Experiment 3

lose trago fañon

Name:fredo
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11
Section: ______________ Date: March 1912021
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ANALYSIS, MAKING OBSERVATIONS AND

CALCULATING CONCENTRATIONS
Laboratory Report

Observations, Data and Calculations

1. Fill in the data and observation tables and calculate the required information. Show your
calculations (required for full marks) on the back of the sheet or on a separate sheet.

(6 marks) Table 1. Initial appearance of each solution and calculated concentrations

Observation(s): Is it a Concentration
initial colour & Solution/Suspension?
appearance

M of I2
Has a brown Is a solution

Colour because there are

tincture of iodine
solution no particlessuspending 0,487M

Traslucid
appearance but Is a suspension the % (w/w)
the closestcolour iswhite white dust mustbeflour
there is somewhite
starch solution dustat the bottom so it isnotdissolved
0.4

Orange Colour but Is a sinceeven

pension
theVitaminC
vitamin C solution
withsome piecesfloating
Most
Of
andmakethewater
disolved
0.0277M
mg of ascorbic acid look butstillhavesomepieces
orange
on label: thatdidn'tdissolve
___________
502mg
___ M of ascorbic acid
a # of tablets used

CHEM 205 LAB 3: Analysis 6

 Experiment 3

(6 marks) Table 2: Reaction of vitamin C and iodine: observations and calculations

Observations Initial Final Total volume Molarity of vitamin

(colour, reading reading of tincture of C in the 75.0 mL
appearance) volume volume iodine solution
Solution tincture tincture solution (show calculations on
of iodine of iodine added (mL): the blank page)
(mL) (mL) Vol final –
Vol initial
25mL0mL
vitamin C Darkbrowncolour
0.0277M
solution 0mL 25mL 25mL
Kimi0mL
fresh citrus Dark
bluecolour
fruit juice III 0mL 4.7mL 4.7mL 1.438 10 M
2. (0.5 mark) What type of reaction occurs between vitamin C and iodine?

q Hard I change
Redox reaction since thecharges

3. (1.0 marks) Write the two half reactions required to represent the reaction between
vitamin C and iodine.
GHo0qaqstIaqs.coHoO alta 2
C.HN
Oxidation scd.IN tanta tré
Iraqiré
Reduction
2kg
4. (0.5 mark) What is the role of starch in the reaction?

Thestarch act as an colourindicator so it is possible ustoknow whenthe reaction between ascorbicacidand

iodine iscompleted Thishappens because the iodine starts
for
reading withthestarch afteritisinexcesswiththe ascorbic
acid

5. (1.0 mark) How much vitamin C in mg does the fresh fruit sample contain? Show your
calculations.

It contains 0.0019g

CHEM 205 LAB 3: Analysis 7

 Experiment 3

Insert your photos and show calculations on the remainder of this page for Tables 1 and 2. Add
an extra sheet if you need it.

starch solution M g Ascorbicacid Molan.ly in litros Juice

1 starchmass waterV Vitaminamass thereare80mgserevery100g
watery
0.2 sozmg.o.su
Vitamin C g
ascorbicacid
50mL 50g 100mL
son 0.00
acid 97.1
Ascorbic solution
V 1009 c0.001g
100mL0.1L
23.74
ftp.iooio0ir 91 w
10050.50 sdutemdio 6g
0.95g
00277molf.fm ami
Nlofiodine Molamass176.124mA
089µm

iodine2.5 Molarmass II253.809no 176.12g

a0.0020mmol
0019g
o.ozzqydmoi jo
Imai m 0
ami xml
100mi son
qq.Y.s.io
emo M GE fsmd
V000277mi O1.07910 01
x0.75mL mi
0.0146
d
Por iodine4.939mi M0.00277mu002AM
MaIa on M.to
oYffjsId l438xIo'M
t.az y
o.owmo lmio.am 0.487M
aos
y.s.ro

Finalsolutionir VitaminCandelasjuicewithtincture iodine

g

Vitamin C citrusjuice

CHEM 205 LAB 3: Analysis 8