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DATE: _____________

EXPERIMENT NO. 9

OBJECT:
To prepare and perform standardization of 0.1N NaOH with 0.1N Oxalic acid.

REQUIREMENTS:
Weighing balance, Burette, Beaker, Conical flask, funnel, volumetric flask, pipette, spatula, glass rod,
oxalic acid , NaOH, Phenolphthalein , Distilled water.

THEORY:

Same as experiment no 3.

PROCEDURE:
1. Rinse all the glassware.
2. Take a calculated amount of oxalic acid in a beaker & dissolve it in water and make up the
volume up to 100ml distilled water.
3. Take a calculated amount of Sodium hydroxide in a beaker, dissolve it in water, and make up the
volume up to 100 ml distilled water.
4. Fill up the burette with NAOH solution up to the mark.
5. Take a 10 ml solution of oxalic acid in a conical flask.
6. Add one or two drops of phenolphthalein as an indicator and titrate it against NaOH solution
until the solution appears pink.
7. Note the reading of burette.
8. Repeat the process 3- times, take concordant reading and determine the concentration of oxalic
acid.

OBSERVATION
S.no Initial Reading Final reading Difference Concordant reading
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CALCULATIONS:

RESULT
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DISCUSSION:

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