TMAZ), weld nugget zone near advancing side (A-WZ),
servo universal testing machine MTS858 with a displacement weld nugget zone near retreating side (R-WZ), thermo-
rate of 0.6 mm/min. The fatigue tests were carried out on tester mechanically affected zone of retreating side (R-TMAZ),
MTS858 under stress-controlled sine wave loading mode at a and heat-affected zone of retreating side (R-HAZ).
stress ratio of 0.1 and frequency of 10 Hz. The traces of short The metallographical morphologies of the joints with most
cracks were obtained with cellulose acetate film replica tech- welding parameters are shown in Fig. 2a. Welding defects of
nique. The fatigue tests were temporarily paused after a certain cavities and block materials that are not being mixed evenly
are found in the A-WZ. The cavity defects in Fig.2b–d appear
Table 1 Chemical composition of 2024-T4 and 7075-T651 Al alloys in some joints. Block materials in Fig.2 are found in all the
(wt%) joints except the joints with welding parameters of ω =
900 rpm and v = 100 mm/min and ω = 900 rpm and v =
Material Si Fe Cu Mn Mg Cr Zn Al
120 mm/min. The joint defects are close to the interface of
2024-T4 0.40 0.27 4.58 0.56 1.36 0.001 0.02 Bal. the A-TMAZ and the A-WZ. All such cases can be attributed
7075-T6 0.225 0.20 1.49 0.10 2.40 0.23 5.59 Bal. to frictional heat and the extrusion of metal flow during the
welding process.
Weld World (2019) 63:1761–1769 1763
The heat input per unit can be calculated with Eq. (1) as larger, as shown in Fig. 2b, d. The insufficient material defor-
follows [17]: mation caused by low heat input failed to form a fully consol-
idated weld. A joint with free defects and good quality needs
aq 4 2 ω ω
Q¼ ¼ π aμPR3 ¼ β ð1Þ an appropriate heat input. The joint microstructure without the
v 3 v v defects shows the teeth-shaped interface of different materials
where Q is the heat input per unit length, α is the heat input and the alternate lamella material flow pattern, as shown in
efficiency, q is the heat input, v is the traverse speed, μ is the Fig. 2e.
friction coefficient, P is the pressure, R is the shoulder radius,
and ω is the rotation speed. α, μ, P, and R are assumed to be 3.1.2 Mechanical properties
the constants if the welding process is fixed, and they can be
put together to be the coefficient β. So, only ω and v are Tensile results of the joints are listed in Table 3. Tensile
variables. strength values of the joints range from 209 to 437 MPa,
The factors affecting the welding heat input contain the which account for 45–95% those of 2024 alloy. The tensile
rotating and the traverse speed. The magnitude of heat input fracture mainly occurred in the A-WZ and the A-TMAZ. The
can be qualitatively expressed by the value of ω/v. Therefore, boundary area of the A-WZ and the A-TMAZ is considered
the variation in microstructure caused by heat input is attrib- the weakest zone of the dissimilar FSW joints for the tensile
uted to the different values of ω/v. It is observed that the ratio specimen, where the defects and the minimum hardness are
of tool rotating speed to traverse speed (ω/v) plays a leading prone to appear. The joints with the welding parameters of
role in forming defects. It is observed from Fig. 2b, c that the traverse speed 100 mm/min and rotation speed 900 rpm have
size of the cavity defect gradually becomes larger when the the best ultimate strength.
rotation speed increases from 1000 to 1100 rpm under the
constant traverse speed of 150 mm/min, while the correspond- 3.1.3 Microhardness distribution
ing value of ω/v is from 6.7 to 7.3. It is considered that the high
rotation speed results in the excessive plastic deformation, Microhardness profiles of the dissimilar FSW joints in Fig. 3
which leads to the appearance of void defect [18]. As the can reflect the mechanical properties of the joints in a certain
traverse speed increases from 150 to 180 mm/min under the cross section. The profiles along the centerline of the cross
constant rotating speed of 1000 rpm, the corresponding value section show typical characteristic of “W” curves. The joints
of ω/v decreases from 6.7 to 5.5. The cavity defects become of no. 3-3 and no. 5-4 with free defect have the higher
Fig. 1 Metallographical
morphology in cross section of
the joint
1764 Weld World (2019) 63:1761–1769
Fig. 2 Cross-sectional
morphology and metallographic
microstructure of FSW joints with
different process parameters. a
ω = 1100 r/min, v = 120 mm/min.
b ω = 1000 r/min, v = 150 mm/
min. c ω = 1100 r/min, v =
150 mm/min. d ω = 1000 r/min,
v = 180 mm/min. e ω = 900 r/min,
v = 120 mm/min
hardness values than others. The lowest hardness occurred at WZ on the whole. So the joints with the welding parameter of
the boundary areas of the A-WZ and the A-TMAZ. The hard- rotating speed of 900 rpm and traverse speed of 100 mm/min
ness of no. 5-4 is greater than that of no. 3-3 in the TMAZ and are selected to perform the fatigue tests.
120
110
100 Advancing side
Retreating side
90 2024-T4 7075-T651
80
70
Hardness test line
60
-14-12-10 -8 -6 -4 -2 0 2 4 6 8 10 12 14 16 18 20
Distance from weld centre, mm
Weld World (2019) 63:1761–1769 1765
3.2 Fatigue result analysis The fatigue endurance curves of the 2024-7075 FSW joints
and base materials are shown in Fig. 4. As expected, welding
3.2.1 Fatigue crack initiation of dissimilar materials causes a significant drop of the fatigue
lives of the materials.
Fatigue results under different stress levels at a stress ratio of Some short cracks initiated around the inclusion particles
0.1 are listed in Table 4. More than 80% of fatigue crack of WZ, as shown in Fig. 5. The short crack is winding near the
sources appeared in the WZ and others appeared in the base inclusion particle. The weak bonding force between inclusion
material of 2024. The crack mainly initiated in the A-WZ and particles and surrounding grains causes the crack initiation
it did not happen at a fixed surface. It is found that the stage of and propagation. The crack propagates straightforward after
fatigue short crack initiation takes up about 3% of total fatigue passing the inclusion particle. The possibility of causing
life with the replica technology, which means the fatigue pro- cracks is more when the inclusion particle size is higher,
cess of dissimilar FSW joint is mainly a crack propagation which causes the higher stress concentration by the greater
process. particles. The crack initiation preferentially occurs at particles
300
250
200
150
4 5 6
10 10 10
Number of cycles to failure, Nf
1766 Weld World (2019) 63:1761–1769
Fig. 6 Short crack growth process under maximum stress of 260 MPa. a 800 cycles. b 3800 cycles. c 12600 cycles. d 23000 cycles
Weld World (2019) 63:1761–1769 1767
(a) 2550
3.2.3 Effects of stress intensity factor on short crack growth
2400 Crack 1
2250 Crack 2 rate
2100 Crack 4
1950 Crack 5
1800 Crack 7 The calculation of the stress intensity factor range (ΔK) for
Crack length (µ m)
1650
Crack 3
1500 short cracks is calculated by Eq. (2) [25].
1350 Crack 6
Crack 8 qffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi
1200 pffiffiffiffiffiffiffiffi
1050 ΔK ¼ 0:65Δσ π area
900 ð3Þ
750 σmax ðσmin ≤ 0Þ
600 Δσ ¼
450 σmax −σmin ðσmin > 0Þ
300
150
0 where area is the projected area of the crack, σmax is the max-
-150 imum stress, and σmin is the minimum stress.
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0
Life ratio (N/Nf) Figure 9 shows the relation of short fatigue crack
growth rate versus stress intensity factor. The curve un-
(b) 3000
der a maximum stress level of 260 MPa shows a more
2500
intense fluctuation because at least three combined
cracks formed during the growth. The higher the stress
level, the higher the growth rate at the same ΔK in the
Crack length (µ m)
2000
beginning stage. The curves of two different stress
1500 levels are close at a larger growth rate in the late stage
of crack propagation. A low propagation rate appears at
pffiffiffiffi
1000 2.6 and 2.9 MPa m of the ΔK under a stress level of
220 MPa and 260 MPa. Short crack growth rates pre-
500
sented a trend of first falling and then rising, as shown
in Fig. 9.
0
0.0 0.2 0.4 0.6 0.8 1.0 1.2
Life ratio (N/Nf)
Fig. 7 Relationship between crack length and life cycle ratio at different
3.3 Fracture surface morphologies
stress levels. a 260 MPa. b 220 MPa
The fracture surface morphologies of WZ for the FSW
two cracks, as shown in Fig. 8. The observed acceleration and dissimilar joint under a stress level of 220 MPa were
retardation in the process of short cracks are considered as a observed by JEOLJSM 6500F SEM. Figure 10a shows
result of the crack coalescence or the cracks propagating that the fatigue crack source locates in the subsurface.
through the inclusion particles [23, 24]. The tearing ridge in Fig. 10a and the secondary cracks
and microvoids in Fig. 10b show a quasi-cleavage frac-
ture. The transgranular propagation is the main mode in
0
10 Crack 5
Crack 6
New combined crack 7
da/dN (µ m/cycle)
-1
10
-2
10
-3
10
2 3
10 10
Crack length (µm)
Fig. 8 Variation of crack growth rate along with cycles under stress level
of 260 MPa Fig. 9 Short fatigue crack growth rate versus stress intensity factor range
1768 Weld World (2019) 63:1761–1769
11. Miller KJ (1987) The behaviour of short fatigue cracks and their 19. Oskouei RH, Ibrahim RN (2011) The effect of a heat treatment on
initiation. 2. A general summary. Fatigue Fract Eng Mater Struct improving the fatigue properties of aluminium alloy 7075-T6 coat-
10(2):93–113 ed with TiN by PVD. Procedia Engineering 10:1936–1942
12. Besel Y, Besel M, Mercado UA, Kakiuchi T, Hirata T, Uematsu Y 20. Prudhomme M, Billy F, Alexis J (2018) Effect of actual and accel-
(2017) Influence of local fatigue damage evolution on crack initia- erated ageing on microstructure evolution and mechanical proper-
tion behavior in a friction stir welded Al-Mg-Sc alloy. Int J Fatigue ties of a 2024-T351 aluminium alloy. Int J Fatigue 107:60–71
99:151–162 21. Yan L, Fan JK (2016) In-situ SEM study of fatigue crack initiation
13. Deng CY, Gao R, Gong BM, Yin TH, Liu Y (2017) Correlation and propagation behavior in 2524 aluminum alloy. Mater Design
between micro-mechanical property and very high cycle fatigue 110:592–601
(VHCF) crack initiation in friction stir welds of 7050 aluminum 22. Alexandre F, Deyber S, Pineau A (2004) Modeling the optimum
alloy. Int J Fatigue 104:283–292 grain size on the low cycle fatigue life of a Ni based superalloy in
14. Rodriguez RI, Jordon JB, Allison PG, Rushing T, Garcia L (2016) the presence of two possible crack initiation sites. Scr Mater 50:25–
Low-cycle fatigue of dissimilar friction stir welded aluminum al- 30
loys. Mater Sci Eng A 654:236–248 23. Tan JT, Chen BK (2013) Coalescence and growth of two coplanar
15. Jordon JB, Bernard JD, Newman JC (2012) Quantifying short cracks in AA7050-T7451 aluminium alloys. Eng Fract Mech
microstructurally small fatigue crack growth in an aluminum alloy 102:324–333
using a silicon-rubber replica method. Int J Fatigue 36(1):206–210
24. Guan J, Wang LQ, Zhang CW, Ma XX (2017) Effects of non-
16. Brochu M, Verreman Y, Ajersch F, Bouchard D (2012) Propagation
metallic inclusions on the crack propagation in bearing steel.
of short fatigue cracks in permanent and semi-solid mold 357 alu-
Tribol Int 106:123–131
minum alloy. Int J Fatigue 36(1):120–129
17. Kim YG, Fujii H, Tsumura T, Komazaki T, Nakata K (2006) Three 25. Murakami Y, Endo M (1986) Effects of hardness and crack geom-
defect types in friction stir welding of aluminum die casting alloy. etry ofΔKthof small cracks. J Soc Mater Sci Jpn 35(395):911–917
Mater Sci Eng A 415(1–2):250–254
18. Trimble D, O’Donnell GE, Monaghan J (2015) Characterization of Publisher’s note Springer Nature remains neutral with regard to
tool shape and rotational speed for increased speed during friction jurisdictional claims in published maps and institutional affiliations.
stir welding of AA2024-T3. J Manuf Process 17:141–150