UNIVERSITY OF SOUTHERN PHILIPPINES FOUNDATION

SALINAS DRIVE, LAHUG, CEBU CITY

Product name: Dishwashing Liquid Date Manufactured: February 2, 2017

Batch number: (WA KO KAHIBAW) Expiry Date: February 2019

RATIONALE

In every happy occasions there are always people behind the scenes and those people are

the one who washes the dishes after every their done celebrating and eating, and their most

trusted companion in these times are dishwashing liquids.

Dishwashing liquids are detergents that are used to assist in hand washing as well as

machine washing of glasses, plates, cutlery and cooking utensils. These detergent products are

usually a high-foaming mixture of surfactants with low skin irritation. Regardless of brand, few

characteristics and features are vital in a hand dishwashing liquid that include - lasting suds,

mildness to hands, superior cleaning performance, safety for dishes and other washables, storage

stability, pleasing appearance and fragrance, convenient packaging as well as dispensing. In

formulating and designing a dishwashing liquid to meet this criterion, manufacturers typically

use certain basic ingredients. 

UNIT DOSE FORMULATION

FORMULATION % v/v PER 350 mL

Sodium lauryl ether sulfate 1.083% 10.83 g

Sodium triphosphate 0.25% 2.5 g
Coco diethanol 0.417% 4.17 mL
Sodium chloride 0.166% 1.90 g
Downy scent oil 0.083% 0.83 mL
Water soluble dye (blue) 0.0108% 1.08 mL
 UNIVERSITY OF SOUTHERN PHILIPPINES FOUNDATION
SALINAS DRIVE, LAHUG, CEBU CITY

Distilled water q.s q.s

PROCEDURE:

1. Accurately weigh the quantities of each ingredient using an analytical balance.

2. Transfer the SLES to a beaker and add a little water. Stir the SLES very well.
3. Add CDEA to the SLES. Mix well with a stirring rod.
4. Continue stirring the mixture until it becomes creamy. Add water once in a while to
prevent the mixture from foaming while stirring.
5. Meanwhile, dissolve the STPP in a little amount of water. Mix well and set aside.
6. If the CDEA-SLES mixture is already creamy, transfer it to a small pail or a stainless
steel container. Add a little amount of water while stirring continuously.
7. Transfer the mixture to the mixer then switch on. When the mixture is already foamy, add
the dissolved STPP slowly while mixing continuously.
8. Dissolve the salt in a little amount of water. Add this to the mixture, which is being
mixed continuously.
9. Next, add downy scent oil as fragrance and the dye as colorant.
10. Continue mixing until the mixture thickens. Set aside.
11. Once thickened, pour the mixture into a clean container and set aside for about 2 hours.
12. When there are no more suds, pour the liquid detergent into clean bottles.

TECHNICAL SPECIFICATIONS OF RAW MATERIALS

Sodium Chloride
 UNIVERSITY OF SOUTHERN PHILIPPINES FOUNDATION
SALINAS DRIVE, LAHUG, CEBU CITY

CAS Registry Number: 7647-14-5

Molecular formula: NaCl
Molecular weight: 58.44
Synonyms: Salt, common salt, table salt, rock salt, halite, evaporite (when it is left after salt
water has evaporated), brine (when dissolved in water) and NaCl

Description:Sodium Chloride contains not less than 99.0 percent and not more than 100.5
percent of NaCl, calculated on the dried basis.
Packaging and storage: Preserve in well-closed containers.
Labeling: Where Sodium Chloride is intended for use in the manufacture of injectable dosage
forms, peritoneal dialysis solutions, hemodialysis solutions, or hemofiltration solutions, it is so
labeled. Where Sodium Chloride must be subjected to further processing during the preparation
of injectable dosage forms to ensure acceptable levels of Bacterial endotoxins, it is so labeled.
Where Sodium Chloride is sterile, it is so labeled.
Appearance of solution: Dissolve 20.0 g of Sodium Chloride in carbon dioxidefree water, and
dilute with the same solvent to 100.0 mL. This solution is clear and colorless.
Identification: It responds to the tests for Sodium 191 and for Chloride.
Chloride: Dissolve about 3 mg of Sodium Chloride in 2 mL of water. Acidify with diluted nitric
acid and add 0.4 mL of silver nitrate TS. Shake, and allow to stand. A curdled, white precipitate
is formed. Centrifuge, wash the precipitate with three 1mL portions of water, and discard the
washings. Carry out this operation rapidly in subdued light, disregarding the fact that the
supernatant may not become perfectly clear. Suspend the precipitate in 2 mL of water and add
1.5 mL of 10 N ammonium hydroxide. The precipitate dissolves easily with the possible
exception of a few large particles, which dissolve more slowly.
Bacterial endotoxins 85: The level of Bacterial endotoxins are such that the requirement under
the relevant dosage form monograph(s) in which Sodium Chloride is used can be met. Where the
label states that Sodium Chloride must be subjected to further processing during the preparation
of injectable dosage forms, the level of Bacterial endotoxins are such that the requirement under
the relevant dosage form monograph(s) in which Sodium Chloride is used can be met.

TECHNICAL SPECIFICATIONS OF FINISHED PRODUCT

PARAMETERS SPECIFICATIONS

1. Organoleptic Evaluation
1.1 Color Blue
1.2 Odor/Flavor Downy Scent
1.3 Appearance Clear
1.4 Form Liquid
2. Physical Properties
 UNIVERSITY OF SOUTHERN PHILIPPINES FOUNDATION
SALINAS DRIVE, LAHUG, CEBU CITY

2.1 pH 7-8
2.2 Specific gravity 1.0
2.3 Viscosity high
3. Chemical Properties
3.1 Assay: Each 350 mL of Dishwashing Liquid contains
Sodium Lauryl Ether Sulfate 1.083%
Degradation product
4. Microbiological Testing
4.1 Standard Plate Count not more than 100 cfu
4.2 Salmonella Count 0 cfu
4.3 Coliform Count 0 cfu
4.4 Molds and Yeast Count not more than 10 cfu

CERTIFICATE OF ANALYSIS

PARAMETERS SPECIFICATIONS ACTUAL RESULTS

1. Organoleptic Evaluation
1.1 Color Orange Orange
1.2 Odor Orange Scent Orange Scent
1.3 Appearance Clear Clear
1.4 Form Liquid Liquid
2. Physical Properties
 UNIVERSITY OF SOUTHERN PHILIPPINES FOUNDATION
SALINAS DRIVE, LAHUG, CEBU CITY

2.1 pH 7-8 8
2.2 Specific gravity 1.1-1.3 1.2
2.3 Viscosity 200-500 cps 300 cps
2.4 Deliverable volume 95-100% 98%
3. Chemical Properties
3.1 Assay: Each 350 mL of Dishwashing Liquid contains
Sodium Lauryl Ether Sulfate 1.083% 1.082%
3.2 Degradation product
3.3 Homogeneity nmt 6% 5%
4. Microbiological Testing
4.1 Standard Plate Count nmt 100 cfu 0 cfu
4.2 Salmonella Count 0 cfu 0 cfu
4.3 Coliform Count 0 cfu 0 cfu
4.4 Molds and Yeast Count nmt 10 cfu 0 cfu

FULL DESCRIPTION AND METHOD USED IN THE PRODUCT MANUFACTURE

Dishwashing liquid contains anionic surfactant, nonionic surfactant, amphoteric

surfactants and cocamidedea as stability of foam. Also, it has dye, preservative and fragrance. In
addition to sodium chloride or magnesium sulfate is used to viscosity. For making antibacterial
liquid dishwashing, it also include antibacterial agent that can be used different ingredients as
antibacterial. Dishwashing liquid also known as dishwashing soap, dish detergent and dish soap,
is a detergent used to assist in dishwashing. It is usually a highly-foaming mixture
of surfactants with low skin irritation, and is primarily used for hand washing of
glasses, plates, cutlery, and cooking utensils in a sink or bowl. In addition to its primary use,
 UNIVERSITY OF SOUTHERN PHILIPPINES FOUNDATION
SALINAS DRIVE, LAHUG, CEBU CITY

dishwashing liquid also has various informal applications, such as for creating bubbles, clothes
washing and cleaning oil-affected birds.

The blending procedure or method was used during the process. The ingredients were
added in the order listed with continuous mixing until a clear, smooth and homogenous batch is
obtained that is free of lumps and particles. Laboratory equipments are essential in the
manufacture of various products. One of the materials used in product manufacture is the
analytical balance. An analytical balance (often called a "lab balance") is a class of balance
designed to measure small mass in the sub-milligram range. Beaker is a common container in
most laboratory. It is used for mixing, stirring, and heating chemicals. Hot plates for laboratory
use provide a good source of heating for reactions and other testing procedures. A glass rod,
stirring rod or stir rod is a piece of laboratory equipment used to mix chemicals and liquids for
laboratory purposes. They are usually made of solid glass, about the thickness and slightly longer
than a drinking straw, with rounded ends. A graduated cylinder, measuring cylinder or mixing
cylinder is a common piece of laboratory equipment used to measure the volume of a liquid. It
has a narrow cylindrical shape. Each marked line on the graduated cylinder represents the
amount of liquid that has been measured.

STABILITY STUDY

Packaging
1. Immediate: Amber Bottle with PP cap Temperature: 40° C
2. Secondary: Box Relative Humidity: 75%

Parameter Specifications Initial 3 mos. 6 mos. 9 mos. 12 mos.

Testing
 UNIVERSITY OF SOUTHERN PHILIPPINES FOUNDATION
SALINAS DRIVE, LAHUG, CEBU CITY

Color Blue Blue Blue Blue Blue Blue

Odor Downy scent Downy Downy Downy Downy Downy

scent scent scent scent scent

Appearance Clear Clear Clear Clear Clear Clear

Form Liquid Liquid Liquid Liquid Liquid Liquid

pH 7-8 8 8 8 8 8

Specific 1.1-1.3 1.2 1.2 1.2 1.2 1.2

gravity

Viscosity 200-500 cps 300 cps 300 cps 300 cps 300 cps 300 cps

Deliverable 95-100% 98% 98% 98% 98% 98%

volume

Homogeneity Nmt 6% 5% 5% 5% 5% 5%

STABILITY STUDY

Packaging
1. Immediate: Amber Bottle with PP cap Temperature: 30° C
2. Secondary: Box Relative Humidity: 75%

Parameter Specifications Initial 3 mos. 6 mos. 9 mos. 12 mos.

Testing

Color Blue Blue Blue Blue Blue Blue

Odor Downy scent Downy Downy Downy Downy Downy

 UNIVERSITY OF SOUTHERN PHILIPPINES FOUNDATION
SALINAS DRIVE, LAHUG, CEBU CITY

scent scent scent scent scent

Appearance Clear Clear Clear Clear Clear Clear

Form Liquid Liquid Liquid Liquid Liquid Liquid

pH 7-8 8 8 8 8 8

Specific 1.1-1.3 1.2 1.2 1.2 1.2 1.2

gravity

Viscosity 200-500 cps 300 cps 300 cps 300 cps 300 cps 300 cps

Deliverable 95-100% 98% 98% 98% 98% 98%

volume

Homogeneity Nmt 6% 5% 5% 5% 5% 5%

PACKAGING

Bottles and closures

UNIVERSITY OF SOUTHERN PHILIPPINES FOUNDATION
SALINAS DRIVE, LAHUG, CEBU CITY

Label