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2020 Jithin S JMP
2020 Jithin S JMP
Technical Paper
A R T I C L E I N F O A B S T R A C T
Keywords: In the current work, a comprehensive three-dimensional topography characterization of electrical discharge
Surface topography textured SS304 surfaces is performed under the following heads: quantitative representation, microstructures
Surface texture and their distributions, and surface functionality. Topography analysis reveals that peak count distribution tends
Areal texture parameters
to become flattened with their mean shifting to higher heights when discharge energy increases. Higher
EDT
discharge energy generates rougher textured surfaces with taller and sharper, but less densely distributed peaks.
SS304
These textured surfaces also show improvement in wetting and sealing properties, more running-in period wear
MSC:
00-01
volume, more surface area for load carrying, and improved lubricant retention capacity.
99-00
* Corresponding author.
E-mail address: ssjoshi@iitb.ac.in (S.S. Joshi).
https://doi.org/10.1016/j.jmapro.2020.10.066
Received 18 July 2020; Received in revised form 20 October 2020; Accepted 23 October 2020
Available online 2 November 2020
1526-6125/© 2020 The Society of Manufacturing Engineers. Published by Elsevier Ltd. All rights reserved.
S. Jithin et al. Journal of Manufacturing Processes 60 (2020) 384–399
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S. Jithin et al. Journal of Manufacturing Processes 60 (2020) 384–399
to each of these aspects. The different aspects of surface topography components are filtered on the scanned surface to get roughness (S-L)
classification, their sub-focuses/purposes, and the corresponding areal surface, which has only the roughness components. A Gaussian filter
texture parameters used in this analysis are given in Fig. 2. Initially, the with a suitable cut-off wavelength (λc ) needs to be applied to obtain the
authors perform a quantitative representation of the textured surfaces S-L surface. It is essential to select a proper λc for filtering. The average
under two heads: roughness estimation and surface height. Secondly, we inter-peak and inter-valley distance on the surface topography was
characterize the microstructures and their random distribution in EDT evaluated to be 100 μm, at the lowest discharge energy (0.5 mJ) used for
surface topographies generated under groups such as surface symmetry, EDT experiments. As per the usual rule of thumb, the cut-off wavelength
isotropy or anisotropy, peak distribution, peak roundedness or sharp (λc ) is selected as five times this inter-peak distance. Thus, λc is 500 μm
ness, and surface complexity. Finally, we investigate the applicability of or 0.5 mm. Short-wave (λs ) filtering also needs to be applied on the
the textured surfaces in various functions under four classes: wetting and surface. ISO suggests a bandwidth (λc /λs ) of 300:1 for S-filtering or
sealing properties, wear volume available for the running-in period, short-wave filtering [23]. Thus, S-filter is performed with a λs value of
surface post-running-in wear, and lubricant retention. We also investi 1.67 μm. The topography images and areal texture parameters are
gate how these topography aspects vary with a change in discharge measured on this S-L surface obtained after filtering. The areal feature
energy used for generating the EDT SS304 surfaces. Thus, we arrive at a parameters such as ten-point height (S10z), density of peaks (Spd), and
comprehensive characterization of EDT SS304 surface topography. arithmetic mean peak curvature (Spc) are evaluated at 5% Wolf pruning.
We employ a 3D optical profilometer known as Alicona Infinite
Focus Microscope for scanning the surface topography of EDT SS304 3. Results and discussion
samples. Readings are taken at each quadrant of the textured circular
region on SS304 samples, at 10× magnification. Readings are repeated In this section, initially, we analyze the scanned surface topography
at these quadrants a few times and averaged to reduce errors. We used images to study the surface characteristics. Further, EDT SS304 surfaces
MountainsMap software to process the scanned data and to evaluate the are characterized to obtain a quantitative representation of the textured
different areal texture parameters required. Initially, the scanned sur surfaces, to characterize the surface microstructures and their distribu
face is leveled, and then, the outliers are removed. Form and waviness tions, and to analyze surface functionality in various applications.
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Fig. 6. Surface profiles at random locations of textured surfaces generated at different discharge energy (E).
(see Fig. 4(b)), can be observed by a reduction in the highest peak count discharge energy. We understand from the graphs that Sa and Sq show
to 29 peaks/mm2 , which is at a higher surface height of 45.5 μm. As the an increase with an increase in discharge energy (see Fig. 5(a) and (b)).
discharge energy is further increased to 500 mJ (see Fig. 4(c)), we Thus, the roughness of the textured surfaces, in terms of common
observe that the highest peak count reduces to 16 peaks/mm2 , which is roughness indicators, such as Sa and Sq, increases with an increase in
at an even higher surface height of 60 μm. discharge energy. This is due to larger peaks and valleys generated at
high discharge energies, as discussed in the previous section. We can
observe this increase in heights of peaks and valleys with an increase in
3.2. Quantitative representation of textured surface discharge energy by making a visual comparison of surface profiles
evaluated at random locations on these textured surfaces (see Fig. 6).
A quantitative representation of the EDT surfaces is required as an The curve fit equations for Sa and Sq show a good fit with high R2 values,
identifier of the topographies generated. The section aims at developing indicating a consistent trend for these parameters with varying
a quantitative representation of the textured surface topographies under discharge energy. It is also observed that for the initial increase in
two heads: roughness estimation and surface heights. discharge energy from 0.5 to 5 mJ (10 times increase), Sa and Sq show a
significant increase from 1.78 to 3.65 μm (105% increase) and 2.28 to
3.2.1. Roughness estimation 4.65 μm (104% increase), respectively. Whereas for further increase in
Roughness estimation is aimed at forming a representation of the discharge energy from 5 to 50 mJ (10 times increase), Sa and Sq show
roughness of the textured surface. This enables classification of the increase from 3.65 to 5.45 μm (49% increase) and 4.65 to 7 μm (51%
textured surface as a fine or a rough finish. The areal texture parameters increase), respectively. At last, the increase in discharge energy from 50
used in roughness estimation are arithmetic mean height (Sa), and root to 500 mJ (10 times increase), Sa and Sq only show an increase from
mean square height (Sq). Their variation with discharge energy is rep 5.45 to 7.35 μm (35% increase) and 7 to 9.58 μm (37% increase),
resented in Fig. 5. It is observed that there are two sets of data at three respectively. This gradual decline in percentage increases of Sa and Sq
discharge energy levels of 100, 250, and 375 mJ. Such double data sets with increasing discharge energy is because the crater dimensions do not
were because two different combinations of current, pulse on-time, and increase linearly with an increase in discharge energy. This trend of
voltage used for these experiments, which resulted in the identical
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crater dimensions is due to a larger volume of material to be eroded (as 3.2.2. Surface heights
the volume is the third power of crater dimensions) and an increase in We undertake this analysis for forming an estimate of surface
molten material resolidification, as discharge energy increases. heights. This forms another mode of quantitative representation of the
surface topography. This analysis is performed with the help of two areal
Fig. 9. Projected area percentages above and below mean plane for different discharge energy (E).
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Fig. 10. Variation in surface isotropy/anisotropy parameters with discharge energy (E).
texture parameters: maximum height (Sz) and ten-point height (S10z). above and below mean plane (see Fig. 9(a)). However, for the topog
The variation of Sz and S10z with discharge energy is shown in Fig. 7. raphy generated at 5 mJ, we observe that the projected area percentage
We understand that from Fig. 7(a) that the maximum height (Sz) of the below mean plane (52.11%) is larger than that above mean plane
surface topography shows an increasing trend with discharge energy. (47.89%) (see Fig. 9(b)). As discharge energy is increased to 50 mJ, the
This increase in Sz can be attributed to the increase in crater dimensions projected area percentage of points below the mean plane increases to
with discharge energy, as explained before. 54% (see Fig. 9(c)). And for topography generated at 500 mJ, this pro
Ten-point height (S10z), which takes into consideration the five jected area percentage further increases to 55.86% (see Fig. 9(d)). This
topmost and bottom-most surface points, also display an increasing confirms that as the discharge energy increases, we observe that the
trend with an increase in discharge energy (see Fig. 7(b)). S10z, an areal surface tends to become asymmetric with more points lying below mean
feature parameter, is a more reliable measure for maximum peak-to- plane as compared to those lying above the mean plane. This shift of
valley height of the surface compared to Sz, as it is not significantly surface points could be because the crater dimensions increase with an
affected by a single surface outlier as that by Sz. Both Sz and S10z curve increase in discharge energy, which leads to larger valley regions
fit equations display a good fit with high R2 values. (formed by craters) compared to the peak regions (formed between
craters). The curve fit model for Ssk in terms of E shows a good fit with a
high R2 value of 0.8298.
3.3. Characterization of microstructures and their distributions Kurtosis (Sku) is an indicator of the presence of sharp (Sku > 3) or
blunt (Sku < 3) peaks on the surface. A perfectly symmetric surface will
The surface topographies generated using EDT have microstructures have a Sku value of 3. It is observed that the Sku values of the textured
of irregular shapes and sizes, and are randomly distributed over the surfaces are more than 3 at all discharge energy levels (see Fig. 8(b)).
surface. Hence, the characterization of microstructures and their dis This indicates that the textured surfaces display slightly sharper peaks
tribution on EDT surface topographies is essential to understand the and valleys as compared to those on a perfectly symmetrical surface.
contours and appearance of the surface. In this section, we undertake However, Sku does not show any significant change with discharge en
this characterization with five purposes: surface symmetry, isotropy or ergy. This could be understood from the curve fit equation of Sku in
anisotropy, peak distribution, peak roundness or sharpness, and surface terms of E, which has a poor R2 value. Sku tends to vary slightly around a
complexity. value of 4.
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Fig. 11. Polar direction graphs (a–d) obtained for surface topographies obtained at similar parameter settings (50 A, 50 μs, & 100 V).
Fig. 12. Variation in peak distribution parameters with discharge energy (E).
Fig. 13. Surface topographies obtained at E = 100 mJ with different parameter combinations.
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graphs for surface topographies scanned at four different locations of the insignificant summits are merged to nearby significant peaks. Spd is a
textured surface at a parameter setting (50 A, 50 μs, & 100 V) are shown better parameter to represent EDT surfaces, compared to Sds as it takes
in Fig. 11(a–d). From these polar graphs, we observe that there are no into consideration only significant peaks. Spd displays a decrease with
individual prominent arms in any direction in the polar direction graphs. an increase in discharge energy, as per the curve fit model (see Fig. 12
Thus, we can conclude that no direction has significant prominence over (b)). However, the model does not give a good fit, according to its low R2
the other directions, which indicates a high isotropic nature of the EDT value. It was also observed that Spd of surface topographies obtained for
surfaces. similar discharge energies, but different combinations of operating pa
rameters, display large differences (see Fig. 13). Hence, the variation of
3.3.3. Peak distribution Spd with current, pulse on-time, and voltage is thus of interest and is
Peak distribution is essential to be analyzed to get an understanding plotted in Fig. 14. It is understood that a significant variation in Spd is
of the microstructure distribution on the EDT surface topography. The only observed with an increasing pulse on-time (ton ). Spd decreases with
parameters analyzed for this purpose are density of summits (Sds) and an increasing ton . Spd displays a slight decrease with an increasing
density of peaks (Spd). The influence of discharge energy on these pa discharge current (I) and a decreasing gap voltage (V). Hence, we
rameters is represented in Fig. 12. Density of summits (Sds) represents conclude that the peak density of the surface decreases with an increase
the number of summits per unit evaluation area. As Sds decreases, the in pulse duration. Furthermore, this decrease in peak density can lead to
contact stresses increase, which leads to surface damage. Hence, low Sds an increase in contact stresses of the surface.
is not desirable in contact applications. Sds does not show any identifi The microstructures or peaks on the textured surfaces are also
able trend against a change in discharge energy (see Fig. 12(a)). The studied using SEM images to form a better understanding of their shape,
curve fit equation for Sds does not give a good fit. Hence, we proceed to size, and distribution. SEM images of textured surfaces obtained at
analyze the density of peaks (Spd), which is a more reliable parameter to discharge energy values of 200 mJ and 2000 mJ are compared in Fig. 15.
characterize the peak distribution on the surface. For both textured surfaces, a random distribution of microstructures in
Density of peaks (Spd) represents the number of significant peaks in a location, size, and shape can be observed. This is due to the stochastic
unit of evaluation area. For the evaluation of Spd, all smaller and nature of spark occurrence during the EDT process. Individual discharge
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Fig. 16. Variation in peak roundness or sharpness parameters with discharge energy (E).
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Fig. 18. Variation in wetting and sealing parameters with discharge energy (E).
Fig. 19. Measured contact angles (θm ), Sdq, and Sdr at discharge energy (E) values of (a) 0 mJ (non-textured surface), (b) 0.5 mJ, and (c) 250 mJ.
Fig. 20. Representation of functional (volume) parameters in Abbott-Firestone curve for different discharge energy (E).
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Fig. 21. Representation of functional (stratified) parameters in Abbott-Firestone curve for different discharge energy (E).
energy indicates an improvement in the wetting and sealing properties less than 90◦ . In contrast, we observe that for both textured surfaces, θm
of the textured surfaces [25]. Guo et al. [26] analyzed the sealing effect is greater than 90◦ , indicating that they are hydrophobic or water-
in terms of a parameter known as area ratio, which is similar to Sdr. They repelling in nature. This indicates that the EDT process results in
found that higher the area ratio of the texture, more efficient is the changes in surface chemistry which lead to wetting property change. It is
sealing effect. They have also reported that the preferable area ratio for observed that at a low discharge energy value of 0.5 mJ, the textured
good sealing is 5 to 20%, which is similar to Sdr range obtained in surface has Sdq and Sdr values of 0.32 and 4.9%, respectively, and
current work using EDT process. Since surface textures generated using correspondingly θm measured has a value of 112◦ (see Fig. 19(b)). As
EDT at higher discharge energies have higher Sdr as compared to that of discharge energy increases to 250 mJ, Sdq and Sdr on the textured sur
textures generated at lower discharge energies, the former offers more face increase to 0.57 and 12%, respectively, and correspondingly θm
efficient sealing. measured on the textured surface increases to 127.5◦ (see Fig. 19(c)).
The improvement in wetting property of textured surfaces generated Therefore, we can conclude that with an increase in discharge energy,
at higher discharge energies is confirmed by performing a few contact Sdq and Sdr parameters increases, which leads to an improvement in the
angle measurement experiments. This also enables checking of variation wetting property of textured SS304 surfaces.
in wetting property with Sdq and Sdr parameters. The contact angle For the next three studies in this section, we utilize functional pa
measurements were made using water droplets (of size 1.8 μl) on the rameters, which fall into two categories: volume (includes Vmp, Vmc,
textured surfaces, following the sessile droplet method. The measured Vvc, and Vvv) and stratified (includes Sk, Spk, and Svk) parameters.
contact angle (θm ) on non-textured and textured surfaces at different These parameters are derived from the Abbott-Firestone curve or
energy levels, and their corresponding Sdq and Sdr values are given in bearing area curve of the surface topography. The functional (volume)
Fig. 19. The contact angle reading on the non-textured surface was and functional (stratified) parameters for EDT surface topographies
observed to be 42.5◦ (see Fig. 19 (a)). This indicates that the non- generated at different energy levels are represented in Abbott-Firestone
textured SS304 has a hydrophilic or water-attracting nature, as θm is curves, as shown in Figs. 20(a–d) and 21 (a–d), respectively. Their
Fig. 22. Variation in running-in wear volume parameters with discharge energy (E).
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Fig. 23. Variation in parameters representing surface post running-in wear with discharge energy (E).
variations are discussed in the upcoming subsections. 23 (a), it is understood that Vmc increases with an increase in discharge
energy. An increase in discharge energy from 0.5 to 500 mJ, leads to an
3.4.2. Wear volume available for running-in period increase in Vmc from 1.972 × 10− 3 to 8.206 × 10− 3 mm3 /mm2 (316%
Wear volume available for running-in period represents the amount increase) (see Fig. 20(a–d)). From Fig. 20(a–d), we also understand that
of material removed from the surface during the running-in period of for incremental increases from 0.5 to 5 mJ, 5 to 50 mJ, and 50 to 500 mJ,
contact applications. This surface aspect is studied in terms of peak Vmc shows corresponding increases of 117%, 41%, and 36%,
material volume (Vmp) and reduced peak height (Spk). Peak material respectively.
volume (Vmp) represents the volume of peak material eroded from the Core void volume (Vvc) represents the core space available on the
surface during its running-in period in contact applications. From surface after the running-in period is completed. We understand that
Figs. 20 and 22 (a), it is understood that Vmp increases with an increase Vvc increases with an increase in discharge energy (see Figs. 20 and 23
in discharge energy. As the discharge energy increases from 0.5 to (b)). An increase in Vvc from 2.695 × 10− 3 to 1.266 × 10− 2 mm3 /mm2
500 mJ, Vmp increases from 1.161 × 10− 4 to 7.153 × 10− 4 mm3 /mm2 (370% increase) is resulted when discharge energy increases from 0.5 to
(516% increase) (see Fig. 20(a–d)). For various increments of discharge 500 mJ (see Fig. 20(a–d)). We also observe that incremental increases in
energy from 0.5 to 5 mJ, 5 to 50 mJ, and 50 to 500 mJ, the corre discharge energy from 0.5 to 5 mJ, 5 to 50 mJ, and 50 to 500 mJ, results
sponding increases in Vmp are 123%, 69%, and 63.5%, respectively (see in corresponding increases of 112.5%, 57%, and 41% in Vvc, respec
Fig. 20(a–d)). Thus, there is a significant increase in the wear volume tively (see Fig. 20(a–d)). Thus, the core space available on surface post
available for running-in period, as discharge energy is increased. running-in wear increases for topographies generated using higher
Reduced peak height (Spk) is the height difference between the discharge energies.
Abbott-Firestone curve and the equivalent line at 0% material ratio. It Core roughness depth (Sk) is the height difference for material ratios
represents the average of peak heights above the core surface. From 0% and 100% on the equivalent line. Sk is a measure of the peak-to-
Figs. 21 and 22 (b), we understand that Spk increases with an increase in valley height of the surface with predominant peaks and valleys
discharge energy. For an increase in discharge energy from 0.5 to removed. From Figs. 21 and 23 (c), we understand that Sk increases with
500 mJ, Spk increases from 2.325 to 14.64 μm (530% increase) (see discharge energy. We observe that an increase in discharge energy from
Fig. 21(a-d)). For various increments of discharge energy from 0.5 to 0.5 to 500 mJ results in an increase in Sk from 5.683 to 22.41 μm (294%
5 mJ, 5 to 50 mJ, and 50 to 500 mJ, the corresponding increases in Spk increase) (see Fig. 21(a–d)). We also observe increases in Sk of 115%,
are 122.5%, 75%, and 62%, respectively (see Fig. 21(a–d)). This in 38%, and 33% for corresponding increments in discharge energy from
crease in Spk indicates that the surface topography generated at higher 0.5 to 5 mJ, 5 to 50 mJ, and 50 to 500 mJ, respectively (see Fig. 21
discharge energy comprises taller peaks compared to those on topog (a–d)). This increase in Sk with an increase in discharge energy indicates
raphies generated at low discharge energy. The presence of high peaks that the surface area for load-carrying after the running-in period of the
increases the volume available to be worn-off during the running-in texture is higher when generated at higher discharge energy.
period. Thus, a study of variation of Vmp and Spk with discharge en
ergy indicates an increase in running-in wear volume. 3.4.4. Lubricant retention
EDT surface topographies have previously been employed in the
3.4.3. Surface post running-in wear texturing of rake face of tool inserts for lubricant retention leading to a
After the completion of running-in wear, the resultant surface is the reduction in cutting forces [3]. Thus, an analysis of the lubricant
one that takes part in contact applications for a majority of the com retention property of the EDT surface topography is critical. It is also
ponent’s running life. Thus, it is essential to characterize this aspect of desired to understand the variation in lubricant retention for surface
the EDT surface topography. The surface post running-in wear is topographies generated at different discharge energies. Lubricant
analyzed in terms of parameters such as core material volume (Vmc), retention of EDT surface topographies is analyzed in terms of two pa
core void volume (Vvc), and core roughness depth (Sk). Core material rameters: valley void volume (Vvv) and reduced valley height (Svk).
volume (Vmc) represents the surface volume that does not play any Valley void volume (Vvv) represents the volume available for lubricant
significant role in contact applications or lubrication. From Figs. 20 and retention on the surface. We understand that Vvv increases with an
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Fig. 24. Variation in lubricant retention parameters with discharge energy (E).
Fig. 25. Furrows on surface topographies generated at different discharge energy (E).
increase in discharge energy (see Figs. 20 and 24 (a)). An increase in (a–d)). For incremental increases in discharge energy from 0.5 to 5 mJ, 5
discharge energy from 0.5 to 500 mJ results in a corresponding increase to 50 mJ, and 50 to 500 mJ, there are 127% increase, 37% increase, and
in Vvv from 2.459 × 10− 4 to 7.735 × 10− 4 mm3 /mm2 (214.5% in a 17% decrease, respectively (see Fig. 21(a–d)). A higher Svk for to
crease) (see Fig. 20(a–d)). For increments of discharge energy from 0.5 pographies generated at higher discharge energies indicates a higher
to 5 mJ, 5 to 50 mJ, and 50 to 500 mJ, the corresponding percentage depth of the area for liquid accumulation, thereby improving lubrication
increases in Vvv are 118%, 36.5%, and 6%, respectively (see Fig. 20 properties. Thus, an increase in Svk with discharge energy, combined
(a–d)). Thus, the lubricant retention capacity of surface topographies with an increase in Vvv, indicates an improvement in the lubrication
increases when they are generated using higher discharge energies. retention capacity of the EDT surface topographies.
Reduced valley height (Svk) is the height difference between the Furrow analysis of topographies is also performed to study the
equivalent line and the Abbott-Firestone curve at 100% material ratio. It change in lubricant retention capability of textured surfaces generated
represents the average of valley depths below the core surface. Svk is at different discharge energy values. The furrows on the surface texture
found to increase with an increase in discharge energy (see Figs. 21 and act as a lubricant reservoir in contact applications. Hence, as furrow
24 (b)). We observe that Svk increases from 2.103 to 5.608 μm (167% dimensions increases, the lubricant retention capability of the surface
increase) as discharge energy increases from 0.5 to 500 mJ (see Fig. 21 texture also increases. The furrow images of topographies generated at
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Table 1 lying below the mean plane, while accompanied by a slight reduction in
Concluding remarks of surface characterization of EDT SS304 surfaces. the surface’s isotropic nature. Textured surfaces generated at higher
Surface topography Specific purpose Low discharge High discharge discharge energies display a reduction in peak density, but the indi
aspect energy energy vidual peaks tend to become sharper. Higher discharge energy also re
Roughness sults in a reduced surface complexity of the textured surface. The
Low surface High surface textured surfaces show high wetting and sealing properties as a conse
estimation (in
Quantitative roughness roughness
terms of Sa and Sq) quence of being generated at high discharge energy. Similarly, textures
representation of the
textured surface
Surface heights (in Low peaks and High peaks generated at high discharge energy tends to provide higher running-in
terms of Sz and shallow and deep wear volume, more surface area for improved load carrying capacity,
S10z) valleys valleys
and higher lubricant retention capacity.
Symmetry (in terms Lower surface Higher surface
of Ssk and Sku)
Acknowledgement
asymmetry asymmetry
Higher Lower
Isotropy (in terms
isotropic isotropic We want to express our gratitude towards Department of Science and
of Str and Std)
nature nature Technology, Advance Manufacturing Technology Committee, Govern
Peak distribution ment of India, for supporting this work under the project titled
Characterization of Higher peak Lower peak
(in terms of Sds and
microstructures and density density “Generating Functional Quality Textured Surfaces using Electrical
Spd)
their distributions Discharge Machining for Biomedical And Machining Applications” (DST
Peak roundness or
sharpness (in terms
Rounded
Sharper peaks
File No: DST/TSG/AMT/2015/239). We also thank Digital Surf, France,
peaks for exceptionally extending the free trial of their MountainsMap® soft
of Ssc and Spc)
Slightly more Slightly less ware for this study.
Surface complexity
(in terms of Sfd)
complex complex Conflict of interest: The authors declare no conflict of interest.
surface texture surface texture
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