Professional Documents
Culture Documents
PULGA
PEDELÌ
Conservation Practices on Archaeological Excavations
The relationship between archaeology
and conservation has long been a complex
and challenging one. Yet it is often initial
conservation in the field that determines the
long-term survival and intelligibility of both
movable artifacts and fixed architectural
features. For this reason archaeologists and
conservators must work successfully together
to ensure that recovered material culture—
and the many meanings it carries—is properly
preserved for future generations.
Conservation Practices
on Archaeological Excavations
Getty Publications
(800) 223-3431
www.getty.edu/publications
PRINCIPLES AND METHODS
Printed in Canada
Conservation Practices
on Archaeological
Excavations
Principles and Methods
Corrado Pedelì
Stefano Pulga
The Getty Conservation Institute works to advance conservation practice in the visual arts, broadly
interpreted to include objects, collections, architecture, and sites. It serves the conservation community
through scientific research, education and training, model field projects, and the broad dissemination
of the results of both its own work and the work of others in the field. And in all its endeavors, it focuses
on the creation and dissemination of knowledge that will benefit professionals and organizations
responsible for the conservation of the world’s cultural heritage.
This book was originally published in Italian in 2002 by Edizioni del Giglio, Florence, Italy. It was
created as a consequence of a training course taught by the authors and organized and funded by the
Museo Internazionale delle Ceramiche (MIC), in Faenza, Italy. The course was developed through
the hard work and dedication of Anna Maria Lega, who at the time was the coordinator of the MIC’s
department of conservation and today is assistant director of the Istituto Statale d’Arte G. Ballardini
in Faenza. The authors owe Anna Maria a great debt of gratitude for her enthusiastic support of this
project from its inception.
Getty Publications
1200 Getty Center Drive, Suite 500
Los Angeles, California 90049-1682
www.getty.edu/publications
Front cover: Lacuna being infilled during stabilization treatment of a mosaic in situ. Jebel Oust, Tunisia.
Photo: Elsa Bourguignon © J. Paul Getty Trust
Printed in Canada
Chapter 2 Chapter 7
Environmental Issues 13 Stabilization 63
The Soil 13 Structural Intervention 63
The Buried Object or Feature 14 Mechanical Interventions 67
The Burial Environment 15
Chapter 8
Messa in luce: Principles
and Conservation Issues 18 Prevention of Biological Attack 71
Direct Methods 71
Chapter 3 Indirect Methods 72
Properties
and Deterioration Treatment Strategies 72
of Archaeological Materials 21
Biocides 74
Overview 21
Biochemical Methods 76
Materials Common to Structures 21
Inorganic Materials Common to Objects 23 Chapter 9
Organic Materials Common to Objects 27 Consolidation 77
Preliminary Considerations 77
Chapter 4
Methods of Consolidation 78
Messa in luce: Exposing or
Unearthing Objects and Structures 31 Consolidation and Stabilization
of Stratigraphy 81
Conservation Issues 31
Principles of Exposure/Unearthing 32 Chapter 10
Conservation Techniques Detachment and Removal 83
for Exposure/Unearthing 34 Fixed Structures 83
Movable Objects, Features, or Materials 86
Bibliography 147
Chapter 14
On-Site Temporary Storage 107 Index 151
General Characteristics 107
About the Authors 159
Basic Requirements for Temporary Storage 107
Examples of Temporary Storage Systems 108
Chapter 15
Documentation 111
Conservation Log/Report 111
Conservation Activities and Treatments 111
Type of Material Used 112
vii
viii
that involve relatively simple techniques and easy-to- ered materials—when the priorities of one discipline
find tools and materials and that may not necessarily are advanced at the expense of the other. Both profes-
require a conservator to implement them. In chapter 11 sions ultimately aim to achieve the same objective: to
the stages of exposing or unearthing archaeological understand and preserve the past through the material
materials are considered in relation to the conserva- record. We hope that this book can serve as a referen-
tion question of preliminary cleaning; this allows us to tial framework for the proper planning and budgeting
identify the critical features of each of these important of both archaeological and conservation activities,
activities, clarify their points of reciprocal influence, which are—or should be—inextricably linked.
identify potential conflicts, and suggest possible prac- Finally, it is perhaps fitting that the introduction
tical solutions, thereby facilitating a seamless continu- to a book very much concerned with methodology
ity from archaeology to conservation. Proper packing should say something about the method of its own
and labeling are also treated in some detail, to empha- composition. All that has been written in the following
size the importance of the management and storage pages is based in the authors’ personal experiences,
of archaeological materials as a critical component acquired in the field over many years. These experi-
of their recovery and survivability. Finally, generous ences were examined critically against the published
space is devoted to possible solutions for medium- findings and concerns of professionals of differing
and long-term preservation, such as reburial of fea- nationalities who deal directly with issues concern-
tures and the capping and repointing of masonry. ing the conservation of archaeological remains. There
Throughout we set aside most general theories, followed the task of adapting the ethical principles
broad assumptions, and rigid emphases on exclusive and operational practices of conservation generally to
areas of competency in favor of a simple, inclusive, the specific realities of Italian archaeology. This, from
and pragmatic approach that is realistically applicable the very beginning, was the primary objective, for it
in the field. This is true not only for systematic exca- obliged us to examine the problems common to exca-
vations but also—and even more emphatically—for vations from a range of perspectives and to propose
situations involving the need for rescue or emergency solutions of maximum flexibility.
excavations, the frequency and constraints of which The result is a book that has been written in a
are growing ever greater, to the detriment of both eth- spirit of close and fruitful collaboration. Each chap-
ical practice and archaeological remains themselves. ter attempts to merge the authors’ knowledge and
It is our belief that meaningful results can be experiences in such a way as to arrive at a common
obtained by focusing on the specific conservation understanding. We have tried our best to make every
needs of material heritage, whether or not it is to be sentence useful to those who seek to understand the
excavated. For us the concern is, and should remain, conservation issues that characterize archaeologi-
methodology. There is no overriding benefit to archae- cal excavations and who are willing to attempt to
ologists or conservators—or, for that matter, to recov- resolve them.
time to fully unearth sensitive archaeological materials Because, realistically, few sites have medium- to
in order to minimize the potential for environmental long-term conservation measures implemented to
shock and, even before this, implementing appropriate ensure their preservation, it is widely accepted that the
systems of shelter or protection and having the appro- best option for the conservation of small or movable
priate materials on hand to deal with any eventuality. artifacts and features is their removal to a laboratory
Excavation is rarely complete at the end of just or storage facility. With respect to the sites themselves,
one season. The issues of protecting in situ features some will inevitably be destroyed or disturbed by
or remains between excavation campaigns should construction or development, and others, without the
thus also be considered, planned for, and, if needed, potential or significance for visitation, will be reburied
financed. Virtually every choice related to the whole to ensure their preservation. Very few sites are consid-
or partial protection of an excavated site is ultimately ered important enough to be fully preserved and have
the result of a compromise between archaeologists full measures carried out for their long-term preserva-
and conservators. Ideally this compromise should be tion and presentation. In any case, no excavated site
in favor of the basic principles of preventive conserva- should be abandoned and left to inevitable deteriora-
tion, but this is not always the case. For this reason, it tion and ruin.
is useful to evaluate the pros and cons of implement- It is important to fully evaluate the resources
ing preventive conservation measures well beforehand necessary to partially or fully preserve a site, in both
instead of near the end of an excavation season, a practical and financial terms. Conservation, once
critical moment when preventive conservation mea- undertaken, is not static but rather is an ongoing and
sures are often seen as an extra burden in terms of active commitment that must be carried out full-time.
work and funds. Underestimating the need for pre- Sufficient funds and personnel must be available to
ventive measures will almost always result in some undertake regular and extraordinary maintenance,
form of physical and mechanical deterioration, to the environmental monitoring, and, if possible, some form
detriment of the preserved archaeological artifacts, of climate control dealing with light and temperature
features, and stratigraphy, leading to a loss of informa- (this can be in the form of shelters), not to mention
tion and context. security of some sort to prevent vandalism or theft.
Another issue that may arise during the course of
an excavation is the differing professional responsibili-
ties and objectives of archaeologists and conservators. Factors That Characterize
Usually conservators want to remove fragile or sensi- and Influence Archaeological
tive archaeological objects as soon as possible to avoid Excavations
further deterioration. Archaeologists, on the other
At the moment of excavation at least two objectives
hand, want to know the context of the object and its
are crucial:
relation to other artifacts or remains and thus do not
want it removed too quickly. The outcome in these • Definition and systematic documentation of the
instances can be negative if appropriate measures to relationship between the archaeological finds and
ensure stability are not implemented in a timely man- their spatial and stratigraphic context
ner. Here too a compromise is often necessary, one • Avoidance of further deterioration or loss of fragile
that takes into account the needs of the archaeologist or highly degraded archaeological materials that
in association with those of the archaeological mate- are chemically and physically unstable
rial to ensure its stability and preservation. As with
These two priorities, one archaeological and the other
all the previously mentioned issues, the planning
conservation driven, are often downplayed or disre-
and coordination of operations is of fundamental
garded because of administrative or logistical factors.
importance, as is mutual respect for professional
These factors include the following:
competencies.
• Site typology and archaeological relevance, for
example, necropolis, urban or rural settlement,
Conservation after Excavation monument, road, dump
At the end of most excavations there are typically two • Type of excavation, for example, academic
different types of interventions carried out, depending training program, professional excavation, rescue
on the fate of the site itself: preventive (active main- excavation, explorative excavation, recovery
tenance, e.g., drainage, covers) and therapeutic (to
A site’s typology, its potential archaeological relevance,
reduce the rate of deterioration).
and the type of excavation often overwhelmingly
define the goals of excavation and, by extension, the per week); organization of meals (where the major
priorities. The very methodology by which excavation meals of the day are taken, whether exclusively at
is to be undertaken will be directly influenced by these the excavation house or on the site or some combi-
factors, as will the organization of responsibilities and nation of the two); basic sanitation and health con-
activities, including those regarding personnel, bud- ditions conducive to minimizing illness and days
get, and allotted time. missed due to sickness
The decision to preserve a site will determine, first • Technological logistics: availability of basic services
and most important, the type and extent of conserva- (running water, electricity, heat, etc.), temporary or
tion measures undertaken to effect its presentation permanent structures for housing personnel and
and accessibility. The perceived significance of the site for dealing with recovered materials (tents, houses,
as a whole or a particular feature of it will influence laboratories, warehouses); security (alarm systems
the type and extent of conservation intervention car- or security personnel, communication systems);
ried out in the excavated areas, the creation of shelters availability of equipment and supplies for archaeo-
and/or protective structures, and the preservation logical and conservation operations; proper drain-
of movable artifacts or features in situ, as well as the age of rainwater
development and financing of a maintenance plan. • Bureaucratic factors: permits for excavation
The decision to temporarily or permanently rebury (whether determined by a bid contract or outside
a site will determine the necessary minimum level of or independent funding); agreements and issues
documentation, as well as the types of possible consol- involving multidisciplinary competencies common
idative structural interventions to be applied to dete- to excavation (whether overseen by a university or
riorated or at-risk features, and the implementation of administrative body or a private company)
various stabilizing and protective measures aimed at • Shareholder involvement: promotion of the sig-
counteracting the deleterious effects of natural (rain, nificance of the excavation to local and regional
groundwater, and the weight of soil) and anthropo- populations as a reflection of their heritage and
logical (foot or vehicular traffic) phenomena. as having potential political or economic benefits
The inevitability of the destruction of a site due to associated with tourism or visitation to a site to
development or other causes will determine the more foster a sense of connection to and responsibility
meticulous and definitive level of necessary documen- for the site and its excavation
tation with respect to the previous two options and • Safety issues and regulations: adherence to and
the possible removal of large or immovable archaeo- implementation of accepted and regulated safety
logical features (e.g., mosaic floors, frescoed walls, measures pertaining to working conditions, safety,
renderings) that otherwise would be irreparably lost. operation of equipment, and building codes associ-
The following factors can have a profound influ- ated with the various professional competencies
ence on the nature of the excavation: common to excavations
• Time available for completion of work: the time
• Site location and climatic conditions: if outdoors
necessary to undertake all the disciplinary opera-
whether in an urban area or in the countryside
tions associated with excavation, not just the
and if indoors whether within a building or a
excavation itself
naturally protected area such as a cave; the days,
• Professional factors: number of professionals,
weeks, and/or months that are financially and, in
whether part of the administrative structure of the
terms of seasonal weather, climatically feasible for
excavation or as outside contractors, and the level
archaeological excavation to take place (i.e., a short
of professional training associated with each (e.g.,
time in areas of the world with severe winters and
excavators may be part of a training program, while
most of the year in areas that are temperate and
the architects or conservators are professionals)
thus more conducive to outdoor work)
• Human (and psychological) factors: the individual
• Material factors: topography of the terrain to be
character of the personnel involved with excavation
excavated and its soil composition, as well as the
activities, their collective or individual profession-
nature and state of preservation of the finds
alism and organizational skills, their level of inter-
• General logistics: distance of the site from the base
est and involvement, as well as their reasons for
of operations (where people are fed and housed
involvement (academic, moral, financial, etc.)
and where recovered materials are worked on
• Other factors: unexpected events, such as weather
and stored); transportation (whether the site is
or illness; external pressures such as financial, emo-
reached by foot, car, or other means); work sched-
tional, or outside circumstances
ule (number of hours per day and number of days
• Economic factors: limited or nonexistent financ- excavation, continuing through the period of study
ing for active or preventive conservation measures and interpretation, and concluding with publication
(most archaeologists prefer to direct as many of the final report. British archaeology, in its approach
of their resources as possible to actual excava- and management, has always been considered a model
tion rather than to fund related activities such as by archaeologists around the world. Even most con-
conservation) servation professionals who deal with conservation
• Time factors: possible conflict between objectives and preservation issues in the field consider the Brit-
of archaeologists and constraints imposed by bud- ish model exemplary, albeit one in which local regula-
getary imperatives, especially in such projects as tions and/or realities may necessitate an adjustment in
public works in which archaeological remains are its practices and implementation. This is, in fact, the
deemed insignificant or the project (e.g., construc- main intent of the present volume: to make conserva-
tion of roads, subways, underground parking struc- tion activities applicable to general archaeological
tures) is deemed of high value or priority problems and to underscore why it is paramount to
• Interdisciplinary collaboration and cooperation: include preventive and conservation measures from
the rare case in which conservation priorities are the very beginning of planning operations and actual
given precedence over archaeological activities, excavation.
when some or a substantial portion of the funding
of an excavation is used to slow or delay actual What Necessitates Conservation Measures
excavation Ethical and conservation principles were set forth by
the UNESCO General Assembly at its December 5,
Certain inherent, or “natural,” factors cannot be 1956, meeting in New Delhi in the “Recommendation
changed or modified in any way. These include the on International Principles Applicable to Archaeologi-
geographic location and archaeological relevance of a cal Excavations 1” (see Appendix 1). The so-called
site, its topography and soil composition, and the con- Restoration Charters were initiated in 1932 by the
dition of its finds and features. Most of the remaining Consiglio Superiore per le Antichità e Belle Arti (IT)
factors—the available budget, general logistics (hous- and reelaborated in 1972 by the Italian Ministry of
ing, transportation, work schedule), and human issues Education. And on May 12, 1983, the ICCROM Gen-
(professionalism and motivation)—are adaptable and eral Assembly in Rome issued guidelines in its Twelfth
can be changed or improved. With respect to conser- Session report.
vation, it is possible to intervene in some technical- It is useful to recognize the practical realities of
logistical factors, for example, bureaucratic ones and many or all the professional disciplines associated
public and political opinion. From a technical point of with the recovery, study, and preservation of archaeo-
view, attention to the organization and coordination logical and historical materials (independent of their
of activities, the associated personnel and their profes- typology or actual or associated value) in relation to
sional competency, and, ultimately, personal safety these governing documents. Despite their long exis-
should be a priority. tence, reconfirmation, and further definition, many
of the practices stated in these documents are often
Conservation Activities flouted or simply disregarded. The loose interpreta-
tion of the signifier “rescue excavation” or “explor-
on an Excavation ative excavation” subverts the principles of these
In 1991 English Heritage published volume 2 of Man- documents. Today, at the beginning of the third mil-
agement of Archaeological Projects (MAP2), which lennium, where this is the case archaeology and con-
provides clear guidelines for planning and organizing servation are commonly perceived not as instruments
archaeological projects and emphatically underlines the to recover, understand, and preserve “human cultural
importance of calculating potential conservation needs patrimony” but as inevitable and obligatory impedi-
on any excavation (Andrews 1991). In 1994 the Insti- ments to modernization. The ability of archaeologists
tute of Field Archaeologists affirmed that any profes- and conservators to influence the time frame of devel-
sionally coordinated archaeological excavation, includ- opment and construction is often negligible. Instead
ing its eventual publication, must involve conservation. excavation is subordinated to the will and desires of
It is interesting to note that both of these initiatives developers, architects, engineers, and politicians. This
originated from the discipline of archaeology. MAP2 is in complete contradiction to the principles, perhaps
in particular defines conservation as an integral part idealistic but nonetheless logical and sound, defined
of the archaeological process, starting with the act of in the charters of half a century ago.
It is striking that the above-mentioned documents • The postponement of the systematic study of
give a great deal of attention to small, movable arti- archaeological finds and their context
facts and materials but do not mention immovable
Emergency excavations are an ever-increasing real-
structures and features in situ. These structures and
ity that produce an inevitable confrontation between
features should be given the same attention and con-
compressed deadlines and scarcity of means, person-
sideration, as they often provide the functional, archi-
nel, and funds. Such circumstances are typically set
tectural, and urban contexts for all movable objects.
in motion by those who decide the fate of heritage
Unfortunately, once the small artifacts have been
on paper according to the need to offer a token ges-
removed, fixed features are typically disregarded and
ture to preservation. This gesture puts archaeologi-
left to certain and often rapid decline. Full or partial
cal procedures and conservation practices and their
preservation of a site (for presentation and interpreta-
principles to the test. In such situations, a momentary
tion) is rare, as is reburial. Once abandoned, a feature
delay is sufficient to witness an act of almost complete
is exposed to atmospheric conditions and biological
destruction by an excavating machine whose use
attack, leading to unfettered alteration and loss in a
and permission to proceed were decided by the same
matter of a few years. Even when full documentation
authorities charged with making decisions on cultural
of the archaeological context has been conducted, the
activities.
physical loss of this context is usually ignored.
As long as there is not a greater common aware-
There are essentially three principal causes of the
ness or a more positive valuation of archaeological
demise and loss of archaeological features: bureau-
heritage, a strategy that is more pragmatic and less
cracy, insufficient planning, and climate. Of the three,
philosophical or theoretically ethical will be neces-
it is certainly easier to ameliorate the negative aspects
sary. If archaeology has to deal increasingly with
of climatic conditions that those of bureaucracy.
the pressures and realities of development, where
Climate responds to dynamics dictated by the laws
rules and rhythms are dictated by the cost of labor
of basic physics, which are scientifically exact and
and materials, then applied conservation techniques
verifiable. The same cannot be said of bureaucracy.
may also need to be adapted to aid archaeological
Insufficient planning can be overcome, especially if an
practice.
interdisciplinary approach is practiced. As enshrined
in the charters, this has been identified as being indis- The Nature of Conservation Interventions
pensable but as yet is not a widespread reality. Beyond the various criteria or terms that might be
used to define the nature of conservation activities
r e l i a b i l i t y o f i n f o r m at i o n in the field, perhaps the most appropriate is that they
An altered or deteriorated artifact may become an should be complementary to archaeological activities
unreliable or misleading document for classifica- (fig. 1.1). Assuming that proper archaeological meth-
tion and, more generally, for the understanding of odology is followed, conservation measures should
historical or archaeological context. Most archaeo- become an integral part of excavation and material
logical artifacts contain a good amount of significant recovery, one that supports archaeological activities
information within their constituent materials. The by providing prompt technical assistance to prevent
preservation of this information is linked directly to deterioration of any recovered materials or, in the
the intrinsic chemical and physical properties of the worst instance, limits loss of its inherent informational
material and its stability and condition at the time of value. Conservation measures undertaken ethically
excavation. Conservation measures undertaken in should act in unison of purpose with excavation and,
the field during excavation can actually help slow any in so doing, avoid many of the potential logistical
potential alteration or deterioration and the definitive issues mentioned above.
loss of information. In order to be accepted and integrated into archae-
ological practice, conservation activities should be
c o n t i n g e n t fa c t o r s underpinned by these guiding principles:
The following may be regarded as contingent factors:
• They should not be at odds with the basic
• The increasing frequency of “emergency” or methodologies of excavation. That is to
“rescue” excavations relative to “systematic” ones say, an artifact or material should not be
• The decrease in funding for both archaeological removed for conservation reasons when this
excavations and conservation, long-term preserva- might compromise the understanding of the
tion, and maintenance archaeological stratigraphy without full and proper
documentation or before conferring with the most of these principles can be adhered to without
archaeologist responsible. recourse to extraordinary measures. Common sense
• They should operate in association and synergy and sufficient planning, coupled with goodwill, basic
with all other excavation activities. training and skills, and a modest budget to acquire
• They should be undertaken in an expedient and simple equipment, are usually enough to ensure a
efficient manner so as to not excessively interrupt positive outcome.
or unduly delay excavation.
• They should not impede but rather foster and con- Planning for Conservation
tribute to further study and understanding. Conservation activities should be conceived during
• They should not impede or otherwise compromise the planning phase of an excavation. This will ensure
future conservation interventions. greater integration and appropriate prioritization of
• In the absence of a conservator in the field, some activities and funding. Planning should be undertaken
basic and remedial operations can be undertaken by an interdisciplinary group that consists at the very
by knowledgeable and appropriately trained least of a director of field operations (archaeolo-
excavators. gist), a director of scientific activities (geophysicist or
• They should be noninvasive. archaeometrist), and a conservator. The inclusion of
• They should be as fully reversible as possible. sponsors as other sources of revenue is also common
• They should be preventive as well as conservative. if grants are not sufficient (Pedelì and Pulga 2000).
• They should always be documented fully. In the case of rescue or emergency excavations,
• They should use easily obtained and maintained planning translates into a predetermined set of rules
equipment. and actions that encompasses the majority of plau-
• They should be cost-effective. sible eventualities and minimizes risks. For systematic
• They should be well planned and organized. excavations, planning involves organizing all facets
of an interdisciplinary effort in order to extract the
If these basic principles are not respected, any materi- maximum amount of information. Most bureaucratic
als treated in an urgent or rescue situation could easily systems that use a bidding process to decide who
be subjected to further deterioration and any later will undertake excavation do not allow for accurate
interventions jeopardized or complicated. The goal technical or scientific planning, let alone recognize or
of intervention should be to stabilize or maintain the encompass conservation activities (De Gattis 2001).
condition of the object so as to preserve its material Aside from their negative influence on the quality of
significance and informational value. Fortunately, work in general and the archaeological outcome in
Figure 1.2 Typical bad situation during excavation due to inadequate planning. Archaeological features
have been covered with polyethylene sheeting while waiting for a temporary shelter to be constructed.
In the meantime, rain has flooded much of the excavated area, and the materials to be used to construct
the shelter have been placed directly on top of the archaeological features. Many potentially harmful
situations can be avoided with proper realistic planning of the time and sequence of activities.
particular, many bureaucratic practices do not even In order for these proposals to work in a broader
consider the conservation needs or the potential for sense, they must involve on the part of the planners:
the preservation of recovered materials, whether mov-
• Understanding the region in question and its
able or immovable.
terrain (likely locations of sites according to natural
A proposal of the Department of Cultural Heritage
features and terrain)
of the Aosta Valley (Italy) that was carried out initially
• Understanding the basic climatic and seasonal
in 2000 and 2001 and continues today provides that all
conditions of the region in question (mean sea-
bids for archaeological contracts include a technical
sonal temperature, highs and lows, number of days
and scientific plan for the recovery and preservation
with subzero and near-zero temperatures, average
of finds (Pedelì 2002). Another proposal by the same
seasonal precipitation, orientation of sites in rela-
service and under examination at the time of writing
tion to the sun and primary winds, and, if possible,
calls for the production of a “plan for intervention
groundwater levels)
and conservation” for any emergency excavation in
• Understanding the location of natural and
the region, as these, by their very nature, rarely have
human resources (sources for materials such as
a preliminary plan. Both of these proposals assume
stone, wood, and water; businesses specializing
common goals for all the disciplines involved toward
in building and art supplies; presence of profes-
a singular objective: greater knowledge about and pro-
sional archaeologists, conservators, and general
tection of cultural heritage.
technicians)
• Understanding and anticipating the types of mate- from those necessary for the treatment of materials
rials, and the nature of their manufacture, likely to from nonarchaeological contexts and, because they
be encountered during excavation (i.e., the excava- are on-site, in laboratories. A particular sensibility
tion of a Roman site might reveal mosaics or floors and familiarity is essential. One of the major issues
in opus signinum, which would not be likely mate- facing conservation on-site is the lack of recognized
rials encountered on a prehistoric site) value of this distinct skill set, which often means that
• Understanding the professional competencies adequately employed and compensated profession-
involved in an excavation and putting in place als are rarely engaged. Therefore, based on personal
a well-organized structure of cooperation and experiences, and corroborated by professionals
communication between them, coupled with involved in excavations in other parts of the world,
an awareness of conservation issues related to we have developed in the Autonomous Region of the
proper caretaking of movable and immovable Aosta Valley an alternative solution: a first aid opera-
materials, including having the basic equipment tional unit (FAOU), composed of individuals with an
and materials on hand to undertake common affinity for the issues specific to archaeological recov-
conservation treatments and preventive measures, ery and in situ preservation.
as well as a defined set of actions relating to As conceived, an FAOU is ideally suited for local
unearthing, protection, conservation, and removal and regional development and construction surveys
and rescue archaeology operations. However, because
Proper planning will truly bear fruit only if the
all forms of excavation involve the recovery of mate-
overall operational budget includes the expenses
rial artifacts, an FAOU can also be seen as a basic
related to protective covers and structures and their
model that can be adapted to all types of archaeologi-
maintenance during excavation operations and
cal projects. As such, its function is to work in concert
between campaigns. It would be frustrating, not to
with archaeologists and conservators to perform the
mention potentially destructive, to have to inter-
more standard and remedial aspects of both activities,
rupt excavation for any number of reasons without
freeing them to focus their energies on larger, more
adequate protection for the excavated area. The most
complicated, intensive, or specialized undertakings.
common recourse in these instances is the use of
Such units are already a reality in England but are still
plastic sheeting to cover large areas; however, plastic
lacking in many places where, more than ever, they
tends to puddle and collect rainwater, creating stresses
would be an invaluable component of the excavation
on the materials beneath it and creating a microen-
process.
vironment that traps moisture and invites biological
growth.
Hypothetical Profile of an faou
The fact that rescue and emergency excavations
An FAOU can consist of one or more persons who do
are now fairly common does not mean that planning
not necessarily have to be archaeologists or conserva-
principles are inapplicable or superfluous. Instead,
tors, although these would be preferred professional
they are of the greatest importance to avoid delayed
backgrounds, even if they may present a slight bias
reaction times or decision making in crucial moments
in their approach. It is important to note that the
because of the temporary unavailability of conserva-
concept of the FAOU was not developed to replace
tion professionals (Pedelì and Pulga 2000). A general
conservators or to undertake the primary and final
knowledge and understanding of the basic principles
interventions on artifacts or a site. The very name
and issues of in situ conservation is fundamental to
“first aid operational unit” was chosen for its neutral
anyone involved in archaeological excavation.
terminology, in the belief that it would help distin-
guish the roles of the operational unit members from
the responsibilities of the archaeologist or conservator
First Aid Operational Unit (Carandini 2000; Barker 1981).
Definition and Function If properly trained and instructed, experienced
If archaeological materials are distinct from other and competent individuals could undertake certain
materials because of the very nature of their manu- tasks that require no specific specialization, ostensibly
facture, interment, and survival, then it is equally filling the philosophical void between archaeolo-
true that materials originating from excavations have gists and conservators and providing methodological
specific conservation issues pertaining to the nature continuity between the two professions. For example,
of their recovery. These issues, in turn, require par- as a medium-term strategy, specific personnel could
ticular conservation skills that are somewhat different be instructed on the basic notions of excavation
techniques, climatic and environmental factors, and • Have the necessary materials and equipment to
their deleterious effects on different types of materi- undertake the prescribed conservation and preven-
als. Building on this, they could be trained in specific tive actions
methods for unearthing sensitive materials, as well • Be involved with site activities from the beginning
as their lifting, packing, and transit. In addition, they • Monitor the condition of artifacts and features in
could evaluate the condition of recovered materials situ and those that have been packed and readied
and their susceptibility to environmental factors and for transport
ongoing excavation activities, as well as the potential • Assess that the prescribed work is being properly
repercussions of different forms of action (leaving in implemented and, if needed, undertake specific
situ vs. removal, etc.). Moreover, they could assess the measures to respond to the situation
ongoing state of preservation and undertake basic pre- • Adjust prescribed activities to evolving situations
ventive measures (stabilization, protection, packing) when unforeseen or unexpected problems are
without turning to more direct and intensive forms of encountered
interventions that would affect or alter the properties • Document all activities, whether conservation or
of a material and that are better performed by a pro- preventive, with forms compatible with the proce-
fessional conservator. Recently there have been several dures of archaeologists and conservators, complete
courses on this subject funded by ICCROM and the with photographs and illustrations suitable for
European Community in Serbia, Albania, and Jordan. incorporation into a final report
In cases involving urgent intervention there is little • Interface with archaeologists, conservators, and
to no room for experimentation, and the necessary all other professionals or specialists involved in
materials and equipment must be readily available. In excavation
this respect, experience gained in the field and objec- • Interface with those responsible for the manage-
tive analysis of the achieved results are fundamental. ment of the storage facilities of the materials
In this light an experienced FAOU can be seen as a removed from excavation
potentially vital link between the realities of archaeo- • Follow all rules and regulations regarding safety
logical excavations and the requirements for long-
In addition, an institutional FAOU could:
term preservation of both movable and immovable
heritage. If this link is weak or nonexistent, recovered • Have a budget that allows for the procurement
archaeological materials will undoubtedly be adversely of the necessary basic annual equipment and
affected, and perhaps too deteriorated to conserve or materials, as well as any specific supplies particular
to provide reliable information. to the type of impending excavation
• Locate and purchase the materials needed for
Duties and Responsibilities the regular maintenance inherent in long-term
In agreement with the archaeologist directing excava- preservation
tion activities or with the department or entity over- • Give presentations on the techniques and mate-
seeing operations, the FAOU as conceived could and rials of intervention to new personnel prior to
perhaps should undertake and oversee certain duties: excavation
• Control spending of portions of the budget
• Participate in the preliminary planning of the
excavation endnote
• Define the parameters of their responsibilities and 1 This chapter is based on Stanley Price 1995.
conservation and preventive procedures therein
Environmental Issues
in alkaline soils (e.g., iron, bone, wood, and cellulose- oxygen, water, and pH levels (see above). In gen-
based textiles or fabrics like cotton). In general, how- eral, the lower the level of oxygen and water and the
ever, it is neutral soils that preserve the largest amount closer to neutral the pH, the greater the probability
of archaeological materials. of preservation of the object.
Temperature directly influences the rate of chemi- Alteration phenomena occur quickly and intensely
cal reaction. Theoretically for every 10°C increase in during the initial period of interment. Subsequently
temperature, the rate of reaction is believed to double. the object gradually reaches what is often defined as a
The rate of deterioration may be similarly affected, state of equilibrium with the surrounding burial envi-
doubling at 20°C as compared to 10°C. Both tempera- ronment, wherein chemical, physical, and biological
ture and oxygen levels tend to decrease with greater interactions between the object and the soil continue
depth. This seems to indicate that there is a greater but at a much reduced and less aggressive rate. Each
probability of better and longer preservation of mate- material type reaches its own state of equilibrium at
rials in the deeper layers of soil. the expense of its original properties and characteris-
tics. This can take multiple forms, including chemical
enrichment through the absorption of compounds
The Buried Object or Feature dissolved in the soil (soluble salts and pollutants car-
While buried, archaeological materials are inevitably ried by moisture) and/or chemical depletion of con-
subjected to many chemical, physical, and biologi- stituents due to hydrolysis, dissolution and leaching,
cal phenomena of alteration and deterioration that structural changes (expansion, contraction, cracking,
not only change their appearance but also alter their disaggregation, etc.), or corrosion (metals and glass).
very nature. The manner in which these phenomena Any or all of these phenomena may produce changes
occur and the changes they create are dependent on in appearance (shape, color, size) and weight. Certain
the structure and composition of the archaeological materials deteriorate but remain in some form of
object or feature, as well as the surrounding soil’s preservation, generally altered in appearance and
Table 2.1 Materials with the Possibility of Preservation (related to hypothetical and generalized burial environment)
Neutral pH Neutral pH
(slightly acidic/ (slightly acidic/
Acidic pH (1–5) basic) (6–8) Alkaline pH (9–14) Acidic pH (1–5) basic) (6–8) Alkaline pH (9–14)
Gold, silver, and Gold, silver, Gold, silver, Gold, silver, and Gold, silver, Gold, silver,
their alloys copper, lead, tin, copper, lead, and alloys copper, lead, tin, copper, tin, zinc,
Roman glass zinc, and their their alloys Shale zinc, and their lead, and their
alloys Iron alloys alloys
Shale Wood
Limestone Bone Shale Shale
Amber Leather
Marble Limestone Limestone Limestone
Porcelain Keratin, horn
All ceramics Alabaster Alabaster Alabaster
Stoneware Amber
Glass Marble Marble Marble
Glazed ceramic Jet
Bone Unglazed ceramics Amber Amber
Porcelain
Shale Jet Jet
Stoneware
Glass Bone
Earthenware
Wood Wood
Textiles (silk,
wool, proteinic Leather Leather
fibers) Textiles Textiles (vegetable
Horn fibers, linen, flax
hemp)
Bone
Iron
All ceramics
Iron
Table 2.2 Materials with Little Possibility of Preservation (related to hypothetical and generalized burial environment)
Neutral pH Neutral pH
(slightly acidic/ (slightly acidic/
Acidic pH (1–5) basic) (6–8) Alkaline pH (9–14) Acidic pH (1–5) basic) (6–8) Alkaline pH (9–14)
Copper, lead, tin, Tin, zinc, and Tin, zinc, and their Lead, tin, zinc, Lead, tin, and their
zinc, and their their alloys alloys and their alloys alloys
alloys Textiles Textiles Textiles Textiles
Iron Wood Wood (vegetable fibers) (proteinic fibers)
Wood Leather Leather Bone Horn
Leather Horn Horn Glass Glass
Horn Alabaster Alabaster Terracotta
Textiles Limestone Limestone Limestone
Bone Alabaster
Limestone
Alabaster
Low-fired ceramics
Medieval glass
structure. Other materials deteriorate altogether and tional standard in Europe, taking its points of refer-
leave little to no trace on excavation. ence from the freezing point of water (0°C) and its
Although the specific processes that cause altera- boiling point (100°C).
tion and deterioration are still not fully understood, Temperature is significant because it affects many
it is possible to construct a fairly detailed account of physical-chemical phenomena important to the pres-
the reactions and events affecting the different types ervation of archaeological materials:
of materials. Tables 2.1 and 2.2 give a basic outline of
• All chemical reactions are accelerated by an
the theoretical relationship between a specific burial
increase in temperature.
environment and material type and the probability of
• Heat causes expansion of materials; conversely,
preservation. Both tables refer to northern European
cooling causes contraction (with the single excep-
soil types, especially British, and differ from tables
tion of water).
for dry sites found in the international literature
• Biological growth, such as bacteria and plants, is
(Sease 1992).
supported by certain temperature ranges.
• Temperature directly affects the relative humidity
of the air and, by extension, the state of equilibrium
The Burial Environment of archaeological materials and their surrounding
The main environmental parameters that have a signif- environment.
icant effect on archaeological objects and features, both
interred and excavated, are temperature (T) and rela- Absolute Humidity and Relative Humidity
tive humidity (RH). These are significant because they The gaseous mixture known as air may contain certain
are fundamentally linked while being highly variable amounts of water in the form of vapor. The amount
and cyclical and can change in intensity and frequency. of potential water vapor in the air is dependent on
its temperature. The warmer the air, the greater the
Temperature amount of water vapor it can contain. Hygrometers
The concept of temperature is relative. In physical are used to measure the actual amount of water vapor
terms it is related to the action of infrared radiation in the air and are based on what is known as the
(IR). There are numerous measurement systems for saturation line, which is the amount of water vapor
temperature: the Celsius scale (°C), the Fahrenheit contained in the air as a function of its temperature.
scale (°F), and the Kelvin scale (°K). Conventionally The maximum amount of water vapor that the air
the Celsius scale is used as the scientific and interna- contains at a given temperature is known as the
absolute humidity (AH). Both the saturation line and All psychrometric charts used to measure humidity
the absolute humidity are expressed in grams of mois- give three parameters:
ture per cubic meter (g/m3) of air. Above any point on
the saturation line, air is not able to absorb or contain • Temperature (T), expressed in °C
any more water vapor, causing any excess moisture to • Absolute humidity (AH), expressed in g/m3
come out of the gaseous state into its liquid form as • Relative humidity (RH), expressed as a %
condensation.
Below the saturation line, air does not always Knowing two parameters will always allow the third to
contain the maximum amount of moisture possible. be calculated.
This is measured with reference to the saturation line
and is better known as the relative humidity (RH). Dynamics and Effects of Climate
For example, as shown in the psychrometric chart Clearly, then, there is a very close correlation between
(fig. 2.1), a single cubic meter of air at 10°C can hold temperature and humidity. Air temperature is directly
up to 10.5 grams of water vapor. If, however, this cubic related to the presence of infrared radiation and will
meter of air contains only 5 grams of water vapor, then therefore be directly proportional to the intensity and
the amount of water vapor present is 50% relative to duration of solar radiation (daylight). Thus tempera-
the saturation line for this quantity of air. Accordingly, ture variations will be greatest on clear sunny days
for this example, the relative humidity would be 50%. and at their minimum on cloudy or overcast days.
Relative humidity is therefore the percentage of satu- Absolute humidity is closely linked to precipitation
ration for a given volume of air at a given temperature and evaporation from bodies of water (rivers, streams,
and is expressed as a percent. lakes, oceans) and the ground.
Figure 2.1
Figure 2.2
Relative humidity is a correlation of both tem- By considering some of the most common weather
perature and absolute humidity. To illustrate this patterns (clear, overcast, rain) it is possible to under-
correlation, the same value of absolute humidity can stand that external climate can be devastating to
have a high relative humidity at a low temperature or archaeological materials. In good weather conditions
a very low relative humidity at a higher temperature the temperature and relative humidity cycle rapidly
(fig. 2.2). In the natural environment the changes in about every twelve hours, with temperature increases
temperature and relative humidity are continuous and and subsequent decreases in relative humidity during
cyclical. Limiting the effects of these variations is of daylight hours, followed by lower temperatures and
paramount importance for the conservation of objects higher relative humidity in the evening and into the
that have remained interred for centuries under stable night. This is, of course, somewhat theoretical given
(nonfluctuating) temperature and moisture levels. that there is a significant difference, depending on
Natural cycles of temperature and relative humid- distance from the equator, in the hours of daylight in
ity variation can be of very long duration (glaciation/ summer and winter. All the same, this still holds true
deglaciation), long duration (seasonal), short duration as a cycle, and in their attempt to reach natural equi-
(days), or very short duration (weather events such as librium with the ambient moisture levels all archaeo-
storms). Seasonal changes are slow and progressive, logical materials will lose moisture during the lower
which can allow materials and objects to slowly adjust relative humidity phase of the cycle and absorb mois-
and find their equilibrium without substantial ill effects. ture during the higher relative humidity phase.
Short-term and rapid environmental changes do not If the weather is overcast or cloudy, variations in
permit objects and materials sufficient time to find their temperature tend to be less severe. Likewise, varia-
equilibrium and therefore result in greater damage. tions in relative humidity tend to be less pronounced,
which means the theoretical danger to archaeological tions simultaneously within the limits of the inter-
materials is also somewhat diminished. preted archaeological layer or stratum. This process is
In the case of rain or snow, archaeological materi- repeated for each successive layer (fig. 2.3).
als would be in direct contact with moisture, in the From the moment of exposure, minutes, hours,
liquid or solid state, and absorption of water would days, weeks, or even months may pass before the full
be rapid. This in turn would cause an increase in vol- excavation and removal of an object or recovery of an
ume in some materials, while all would be subject to archaeological feature. Objects can remain in this state
mechanical forces as water moves over their surfaces. of transition for various reasons, including the excava-
Given that rain is eventually followed by sun or winds, tion of surrounding or adjacent areas or the comple-
the gradual evaporation or sudden loss of water from tion of graphic documentation. During this period,
saturated archaeological materials can produce or the partially excavated object is constantly exposed
provoke many common deterioration mechanisms, to an environment that is different from that of inter-
such as salt crystallization or structural expansion and ment. Some objects or features, especially those that
contraction phenomena. If precipitation occurs in the are large or vertical, such as walls or large pots, can
winter, sudden drops in temperature are possible and simultaneously occupy two different environments.
could lead to the deterioration of objects or materials In these instances both the subsoil and the external
as water freezes within their porous structures. All climate are acting on the object. If the subsoil is wet or
the climatic eventualities mentioned in this paragraph damp, this can favor the migration of soluble salts to
lead to the irrefutable conclusion that most archaeo- the unearthed portion of the object by means of capil-
logical materials directly exposed to wet weather will lary action, channeling moisture from the soil to areas
suffer some form of deterioration. in contact with the air and provoking evaporation.
Starting from this conclusion, it is clear that From the perspective of conservation, the moment
archaeological materials must be considered in rela- of exposure, whether partial or whole, is one of the
tion to their previous, current, and future environ- most traumatic for any type of archaeological find
ments and protected from the moment of their regardless of its nature and whether it was originally
excavation (see chap. 6). This seems self-explanatory created for external or internal use. After centuries
for fragile, sensitive, or deteriorated materials but of adaptation to and permanence in subsoil climatic
equally holds true for stable materials. Accordingly, it conditions, the object is subjected to sudden disrup-
is important to understand that an ideal environment tion of its established physicochemical state of equi-
for archaeological materials’ preservation is not and librium. From the first minutes after unearthing the
cannot be an absolute concept but rather is based on adjustment to the new environmental parameters can
their individual condition and specific physical- cause strong chemical and physical stresses within the
chemical characteristics. object, leading inevitably to alteration, possible dete-
In summary, given the dynamics of climate and rioration, and potentially complete loss.
weather, especially those typical of most open-air Features or objects intended to remain in situ face
excavations, it is important to understand and to take further risk of deterioration, especially if no form of
into account the various deterioration mechanisms covering or adequate localized protection is afforded
these can cause so as to be able to quickly intervene to the excavated area (see chap. 6). Any such archaeo-
limit their effect on the preservation of a number of logical finds are confronted with a different and more
different materials. variable climate than that of interment, and one can
reasonably expect:
Messa in luce: Principles • The significant presence of oxygen
• Temperature variation, seasonal (most pronounced
and Conservation Issues
during the warm seasons), daily (transitions from
The criteria under which archaeological objects or day to night), and sudden (storms)
structural features are unearthed—or “brought to • Relative humidity fluctuations subject to tempera-
light”3—are closely linked to the methodology of ture changes
archaeological excavation. The basic principle of • Moisture-level fluctuations: times of extreme wet
excavation is the systematic removal of superimposed (rainfall, snowfall, flooding, etc.) to extreme dry
earthen layers. In physical terms this translates into (summer months, windy days, drought, etc.)
the progressive removal of soil in the horizontal and • The presence of gaseous pollutants (CO2 and SO2)
the vertical, beginning from the top and working • The presence of light radiation in three forms:
toward the bottom. Soil is removed in both direc- visible, IR, and ultraviolet (UV)
Figure 2.3 Sectional and overhead diagram of the various phases of unearthing during excavation.
In general, all these phenomena reactivate and accel- ing objects from fluctuations in relative humidity, on
erate deterioration mechanisms such as biodeteriora- the other hand, is far more difficult; objects will be
tion and corrosion and precipitate the rapid drying of affected from within minutes of their unearthing, even
materials recovered wet or moist, potentially causing when sheltered or in temporary storage.
structural weakening. Changes in relative humidity cause archaeological
Theoretically since oxygen and relative humidity metals and glass to undergo chemical changes, whose
are the main sources of deterioration phenomena they effects are manifested through corrosion, which
should both be eliminated to guarantee conserva- makes these materials gradually more sensitive to fur-
tion (Thomson 1986). In reality, however, preventing ther humidity fluctuations (see chap. 3). The corrosion
oxygen from interacting with objects on-site is practi- of ferrous metals, although extremely slow within the
cally impossible, and affecting temperature can also burial environment, begins within a matter of minutes
prove very difficult. For these practical reasons climate after excavation in ambient relative humidity levels
control in situ is usually limited to protecting objects exceeding 35 to 40%. This level of relative humidity
or features from direct exposure to sunlight, rain, or is considered relatively dry at many latitudes but is
wind. It is relatively easy to prepare simple systems of harmful to ferrous metals, potentially provoking the
protection against direct sun, wind, and rain. Protect- creation of small brownish liquid droplets that are
the telltale sign of the reactivation of corrosion of the all the factors mentioned in the previous paragraphs
remaining metal. must be factored into the later handling of objects,
The same humidity level (40% RH) also causes especially packing (see chap. 12) and on-site storage
serious damage to water-saturated materials, whether (see chap. 14).
organic or inorganic. For example, in the case of Despite the multiple conservation issues inherent
saturated wood or leather a rapid loss of moisture in the ambient environment and the varying effects
leads to significant dimensional variations and distor- these can have on archaeological materials, most
tions within a few hours and can ultimately cause the objects will respond to such forces in a predictable
complete structural collapse of the object. In certain manner (see chap. 4). This predictability is an advan-
types of low-fire ceramics a rapid loss of moisture can tage, allowing for a number of preventive measures
produce expansion/contraction forces that result in to be planned and prepared prior to excavation. Even
the microfissuring or cracking of the ceramic fabric, so, all conservation efforts can prove to be in vain if
detachment of ceramic or vitreous slips, and much appropriate measures and steps are not undertaken
more. (See chap. 3.) after the completion of excavation and materials are
Other than the archaeological objects and materi- consigned to storage or for treatment.
als themselves, certain substances contained within
their structure as contaminants are also susceptible to endnotes
fluctuations in relative humidity. Of primary impor- 1 This chapter is based on Bergeron and Remillard 1991;
tance in this category are soluble salts, absorbed by and Watkinson and Neal 1998.
the object during burial. Once the object is unearthed, 2 pH is a measurement scale, from 1 to 14, based on
salts acclimatize to environmental humidity levels the concentration of hydrogen ions (H+). Low pH
values indicate a predominance of acid, high values a
by either losing or gaining water from the air, caus-
predominance of base. A pH of 7 is neutral; and the
ing a cycle of deliquescence and crystallization of the farther from 7 the number, the greater the acidity or
salt crystals, together with migration into the porous alkalinity.
structure of the archaeological remains. Porous mate- 3 The Italian expression messa in luce means literally
rials are especially affected, in particular, ceramics and “to bring to light.” In English, “initial exposure” or
stone, which can have disaggregation and efflores- “unearthing” best expresses its meaning in this context.
cence at the microstructural level of their pores. The term is used here to refer to the operation or
The conservation issues of excavated materials moment in which an object or feature is brought to light
associated with climatic fluctuations do not cease after or progressively revealed during the course of excavation
the object has been removed from the soil. Almost by removal of the surrounding soil.
21
considerable adhesive strength between themselves in climates characterized by low precipitation, such
and any aggregates they are in contact with. as deserts. In contrast, such clay-based features are
Masonry walls and floor coverings held together not greatly affected by rising damp through capillary
with or made from aerial binders, especially lime and action because water makes them swell, ostensibly
clay, are common among recovered archaeological closing off the pores within them. It is for this reason
structures. More rarely features can be composed that clays were employed in the past as a moisture bar-
entirely of or held together with gypsum plaster,2 the rier in structures. Even today bentonite is employed as
only true hydraulic binder known in antiquity. Lime a water barrier.
mortars tend to survive well in moist or wet environ- Given these basic characteristics, one can readily
ments, whereas clay- or gypsum-based mortars do not deduce that the general preservation of clay features
and if preserved at the moment of excavation prob- is threatened when they are exposed to a less humid
ably have lost much of their structural cohesion and environment, such as occurs on removal of the envel-
continue to be held together primarily by the moisture oping damp earth during excavation. Even assuming
present in the soil. Once drying begins these mortars that the clay has survived in its original form, expo-
deteriorate rapidly, while lime mortars will remain sure to the open air will begin the process of evapora-
relatively stable. The physical and chemical properties tion and the consequent loss of volume and structural
of each of these types of binders are explored more consistency. Maintaining the original level of moisture
fully below. or implementing controlled slow drying followed by
gradual impregnation with ethyl silicate is the only
Clays feasible option for conserving artifacts of unfired
properties clay (adobe), although this method has drawbacks
Various minerals diffused in the natural world and (see chap. 9).
accumulated in large natural deposits by alluvial or
fluvial action are classified as clays. The two primary
clay minerals are silicon dioxide or silica (SiO2) and Gypsum
properties
aluminum oxide or alumina (Al2O3). At the molecular
level both minerals demonstrate a basic structural Together with clay, gypsum is one of the oldest known
foundation of platelet-like units. By virtue of this binders, its use having been attested in Egypt more
structure, clay particles have a lamellar shape. than five thousand years ago. Gypsum plaster can be
Clays swell when mixed with a small quantity of used without additives or aggregate fillers but remains
water and become cohesive and plastic, which allows susceptible to moisture. For this reason it tends to pre-
them to be easily modeled and manipulated and to serve and be recovered from interior contexts or from
retain a given shape. Plasticity and cohesion are both regions with a dry climate.
linked to the presence of a thin film of water between Gypsum (CaSO4H2O)2 is obtained by the heating of
the lamellar particles. This aqueous film permits the selenite. When mixed with water gypsum undergoes a
particles to slide past one another and at the same chemical reaction that results in the creation of a rigid
time provides the adhesion between the particles that crystalline structure with good resistance to mechani-
keeps the clay mass together. cal stresses.
Clays lose some of their volume during drying as
water between the particles is lost through evapora- d e t e r i o r at i o n
tion. The result is a loss of plasticity and a general The resulting material at the end of the chemical
embrittlement of the clay. To counteract these ten- reaction or hardening of the plaster remains vulner-
dencies, aggregate additives such as sand or quartz able to water and can deteriorate in moist environ-
tend to be mixed into clays, as are organic materials ments. Because of this property it is probable that
like straw, hair, wool, or animal dung that not only gypsum mortars and plasters recovered from a moist
resist shrinkage and cracking phenomena due to burial context will not retain their original mechani-
volume loss but also provide mechanical support cal properties. They will very likely appear slightly
and resistance. pink in color and have a crumbly texture indicative
of physical and chemical deterioration. The possible
d e t e r i o r at i o n conservation interventions and treatments in such
Walls and wall coverings based on clays are suscep- cases are generally highly problematic and virtually
tible to the mechanical action of water (runoff, rain) unfeasible (for suggestions, see Mora, Mora, and
and therefore have a reasonable “life expectancy” only Philippot 1977).
Lime Aggregates
properties properties
Lime is created by heating naturally formed lime- Aggregates are defined as both the materials added
stone or marble composed of calcium carbonate to binders during the production of mortars (sand,
(CaCO3) and various impurities (silicates, alumina, pumice, straw, hair, etc.) and the structural elements
iron oxides). Heating releases carbon dioxide (CO2) held together by the binders themselves (bricks,
from the stone, leaving a basic powder of anhydrous stones, tesserae, etc.). The list of possible aggregates
calcium oxide (CaO), better known as quicklime. If one may encounter during the course of an archaeo-
this powder is immersed in water (CaO + H2O), a soft logical excavation is exceedingly long, and their
paste of “slaked” lime results (Ca(OH)2). Slaked lime characteristics cannot be addressed here in detail
reacts with carbon dioxide present in the atmosphere (see works cited in the bibliography). In general,
(Ca(OH)2 + CO2) to again produce calcium carbonate, however, aggregates can be divided into two main
from which it originally derived (for further informa- groups: natural (e.g., stone) and artificial (e.g., brick).
tion about the cycle of lime, see Appendix 3).
Lime-based mortars always include aggregates such d e t e r i o r at i o n
as sand or pumice because lime alone has very little Every aggregate will react differently to the forces act-
mechanical strength after setting. If aggregates are ing on it depending on its own physical or chemical
added to the lime, the crystalline structure that forms characteristics. By extension, each will have its own
during setting bonds to the granules of the aggregate form of weakness. A porous calcareous stone, for
and creates a material with very strong and notable example, will have a different resistance to deteriora-
properties. tion than a nonporous siliceous stone. Likewise, fired
clay, such as bricks or paving tiles, will have the prop-
d e t e r i o r at i o n erties of a porous material but a resistance to deterio-
Lime-based mortars are generally susceptible to the ration forces dependent on its specific composition,
effects of water, to atmospheric sulfur dioxide, which level of firing, and so on.
transforms the calcium carbonate into a calcium sul-
fate (i.e., gypsum as a sulfate crust), and to the acid- Inorganic Materials Common
ity of soil. Lime mortar interred for a long period in
damp soil will typically be weakened, especially if the to Objects
soil has an acidic pH (see chap. 2), in which case one Metals
may expect the mortar to be friable and less resistant Metal objects can be pure (gold, silver, copper, iron)
to mechanical stresses, with a tendency to powder or alloys (bronze, pewter).3 However, archaeological
during drying. finds of pure metal are extremely rare (occasionally
Table 3.1 Metals and Alloys (late Neolithic to 3rd century a.d.)
gold and copper); they are more commonly composed that is, those that are more reactive (iron and copper),
of some form of alloy. Iron, for example, is usually are inevitably subject to corrosion.
combined with some carbon atoms. Corrosion processes are caused by electrochemi-
cal reactions that occur between the metal and the
properties moisture and oxygen present in the environment,
In general, metals and metal alloys are lustrous, hard, whether ambient or terrestrial. These reactions first
and nonporous and have a crystalline molecular struc- affect the outer surfaces of the metal, partially trans-
ture and high mechanical strength and high chemical forming them into progressively more nonmetallic
reactivity, meaning they oxidize and are susceptible compounds, or corrosion products (oxides, carbon-
to attack by acids and alkalis. In addition, metals melt ates, and sulfides), which in themselves can alter
rather than burn. the appearance of the object. In some instances, as
with iron, corrosion can be so severe that recovered
d e t e r i o r at i o n objects may bear little to no resemblance to their
All metal artifacts with the exception of gold are pro- original form.
duced by first extracting a metal from an ore. This Corrosion can be inhibited but not stopped alto-
takes an enormous amount of energy, which makes gether. It is a spontaneous, inevitable, and irreversible
the extracted metals chemically unstable and subject process. Theoretically the majority of corrosion occurs
to corrosion phenomena that create greater thermo- in the burial environment, suggesting that the greatest
dynamic equilibrium by returning to a state close alteration to the chemical, physical, and mechanical
to that of the ore from which they were obtained. properties of a metal object take place after interment.
Figure 3.1 summarizes the typical life cycle of a It is equally true, however, that the rate of chemical
metal object. reaction rapidly decreases in the burial environment
Instability is dependent on the composition of the and eventually ceases. At this point equilibrium has
metal artifact and its reactivity with external environ- been established between the metal and its surround-
mental elements (O2, SO2, CO2, H2O, salts, acids, etc.) ing environment. As soon as this equilibrium is dis-
contained in the soil or the air. More stable metals rupted or altered (an increase or decrease in oxygen
(gold and silver) are less reactive and therefore more levels, moisture, or pollutants) the corrosion process is
resistant to atmospheric agents. Less stable metals, restarted. Importantly, this is exactly what happens at
Source: Garzanti Technical and Scientific Encyclopedia, 1984; Watkinson and Neal 1998; Plenderleith and Werner 1986.
the moment of excavation, when the object is removed susceptibility and reaction to environmental factors.
from the ground and exposed to a new environment. In wet or humid burial or climatic conditions, poros-
ity allows water in liquid or vapor form to penetrate
Stone into the interior of a stone object or feature, coating all
An infinite number of minerals and rocks (mineral the internal surfaces until eventually achieving com-
aggregates) can be included under this broad clas- plete saturation. During this process water can deposit
sification. Conventionally stones are divided into two substances dissolved or suspended within itself (salts,
major categories: building stones and precious stones. acids, alkalis, gases, biodeteriogens, etc.), which can
Table 3.2 presents the basic typologies of rocks and interact with the stone and initiate chemical reactions,
minerals commonly recovered from archaeological such as acids dissolving carbonates, or give rise to
contexts. cyclical physical phenomena like the crystallization/
deliquescence of salts. In climatic conditions at or
properties under 0°C or 32°F, water itself can freeze inside the
In general stones have a crystalline structure and high larger pores, transforming into a crystalline solid of
resistance to compressive forces and do not burn. greater volume than its liquid form. Following reac-
Stones that contain large metallic inclusions, such as tions between acids and carbonaceous stones, the
iron or copper, may show localized oxidation or dis- objects or features may undergo cycles of partial dis-
coloration. Carbonates, such as most limestone and solution and leaching that further deplete and weaken
marble, can be susceptible to biological attack and their internal microstructure.
acid degradation. The phenomenon of crystallization, whether from
One of the properties that, more than anything water itself or from deposited salts, creates great
else, characterizes most stone is porosity. This can be physical stress within the porous structure of stone,
defined as the hollow or air space between particles in eventually provoking small lesions, cracks, surface
a solid material. The amount of porosity inherent in a exfoliation, and, eventually, complete detachment of
stone has a direct effect on its ability to absorb liquids portions of the object or feature. The presence of water
or vapor, on how it responds to thermal stresses, and in liquid or vapor form (humidity) can cause moder-
ultimately on its mechanical strength and resistance. ate expansion of the total volume, depending on the
nature of the stone and its state of preservation. Any
d e t e r i o r at i o n of these phenomena alone or in combination could
Porosity is the primary factor regulating the surviv- have occurred to a limited degree within the burial
ability of stone objects and features, specifically their environment prior to excavation.
ing or lifting of the slip and localized fragmentation to “weeping” or leaching when too much calcium
and eventually lead to partial or complete separation carbonate was used as a stabilizer. Most glass, with
of the surface from the ceramic body. Examples of this the exception of glass pastes, is characterized by its
behavior are often seen on Roman-era clear sigillata transparency. But transparency is directly affected by
vessels as well as excavated majolica. the amount of mineral impurities in the glass, which
Finally, breakage in all its manifestations (fis- can endow haziness and color, cause air bubbles, and
sures, cracks, flaking, exfoliating, etc.) should not influence the actual state of preservation.
be overlooked as the principal form of damage and
deterioration for ceramics. This is especially true in d e t e r i o r at i o n
that breakage typically allows for the previously men- Archaeological glass is subject to corrosion of a sort.
tioned forms of chemical and physical deterioration The phenomenon is different and more complex
by exposing the porous body of a ceramic to intrusion than that previously described for metals. Consider-
by moisture. ably simplified, glass corrosion is due to the selective
loss of sodium or potassium from the glass matrix,
Glass initially from the external surface. Corroded areas
Ancient glass was created from the fusion of silicon subsequently become more fragile and susceptible to
dioxide (SiO2), in the form of sand, with an alkali flux further corrosion that penetrates deeper into the glass
(sodium or potassium) and an alkaline-earth stabi- (Watkinson and Neal 1998). As a result, affected areas
lizer (such as calcium). Sometimes lead (Pb) was used may show signs of differing degrees of deterioration:
instead of sodium, conferring a greater transparency porosity, pitting, opalescence (partial loss of transpar-
to the glass. Colored glasses were obtained by the ency), pearly or silvery iridescence, surface crystalliza-
addition of metallic oxides, such as iron, manganese, tion (“crizzling”), flaking, and detachment, leading to
or lead. an overall thinning of the glass mass.
properties
Organic Materials Common
In the strictest sense of the term glass has not a
crystalline structure but rather an amorphous one. to Objects
This ambiguous structure has many advantages—for All organic materials have a cellular structure (lattice,
example, it makes glass nonporous and chemically lamellar, spongy, fibrous, or canalled) and are, to vary-
resistant—but also some disadvantages. Chief among ing degrees, flexible. Organics are highly hygroscopic
the latter are poor resistance to compressive, tensile, and able to absorb or release large amounts of mois-
or shock forces, rendering glass fragile and sensi- ture. This is due to their tendency to keep their relative
tive to temperature changes. Too little or too much humidity in equilibrium with the ambient environ-
alkali as a flux can make glass hygroscopic and sus- ment. If drier than their environment, organic materi-
ceptible to damage from moisture (Plenderleith and als will absorb moisture; when wetter, the contrary is
Werner 1986). Soda glass, so called because of the true. The capacity for absorption is related directly to
use of sodium as the flux, is particularly susceptible the material’s cellular structure. Organic materials are
Animal Vegetal
Bone, ivory, antler Wood, cork
Hair Paper
Horn Cotton
Nails, hooves, feathers, cuttlebone Linen
Leather, hide Hemp
Wool Jute
Silk Grains
Seeds
Protein as principal constituent Cellulose as principal constituent
Source: Based on Ginier-Gillet, Hiron, and La Baume 1987; Watkinson and Neal 1998; Berducou 1990.
d e t e r i o r at i o n
Leather can be recovered in a fair state of preservation
where the burial environment is completely dry
(desiccated) or very wet (saturated), the oxygen con-
tent is very low, and the pH acidic (< 7). As with wood,
in wet conditions water can play a dual role: initially
dissolving and leaching out some of the leather’s
Figure 3.2 Simplification of the structure of wood (based
components, such as tannins, which creates gaps and
on de Guichen 1995): a) normal wood: lignin + cellulose;
b) water-saturated or waterlogged wood: lignin + cellulose
voids in the cellular structure, and then filling these
+ water; c) wood exposed to the environment on recovery: hollows and making itself an integral stabilizing part
deteriorated lignin + cellulose. of the structure. Under wet conditions, the leather
can act as a form of filter, trapping various inorganic
materials dissolved in the water (carbonates, silicates,
begins to evaporate and the remaining lignin is no oxides, etc.). Leather has an affinity for insoluble iron
longer sufficiently supported and will collapse salts, which on initial crystallization contribute to the
(fig. 3.2c). weakening of the fibrous structure and subsequently
confer a blackish-brown color and increased brittle-
Leather ness on the leather. Leather can already begin to
properties delaminate within the burial environment because of
Leather as we know it is obtained by chemically treat- such reactions.
ing animal skins, known as the tanning process. The
various substances used in this treatment (tannins, endnotes
oils, smoke, etc.) serve to conserve the principal com- 1 This section is based on de Guichen 1995.
ponent of skin, collagen. As such, leather has a tangled 2 “Gypsum plaster” refers to natural materials based on
fibrous structure that endows it with good physi- calcium sulfate plus a variable amount of water (see
cal durability. Despite being quite resistant and less Appendix 3).
hygroscopic than wood, leather is very sensitive to the 3 This section is based on Berducou 1990; Leoni 1984; and
presence of water, which can lead to biological attack Watkinson and Neal 1998.
and to its complete deterioration.
31
organic items (wood, leather, ivory, textiles), which if numbered, can help with the documentation
should be kept moist or dried very slowly in a of specific find spots after the objects have been
controlled manner and then kept dry. If objects are removed. In areas where a great number of small
recovered dry, they should be maintained in this objects are recovered, this system can also create
state and not exposed to high humidity or direct a ground map of finds without having to use the
moisture. objects themselves as markers.
• When removed: It is good practice during excava-
5. Stabilize structural integrity: tion to keep an initial basic registry of small finds
• Unstable edges and walls of earthen trenches or and objects, noting their basic material and condi-
those areas of excavation to be left exposed to the tion, as well as any particulars. Preprinted forms
elements should have some form of containment or that include basic identification information—
support, such as netting, textile facings, or artificial provisional or excavation inventory number, state
bulwarks like stakes with plywood or dry masonry/ of preservation—using unequivocal and generally
brick containment walls. The same approach accepted terms can be used (see chap. 13).
should be considered for archaeological features
like walls and wall plaster that have a propensity to 7. Protect excavated surfaces from mechanical
erode or collapse. damage:
• Medium-sized to large features or objects (inscrip-
• Protect horizontal features (mosaics, earthen
tions, stelae, columns, etc.) that have sections that
floors, or archaeological layers) as they are being
are detaching may need to be held in place with
excavated. Protection serves for both conservation
strapping, ropes, or tourniquets or by combining
and continued excavation, especially when no
such techniques with systems of shoring and con-
temporary or permanent shelter is planned for the
tainment. (See chap. 7.)
excavated area and the area is still subject to traffic
• Medium-sized to small objects and features
from personnel and excavation equipment such
(inscriptions, capitals, statues, ceramics, etc.) may
as wheelbarrows. Protective measures should be
need to have fragments and/or flaking portions
able to withstand any mechanical stresses caused
adhered in place with reversible resins. In the case
by foot traffic or regular excavation activities and
of larger objects and features, adhesives can be
minimize the transmission of any of these forces to
combined with gauze or other open-weave textiles
the underlying soil or feature to avoid aggravating
to create a reversible surface netting for contain-
already weak or fragile areas. They should be
ment. (See chap. 7.)
lightweight and easily removable to facilitate
• Fairly complete objects of medium size (broken
further excavation if necessary. In this regard
vases, statues, etc.) that are highly fragmented or
various textiles (see chap. 6) or shock-absorbing
have detaching sections or surface exfoliation may
materials (see chap. 12) can be used, as well as
require containment created with temporary wrap-
scaffolding planks or boards or any combination of
pings or open-weave textiles combined with revers-
the two, as befits the situation.
ible resins. (See chap. 7.)
• Protect exposed vertical surfaces (archaeological
• In the case of archaeological features or objects
sections, wall plaster, frescoes, etc.) from erosion
that are crumbling, flaking, or detaching from their
and man-made damage such as surface abra-
structural support and are destined to remain in
sion and scratches due to visitation or ongoing
situ indefinitely or for a long period, consolidation
excavation.
should be considered, combined with the creation
of adequate shelter and protection from the ele-
ments (see chap. 9). 8. Reduce the amount of time an excavated object is
left exposed:
6. Document the presence of small, movable objects:
• Depending on soil type, climatic conditions, and an
• In situ: When small objects cannot be removed and object’s condition, and after proper documentation,
packed immediately after excavation, prevent them objects should be removed as soon as possible (see
from being inadvertently stepped on or damaged chap. 10). The closer removal of the object is to
in any other way by placing small vertical flags the moment of its full exposure, the better. At the
(such as those used in construction to indicate very least, objects should be removed before the
boundaries) in proximity to them. The same flags, excavation is completed and closed.
Figure 4.1 Preliminary
cleaning of flooring in opus
signinum for the purposes
of documentation showing
before and after.
methodology
A satisfactory preliminary cleaning technique for
robust uneven or rough floor surfaces such as opus
signinum or mosaics includes using brushes with
short, natural or synthetic, soft bristles (such as those
used in shoe polishing) in combination with water,
spray bottles, natural sponges, and absorbent paper
toweling (figs. 4.1, 4.2). Application should proceed
one square meter at a time, as follows:
1. Lightly apply a clean, wet brush to a dirty surface
area, and, while holding the brush in the same
position, make a series of small semicircular
movements to dislodge large soil particles with
the brush.
2. Apply one or two sprays of water to the same area,
and again apply the brush in one quick and larger
semicircular motion to definitively move the par-
ticles loosened in step 1.
Figure 4.2 Detail of the preliminary cleaning of a section of
3. Immediately afterward apply a clean and slightly
flooring in opus signinum for the purpose of documentation.
moist, not wet, natural sponge with light pressure
to the treated area so as to absorb and retain any
dislodged soil particles as well as those finer par-
ticles dissolved by the water.
4. Finally, place a sheet of absorbent paper towel on
the area to absorb any remaining moisture or soil
particles. The paper towel can also serve as an
indicator of whether cleaning should proceed or be chemical stresses than materials associated with fixed
suspended. A towel showing particles of anything structures or features, whose mass can often better
other than the soil is a sign to stop all treatment. absorb vibration from excavation activities and cli-
matic shock associated with unearthing.
These steps can be repeated several times as needed to
Because of the great number of object types and
achieve a preliminary cleaning appropriate for docu-
potential states of preservation possible, it is difficult
mentation. Afterward, dampened sheets of Japanese
to suggest general techniques for preliminary cleaning
tissue or a breathable fabric can be placed over treated
of small objects in situ. All the same, given that it is
areas to encourage a gradual and slow drying that
inevitable that many objects will need some degree of
should reduce the possibility of efflorescence forming.
exposure in order to recognize them and understand
Although preliminary cleaning such as this is
their archaeological context, some recommendations
intended to be performed meter by meter, the major
for good practice are indispensable. The techniques
preoccupation of many excavation directors is the
described below may prove applicable in many cases
amount of time needed for such operations to be
but may be inappropriate in cases of extremely fragile,
performed. As an illustration, a square meter of opus
unstable, or deteriorated organic objects made from
signinum can be cleaned in approximately two hours
leather, wood, or textiles and for inorganic artifacts like
by appropriately trained personnel. It must be stressed
heavily corroded metals or glass. More than a specific
that this type and level of cleaning should not be
technique, what is essential is a clear understanding of
confused with full cleaning, which by its very nature
what should and what should not be cleaned.
may involve a slight amount of physical damage to
the surface.1 All the same, the extent of this damage is
removing soil close to small objects
hardly comparable to the resulting damage if the sur-
The removal of soil around objects requires great
face were to be unearthed completely with trowels or
attention and caution because of the often small and
spatulas. Equally, this technique can prove dangerous
fragile nature of the objects to be unearthed as well as
to surfaces that are virtually dry, especially if excessive
the stresses placed on them by soil removal. Slightly
amounts of water are used.
moist soils are favorable for excavation; however,
A similar technique can be adopted for the clean-
the full unearthing of artifacts is fraught with risk,
ing of terracotta surfaces by simply eliminating the
whether the soil is dry and hard or wet and muddy.
use of brushes and working exclusively with a sponge
When one is dealing with dry soils, small amounts
(fig. 4.3).
of soil should be moistened sequentially, not wet-
ted, avoiding any areas of the object that are already
Small Objects
exposed. A good technique is to spray a fine mist of
The act of exposure may require much greater atten-
water in the air over or around the soil to be removed
tion and care for small finds. This is particularly true
and then allow it to be absorbed. Repeat this process
for smaller or very delicate objects. Such materials
until no additional moisture is absorbed. At this point
can usually withstand fewer mechanical and physico-
the mass of soil should appear moist but not wet and
will be slightly expanded and softened and thereby
easily removable. Ideally humidification is limited to
the soil alone and does not involve the artifact surface,
in which case the soil will virtually come off on its
own due to the movement involved in the expansion
of the soil (fig. 4.4).
A flexible metal spatula can be used to remove
thicker layers of soil (no less than 2 cm) from around
an object. As work progresses toward the surface, the
spatula should be replaced with finer and/or softer
tools such as scalpels (interchangeable, with no. 10 or
15 blades) or plastic or wooden spatulas like tongue
depressors and bamboo skewers. Dry residual surface
soil can also be removed with soft natural- or nylon-
Figure 4.3 Preliminary cleaning with a synthetic sponge of a bristled brushes. Brushes should not be used in the
Capuchin tomb made up of terracotta slabs. case of wet or muddy soils.
Figure 4.4 Soil removal with a wooden spatula after initial Figure 4.5 Initial cleaning of a terracotta amphora with a
wetting with nebulized water. Once small portions of soil synthetic sponge.
swell, they become easier to remove.
Removing muddy, clay, or silt soils is much more spatula, and all types of brushes should be stopped
problematic. On the one hand, if these soils are immediately once the majority of soil in proximity to
allowed to dry out, some objects, particularly any the object has been removed. The last layer of fine soil
organic materials, can be severely damaged or even can then be removed in the following ways:
lost. On the other hand, removal of wet, sticky, or
a) If the soil is dry, small brushes with extrasoft,
pasty masses of soil can cause more vulnerable objects
average-length bristles can be used (typically
to break or, as in the case of leather or textiles, to tear.
size 1 to 20, with natural or extrasoft nylon
A uniform strategy is difficult; much depends on the
bristles of 15 mm length).
specific nature of the site and the object and mate-
b) If the soil is damp or wet, brushes will create a
rial types recovered. Ideally objects are block lifted
mud that can act as an abrasive paste if worked
(see chap. 10) and microexcavation performed in a
over the surface. Instead, small commercially
controlled laboratory environment. Barring this, work
available sponges, cut to shape and slightly
can be performed on-site with extreme caution using
moistened, are ideal for preliminary cleaning
rounded semihard tools of plastic (spatulas, spoons,
in such conditions (see chap. 11). The sponges
tongue depressors, etc.) or even of soft wood such
should not be rubbed or slid along the surface;
as balsa.
instead small sections of the sponge should first
be moistened with water spray and then tamped
cleaning small and fragile objects
lightly on the surface (fig. 4.5). Soil particles will
In principle the considerations described for removing
be absorbed into the pores of the sponge and
soil from near a feature hold true for small objects. In
held in place. This technique is highly effective
these cases, however, any type of preliminary surface
in wet conditions but should not be used on dry
cleaning can prove even more difficult and, by exten-
objects or on archaeological metals or glass.
sion, carry greater risk of damage or loss. With this
said, if at all possible thorough cleaning of small or
endnote
friable artifacts should be done in a laboratory envi- 1 It is perhaps appropriate to say that any form of cleaning,
ronment by conservators. even that undertaken during conservation treatments,
If preliminary cleaning in situ is deemed necessary will involve superficial abrasion and loss of minute
and unavoidable, the nature of the material, its mois- amounts of the material being cleaned. This is usually
ture content, and its condition must all be taken into perceptible not to the naked eye but only by careful
careful consideration. The use of trowels, any kind of examination under magnification (10× or higher).
39
Painted Wall Surfaces The types of possible plaster conditions one may
w h at m ay a p p e a r encounter can be summarized as follows:
Many wall remains may have sections or fragments of • Various degrees of friable and crumbly rendering
painted plaster still preserved on their surface. Like • Partially detached from the wall itself
walls themselves, these can be divided into two • Cracked and with large lacunae
Lime-Based Floors (Cocciopesto, Opus • Edging and pointing of all crack and void edges
Signinum, Opus Sectile) with a lime-based mortar (see chap. 7)
w h at m ay a p p e a r • Specific consolidation of the stone constituents
All lime-based floors share a common basic composi- (see chap. 9)
tion: lime and various aggregates mixed with colored
river stone or ceramic fragments (opus signinum) or Mosaic Floors
ceramic fragments only (cocciopesto) or stone pieces w h at m ay a p p e a r
inserted in a regular geometric pattern (opus sectile). At the moment of excavation, it may be difficult
The visual differences are notable, but their conserva- to fully assess the condition of a mosaic floor. The
tion concerns are largely the same due to their shared spaces between individual tesserae will most likely be
lime mortar composition. filled with moist soil or sand, which can give a false
The major conservation issues for these three types impression of completeness and stability. Using small
of flooring and thus lime-based floorings in general brushes, sponges, or swabs, very carefully remove any
are as follows: obscuring and incoherent soil from the grouting to get
a better sense of whether:
• Lack of cohesion within the lime mortar itself
• Insufficient adhesion of the stone or terracotta • The tesserae are well embedded and still adhered to
fragments to the lime mortar the bedding mortar
• Cracks, fissures, or missing areas whose edges are • The tesserae themselves are deteriorated
unstable and susceptible to continued deterioration • Hollows or voids are present where the mosaic has
• Specific deterioration of the aggregate constituents detached from its bedding mortar
• Lacunae exist
w h at m ay h a p p e n
w h at m ay h a p p e n
• The lack of cohesion within the lime mortar may
Obscuring or overlying soil that dries at all, especially
not be visible when the flooring is still damp
if it contains clay, will often shrink in volume, creating
following excavation. This lack of cohesion will
stresses and strains on the mosaic that can provoke:
become more apparent during drying as the
resultant stresses cause crumbling and powdering. • Progressive detachment of the tesserae from the
Such mortars are highly susceptible to mechanical lime mortar
forces. • Progressive deterioration of stone or glass tesserae
• Although the lime mortar may still have good • Sinking or collapsing of areas of the mosaic over
adhesion, the lack of adhesion between the lime hollows or voids
matrix and the stone or terracotta components can • Further erosion of the edges of cracks or areas
lead to their loss through foot traffic, sweeping, and of loss
so on. • Creation of new cracks or losses due to human
• Borders, whether of cracks or missing areas, are mechanical stresses such as trampling
generally quite fragile and will continue to erode
and deteriorate. w h at c a n b e d o n e
• The deterioration of the terracotta and stone con-
• Adhesive consolidation of loose tesserae and the
stituents can, in turn, cause new voids, which can
mortar bedding (see chap. 9)
lead to accelerated border erosion.
• Cohesive consolidation of the bedding mortar and
grout (see chap. 9)
w h at c a n b e d o n e
• Application of a temporary facing to all fragile tes-
• Cohesive consolidation of the lime mortar (see serae or temporary removal of any loose tesserae
chap. 9) (see chap. 7)
• Adhesive consolidation to re-create physical bonds • Edging and pointing of all edges of cracks and
between stone or terracotta constituents and the voids (see chap. 7)
lime mortar (see chap. 9) • Temporary covering of the flooring to protect it
from mechanical damage
Movable Objects Composed tion, which is very important for iron objects. For this
purpose accurate observation of the actual shape and
of Inorganic Materials overall volume of the object are better indicators. It
Iron can be useful to use a small magnet, which will indi-
A rusty reddish-brown color is a key indicator for cate if there is any surviving noncorroded iron. See
iron material. It reveals past corrosion phenomena tables 5.1–5.4.
but does not signify the actual degree of mineraliza-
Table 5.1 Iron
Irregular and blistery details and edges; rough, Advanced or fully mineralized object (more stable)
irregular surface; highly altered and virtually
unrecognizable object form or shape
More or less universally blistery details and edges; Partially mineralized object = Active material
rough but still regular surface; recognizable object state! (unstable)
form or shape
More rarely
Whitish/light gray surface color Chalky soil
Black surface color with bluish spots Anaerobic soil
Table 5.2 Iron
Field test
Objective Type of test Result Meaning
Confirm the extent of Small earth magnet (flat, Attraction Some preserved metal
mineralization of the cylinder shaped); do not
Minimal or no attraction Full mineralization
archaeological metal use horseshoe-shaped
(complete corrosion), no
magnets because too
preserved metal
strong
Table 5.3 Iron
Table 5.4 Iron
Copper Alloys
Unlike iron, copper alloys can vary considerably in
appearance depending on the type of soil in which
they are found. In general copper alloys are chemically
less reactive than iron but still susceptible to corro-
sion. See tables 5.5–5.7.
Table 5.8 Silver and Gold Table 5.10 Silver and Gold
Table 5.12 Lead and Lead Alloys (Pewter) Table 5.14 Stone
Table 5.18 Ceramics
Table 5.22 Glass
Table 5.29 Leather
Table 5.30 Leather
Field test
Objective Type of test Result Meaning
Verify structural condition Needle (insert a needle Easy and complete pen- Structural loss
perpendicularly) etration of the needle with
little resistance, gelatinous
consistency
Partial penetration with some Partial preservation of
resistance structure
Verify the surface condition Absorbent paper, small Black and brown residue Exterior layer or surface is
(only if not gelatinous in sponge, or soft white fabric deposited onto the surface of altered (may not exclude the
consistency) (pass gently over a section of the absorbent paper, sponge, total alteration of the leather
the surface of the object) or clean soft white cloth structure)
Table 5.31 Leather
Table 5.32 Leather
scholarship can be found in postprints of the of protection against moisture while also providing
ARKOS group (AA.VV. 2000). resistance to the mechanical action of rainfall or the
weight of accumulated snow. Combined with its low
Basic Requirements for Temporary Shelters cost, availability, simple adaptability to various situa-
and Coverings tions, and simplicity of placement and removal, these
Based on their typology, temporary shelters and cov- advantages make it easy to understand why plastic
erings must fulfill certain basic requirements: sheeting is widely used. However, these advantages
should not overshadow the potential damage that can
• Protect excavated areas from climatic factors such be caused by improper use, which then must be rem-
as direct sun and moisture edied by conservation, adding to costs and schedules.
• Not provoke or exacerbate environmental factors, Impermeability can also prove to be a negative
such as increasing humidity levels or temperatures, characteristic in some situations. After heavy or pro-
that can prove detrimental to objects or features longed precipitation, rainwater can accumulate and
• Not chemically or physically interact with or alter pool in the lower areas between features or in the
archaeological features or objects voids and recesses of uneven pavements or excava-
• Not impede dramatically further excavation, docu- tion floors. The weight of the water can create strain
mentation, or study on the plastic sheeting, resulting in tears and possible
drainage under the covering. Even worse, much of
Coverings: Sheeting, Textiles, Netting this force may be transferred to the highest points of
From the vast array of industrially manufactured and features, such as the tops of walls. If the plastic cover-
commercially available forms of synthetic sheeting, ing is large in scale, removal after storms can become
textiles, and netting, only a few have found wide- problematic because of accumulated water and, if
spread use and application in both conservation and not done with care and planning, can even run a risk
excavation. The majority of these are polyethylene, of wetting the very features that the covering was
nylon, polyester, or polypropylene and have been vari- intended to protect.
ously used to cover or shelter whole areas or particular All these examples indicate that the greatest misuse
features during excavation and between excavation of plastic sheeting is putting it in direct contact with
campaigns. Of these, some, such as geotextiles, have structures, features, or artifacts. This is more egregious
also found routine use in both temporary and perma- if the plastic sheeting is fully or semitransparent and
nent reburial. the covered areas are in direct sunlight. In these cases
an inevitable warm and humid microclimate will be
plastic sheeting created that not only favors bacterial and plant growth
The most common form of temporary or improvised but also leads to the chemical depletion and physi-
covering is waterproof plastic sheeting, made by cast- cal weakening of the materials that make up features
ing molten plastic in mass. It is therefore appropriate and objects. A further consideration and risk is that
to devote ample space to this material, its specific condensation can form under plastic sheeting when
characteristics, potential impact on archaeological temperatures fall, such as during the night. Combined
artifacts and features, and common misuse. with normal temperature changes between day and
Polyethylene and nylon are the most typically used night, a cyclical change between humidity (gas) and
forms of plastic sheeting. These are similar in appear- condensation (liquid) can lead to the saturation and
ance, usually semitransparent white or solid black, eventual deterioration of archaeological materials.
but differ in chemical composition, which translates If exposed to solar radiation and sunlight for long
to differing molecular weights and, in practical terms, periods, all plastic sheeting will begin to deteriorate.
varied resistance to puncture and tear. Importantly, This is usually manifested in a gradual hardening of
neither is permeable to water or air. This can have the plastic, resulting in eventual cracking and tearing.
both positive and negative implications. A similar effect can be caused by continued exposure
On the positive side, plastic sheeting can be useful to freeze/thaw cycles. Consequently, any plastic cov-
where saturated artifacts must remain wet or must erings used long term should be subject to regular
be dried very slowly and, for various reasons, cannot monitoring and should be replaced when necessary.
be immediately removed or stored under appropriate For the proper use of plastic coverings:
environmental conditions. Equally, in emergency situ-
ations such as sudden rain or snow, these sheets can • Avoid covering objects and features that will
make an important contribution by creating a barrier continually be in direct sunlight. Coverings are
• Wide enough to completely cover the excavated This type of shelter is especially well suited for
area and to be structurally stable, even under ongoing excavations because of its adaptability. A tra-
strong winds, but with as few supports as possible ditional scaffolding-and-corrugated-roof shelter may
so as to not physically interfere with, interact with, initially be a small structure and then be expanded
or alter the archaeological features or objects up to a size of 80 to 100 square meters as excavation
• Reversible, even if used for a long time, by means continues. In all of its manifestations, whether small,
of dismantling with a minimum of risk to the medium-sized, or large, it is important that this type
structures and artifacts below of shelter be constructed taking into consideration its
• Reusable (if possible) overall weight and the loads it can support, as well as
the slope of the roof and the direction of water runoff
traditional shelters and drainage. By calculating and designing for these
Traditional shelters are among the most common and three factors, disastrous accidents due to the failure
practical forms of adaptable shelter ever devised, con- of the roof or the entire structure can be avoided
sisting of a vertical structure of metal scaffolding tubes (figs. 6.2, 6.3).
(A), a horizontal element made of the same scaffold- With this in mind, we provide some basic guide-
ing tubing (B), and a roof (C) of corrugated fiberglass lines for building traditional tube-and-corrugated-
or tin sheets or any form of conventional impermeable roof shelters. First, an example of traditional shelter
covering (fig. 6.1). Roofing with industrial insulated construction follows.
panels (metal or painted plastic outer skin with a In the case of a trench of 2 × 3 m (A), a shelter
polyurethane fire-retardant core) may be particularly of 4 × 5 m should be designed to allow for sufficient
useful for sheltering structures or features exposed to cover from rainfall and sunlight (B), leaving an
large amounts of direct sunlight. Roofs of this type can earthen perimeter of roughly 1 meter on all sides to
dissipate the heat buildup of solar radiation by acting act as a walkway or space for temporary storage of
as a heat sink. materials and equipment (C) (fig. 6.4a). If the edge
impact on the appearance of a site or feature. Even By contrast, there are a few disadvantages:
so, they are highly effective in many respects (eco-
nomic, organizational, logistical, and technical) and • They need many vertical supports around their
are practical and adaptable to most archaeological perimeters (usually one per meter), which can
situations. It is for these reasons that, with or without be physically disturbing to ongoing excavation
perimeter fences, this basic form of covering is the and documentation and visually disturbing to the
most commonly used for ongoing excavations and for presentation of the site, structure, or feature.
protection between excavation seasons. In general, • They may incur the costs of short- or long-term
scaffolding framework (fig. 6.5) and simple roof shel- rental.
ters offer the following advantages:
Excavated areas can also be successfully cov-
• They protect artifacts from precipitation (rain, hail, ered using alternative sheltering systems. Small
snow) and direct sunlight. to medium-sized trenches (up to 4 × 6 m) can be
• They reduce the action of wind while simultane- effectively covered by ready-made modular tents or
ously allowing for moderate air circulation, which greenhouse structures, better known as tensile struc-
can be useful to inhibit the growth of macro- and tures, which consist of a constructible/collapsible
microorganisms. frame that is kept in tension with sheeting (prefer-
• They may inhibit or prevent the formation of sur- ably white cotton or polyester rather than PVC).
face frost on excavated areas and structures in areas One drawback is that these need to be anchored
with cold winter climates. well to the ground for stability in strong winds.
• They lower costs by reducing or preventing dete- This can involve cords, stakes, or rods that might
rioration of in situ structures or artifacts as well as impede movement outside of these structures or be
stratigraphic sections, which in turn minimizes the obstructive to other activities on-site. A bigger and
amount of recleaning of excavated areas and the more advanced adjustable tensile structure could be
need for conservation intervention. applied in the case of more extended areas (fig. 6.6).
• They allow continuous visual monitoring of the In the event of large or irregular excavation areas
state of preservation of recovered materials and (larger than 30 m2), traditional scaffolding shelters
features. may be better than small, prefabricated modular cov-
• They allow for excavation work or conservation erings. Beyond these dimensions an ad hoc approach
activities to continue unimpeded in all weather to either type of system is advisable.
conditions. Specifically constructed shelters can also be
• They avoid the complicated operations of repeated designed and created to the exact conditions and
covering and uncovering of excavated areas. planned operations of a site. An effective example
features they are meant to shelter. These can be com- arches from small garden greenhouses with a polyes-
mercially available structures, such as collapsible tents ter tent fabric as the covering to create a tunnel-like
or canopies, which can be easily modified and adapted structure (fig. 6.8). The total dimensions were 1.20 m
to any particular situation. Likewise, these can be long by 0.80 m wide by 0.70 m high. The fabric did
structures designed and fabricated specifically to and not cover the two short ends or the very bottom of the
for a particular set of parameters. long sides so as to prevent it from coming into contact
The following are basic requirements for localized with moist earth or pooled water and from losing its
structures: impermeability through capillary action.
The tent fabric is removable. It is secured to the
• Must be lightweight, self-supporting, adjustable,
frame by a series of Velcro anchor points, making it
noninvasive, easy to assemble and use, and easy to
easy to remove for washing or to be replaced with
remove and disassemble
other fabrics depending on the conditions. Under
• Must be able to be fixed in place without external
intense sunlight exposure, the polyester fabric can be
cords or other types of anchors that can damage
replaced with shading fabrics or used in association
the surrounding archaeological stratigraphy or
with a reflective aluminum-coated fabric textile. The
become an obstacle to further excavation
entire shelter is anchored to the ground by small tent
• Must protect the object(s) in question and the area
stakes rather than external straps or poles. Alterna-
immediately around it from all forms of precipita-
tively, small sandbags can be used to weight against
tion (rain, sleet, snow) and direct sunlight
winds and to keep the structure in place. The low and
• Should not create a microclimate that can prevent
round shape, combined with the open ends, makes it
air flow or create condensation
resistant to wind gusts and prevents the creation of a
• Must not interact with or damage the object(s) it is
hot and humid microclimate.
meant to protect
The total cost of this small shelter was roughly
• Must be made of materials that can withstand sun,
35 Euros, including fabric and Velcro. The individual
wind, and rain and will not easily break under sus-
arches provide adaptability in terms of size to meet
tained or sudden load
space requirements or peculiarities of terrain.
• Must be able to function for short (e.g., emergency)
In principle, a similar type of localized shelter
as well as long-term use
of inclined panels to create a triangular tunnel was
A prototype conforming to the above requirements devised in 1989 to protect medium-sized archaeo-
was built in 1999 by the Department of Cultural Heri- logical finds in the petrified forest of Dunarobba in
tage of Aosta Valley (northwestern Italy) for rescue Umbria, Italy (Piperno 1993). Looking to the horti-
excavations and emergency interventions. The small cultural industry, one sees many possibilities for all
shelter consisted of conventional galvanized steel sorts of adaptable modular structures. In particular,
polypropylene structural elements and polycarbonate the other superimposed materials. The next layer is
paneling show great promise for creating affordable common aluminum foil (fig. 6.9, 2), which acts as a
structures of all possible shapes and sizes. thermal barrier, followed by a 4 to 6 cm layer of moist
soft soil applied over the aluminum foil to act as an
“ c l i m at e wa f e r ” external heat dissipater (fig. 6.9, 3). Another layer of
A “climate wafer” is a multilayered covering intended aluminum foil is added over this (fig. 6.9, 5) to insu-
to be in direct contact with the recovered object to late solar radiation and light and keep the earth moist.
maintain the relative humidity and temperature at the In cases where the artifact or feature must remain
time of its excavation. This type of covering becomes covered for long periods, the insulation properties
essential in the case of very fragile, environmentally of the layered wafer covering can be improved by
sensitive materials like organics, especially those incorporating polystyrene foam or insulating foam
recovered from wet, cool, oxygen-deprived soils that between the moistened earth and outer aluminum
may react adversely to ambient environmental condi- layer (fig. 6.9, 4).
tions (see chaps. 3 and 5). Their use can be essential All these layers can easily be removed together and
in guaranteeing the stability of many object types but reapplied if necessary. When such a system is used,
should generally not be considered for metal finds, the type of material and its condition must be consid-
particularly iron. ered carefully and the thickness of layers adjusted so
Several variations of this type of covering can be that the total weight of the covering and the applica-
created in situ depending on the nature of the arti- tion of the different layers does not cause any type of
fact, its state of preservation, and the logistics and damage to the object.
resources available. Based on reported experiences, a In the case of small to medium-sized waterlogged
general illustration is provided here of a wafer cover- or wet organic finds, a possible variation of the lay-
ing designed by the Department of Cultural Heritage ered “wafer” covering is to replace the initial layer
of the Aosta Valley to allow for gradual drying of inor- of geotextile with a thin film of polyethylene food
ganic remains from very wet environments that other- wrap. This layer can be covered with moistened earth
wise would be subjected to rapid drying and resulting and the entire assembly covered with aluminum foil.
decohesion (fig. 6.9). Such an application could be In other words, the wafer covering is a concept; the
effective on friable ceramics or mortars, such as in a types, numbers, and sequence of layers are adaptable
floor of opus signinum. to the nature of the material to be covered. A word
This wafer-like covering is composed of several of caution: aluminum foil should not be put in direct
superimposed layers, the first a prewetted, heavy- contact with an object or feature without an insulat-
weight geotextile (200 g/m2) placed in direct contact ing material in between (geotextile, damp earth, etc.)
and conformed to the specific shape of the object or because, although it acts as an insulator from the
feature in question (fig. 6.9, 1). The geotextile acts sun, it can conduct the resultant heat directly to
as a protective layer to and physical separator from the artifact.
Stabilization
63
relation to the amount of surface area to be treated, plaster, allowing the conservation treatment of rean-
often making it difficult to undertake within the param- choring by mortar injection to be performed without
eters of a regular excavation season. In cases such as obstacle at any point in the future. After treatment, the
this, shoring provides a temporary means to safeguard support can be removed without any adverse effects to
and preserve the structural integrity of the plaster the archaeological substrate. The only potential down-
while allowing the archaeological and conservation side to such a support is the relatively rapid decay
programs to proceed virtually unobstructed or altered. (about ten months) of polyurethane foams when
One of the techniques that can be used to tempo- exposed continuously to UV rays and oxygen.
rarily support large sections of wall plaster is summa- With a similar approach and any number of mate-
rized in figure 7.1: rials that fulfill the basic requirements of barriers and
space fillers, simple braces or supports can be imple-
• The surface of the archaeological remains is
mented throughout a site for many circumstances,
covered with a thin barrier or isolating layer, such
from shoring up portions of walls at risk of falling to
as aluminum foil or polyethylene plastic food wrap.
supporting smaller features or mobile objects.
• A board also covered and isolated by aluminum foil
or polyethylene plastic food wrap is placed in front
Strapping or Ratcheting
of the section of wall plaster at a distance of about
The technique of strapping or ratcheting is based
2 cm from the feature’s surface.
on holding pieces of an object or feature in place by
• The space or void between the board and the plas-
using adjustable strapping around their exterior as a
ter surface is filled with polyurethane resin com-
form of binding. Once in place, the strap is put in ten-
bined with a foaming agent to cause expansion.
sion, which in turn exerts pressure along its length.
• Any excess polyurethane foam from the edges is
The strap thus serves to contain and immobilize any
trimmed after expansion and curing.
exfoliating fragments or large sections that have com-
This type of support has no chemical interaction pletely separated from the rest of the material body
with the archaeological material and effectively sup- (figs. 7.2, 7.3). Where a single strap is inadequate to
ports the entire surface of the plaster by casting any stabilize the object, two, three, or even more straps
peculiarities, details, or undulations in a lightweight can be employed parallel to or crossing one another to
material (expanded polyurethane). Once in place, the cover more surface area. Equally, if necessary, strap-
support effectively counteracts the force of gravity ping can be combined with rigid lengths of wood or
if braced from behind (fig. 7.1) and immobilizes the piping, as well as panels, placed between the strap and
the feature to act as a form of splint or
structural reinforcement.
Field experience has suggested
that this technique is particularly well
suited and effective for cylindrical,
square, and rectangular materials of all
scales. Ratcheting can also be used to
stabilize small to medium-sized por-
tions of composite masonry or remain-
ing earthen features, as long as it is
possible to completely encircle the fea-
ture and an appropriately shaped pan-
eling can be added as reinforcement
(see fig. 7.2). In other cases, ratcheting
can be used with or without boards to
help in block-lifting operations.
The main advantage of strapping
systems is that they are an inexpensive,
quick, and reversible form of support
that does not involve the use of special-
ized equipment, techniques, or person-
nel. Their use can stabilize a situation
Figure 7.1 Section diagram of a support for wall plaster. that otherwise would result in gradual
Facing
The facing technique uses small sections of permeable
natural fabric, usually cotton gauze (gauze strips or
pads typically found in stores or pharmacies are well
suited) or Japanese tissue, applied to the surface of the
object in question with a reversible acrylic resin (e.g.,
Paraloid® B-72 in acetone solution 20% weight/vol-
ume [w/v]) or an acrylic emulsion or dispersion (e.g.,
Primal® AC 33 at 5% volume/volume [v/v]) (fig. 7.6).
The size of the gauze or tissue strips or sheets and the
type and concentration of acrylic resin depend on the
size, material, and specific condition of the artifact.
For example, large stone fragments or crumbling wall Figure 7.6 Cotton medical gauze and acrylic emulsion
plaster may require large strips and a high percentage used to fix portions of a human skeleton to the terracotta
solution of acrylic resin for stability (fig. 7.7), while support slab with which it was found.
loose tesserae on a mosaic or exfoliating flakes of
ceramic may require a thinner acrylic solution with
small gauze strips to hold them in place.
In some instances, such as with mosaics or portions of reconstruction. For this reason, preference should
of wall plaster, the loose or separating portions can be be given to weaker and more chemically reversible
removed and temporarily stored and later rejoined in resins, mainly those that can be softened or dissolved
situ. Of course this should be considered only if there with a common solvent such as acetone or alcohol.
is accurate and extensive graphic and photographic Some resins commonly used in conservation and
documentation. Consolidation and/or edging with appropriate for use in the field are single-component
an appropriate material may also be an alternative to resins: cellulose nitrate based (UHU yellow tube,
stabilization with a facing but will depend on the time UHU ART blue tube, HMG) and vinylchloro/ketone
and conditions available as this method can be more copolymers (UNIMAST red tube). These are easily
labor-intensive and entail ethical concerns. available and simple-to-use manufactured resins that
commonly come in 25, 50, and 100 mg tubes with
Adhesives applicator tips. When any form of resin is used to
Adhesives can be used only for very specific cases and temporarily secure fragments, it is preferable to apply
on a localized scale, such as for chips or small frag- small droplets in a few points rather than cover the
ments that are easier to reattach to their point of ori- entire join surface.
gin than to fix using other mechanical interventions Aside from these commercially available resins, the
such as facings. In such cases, the objective is not to acrylic adhesives common to conservation are a very
reassemble something from its constituent fragments good alternative. The best known of these is Paraloid®
but rather to avoid the loss of connection between B-72, a methyl methacrylate. These can be dissolved in
small fragments or, in extreme examples, the complete different solvents to varying concentrations according
loss of a feature. Reattachment must be exclusively a to the situation. A common solution would be around
preventive measure and not cross over into the realm 30% w/v in acetone (see Appendix 4).
Figure 7.7 Cotton canvas and acrylic solution used to stabilize the edge of a highly fragmentary stone stele. Note
the absorbing cushions inserted into the larger cracks to allow for the slight movement of the individual fragments
while holding them in place.
It is preferable to not use vinyl-based resins. This is bond between the detached feature and its structural
true unless the conditions of recovery are extremely support. Using lime mortars can establish a sufficient
adverse, such as waterlogged or very damp finds. In bond between the two within relatively few hours. In
these cases commercially available wood glues should cases of extreme emergency or where the structural
be avoided, and commercially prepared conservation support and feature are fairly damp, hydraulic lime
resins (e.g., Mowilith DMC2 in solution or emul- mortar mixtures can be used that will create sufficient
sion) or specially prepared vinyl resins (e.g., polyvinyl adhesion in roughly twenty minutes.
acetate or polyvinyl alcohol dissolved in denatured When working in the vertical, where the weight
alcohol) should be used instead. of the injected mortar can be the cause of detach-
Bicomponent, or two-part, resins such as epox- ment, this form of intervention usually involves
ies (Araldite) or polyesters (Sintolit) should only be having to also create some form of external sup-
employed by conservation professionals. port, whether structural or mechanical. These
Finally, cyanoacrylate (Superglue, Loctite, Cyanolit, external supports, whether a facing or a bracing,
etc.) should be avoided at all costs. must remain in place only for the amount of time
necessary to reestablish adhesion. Typically such
Grouting supports are made with braces of wood with a foam
Grouting is typically used on detaching wall plaster insulator and aluminum foil as a barrier layer. How-
or on mosaics or other floors where lime-based ever, any suitable material can be employed because
mortars were used as the original bedding material. the brief time of use creates little risk of biological
If the situation calls for this type of intervention, such growth or condensation.
as large undulations on wall plaster or sizable voids
or hollows under floors, then certainly the treatment Temporary Infilling and Edging
should be undertaken. Mortar injections make use During ongoing excavations, it may be necessary
of watery lime-based mortars with hydraulic addi- to use temporary infilling and edging repairs for a
tives, such as volcanic sand or pumice, to re-create a number of reasons, such as to prevent the leaking of
injected mortar from the borders and cracks of treated In very wet conditions where the setting of lime
wall plasters or to stabilize edges of wall plasters or would be virtually impossible and hydraulic lime
mosaics or other floor materials (edging). It should be mixtures would prove too strong and too hard to be
taken into account that protective edging will eventu- considered temporary, wet clay can be used instead.
ally be removed, and this action should not jeopar- Here, clay is simply pressed and molded into edges or
dize or damage the original archaeological material. gaps as a support. Equally, this technique can be used
Accordingly, a sufficient amount of adhesion must be to secure the borders of mosaics or to immobilize tes-
endowed without being too weak or too strong. This serae in instances where the inherent moisture in the
is typically done by using a so-called lean mortar mix- mosaic would preclude the use of any form of acrylic
ture of 1 part lime to 3 parts volcanic sand or pumice. resins to affix a facing or adhere any small fragments
Color should also be considered; ideally the mixture in place (see above). Clay used in this way has excel-
should be given a color that is different enough from lent elasticity and dimensional stability, provided that
the archaeological material to be discernible as new by it remains moist. If allowed to dry, the clay will lose
the public and by archaeologists and conservators at a volume and become brittle, effectively defeating its
later time. function as a mechanical support.
Indirect Methods
The relationship between the environment and bio-
logical growth makes it clear that the most effective
indirect conservation techniques target the ambient
factors that allow and encourage such growth. These
factors are:
• High relative humidity
• High temperatures
• Poor ventilation
• Sufficient natural light
• Dust, dirt, and grime on the archaeological
material
Figure 8.2 After the plant has been killed. The removal or rot-
ting of the roots can still cause serious damage to the masonry Of these factors, relative humidity and temperature
and may lead to its collapse. have the greatest impact. If the relative humidity is too
high, the following actions may alleviate the problem:
For details, see the diagram shown in figure 8.3. • Isolate the feature or object from capillary action.
Direct treatment can take many different forms: • Create drainage around the areas of excavation.
Mechanical: Removal of early biological growth by • Do not allow water to pool or stand.
hand and with tools. This technique does not remove • Allow for or create ventilation.
all the possible seeds or spores and thus has limited High temperatures promote the growth of microor-
effectiveness over time. ganisms, as well as the reproduction of insects (espe-
Physical: Various physical techniques such as expo- cially at or above 15–16°C). Another possible effect of
sure to UV light, gamma rays, ultrasonic waves, low- high relative humidity and temperatures is condensa-
frequency current, and cold show good experimental tion and the wetting of the objects or features at night
results. Unfortunately, all such methods prove harmful when cooler temperatures prevail. This is especially
to the original archaeological material. true for more conductive materials like some kinds of
Biological: This method is based on using a species stone or metals.
antagonistic to or competitive with the undesired bio-
logical growth. This can be highly effective but carries
the risk of replacing one biological agent with another. Treatment Strategies
Chemical: Currently this is the most widely used Treatment approaches are most easily arrived at by
form of direct treatment in that chemistry offers an systematically answering a series of appropriate ques-
unlimited number of possibilities and continually tions. The sequence of questions was well summarized
developing products. Among chemical treatment by Caneva, Nugari, and Salvadori in 1991 and is the
Is treatment necessary?
Is deterioration consistent? NO
YES
Undertake
Are pretreatment measures necessary preliminary
YES
prior to treatment? treatments
NO
Undertake
Can preventive measures preventive
be taken? YES
measures
NO
basis for figure 8.3. The following sections attempt to can be confused with a sulfate crust caused by atmo-
expand on the possibilities for treatment by consider- spheric pollution on limestone or marble surfaces.
ing the many pertinent variables affecting decision To help in identifying the presence of biological
making, as well as the many possible approaches. attack, it is useful to understand that such activities:
• Are usually associated with moisture
Recognizing Biodeterioration • Produce moisture themselves, typically in the form
One of the primary problems one first encounters is of microscopic droplets
recognizing biological attack. It is usually fairly easy to • May vary in color, depending on whether they are
discern plant species or mosses, but algae or bacteria active or dormant, such as green to red to brown
can be easily misinterpreted as a chemical attack,
soluble salts, or earthen particulates. This is particu- Identifying the Type of Biological Attack
larly true for inorganic archaeological materials; for The only truly reliable way to identify the specific
example, bacteria can produce a black encrustation that type of microorganic growth is by in vitro cultures
analyzed by a specialized laboratory. These obviously the microbial population absorbs and assimilates
entail a cost and a time delay in allowing the culture to the biocide, stops growing, and then succumbs.
develop and be interpreted but can provide informa- It is difficult to give a precise duration for this
tion on the specific strain and genus and accordingly phase as it is influenced by various factors (relative
the most appropriate biocide to deal with it. humidity, type of biological growth, life cycle stage,
etc.), but it generally will last between one and
Practical Considerations three weeks.
It is beyond the scope of most excavations in terms of • After this period there will be a quantity of decay-
time and budget to scientifically identify the specific ing organic matter that can become the food source
type of biological attack that may be present. Conse- for the development of biological species that were
quently, to achieve and exercise reasonable control resistant to the biocide used. These species now
over biological growth, the following practical steps find themselves in a virtually ideal environment
should be seen as a priority and should not depend on without natural competitors, where the biocide
the outcome of any form of analysis: has been predominantly metabolized by the dying
organisms and with abundant nutrients for further
• Remove soil, dust, and particulate accumulation growth provided by those same dying organisms.
from archaeological remains that can encourage • The development of biological growth will be
biological growth. localized at this point to areas with a favorable
• Prevent or limit the supply of water to the remains, microclimate and sufficient nutrients.
whether in the form of rain, rising damp, or
condensation. At this stage sampling of any new growth is recom-
• Limit, if possible, the amount of light and new mended to determine the specific species by in vitro
seeds or spores reaching the remains by means of culture. Identification of the species should help in the
shelters or coverings. selection of the appropriate biocide to eliminate all
• Check any biocides that may be used for their com- forms of remaining biological growth.
patibility with the material of the archaeological It should be emphasized again that if the conditions
remains. of relative humidity, temperature, and light are not
• Plan for periodic maintenance and survey of the altered in some way, new growth will begin at some
remains and the efficacy of treatment to determine point because the factors that determine growth have
if some steps need to be repeated or new ones not been changed. If these environmental parameters
implemented. cannot be altered (see chap. 16 on long-term
conservation), then a sustained program of periodic
With regard to selecting a chemical biocide, the cri- biocide application should be planned.
teria for selection have been thoroughly discussed in
numerous publications found in the bibliography and
are discussed below, under “Biocides.” Biocides
Bactericides, Fungicides, Algaecides
Treatment Steps
organic compounds
Because the identification of specific species of bio-
Hydrogen peroxide: Used in its highest concentrations
logical growth is difficult in terms of costs and too
to suppress algae and lichens on the surface of stone.
time-consuming for most ongoing excavations, it does
This is a strong oxidizer and can bleach or lighten the
not make sense to treat with one or many specifically
surface of the treated material, so much care must
formulated biocides that may not be effective because
be taken in its application. It is effective only when
they do not target the growth in question. Instead a
applied directly to the algae or lichen and its action
broad-spectrum treatment is usually considered the
does not last over time.
best option to try to eliminate as many common spe-
Sodium hypochlorite (bleach): Used in aque-
cies as possible. One drawback of this approach is
ous solutions (between 2% and 7%) to eliminate
that it may not overcome resistant species that could
algae and lichens on stone surfaces. This may cause
be eliminated by a specific biocide. Accordingly, this
whitening or bleaching of the surface of the treated
approach can only be considered a short-term solu-
material. Moreover, if not completely removed from
tion, but it does present the following advantages:
the stone surface after use, it can cause yellowing.
• After the application of broad-spectrum biocide Sodium hypochlorite is corrosive to skin and can
there will be a period of quiescence during which lead to sensitization and allergies.
o r g a n o m e ta l l i c c o m p o u n d s mixtures
Mercury derivatives: These were widely used in the Sodium dimethyl dithiocarbamate + sodium
1980s, especially pyridyl mercury acetate, but are now 2-mercaptobenzothiazole (Vancide 51, Vanderbilt) has
generally avoided because of their toxicity. been used successfully on stone, plaster, and painted
Tin derivatives: Tri-n-butyl tin (TBTO, Merck; surfaces for the treatment of algae, bacteria, and fungi.
Thaltox, Wykamol) is an effective algaecide and fun- Tributilene naphthenate + quarternary ammonium
gicide. It has been used with good results on stone salts (Metatin N 58-10/101, Acima Chemical) has
and mural paintings, as well as on wood, where it is proven effective against biodeterioration in subterra-
highly effective against so-called red fungi. Another nean environments.
tin derivative of similar efficacy is tri-n-butyl
tin-naphthenate (Metatin 58-10, Acima Chemical). Insecticides
Most insecticides are very toxic to all forms of life,
phenolic compounds
humans included. Halogen derivatives have been
Phenol is one of the oldest disinfectants known and is found to be generally effective, but they can be dan-
used as a measure of the effectiveness of other disin- gerous to handle and apply. Chlorinated organic com-
fectants. It was widely used in the past but is now sus- pound mixtures are dangerous as well because they
pected of being potentially carcinogenic. It is corrosive accumulate in the food chain.
to metals. Pyrethrin and the pyrethroids are the only known
Penta-chlorophenol (PCP) (Dowicide EC7, Dow products commonly used as an insecticide without
Chemicals) and its sodium salt, sodium penta- known risks to humans.
chlorophenol (PCPNa) (Dowicide G, Dow Chemicals),
Herbicides
were widely used in the past because of their broad-
The control of larger plant growth, such as weeds,
spectrum effectiveness. They are now generally con-
vines, and trees, can be achieved only with products
sidered too toxic for use. They can interact negatively
that interfere with photosynthesis. Such substances
with certain material substrates, darkening wood or
can also be effective against algae. All herbicides are
discoloring and altering basic pigments.
classified as one of two types:
Ortho-phenyl phenol (OPP) (Dowicide 1, Dow
Chemicals; Topane S, ICI) and its sodium salt, • Selective, active on only very specific forms of plant
sodium ortho-phenyl phenol (OPPNa) (Dowicide A, development
Dow Chemicals; Topane WS, ICI; Mystox WFA, • Nonselective, preventing any form of plant growth
Catomance), are highly effective on a broad range
Treatment of architectural remains and features
of algae, fungi, and bacteria. Their toxicity is toler-
usually includes the application of a nonselective
able, with OPP being preferred for use because it
herbicide to prevent any form of large plant growth.
seems to interact less with most material substrates.
These should not be used on textiles or other col- The most commonly used herbicides tend to be nitro-
ored fabrics because they can produce immediate organic in nature:
discoloration. • Ammonium sulfate (Ammate, Du Pont) is
Di-chlorofene (Panacide, BDH). This is a good locally applied to the roots of trees to halt their
product with broad-spectrum effectiveness and very development.
low toxicity. It is commonly used as a disinfectant for • Fluometron (Lito 3, Ciba Geigy) is used against
paper-based food packaging and has little to no nega- mosses and lichens; Monuron and Diuron are used
tive interaction with material substrates, including against the most common weeds and vines that
organic ones. grow on large architectural remains.
Quaternary ammonium and its derivatives • Simazine (Gesatop, Weedex, Ciba Geigy) is widely
(Preventol R50, R80, R90, Bayer; Hynamine 3500, used to prevent the growth of most common weeds
Rohm & Haas; Cequartyl, Rhone Poulenc; Neo and plants, as well as lichens and mosses on archae-
Desogen, Ciba Geigy) are widely used in medicine ological sites.
against bacteria, algae, and fungi (i.e., sterilization • Picloram (Tordon, Dow Chemicals; Uniran, Ciba
of needles and operating rooms). Their effective- Geigy) is a powerful nonselective herbicide used
ness against lichens is debatable. Their effectiveness for total control of any form of vegetation and
is very short-lived because they are unable to kill therefore should be used with extreme caution to
spores. The presence of nitrates can significantly prevent polluting waterways or groundwater and to
reduce their effectiveness. prevent serious environmental harm.
• Imazapyr (Arsenal, Cyanamid) is a recently devel- Enzymes are proteins that act as catalysts for
oped product, especially for root injection, that biochemical reactions within cells. Enzymes have
has been used successfully to control larger plant been used as a biochemical treatment in various
growth. applications, particularly for cleaning stone (Gauri
• Glyphosate (Roundup, Monsanto; Spasor, Siapa; and Chowdury, in AA.VV. 1988). Trypsine, a type of
Pathox, Phase) has been used with success on enzyme, was used to remove lichen-formed encrusta-
lichens and larger plants and has no residual effect tion from the surface of stone. Given its brevity of
once absorbed by the plant(s). effectiveness, greatly influenced by pH and tempera-
ture, its application is too complicated to consider it a
general and recommendable treatment.
Biochemical Methods Pheromones are chemical compounds produced
Biochemical treatments make use of chemical com- by living creatures that have a specific action on other
pounds of biological origin that cannot intrinsically individuals of the same species. Sexual pheromones
be considered biocides. Antibiotics, for example, are have been used to control insect infestations in muse-
substances that are produced from microorganisms ums. These cannot in the strictest sense be considered
and developed to eliminate the growth of competing biocides because they function by luring male spe-
organisms. Streptomycin and penicillin have been cies from infested materials and attracting them into
used to control the growth of bacteria, fungi, and acti- traps, where they are then killed by a specially selected
nomycetes on wall plaster and stone surfaces. insecticide.
Consolidation
77
two organic resins most commonly used in conserva- somewhat controversial, although deserving of note.
tion, acrylics and vinyls. Acrylic resins have many In general, consolidation with calcium hydroxide can
significant positive characteristics: be used for slightly degenerated wall plaster or floor-
ings located in covered locations or exposed to limited
• Good resistance to UV rays, that is, little to no thermal changes (i.e., avoiding severe cold or heat)
yellowing or color change and, above all, away from direct moisture and freeze/
• Good dimensional stability under a range of tem- thaw cycles.
peratures, both low and high Barium hydroxide (Ba(OH)2): Consolidation with
• Good elasticity and resistance to bending and barium was first tested and developed by the Opificio
creep, especially the ethyl-methacrylates delle Pietre Dure (OPD) and S. Lewin (Ferroni and
• Long-term solubility, allowing for future or Dini 1981). The basis of the technique is the chemi-
alternative treatment options over a long period cal reaction between Ba(OH)2 and calcium sulfate
Vinyl resins are very good universal and house- (CaSO4) present in lime-based degraded mortars and
hold resins but tend to be almost too strong for stones. The reaction produces barium sulfate (BaSO4),
common conservation uses and have many negative an insoluble salt that takes the place of the degraded
characteristics: calcareous binder within the mortar or stone. This
method has notable advantages for light-colored mate-
• Age and discolor quickly, becoming grayish rials and for painted wall plasters or true fresco paint-
• Cross-link and slightly insoluble over time ings. Despite the sometimes overenthusiastic literature,
• Viscous in emulsion form, which can limit the however, there are some potential drawbacks to the
amount of penetration use of barium hydroxide in that it may have a negative
Accordingly, of the common resins used as consoli- reaction with basic pH pigments and could blanch or
dants, preference should always be given to acrylics. whiten darker materials and stones. The application
of barium hydroxide is very sensitive and requires
controlled, precise execution. The advantages of this
i m p r e g n at i o n w i t h i n o r g a n i c m at e r i a l s method are related directly to the amount of mineral
Inorganic compounds are molecules comprising the binder present in the material to be consolidated and
mineral elements silicon (Si), calcium (Ca), and barium its conversion from something highly soluble, CaSO4,
(Ba) and their derivatives. As consolidants, they are to something insoluble, BaSO4. Therefore, aside from
similarly dependent on a liquid solution penetrating consolidation, there is a chemical conversion and neu-
into the pores of the material to be consolidated by cap- tralization of any gypsum present in a material.
illary action. Likewise, the solvent vehicle carrying the Ethyl silicate (ethyl silicon esters): Ethyl silicate com-
inorganic compound evaporates, precipitating the min- pounds are made up of a silicon atom bonded to an
eral component and beginning the formation of a crys- ethyl molecule diluted in organic solvents, generally
talline network that binds to all surrounding minerals methyl ethyl ketone (MEK). There are also commer-
present in the original material. Unlike with organic cially available methyl silicates (a silicon atom bonded
consolidants, however, the type of bond that is formed to a methyl molecule), widely used in Austria but
between the consolidant and the material to be consoli- generally not recommended because of their toxicity
dated is a mineral one with physicochemical properties and tendency to attack the optic nerve. Ethyl silicates
analogous but typically not identical to the original with added polysilanes to give hydrophobicity are
material binder that has been lost or diminished. also commercially available. In whatever form, the
Following are the primary inorganic consolidants extreme fluidity, low viscosity, and slow evaporation
used for cohesive consolidation: rate of ethyl silicates allow for deep penetration into
Calcium hydroxide (Ca(OH)2) or slaked lime: Sev- porous materials. The initial evaporation of the ketone
eral experiments have been undertaken with saturated and eventually of the ethyl alcohol solvents leads to
solutions of calcium hydroxide, also known as “lime the precipitation of amorphous silica in the capillar-
water” (Rossi-Manaresi and Tucci 1984). The applica- ies of the material being treated. The silica then forms
tion of calcium hydroxide should begin a reaction covalent (very strong and stable molecular) bonds
of carbonization (see Appendix 3, reaction no. 3) on with surrounding precipitated silica atoms (Si-Si). The
the interior of limestones or mortars, reconstituting depth of penetration and stability and the strength of
the lost or deteriorated original calcium carbonate the formed silica-to-silica bond are the primary rea-
(CaCO3) binder. The results of these experiments are sons ethyl silicates have become widely used.
There are certain disadvantages: injection material is the orientation of the void to be
treated, whether vertical or horizontal.
• Application dependent on temperature and relative
In the first case, such as with partially detached
humidity
wall plaster, gravity will pull all injected mixtures
• Risk of creating a white or glossy film if excess
downward to accumulate in the lower portion of the
product is used and not removed from the surface
cavity. If injections are not done carefully or gradually,
of the treated object before polymerization
the weight of accumulation can cause further detach-
• Slow reaction time (typically about one month)
ment and/or possible fracture or loss of the wall plas-
• Theoretically impossible treatment in the absence
ter under treatment. In such cases, external supports,
of silica in the treated material, such as with pure
reinforcements, and preliminary sealing of the edges
limestones or marbles
can all be used to give the plaster sufficient strength
• Transformation of the chemical behavior of lime-
and cohesion to sustain the weight of the mixture,
stone from basic to acidic
as well as prevent any unwanted leaks. In the case of
• Possibility that the silica bonds can create excessive
injections for horizontal gaps or cavities, such as for
tension in thin clay materials or ones already weak
pavements, the problem of accumulation is not a fac-
and cracked or fissured
tor. Instead, one must consider the potential collapse
Impregnation with ethyl silicates is therefore of the material directly over and/or around the perim-
advisable if: eter of the cavity or void. For this reason, many hori-
• The material to be treated contains silicon zontal injections are of “expansive” mixtures, which
• The porosity of the material guarantees absorption will be described later.
• Temperature and humidity can be partially The need for and implementation of adhesive con-
controlled during treatment and polymerization solidation or reanchoring must be evaluated carefully,
(between 5° and 25°C and between 40 and with consideration of the following factors:
80% RH) • Quantity: The quantity of consolidant to be
Impregnation with ethyl silicates should be injected. Can the material to be readhered support
avoided if: the stress and weight of the injected material? If
the answer is no, staggered injections over time,
• The material to be treated does not contain silicon preliminary cohesive consolidation, or detachment
• The material is not sufficiently porous or absorbent should be considered.
• The temperature is too high (above 25°C) or too • Solubility: Resistance to and solubility in water.
low (below 5°C) Nearly all injection materials used for adhesive
• The relative humidity is above 80% or if the treated consolidation contain some amount of water. Can
material may be exposed to rain in the four weeks the material itself or any components applied to
following treatment the material (e.g., pigments on painted wall plaster)
To slow the evaporation rate of the solvents and ethyl support exposure to water? If the answer is no, pre-
alcohol, it is good practice to cover or wrap the treated liminary cohesive consolidation with a nonaque-
object with aluminum foil or polyethylene sheets for ous consolidant or possible detachment should be
at least two weeks after application. considered.
• Timing: The amount of treatment time needed.
Adhesive Consolidation (Injection) Is the time needed to properly undertake
The filling of cracks, gaps, voids, or cavities between injection and reanchoring of an architectural
structural elements (walls and floors) and their element compatible with the time constraints
coverings (wall plasters and floorings) to re-create of the excavation? If the answer is no, cohesive
structural continuity is a common conservation treat- consolidation and detachment should be
ment on archaeological sites. In all cases, the size and considered. (The problems inherent in detachment
volume of the gap or hollow must be determined in are discussed in chapter 10.)
order to choose which type of injection material will
Following are the primary materials used in injec-
be most effective. Large gaps or cavities are generally
tion and their forms of application:
filled with denser, more thixotropic mixtures with
Lime mortar and sand aggregate: One of the easiest
fine inert aggregates; small cavities and cracks call for
materials to inject and use on both vertical and hori-
more fluid mixtures with even finer inert additives.
zontal gaps and cavities is a standard mortar of lime,
A further generalization to determine the type of
fine sand aggregate, and water to achieve the appropri-
ate fluidity. This type of injection must be done more used widely in the past thirty years due to their easy
than once to compensate for the loss of total volume availability and preparation (dilution with water). As
of the mortar due to the evaporation of the excess previously noted, acrylic resins have many favorable
water needed for fluidity. The overall strength of characteristics, including good chemical and color
this mortar is quite low, so this material and method stability, elasticity, and high resistance to tensile and
should be considered a general filler for voids. shear forces.
In the case of large voids or gaps, aluminum pow- To this list of positives we must add some draw-
der can be added to the lime mortar and sand mixture backs to the use of acrylics in emulsion form:
to create an expansive mortar during setting. Alumi-
• Impermeable to water vapor
num in contact with lime causes the formation of gas,
• Different coefficient of expansion and contraction
which endows a honeycomb or cell-like structure on
as compared to those of the mineral components of
the mortar, causing it to expand in volume. Though
many archaeological materials, potentially causing
this is useful, it must be kept in mind that the action
some stresses between the two (organic/inorganic)
of the gas creates voids in the mortar, which serve to
due to environmental issues, especially temperature
further reduce its overall strength. In addition, as with
change
all fine particles, when using aluminum powder cau-
• Formation of a hydrophobic barrier that can
tion must be taken to avoid irritation or damage to
complicate or exclude any future conservation
one’s respiratory system.
treatments with the same emulsion or with a lime-
Lime mortar with volcanic (pozzolanic) sand aggre-
based mortar
gate: Combining lime with a volcanic sand aggregate
is one of the surest techniques for achieving a strong For these reasons, adhesive consolidation by injecting
adhesive fill material. Crushed brick, grog, or volca- acrylic emulsions should be avoided. It should be used
nic sands confer hydraulic properties to lime mortar, only as a treatment of last resort or in an emergency
which allows its use on wet materials, such as damp (see below) and should never be considered a perma-
walls, or in very moist or high relative humidity envi- nent solution.
ronments, such as inside enclosures. The set mortar
has very good mechanical properties and resistance to
liquid moisture while remaining permeable to water Consolidation and Stabilization
vapor. These properties allow these lime mortars to be of Stratigraphy
used in a wide range of common archaeological situa-
tions where walls and floors or their decorative cover- One of the most common and problematic treatments
ings will remain in situ. a conservator faces on archaeological sites is the con-
Casein and lime: Casein and lime, one of the old- servation of stratigraphy. The nature of stratigraphy
est known traditional adhesives, can be used to fill is intrinsically complex in that layers are sufficiently
small cavities. This mixture is produced by combin- different in composition and compaction properties
ing lactic casein (a protein) and lime in the volumet- to be distinguishable from one another. This, in turn,
ric ratio of 1:7 (casein to lime). In recent decades is what makes consolidation problematic: each mate-
this technique has unjustly fallen into disfavor due rial within each layer has its own problems, needs, and
to the misconception that because casein is organic porosity.
it is sensitive to attack by mold and microbiologi- To approach the issue systematically, the following
cal growth. This simply cannot be true given the questions should be addressed prior to treatment:
numerous examples of pictorial murals throughout • Does the profile of the stratigraphy allow for
Europe that have historically been treated with this consolidation?
technique and are currently in a very good state of • How wet or dry are the layers, individually and
preservation. collectively?
Once set, casein and lime does not have great ten- • Do all layers require consolidation or only selected
sile strength, but it is still a commendable material ones?
for vertical and horizontal injections into voids that • What are the properties of the layers to be
do not exceed 3 to 4 mm and where good adhesion consolidated?
is important. Casein and lime remains permeable to • Are organic materials present (bone, wood, etc.)?
water vapor after setting.
Acrylic emulsions: Acrylic emulsions (Primal®, Each of these questions is developed below as a gen-
Plextol, Acronal, Lascaux Hydrogrund) have been eral guide.
83
Basic Principles of Detachment row of facing can then be applied along the short side,
Detachment usually begins with the adhesion of a thus avoiding irregular alignments that could poten-
strong support, or facing, to the surface of the decora- tially cause undue stress concentrations along any one
tive covering. The facing serves as a structural and line of overlap.
cohesive support of the decorative surface, allowing Facing should begin from the bottom. Starting
mechanical force to be applied to the architectural from the top inevitably results in streaks and drops
sublayers or support layers: underlayers, or arriccio, of adhesive accumulating at the lower portion of the
for frecoes and wall plaster; bedding mortar for mosa- surface to be detached. These in turn can create exces-
ics. The mechanical force can take several forms and sive localized tension, which can pull a pigmented or a
is what ultimately will separate or detach these layers fragile surface or, most likely, become an impediment
from their architectural setting. The amount of force to proper facing of these areas by creating an elevated
required to cause detachment can vary greatly from feature that the cloth must conform to, preventing it
one case to the next. The thickness of the detached from lying flat. After drying, this facing is typically
material can also vary significantly and must be evalu- covered by a more substantial layer of fabric, usually
ated and planned for in advance to avoid being left canvas or jute. This layer is often what endows con-
with overly heavy, unmanageable fragments that are solidative strength to the facing, and the weave and
difficult to handle or move. thread count should be proportional to the size/mass
The first step in detachment is the application of a of the surface to be detached. Typically, adhesive is not
suitably weighted (thread count, warp and weft type) applied to a border that extends roughly 15 cm past
fabric, cloth, or gauze with the appropriate adhesive the surface to be detached, creating a strip from which
for the occasion. The type of fabric weave and thread operations can begin.
count should not be too open or too closed and thick It is imperative to wait for the adhesive to fully dry
so as to make it impossible to contact all irregularities before beginning any further steps. Any premature
and features. The idea is to achieve as much contact as tension on an undried adhesive can cause separation
possible by choosing a weave and thickness of mate- of the facing from the surface, with risk of partial loss
rial that will be sturdy and strong, yet flexible enough of the material one is trying to protect, and the need
to adapt to the morphology of the surface. Equally, the to remove any remaining facing and begin all over
type of adhesive to be used should always be revers- again. This precaution applies to any type of adhesive
ible, but its properties should be in direct relation to used. The advantages and disadvantages of animal
the material to be detached. It is advisable to remove glues and acrylic resins, the two most commonly used
from the surface as much obscuring debris that could resin types for detachment, are considered below.
prevent proper adhesion as possible. Degreasing the
surface with a solvent is also good practice. In the past Traditional Detachment Using Animal Glue
vinegar or ox gall was commonly used for this pur- Animal glues are generally defined as adhesives made
pose, and both are still viable alternatives to common from animal skins and ligaments and consisting
solvents if necessary. mainly of collagen. They are typically sold in the form
The cloth or gauze should be composed of natural of solid beads or blocks and under various names. The
fiber, preferably cotton. The presence of polyester or most common formulas consist of animal collagen
other common synthetic fibers in fabrics must be dissolved in water in a double boiler, with 5% ox gall
avoided because they may react with the solvents used as a surfactant, 2% vinegar as a thinning or liquefying
in the process of detachment. It is recommended to agent, and up to 10% molasses, which functions as
first wash the cloth in boiling water to eliminate any a plasticizer to prevent brittleness once the glue
possible traces of starch or starching agents that are has dried.
typically applied to fabrics. These are often vinyl or Animal glues must be applied while very hot to
cellulose based and can also react unpredictably with ensure their fluidity and proper adhesion (usually
solvents that may be used during treatment. around their boiling point, 115°C, or 239°F). This is
The cloth should be laid out flat and ironed if it has the main drawback of the method, particularly if the
wrinkles or folds that could negatively affect surface work has to be done over a large surface area or over-
contact and adhesion. It should then be cut into strips hang, such as an archway or a vault.
roughly 20 × 30 cm. A rectangular shape is preferable
to a square because the long side can be used as a line Advantages:
of orientation and the starting point for resin applica- • Inexpensive and readily available
tion and adhesion, with successive strips overlapping • Very strong, yet slightly flexible bond
by about 1 cm. Proceeding in this manner, the next • No toxic vapors (apart from the smell)
ing techniques with acrylic resins or animal glues. Mosaic floors are far less susceptible than opus signi-
Decorative floorings vary to a much greater extent in num to damage from movement because the space
their nature and composition and by extension the between tesserae acts as an elastic join that can allow
logistics of their detachment. For this reason, they are for some tension or compression. Equally, the more
the focus of this section. uniform size of tesserae (generally no larger than
1 cm) typically translates to a thinner layer of mortar
opus signinum floors into which they are set, which is itself typically nonhy-
The materials used to create opus signinum floors are draulic and thus less tenaciously bonded to the lower
generally analogous to those used for making mosa- bedding mortar. All these factors combine to make
ics. The major difference between the two floor types mosaics more manageable to remove; the weight of a
detached square meter should be somewhere between eventually have to be relaid in situ, a suitable support
15 and 30 kilos. must be provided for and any form of foot traffic
Detaching a mosaic surface by dividing it into avoided.
sections to be lifted is generally not a problem
because the necessary cuts can be confined to the Transport and Storage of Detached Features
mortar between tesserae and can often follow the Whether originating from a wall or a floor, the applied
borders of different geometric elements. If rejoined, facing constitutes a solid yet flexible mechanical and
rebacked, or relaid, a mosaic that has been lifted in chemical support to the detached decorative surface.
sections can feasibly be reunited with virtually no Even with this support, certain precautions should be
trace of having been divided into pieces. For this taken during transportation and storage:
reason, the sectioning of a mosaic, if approached
prudently, can be performed safely and with every • Any type of flexing or bending should be avoided,
expectation of success. and a rigid support such as wooden planks should
In some instances, a so-called rolling technique has be used during handling or transit.
been preferred to sectional lifting. The concept is the • Bending or flexing is particularly damaging if it
same: a facing is adhered to the mosaic surface and occurs near portions of the surface that have not
then cut from below at the point between mortar lay- been faced, such as the borders. If bending or flex-
ers. With this technique, however, rather than being ing is unavoidable during handling or transport, it
lifted in smaller, manageable sections, the entire floor is is best if limited to or concentrated in the area that
faced and one end of the facing attached to a large tube is reinforced with facing.
along its length and the mosaic progressively pulled • If stacking of removed elements is necessary at any
onto this tube as the weaker bond line between the point during transport or storage, space of at least
bedding planes is exploited. This approach has been 10 cm should be provided between the layers with
used when a mosaic is in relatively good condition a suitable substance, such as extruded polystyrene
and is to be relaid in situ with a new bedding mortar foam or even polyurethane foam. Foam rubber
to provide better support and adhesion. In these situa- should be avoided because of its tendency to com-
tions the integrity of the floor as a whole is preserved. press and deform under weight and trap moisture,
This is an inappropriate technique, however, for mosa- which can encourage biological attack.
ics that have any degree of settlement or large cracks. • Good air circulation is a must for stacked sections
In addition, a major drawback, aside from the need but is generally a good practice for storage.
for specialized equipment, is that a rolled mosaic is • The resins or adhesives used in conjunction with
extremely heavy and unwieldy, making it hard to move textile to make a facing tend to harden over time.
and store. These problems are compounded if re-laying Accordingly, stacked sections should be placed on
is not planned to proceed quickly after detachment. flat supports so as not to create any deformations
or distortions that will be rigidly held once the
b e at e n o r p o u r e d l i m e m o r ta r f l o o r s resin becomes less flexible.
Beaten or poured lime mortar floors are often encoun- • Because the resins tend to harden over time, it is
tered on archaeological excavations, as they were often important to remove the facing material as soon as
used in areas inhabited by the poor or commoners. possible to minimize potential problems or dam-
Use of lime mortar was a rudimentary way of making age. By extension, any plans for rebacking of the
a level floor, and it is typically of very poor quality. material should be taken into consideration prior
Despite the lack of decoration or refinement of these to commencing detachment.
floors, it may be important to preserve a portion as
a representative sample for archaeological represen- Movable Objects, Features,
tation or analysis. Because these floors were purely
functional and rarely intended to be permanent, their or Materials
state of preservation is often very bad; they are gener- Conservation Issues
ally highly friable and discohesive, with little mechani- Removal, lifting, and detachment should be done
cal strength. as soon and as methodically as possible, taking
If one must remove a section of this type of floor- into consideration the circumstances and param-
ing, consolidation with an ethyl silicate to improve eters of the excavation itself, the specific soil and
mechanical properties is almost obligatory prior environmental conditions, and the condition of the
to detachment. In the event that a section should material(s) to be removed.
According to the principles of preventive conser- fragments from the same object or material that
vation, any material to be lifted should be removed are dispersed over an area with little relation to
as soon as possible, preferably immediately on being their complete original form
unearthed or, as in the case of block lifting, prior to b) Whole or large portions of an object that are
being fully excavated (see “Block Lifting” below). The fragmented or significantly cracked from being
urgency of lifting is due to a number of reasons, not squashed, bent, deformed, or distorted but still
the least of which are the problems that can result constitute a recognizable assemblage that is
from prolonged exposure to environmental factors contained within a small amount of soil
(see chap. 2). No less worrisome is accidental damage (fig. 10.1)
during the ongoing excavation, as from incidentally c) More or less complete objects that may be
bumping, scraping, or even stepping on the material highly fractured or collapsed but remain in an
to be removed. Simple loss or theft of smaller materi- intact and recognizable form due to the adhe-
als that can easily go missing or unnoticed must also sive properties of the soil that surrounds them
not be underestimated. Last, from a practical stand- d) A complex assemblage formed by any combi-
point, lifting operations performed while soil condi- nation of types a, b, and c, such as a skeleton
tions are similar to those at the time of unearthing are with preserved bracelets and various funerary
typically less problematic, as for example on a moist accoutrements
soil that has not gotten wet from rainfall.
For finds of categories 1a and 2a, it is sufficient to
Removal can proceed quite rapidly during or imme-
use standard recovery practices (see “Lifting” below).
diately after excavation for multiple fragments or small
For objects or materials related to categories 1b and
materials that can be lifted as a collection (see “Lifting”
1c and 2b and 2c, more specialized lifting techniques
below). The same cannot be said for more fragile, com-
may be required (see “Block Lifting” below). For those
plex, or larger fragments or materials, or those that are
finds of a more complex or composite nature that
important to the stratigraphical context of the excava-
would fall into categories 1d and 2d or simply 3, it is
tion. While a delayed or slower intervention is often
generally advisable to consult or involve specialized
preferable from an archaeological perspective, it is not
conservators.
ideal from a conservation point of view. When removal
of objects or features is not considered or planned for,
Lifting
it will be left to the whim of excavators, who may not
Small fragments or objects can physically detach from
be fully aware of the conservation issues or associated
their surrounding soil due to the contraction of the
consequences. Lifting should always be done as soon
soil during drying. Barring this possibility, such mate-
as feasible, especially as regards fragile, deteriorated, or
rials should be lifted by carefully removing the sur-
chemically and physically unstable objects or materials.
rounding soil with fine tools, avoiding touching their
More difficult lifting operations should be performed
surface directly, or by using suitably soft implements
by a conservator or at the very least with a conserva-
on the material itself that will not abrade or scratch
tor’s consultation and guidance.
its surface (see chap. 4). An acceptable compromise
Object or Material Characteristics
For conventional reasons objects and materials can be
divided into three main categories based on their rela-
tive size:
1. Small objects or materials: seeds, glass beads, coins,
fibulae or brooches, bracelets, ointment containers
(Barker 1981)
2. Medium-sized objects or materials: cups, plates,
bricks
3. Large remains or materials: portions of floors or
walls or ceilings, columns, beams
Small and medium-sized objects can typically be
Figure 10.1 Highly fragmentary glass object incorporated
found in the following combinations:
into a mass of soil with which it forms a singular block (see
a) Fragments or solitary pieces that are basically category 1b) that was lifted without an external support.
intact but scattered on the ground or groups of
Table 10.1 Traditional Materials for Stabilizing and Containing Archaeological Materials prior to Lifting
Type Notes
A Medical bandages in cotton and Need water and will not sufficiently harden in overly humid or damp environments;
gypsum used for making casts require some dexterity and skill to employ properly.
and splints
B Medical bandages in fiberglass Will set in ambient humidity or can be wetted with tepid water; are well suited for
and polyurethane resin for mak- damp, wet environments; are not particularly well suited for small objects or ones
ing casts and splints (such as 3M with elaborate profiles, and are at their most advantageous if they can be used to
Scotchcast) completely envelop a material or object.
C Gypsums Special dental or masonry plasters (scagliola, canary): require water to set, can be
used alone to bond things together or in combination with cotton bandages and
gauze; will not properly set in high humidity or wet environments; require specific
tools, dexterity, and experience to employ properly.
D Waxes Paraffin, beeswax, etc.: can be used alone (casting) or in combination with impreg-
nated bandages and a heat source; can be useful in very humid or wet environments
in which acrylic solutions, emulsions, or resins will not adequately set; cannot be used
in very warm climates.
E Expanding polyurethane foam Have the double functionality of containment and protection from forces; are very
lightweight; have an easy and quick application process if prepackaged industrial
cans are used (the use of a two-component resin with a foaming agent is more dif-
ficult to employ but is often more effective, especially for large objects or features);
can be used in humid, damp, and wet environments; are susceptible to deterioration
from UV light.
F Cyclododecane Cyclododecane is a solid cyclic hydrocarbon (C12H24) that sublimes at room tem-
perature. It can be used for very temporary operations. It appears as a very light
white powder, which can be liquefied when heated in a water bath or dissolved in
various solvents, e.g., Shellsol OMS (white spirit), hexanes, or xylenes. The liquefied
cyclododecane can be directly applied (quickly while it’s dissolved or hot) on different
materials (stone, ceramic, brick, plaster, etc.) and/or combined with cotton gauze
to temporarily immobilize small to medium-sized objects. It is particularly suitable in
damp or wet conditions, where it may be difficult to use other, more common materi-
als. After application the cyclododecane has a short life span because it sublimates
in a few hours, days, or weeks (depending on climate and exposure, as well as thick-
ness of application).
may be to remove both the material and a thin layer of careful excavation may prove impossible or damaging
enveloping soil. to the material itself. In these situations it is always
The full excavation of objects in silt or muddy better to resort to either supported or unsupported
contexts can cause irreparable damage to the objects’ block lifting. (See tables 10.1 and 10.2; categories 1a
surfaces, especially in the case of heavily corroded and 2a.)
glass or artifacts with gilding or fragile painted deco-
rations (see chap. 5). The corrosion layer on glass or Block Lifting
painted or gilded surfaces may actually adhere more Block lifting consists of removing the artifact(s)
strongly to a silty soil than to their own substrate. In together with the surrounding soil as a more or less
such instances, the materials must be lifted together solid and compact unit. Block lifting in concept can
with a fine layer of soil, approximately 1 to 2 mm, still help to avoid undue mechanical and environmental
adhered to the surface. stress on fragile or fragmentary objects by limiting
Phenomena similar to those just described can their disinterment to the initial soil removal that
be encountered in very dry or carbonaceous soils. reveals their presence. This in and of itself reduces the
Accordingly, lifting techniques must be similar but potential for exposure to haphazard or risky excava-
with the one modification that the soil (only the tion or cleaning. In some instances, block lifting can
soil) may need to be lightly moistened to facilitate preserve important information for later study of the
operations. sedimentary context (Berducou 1990). Importantly,
In cases where the material(s) may be highly frag- this technique allows one to delay full excavation
mented, crushed, or distorted and generally structur- until the assemblage can be removed to a labora-
ally unstable, traditional removal by methodical and tory or similar facility where the environment can be
Table 10.2 Some Examples of Common Support Materials Used in Lifting Operations
Type Notes
A Semirigid sheets of copper, Can be inserted easily into trenches cut in the soil, either alongside or underneath an ob-
brass, aluminum, zinc, or ject or material, functioning as temporary supports during lifting; can be used for objects
plastic materials such as and materials of limited scope and weight; otherwise they need additional structural sup-
fiberglass, polyvinylchloride port in the form of planks or panels of polystyrene, wood, or polycarbonate. Plastic panels
(PVC), polypropylene (PP) or sheets are preferable if the support is meant to be more than short term (fiberglass or
polypropylene); otherwise PVC or metal sheeting should be avoided for storage for any
length of time.
B Extruded foam polystyrene These are panels commonly used as insulation in construction of roofs and walls; they
(PS) panels and sheets are typically light reddish/pink, light blue, or light yellow in color. They are lightweight
(insulation for home and and semirigid, can be easily cut with box cutters and knives, and thus can be customized
building construction) to small or medium-sized objects or materials. Such panels are not adversely affected
by humidity, moisture, or dirt and grime but can be susceptible to gradual damage from
UV light and can be dissolved with some chemical solvents.
C Wooden planks or sheets These are particularly well suited to the lifting and support of large objects or features,
especially hardwoods or those precut for carpentry. Typical resinous woods (pine, fir, etc.)
can deform if used in humid or damp environments. Particleboard or panels made with a
resin/wood mixture should not be used. Wood sheeting and panels are more expensive
than polystyrene panels and, accordingly, should be used where their greater structural
strength is necessary.
D Polycarbonate (PC) honey- The semirigidity of polycarbonate honeycomb panels makes them well suited to the lifting
comb panels of small to medium-sized objects and thus they are a good compromise between the
rigidity of wood and the softness of polystyrene and are chemically more stable in the
long term.
controlled. This is essential if meticulous and delicate e) Containment of the exterior of the block; wrap-
operations—such as gradual consolidation—must be ping the block with a flexible material such as
undertaken prior to soil removal, and can be greatly fabric or stretch plastic film or creating a rigid
beneficial in cases of highly fragmentary, fragile, support
or distorted objects. (See tables 10.1 and 10.2; cate f) Secondary cut under the block, effectively
gories 1b, 1c and 2b, 2c.) detaching the block from the soil
If block lifting involves the removal of a large block g) Positioning and immobilization of the block on
or section of earth, some of the surrounding archaeo- a rigid support
logical context may be destroyed. Such a large mass
may also be difficult to handle, load, or transport. unsupported block lifting
Accordingly, any form of block lifting should be care- In unsupported block lifting there is no containment
fully planned and coordinated, considering all these of the exterior of the block. An unsupported block lift
factors. As will be seen, it is possible to address and is feasible only when it is not necessary to employ any
overcome most issues and logistical problems with form of stabilization or consolidation to the archaeo-
some simple steps and basic techniques. logical artifact or feature itself—that is, there is no
Block lifting can be done in many different ways, need for steps b, c, or e—even if there may be cracks,
depending on the specific case, by combining various voids, or deformation (see “Object or Material Char-
techniques and using different forms of equipment. In acteristics” above and fig. 10.1). The conditions neces-
general there are two conventional ways of proceed- sary to opt for the use of an unsupported block lift are
ing, unsupported block lifting and supported block as follows:
lifting (Payton 1992). These techniques have many
• The object must be relatively small in size; in
steps in common, which can be summarized as
principle, applicable to artifacts that relate to
follows:
category 1b.
a) Excavation (see chap. 4) • The soil must be compact: either dry and hard or
b) Stabilization (see chap. 7) very damp or wet (typical for clay or loam soils). If
c) Preconsolidation (see chap. 7) the soil is only slightly damp or loose and sandy, or
d) Initial cut defining the perimeter of the block; potentially both, then there is little probability of
pedestaling success.
that support can follow immediately after excavation. • Polyethylene bandaging strips for wet or humid
Soil removal, surface cleaning, stabilization, and/or objects or features, which can also serve to preserve
consolidation and support operations should be per- the microclimate while providing support
formed in one uninterrupted cycle. • Elastic bandages, which allow for forces to be
The sequence of these procedures is related to the regulated and more evenly distributed on the
nature of the object to be lifted. In cases of exfoliation object or the feature
or high fragmentation, immobilization or consolida-
These immobilization techniques have distinct advan-
tion should be part of excavation to avoid the loss of
tages over any form of chemical consolidation:
spatial relationships between fragments (steps b and c).
This can even apply to seemingly well preserved • They do not involve the use of chemicals of any
objects, such as broken but intact ceramics or cracked sort, whether solvent or resin.
stone blocks, that may have a tendency to open when • They do not invade or alter the chemical-physical
the containing soil is removed. The previously listed nature of the object or feature.
steps a–g should cover all possible operations, but • They are totally reversible.
consolidation may be necessary to varying degrees • They are fast and easily used.
and implemented at various stages depending on the • They are relatively inexpensive.
material characteristics, as follows: • They do not require specialized knowledge
or skills.
• Localized surface application
In very complicated cases where specialized applica-
Immobilizing flakes or exfoliating materials with tions and techniques are necessary or cases where
an open-weave gauze and acrylic resin (see chap. 7) environmental parameters are a major factor, it is best
Adhering detaching or loose fragments with to involve a conservator or someone who has special-
weak, reversible resins (see chap. 7) ized training. These cases typically involve the creation
• Superficial application beyond the surface of structural supports through chemical means,
such as:
Consolidating corrosion on metals or glass or
immobilizing detaching surface layers such as with • Cotton bandages soaked in plaster to create a hard-
wall plaster or frescoes (see chap. 9) shell cast support
Preconsolidation of large or extensive areas that • Fiberglass matting with polyester or polyurethane
are still covered with a thin layer of burial soil (see resin to create a hard-shell support
chap. 9) • Cotton bandages coated or impregnated with
beeswax or paraffin wax to support a hard-shell
• Deeper penetrating application support
Adhesive or cohesive consolidation with acrylic These stabilization techniques are well described in
resins or ethyl silicates, undertaken only in cases of the archaeological and conservation literature and
absolute necessity and, preferably, performed by a have been used traditionally in the removal or lifting
conservator of movable heritage. For this reason the methods of
application are not the focus here but rather, the fac-
In principle, deep penetrating consolidation is under-
tors that influence if and how they should be used (see
taken only on object types or features in categories 1b
table 10.1).
and 2b. Localized surface application or preconsolida-
Once stabilization has been achieved, detachment
tion can be applied to virtually all object types and in
may proceed with the first vertical cuts (step d). For
all situations.
objects in categories 1b and 2b, containment of the
Tall artifacts or vertical features such as wall paint-
object or the object and the block of soil may be nec-
ings (categories 1d and 2d) may feasibly be block
essary. This can be done with a flexible fabric or plastic
lifted with the use of external supports or straps to
film wrapped around the pedestal or by creating a
immobilize the object itself or the object and block of
hard shell over one or the other in plaster, fiberglass,
soil. In many instances the techniques described in the
and resin or waxes, using an isolating barrier to pre-
section on discovery in chapter 7 may be sufficient to
vent their penetration into the matrix of the object or
guarantee success:
soil. Steps f and g proceed as described in the section
• Straps or ratcheting, which can be adjusted to exert on unsupported block lifting.
a determined amount of pressure on a detaching, In cases of large or heavy blocks, an alternative
delaminating, or exfoliating object or feature technique using metal rods instead of semirigid and
e q u i p m e n t a n d a p p l i c at i o n
Table 10.2 lists the more commonly used and more
easily found materials used as the structural base in
block lifting. These have been organized according
to their function. As with all the materials listed in
table 10.1, these should never be used directly on the
surface of any object or feature. In general, when a
material is being used in contact with the object or
soil surface, an isolating barrier of polyethylene plas-
tic film (for steps a, c, e) or aluminum foil (for steps
a, b, c, d, e) should be used. This precaution should
minimize the possibility of adherence, damage, or
alteration and ensure greater success of the operation.
Where resins, waxes, or plaster are used, it is rec-
ommended that the application of these materials be
Figure 10.3
entrusted to conservation professionals or specially
trained individuals. These materials have the advan-
tage of being applicable in a semifluid or viscous state,
allowing them to conform to the particulars of the
undercut and fill any potential hollows or voids
(step f).
“
P reliminary” or “initial” cleaning refers to the first
general cleaning, commonly known as washing,
that is undertaken on most archaeological artifacts
The first phase is implicit in the act of excavation
and cannot be changed other than to be undertaken
with caution and prudence. The second phase, on the
and materials during their recovery, immediately other hand, goes beyond what is typically necessary
after removal from the soil, or in a conservation and can be justified in only a small number of situ-
laboratory. ations where it is not possible to identify the signifi-
cance of the find due to its veiled or obscured nature
or where exhaustive in situ documentation is neces-
Archaeological Practices sary to the point of highlighting the color and every
and Conservation Issues surface feature of a find.
Once removed, the great majority of archaeologi-
Preliminary cleaning is a form of intervention that
cal finds such as ceramics, stone, glass, and even bone
has consequences for the preservation and long-term
fragments are typically washed. Usually this is done
stability, not to mention appearance, of an archaeo-
by submerging masses of fragments still covered with
logical material. As such, for all intents and purposes,
soil in large containers of water and then scrubbing
cleaning should be undertaken with reference to and
them with household cleaning brushes, toothbrushes,
guided by the principles of ethics for acceptable con-
or paintbrushes. Although an entrenched practice
servation practice (Pedelì 2001a). Unfortunately this is
on most excavations and seemingly harmless from a
not the traditional view or practice of cleaning; even
conservation perspective, it in fact contains many det-
today it is applied all too casually to artifacts during
rimental risks if not undertaken with some care and
excavation, when, once removed from the soil, they
attention as to the materials being washed and their
are fully immersed in water.
basic state of preservation. If these basic factors are
In order to better understand these statements,
not taken into consideration, irreversible damage or
it is best to define from the outset what is typically
loss is entirely possible:
involved in the daily practice of cleaning on most
archaeological excavations, where even during ini- • Alteration or removal of organic residues or traces
tial discovery and exposure, an unconscious form of of original use
cleaning that can be divided into two basic phases • Alteration or removal of pseuodomorphs or
often takes place (see chap. 4): impressions from other objects
• Alteration, mechanical deterioration, or removal of
1. Removal of the earth and soil around an
portions or features of an artifact, such as decora-
artifact or feature: up to this point the sur-
tive coverings, painted surfaces, or inlays
face of the object probably has not been
• Exacerbation or initiation of chemical, biological,
touched or had any substances applied to
or physical agents of deterioration
it, not even water. Though it is still some-
what covered with soil, the object can be If washing is followed by rapid drying, aided by
identified in its approximate material type exposure to direct sunlight or strong drafts or winds,
and shape. the potential for damage or loss is increased. At the
2. Surface cleaning: removal of the thin layer opposite extreme, if washed objects are not fully dried,
of soil still covering the surface and partially or are left damp or wet too long, and are then enclosed
masking potential specific details, such as in impermeable storage bags or plastic containers,
color or applied decoration. At this point the the activation phenomena of alteration and eventual
surface is touched by various tools—trowels, degradation are very likely. In particular, biological
spatulas, brushes, or sponges—more or less growth is probable on porous materials such as ceram-
constantly and may have had water applied ics, stone, bone, and wood, while corrosion of metals
to help soften or dissolve the obscuring soil. or glass may occur or continue.
93
Table 11.2 Extract of Technical Data Provided by Giorgio Mischiatti (MG Company)
if it is still deemed appropriate, then only water should been removed can travel downward, in the process
be used. As initial cleaning should in principle be softening, swelling, and ultimately helping to detach
limited to the removal of loose soiling and deposits, the remaining surface deposits. By working in this
water is the most effective general solvent, and there is manner, greater security is guaranteed, because the
no need to resort to the use of other organic solvents fragment and the effects of cleaning can be directly
or acidic or basic chemical reagents. If anything other observed. Importantly, this procedure should mini-
than water is believed to be necessary for washing, mize the amount of saturation of the object being
such a task should be performed by a conservator. cleaned and the amount of time it is fully submerged.
It is recommended practice to wash one fragment Any sediments that are removed should sink
at a time rather than large groups or batches. Washing toward the bottom of the water container, to ensure
should be done by wetting the entire fragment and that the higher reaches of water are free from par-
cleaning first any of the break edges to understand the ticulates and thus usable for continuous wetting of
nature of the material being cleaned and its reaction to the sponge. For this reason it is also important that
this form of cleaning. Break edges can be cleaned with immersed materials not be allowed to sit on the bot-
brushes, while surface cleaning is preferably done with tom of the water container and that sponges not be
sponges to prevent the application of excessive force. wetted from the lower reaches. Frequent water sub-
The removal of soiling, whether from the break stitution should reduce the number of particulates in
edges or the surface, should begin toward the center suspension and help avoid potential abrasion.
of the fragment and gradually work outward to the Drying should occur gradually, preferably in a
edges. Working in a semicircular motion, maintain shaded area free from gusts of wind, drafts, dust, and
a thin film of water so that the particulates that have airborne particulates.
Shape Rectangular
Size and capacity Appropriate to the size and intrinsic weight of the material or objects recovered; capable of
being handled and moved. Typically standard dimensions of commercially available crates are
30 cm W × 40 cm D ×12 cm H (10 L ); 30 cm W × 40 cm D × 22 cm H (20 L ); and
40 cm W × 60 cm D × 22 cm H (40 L )
Modularity Standard sizes for easy stacking and conforming to storage shelves (fig. 12.1)
Interior walls and bottom Straight vertical walls and flat bottom, preferably without many holes and devoid of support ribs
Exterior walls Good amount of vertical and horizontal support ribs to increase mechanical resistance; stable
base with rib configuration that allows for stacking (fig. 12.2a)
Profile and rim Walls and bottom should not be less than 2 mm thick; the rim should have a flat edge capable of
supporting weight
Stacking The underside of the upper container should fit onto or slightly into the rim of the container below,
entering no more than a few millimeters (fig. 12.2b)
Handles No less than two, on opposite sides
Labeling Space for all pertinent data associated with the object and archaeological context on a flat and
smooth surface on either the short or the long side of the container for ease of visibility
Cover If possible, covering system should allow for stacking; otherwise not always necessary
Storage Should occupy as little space as possible when not in use and be able to be stored in uncontrolled
environments
Reuse Should be washable and able to be used in any circumstances where packing is necessary
Table 12.3 Basic Typology of Suitable and Unsuitable rial recovered. These containers are most useful for
Containers small to medium-sized objects or material, such as
Suitable Unsuitable significant pottery sherds, coins, bracelets, rings, and
the like, that must be individually protected. As such,
Polyethylene or poly- Wooden crates or boxes
propylene boxes they are often used from the moment of excavation
Cardboard boxes
Polypropylene or
through to long-term storage. They therefore must be
Metal, typically tin, crates or boxes
wood pallets able to hold objects that are moist or wet and must
Polyvinylchloride containers remain stable under unregulated environmental con-
Large glass containers ditions. See table 12.5.
Plastic shopping bags, fiber baskets As with larger containers, it should be recognized
that they may never be replaced. Therefore, they
should be suitably stable chemically and physically.
Subcontainers A proposed model for subcontainers of the small,
The variable sizes of subcontainers allow for differing quadrangular, semirigid box or “crystal box type,” as
configurations within a larger storage container and, opposed to the small polyethylene bags that are also
importantly, for accommodating the type of mate- commonly used, is as follows.
(a) (b)
Suitable Unsuitable
Plastics Plastics
Polypropylene (PP) Polyvinylchloride (PVC)
Polyethylene (PE)
Polyester (polyethylene terephthalate—PET)
Polystyrene (PS)
Modified polystyrene (ABS, HIPS)
Polycarbonate (PC)
Polytetrafluoroethylene (PTFE)
Metals Metals
Aluminum, zinc, or tinfoil (silver paper) Iron, tin, or painted sheet metal
Glass Glass
Mold blown of suitable thickness Free-formed and irregular, thin or crystal
Paper based Paper based
Nonacidic, archival board Recycled paper or cardboard
Fabric/textile Fabric/textile
Bags, sacks, and screens Leather
Synthetic (nylon, PE, and PET)
Natural (cotton)
Mechanical:
• Semirigid, having some flexibility or give to be able • R esistant to deterioration, deflection, and distor-
to absorb acute forces, but should not permanently tion when under proportional load
deform; should adequately support the intrinsic • Resistant to ripping and tearing
weight of the object and be easy to handle • Nonabrasive to the archaeological material
Chemical and physical: • Closable PE freezer and storage bags, with or with-
• N o chemical reaction or interaction with the out holes
archaeological material • PE tubes (with two open ends) that can be closed
• Will not release or leach chemicals, whether gas using a hot iron or heat sealer
or liquid, even under unstable environmental • Slide containers of PP, PS, and PE
conditions: changes in temperature and relative • Glass sealable canning jars
humidity • Aluminum (AL) takeout containers
• Resistant to atmospheric pollutants
• Resistant to biodeterioration Padding, Cushioning, and Fabrics
• May be slightly susceptible to exposure to UV light Textiles can be used as a separator or a form of inter-
or to common solvents, as long as they are properly face between the artifact and the packing material, or
contained within a larger container that is resistant if bundled or thick enough can be used as a form of
to these factors padding and cushioning to substitute for expandable
materials. All the textiles listed in table 12.6 can be
Many of the most suitable subcontainers are plastic put in direct contact with the artifact’s surface during
and have been developed for food storage by the food first packing and even longer if periodic and regular
industry. This makes them easily available at a rela- checks are made to guarantee their condition. This is
tively low cost. Examples are: especially true for natural textiles, which can be a food
• Polypropylene (PP), polystyrene (PS), and source for biological agents, insects, or rodents. Con-
polyethylene (PE) food containers, with or tainers that contain natural fabrics should be carefully
without lids noted and monitored, especially if the packed objects
• Insulating expanded polystyrene (EPS) contain- were moist or wet or if there is no environmentally
ers, such as disposable coolers or certain ice cream controlled storage.
containers Unsuitable packing materials are listed in table 12.7.
• Hermetically sealable PE boxes In general tightly woven fabrics are preferable, as are
softer and lint-free fabrics. The weave and roughness General Criteria
are important if the fabrics are in direct contact with
• Regardless of their condition and the association
materials or objects with a delicate or highly degraded
or grouping during recovery (see chap. 10), most
surface. These surfaces can be abraded by a fabric that
recovered materials should be packed separately
is rough, and open or loose weaves may snag, espe-
based on their material type (stone, ceramic,
cially during transport or handling, and dislodge some
metal, glass, bone, leather, etc.) and not on their
of the original material.
archaeological typology. This is especially true of
Natural fabrics such as cotton or some geotextiles
sensitive materials such as metals or glass, which
may also have a tendency to cling to surfaces through
should always be packed separately and should not
built-up pile or lint. Most natural fabrics are commer-
be interspersed or mixed with porous materials,
cially treated with glues, starches, dyes, softeners, and
especially if those are damp or wet.
detergents and should be washed prior to use. This is
• Very small, delicate, or damaged artifacts or those
important for eliminating any and all substances that
with the greatest susceptibility to physical or
could be activated in the presence of moisture (ambi-
mechanical alteration during transport or handling
ent or from the object itself) and thus interact with
should be further separated and protected in a
the archaeological material. The hygroscopic nature
manner specific to their needs.
of most natural fabrics should also be considered,
• Artifacts or materials that are fairly complete but
rendering many inappropriate in cases of non-
still very fragile should be packed with padding in
hermetically sealed packing.
a way so as to be as visible as possible; they should
A number of commercially available polyethylene
not be wrapped or enveloped completely in paper
foams of varying density are available in all price
or fabric.
ranges. These are well suited to initial or preliminary
• Any object that had to be removed with a block lift
packing needs on-site, as they are easily cut and
should be packed with padding in such a way as to
shaped to the desired function of support or cradling
be immobilized and separated from other materials
of an object or material. A geotextile or other suitable
as well as from the walls of the container.
nonwoven fabric barrier is advisable if low-density
• If padding is used, it should be used in such a way
polyethylene (LDPE) is used, especially in warmer
as to not create too much force or pressure on
climates, to avoid any potential adhesion between the
the artifacts by being too snug between objects or
object’s surface and the packing foam.
between the object and the container wall.
• Wet or damp materials should always be kept sepa-
Preliminary Packing Techniques rate from dry materials, especially when wet mate-
rials must be kept wet for reasons of preservation.
The criteria and techniques described below should be
• Wet or damp materials that can be allowed to
applied according to the material type and value of the
dry slowly should not be hermetically sealed but
archaeological finds, at the discretion of the archae-
rather placed in subcontainers with suitable holes
ologist or conservator responsible for these activities
or openings that are themselves placed within the
on the site.
container in a manner that permits air circulation.
Artifact Arrangement
• It is advisable to not overload the containers,
particularly transport or storage containers. Avoid
filling them to the rim, preventing them from
being able to be stacked securely and potentially
compromising the well-being of the materials in
other containers. Figure 12.3 An example of packing in sub-, or smaller, con-
• Artifacts or materials should be organized and dis- tainers within a larger container. The objects can be arranged
according to their stratigraphic provenance, material type, or
tributed logically in their containers, based on stra- state of preservation.
tigraphy, material type, size, condition, and so on
(figs. 12.3, 12.4). The criteria for separation must be
shared with the archaeologist in charge.
• Coins should be placed in appropriately sized PE
bags that are secured to a semirigid plastic label
(i.e., alveolar polypropylene) containing all perti-
nent information and associated data. The semi-
rigid label will serve as a type of anchor and should
help in organization and accessibility. Finally, the
semirigid label could be placed within a padded
transport container (fig. 12.5).
• Larger, heavier, and more robust materials should
be placed at the bottom of the container to form
the first layer. In principle, they often do not need
subcontainers. Figure 12.4 An example of an uncleaned metal coin packed
• If the recovered materials are damp or wet, their in a polyethylene bag that is affixed to a sheet of corrugated
polypropylene board.
subcontainers should be stacked in such a way as to
allow for ventilation.
• All materials, artifacts, and subcontainers should,
in theory, be restrained within the container during
transport to prevent damage. This is especially true
for more complete, small, delicate, or block lifted
objects. In these cases, lacking all other alterna-
tives (acid-free tissue or forms of padding), these
can be secured in place by surrounding them with
excavation soil, provided it is free of gravel or other
potentially harmful elements.
Microclimate-Regulating Systems
Packing of Damp and Wet Objects That
Can Be Allowed to Dry
Figure 12.5 Temporary archival storage of uncleaned coins
This situation typically calls for the use of PE, PP, or in a larger container. Such a system is highly organized,
PS plastic containers that have sufficient holes to allow allowing for easy reference to the coins while also providing
for air flow and circulation. (See chap. 5.) Best results optimal storage for small metal finds.
are achieved when the holes are in the upper/higher (polystyrene semirigid foam). This system can
portion of the container or subcontainer, as evapora- be improved by using freezable ice packs to keep
tion is an upward phenomenon. This holds true even the internal temperature low. The insulation of
for artifacts or materials that have been wrapped or the cooler also can be increased by lining it with
bandaged for support. By providing a sufficient num- aluminum foil, internally and externally, buffering
ber of holes, these measures will ensure: ambient temperatures and, in turn, slowing the
potential rate of evaporation.
• Progressive and gradual drying of the artifact,
material, or excavation soil The above-described systems cannot be considered
• Avoiding buildup of moisture or condensation on permanent or long term and thus should be moni-
the interior of the container tored and replaced if necessary.
• Avoiding the possibility of biological growth
Packing of Dry Artifacts and Materials That
Packing of Damp or Wet Artifacts That Must Cannot Be Exposed to Humidity
Remain Damp or Wet In these instances, attempt to reduce the amount of
Theoretically the best way to achieve this form of relative humidity within the artifact or material, as
packing is to use plastic containers that can be her- well as within the sealed subcontainer. This can feasi-
metically sealed and will maintain the seal. These bly be achieved with silica gel, a microporous hygro-
containers prevent the moisture in the material from scopic granulate of silica (SiO2). Silica gel absorbs
evaporating, by not allowing air in to dry out the or releases moisture to achieve equilibrium with the
object. With this said, many general-use plastic con- environment in which it is placed. If the surround-
tainers will not maintain a seal for an indeterminate ing environment is humid, the silica gel will absorb
amount of time and/or may allow vapor to permeate moisture. If dry, it will release moisture. This behavior,
and diffuse through the plastic in both directions. For coupled with silica gel’s ability to absorb up to 40% of
these reasons, it is often better to use alternative solu- its own weight in moisture, makes it an ideal environ-
tions to control the microclimate than to simply rely mental buffer (see Appendix 5).
on the container itself. One of the most effective tech- Use of silica gel:
niques is to use redundant or multiple subcontainers,
• The dry artifact or material to be buffered should
one inside the other. This will create a better overall
be placed in a sealable, clean, and dry plastic
seal and slow or prevent evaporation.
container of PE, PS, or PP, or even glass with a lid
Basic packing systems for maintaining moisture are
and gasket.
as follows:
• Any padding, fabrics, or other packing materials
• The damp or wet material is sealed in an should not be hydrophilic, as are most natural fiber
appropriately sized polyethylene bag with no textiles or paper products.
added water. • Silica gel granules can be preconditioned by heat-
• The artifact and bag are sealed1 within a second, ing them for about 20 minutes at 90–100°C and
closable subcontainer (bag or rigid rectilinear then contained within a relatively open-weave
container) with a certain quantity of water that synthetic fabric bag or an open subcontainer,
is contained in an absorbent material such as which is then positioned within the container with
chemically stable fabric, cotton, or synthetic the artifact. An open-weave bag is preferable to a
sponges. container because it allows for greater surface area
exposure of the silica gel.
For organic materials, the following system is
• Silica gel should not be placed in direct contact
preferable:
with archaeological material.
• Remove all extraneous soil, which may contain • The container holding the artifact and silica gel
salts or microorganisms. subcontainer must then be closed and sealed as
• Use cold storage to prevent biological growth (pref- well as possible; it should not be of a hydrophilic
erably around 3–4°C). If this is not possible, treat material (cardboard, wood, fabric, leather, etc.).
with a suitable biocide (this should be considered a
technique of last resort). endnote
• Use double bagging or a container within a 1 In this case the term sealed indicates that the edge of
container to increase seal, and place the whole the PE bagging is folded several times on itself and then
assembly in a portable plastic or Styrofoam® cooler definitively closed with electrical tape.
recorded on preprinted forms, especially in the fol- • Will not abrade or scratch any archaeological
lowing cases: artifacts or materials
• Will not cause chemical reaction or interaction
• When materials/objects are of particular
with the archaeological material
significance or rarity
• Will not release or leach chemicals in any form,
• Metals and glass
whether gas or liquid, even under unstable envi-
• Organic materials, such as carbonized seeds or
ronmental conditions with changes in temperature,
waterlogged wood
relative humidity, or exposure to IR or UV light
• When the object is in very poor or fragile condition
• Resistant to environmental factors; will not dete-
riorate or react when exposed to visible, UV, or IR
Recording Methods and Tools
light, moisture, changes in relative humidity, or
All transcribed information should be:
temperature variations
• Legible (use capital letters) • Resistant to atmospheric pollutants
• Clear and concise: in general the longer the • Resistant to most common solvents and chemical
description or the more words, the greater the pos- reagents
sibility of illegibility and misinterpretation • Resistant to biodeterioration
• Chemically and physically stable: resistant to minor
abrasion, visible and UV light, and temperature Recommended Label Materials
and relative humidity
• Polypropylene, such as drawing papers and vellums
Alcohol- or solvent-based red or green markers or used in drafting or printmaking
pens are to be avoided as they will fade when exposed • Polyethylene, such as Tyvek, cut into appropriate-
to sunlight. Paint-based or varnish markers should be sized pieces
avoided, whether for labels placed in a container/sub-
container or for labels that might come in prolonged endnote
contact with an artifact. 1 In this case the authors suggest an approach to
registration and labeling in which objects and materials
can be grouped by their physical characteristics or
Labels context of recovery.
Basic Requirements
Many of the characteristics appropriate for packing
materials are applicable to labels, especially those
related to the chemical/physical properties:
107
Documentation
111
• The type of product or material used (e.g., for compatibility. Importantly, this information can be
Paraloid® B-72, lime or hydraulic lime) very useful in interpreting the efficacy of a treatment,
• The type of concentration or solution used or pro- say, consolidation, its sustainability, and potential
portion used in creating a mixture (i.e., ratio of alteration over time.
lime to aggregate) (see Appendix 4)
• The solvent used Types of Solvents Used
• The type or mode of application and number of We cannot go into the chemistry of the different types
applications (i.e., for consolidation, impregna- of solvents and their properties here (see Torraca
tion or rejoining, and by brush, spray, sponge, 1980; Masschelein-Kleiner 1982). It is sufficient to say
injection, etc.) that it is of the greatest importance to always indi-
cate the type of solvent used in a solution or in direct
application, for the following reasons:
Type of Material Used
• The solvent will influence the viscosity of the
If the trade name of a product is used (e.g., Paraloid®
solution, which in turn has a direct effect on the
or Primal®), it is imperative that the industrial or
penetration of the solution into a material. It is not
manufacturer’s designation be included as well (e.g.,
enough to simply state the percentage of a solution;
Paraloid® B-72, Paraloid® B44, AC-33). This is espe-
the solvent must also be included because, for
cially important for some commonly used chemicals
example, a 20% solution of Paraloid® B-72 in an
in conservation that have a wide range of products
aliphatic solvent will be far more viscous than a
(e.g., Rhodorsil and Mowilith, which have many
20% solution of Paraloid® B-72 in acetone.
variants).
• The solvent used determines the volatility of the
As stated above, even lime has several variations,
solution and therefore the drying time. Extremely
the most basic being hydraulic and nonhydraulic.
volatile solvents can concentrate on the surface of
In the case of hydraulic lime, it is important to include
a material once applied and therefore create a sur-
the manufacturer in the documentation because
face film with a great concentration of resin at the
there can be huge variations in properties from one
expense of the area below, which is resin deficient.
manufacturer to the next, as extreme as a difference in
• Solvents have a direct influence on the optical char-
compressive strength of 1 to 2.5 (40 kg/cm2 compared
acteristics, or appearance, of a resin.
to 110 kg/cm2). In Europe, recent regulations have
required that the manufacturer state the nature of the
Method of Application
lime (e.g., NHL = natural hydraulic lime, obtained
Documentation should indicate the method and num-
from the cooking of calcareous and marl stone;
ber of applications of a material:
HL = hydraulic lime, obtained with the addition of
hydraulic compounds to quicklime) and the compres- • With a brush, spray, or sponge or by saturation,
sion resistance after 4 weeks (e.g., 2.5, 3.5, 5, meaning and so on
25 kg/cm2, 35 kg/cm2, 50 kg/cm2). • Single or repeated applications
This information is typically very useful in evaluating
Type of Solution or Proportion
the efficacy of a treatment over time and, if needed,
The concentration or dilution of a mixture must be
in being able to obtain the same result in similar
accurately documented (see Appendix 4). This infor-
circumstances.
mation is essential to achieve comparable results or
113
potential of the remains to warrant site presentation areas that are mistreated or refuse strewn. Aside from
and interpretation. In these instances, reburial should being an eyesore, in most of these circumstances, the
be undertaken with the understanding that the exca- destruction of the archaeological remains is rapid,
vation may be reopened in the future and done in a definitive, and irreversible. Accordingly, what fol-
way that permits future verification or investigation. lows is an attempt to describe conservation interven-
For this reason, the reburial or backfill material should tions that preserve in situ archaeological features by
be clean of all impurities to minimize the potential for accounting for the major factors that determine the
contamination and uniform enough to make it easily degradation of their material composition.
recognizable and distinguishable from the archaeolog- Presentation of an in situ structure or feature
ical soil. The traditional practice of reusing excavated should be taken under serious consideration in the
soil for backfilling is, fortunately, on the wane and following circumstances:
should be avoided to prevent creating a potentially
• The structure or feature is of sufficient significance
confusing situation for archaeologists in the future.
to warrant public presentation
Given that long-term reburial is in place for an
• There is sufficient access to the site for potential
indeterminate amount of time, preference should be
visitation
given to lightweight inorganic materials that are stable
• Sufficient equipment and technology are available
both physically and chemically. These should also be
to ensure the necessary environmental parameters
robust (not susceptible to easy dissolution or pulveri-
for long-term conservation
zation), in order to avoid the creation of depressions
within the filled area, and of a fairly uniform size There are three basic forms of in situ conservation
(between 4 and 10 mm) to decrease the possibility of measures:
segregation and compaction. If these basic parameters
• Exposed and outdoors
are followed in the selection of a material for reburial,
• Under protective structures or shelters
a uniform fill that will not overly compress the archae-
• Inside permanent structures or buildings
ological layer and remains while remaining easily dis-
cernible and ultimately removable should be feasible.
Exposed or Open-Air Conservation
Measures
Exposed or open-air conservation measures are
Conservation Measures for Site
sustainable and feasible only on large structures or
Presentation and Interpretation features. It would be counterproductive to conserve
The theoretical principles and techniques of in situ exposed small features or structures that can easily be
conservation measures are too vast to be dealt with damaged or even stolen. In these cases, reburial would
here. Instead, we examine some of the more universal be more appropriate, creating a greater probability of
basic principles inherent in the consideration and survival.
implementation of these techniques. Conservation measures associated with leaving a
All too often excavated features of any significance structure exposed to the elements generally involve
are kept open at any cost. While allowing for access, the use of sacrificial materials over the original. Con-
continued study, or visitation, this is a major impedi- ventionally these are mortar based, such as with cap-
ment to the preservation of in situ archaeological ping and repointing, and should have less chemical or
remains. For this reason it is paramount to be aware mechanical resistance than the archaeological material
of the many logistical, professional, and economic fac- they are protecting and thus deteriorate instead of
tors implicit in deciding to conserve and preserve an the original material. Whether just mortar or mixed
exposed in situ feature or portion of an archaeological with masonry, these are often used in a manner that
excavation. If these factors are not clearly understood renders them readily distinguishable. (For the basic
prior to treatment, the potential for a site or feature to principles regulating the use of sacrificial material on
have significance to a greater public beyond archaeol- masonry, see the Athens Charter of 1931 and the Ven-
ogy and academia may be squandered. ice Charter of 1968.)
In these cases, it would be preferable and more The use of sacrificial materials requires that this
appropriate to rebury. The examples of poorly planned form of long-term in situ preservation include estab-
or implemented site conservation/presentation mea- lishing a system of periodic monitoring and main-
sures are numerous and readily found throughout the tenance. This, unfortunately, is often more true in
world, often resulting in overgrown sites or, worse yet, theory than in practice. In instances of inadequate
monitoring and maintenance, the most common • Easy maintenance of the structure itself: if the cost
results are as follows: of maintenance is near or equal to that of the exca-
vation, then the use of a shelter is probably prohibi-
• The sacrificial material completely deteriorates,
tive and long-term reburial preferable
leaving the original material exposed to
environmental factors such as precipitation,
Permanent Enclosure or Sheltering
freeze/thaw cycles, solar radiation, and potential
of an Entire Feature or Structure
mistreatment from visitors.
Permanent enclosure or sheltering of an entire fea-
• The sacrificial material proves to be more robust
ture or structure can be undertaken in two specific
than the archaeological masonry to be protected,
instances:
causing its possible preferential and accelerated
deterioration. • When the archaeological feature is already
incorporated in or enclosed by a structure that
Accordingly, these measures should involve some ini-
cannot be restricted in its use by the public, such as
tial treatment for long-term conservation (see below).
churches and historic monuments
• When the importance of the archaeological feature
Protective Structures or Shelters
and/or environmental parameters necessitate the
Shelters are typically used for medium-sized struc-
creation of a permanent protective structure
tures whose significance or surrounding environmen-
tal or climatic conditions necessitate measures more Both cases require a detailed and well-thought-out
substantial than those for open-air features. The types plan in order to minimize or avoid the possibility of
of structures or shelters are numerous and can make creating a microenvironment that could be damaging
use of many different types of techniques and materi- to the feature meant to be protected. The design of a
als as diverse as fabrics and reinforced masonry. (For a long-term, permanent structure should include the
fuller discussion of the various types of structures and following factors:
materials that have been experimented with and tried
• Properly insulated materials, to prevent the
over time, see Stubbs 1995.) In all instances, shelters
creation of condensation or excessive heat
or coverings should ensure these basic requirements:
exchange with the overlying or surrounding
• Protection of an area considerably larger than structures (fig. 16.1)
the excavated feature to avoid possible wetting • Sufficient drainage and directional channeling of
from rain rainwater around the shelter to prevent leaks or
• Reasonable resistance to local environmental ele- seepage from augmenting existing groundwater
ments, such as sun, rain, wind, heat, and cold levels (fig. 16.2)
Protection of Masonry Walls Figure 16.3 Vassos, Arcadia, Greece. The interior of the
(Capping and Repointing) protective covering. Here the entire monument is perfectly
undisturbed and can be seen and visited.
It is worthwhile to consider the issues associated
with the use of lime-based mortars for capping and
Figures 16.4 and 16.5 The archaeological site of San important in the case of glass shelters, because condensation
Salvatore, Turin. Exterior and interior images of a glass and temperatures can easily build up, defeating the purpose
protection created to allow for viewing of the archaeological for which the shelter was implemented.
remains below the modern street level. Climate control is very
repointing of archaeological masonry. Rather than • Most contain cement as the principal binder.
focus solely on the aesthetics related to the use of such • They are often less deteriorated than the
materials, which, in any case, should allow for legibil- surrounding masonry they were meant to protect.
ity and critical interpretation of the original masonry,
The principal reason for the poor state of preservation
this discussion focuses on constitutive materials and
of these interventions is the nature of the materials
methods of application (fig. 16.6).
used and the methods of their implementation. Since
An examination of numerous capping and repoint-
these interventions are all mortar based, one of the
ing interventions carried out in the twentieth century
main reasons for their substandard performance is
makes some generalizations possible:
excessive thickness, which, because of the large mass
• Most are poorly preserved and cracked and of mortar when applied, forms microfissures and
detaching from the underlying masonry. cracks during the shrinkage that accompanies dry-
• Most are generally mortar, with little or no visible ing. Over time these fissures have grown in size and
aggregate. allowed greater access of moisture and water to the
Figure 16.6 Ostia
Antica. Typical mortar
capping from the
1950s. Protection is
ensured at the expense
of the visual impact and
legibility of the ruins.
External mortars will have to deal with direct sun and B. Type of Masonry Materials onto Which the Mortar
sources of moisture, as well as much greater variations Will Be Applied
in temperature, particularly freezing temperatures.
Schematically, the materials commonly used for
Beginning with the principle that a mortar must
masonry, at least in Europe, can be divided into three
have at least the basic properties to sustain itself
basic categories:
in its particular environment of use, mortars for
sheltered contexts need no or a minimal amount of • Bricks and/or fired clay: high porosity, low to
hydraulic binder. The basic recipe can be summa- medium mechanical strength
rized as follows: • Calcareous stones: low to medium porosity,
medium to high mechanical strength
• 10 parts per volume of washed and sieved sand • Siliceous stones: low porosity, high to extremely
• 4 parts per volume of slaked lime high mechanical strength
• Ratio of 2.5:1 aggregate to binder
Based on these basic characteristics, different mortar
This basic recipe yields a mortar that is permeable to recipes are typically used depending on the material
water vapor and sufficiently dense to protect vulner- type.
able masonry. In more humid or moist sheltered envi- In the case of mortars for external use on masonry
ronments, the following variant has proven to set with composed of brick, the following recipe is common:
good moisture resistance:
• 8 parts per volume of washed and sieved sand
• 10 parts per volume of washed and sieved sand • 2 parts per volume of brick or ceramic fragments
• 3 parts per volume of slaked lime • 3 parts per volume of slaked lime
• 1 part per volume of hydraulic lime • 1 part per volume of hydraulic lime
• Ratio of 2.5:1 aggregate to binder • Ratio of 2.5:1 aggregate to binder
Mortars for external or exposed contexts can be best The recipe includes brick or ceramic fragments as
formulated by increasing the amount of hydraulic aggregate to increase the hydraulic nature of the mor-
lime in relation to regular lime and augmenting the tar while still allowing for permeability of water vapor.
amount of aggregate to increase elasticity: For mortars for external use on masonry com-
posed of calcareous stones, the following recipe is
• 12 parts per volume of washed and sieved sand
typically used:
• 2 parts per volume of slaked lime
• 2 parts per volume of hydraulic lime • 10 parts per volume of washed and sieved sand
• Ratio of 3:1 aggregate to binder • 1 part per volume of slaked lime
• 3 parts per volume of hydraulic lime some of the desirable features of the materials that
• Ratio of 2.5:1 aggregate to binder make up the above-recommended mortar mixtures.
Hydraulic lime should be of the type “Pure or
In this instance the amount of hydraulic lime is con-
Highly Hydraulic” and preferably from a natural
siderably increased to ensure greater bonding to the
source (typically of a slightly gray, brown, or reddish-
calcareous matrix of the masonry by replicating the
pink color). Any commercial products labeled as
nature of the calcium-carbonate stone by decreasing
containing “hydraulic binders” should absolutely be
the porosity of the mortar.
avoided, as they often contain substantial amounts of
For mortars for external use on masonry composed
gypsum (calcium sulfate) as a bulking agent to prevent
of siliceous stones, the following recipe can be used:
shrinkage, as well as various plasticizers like polyvinyl
• 12 parts per volume of washed and sieved sand acetates and alcohols to increase fluidity and adhesion.
• 1 part per volume of slaked lime White cement, such as Lafarge Superblanc, is
• 2 parts per volume of hydraulic lime recommended for the above recipes to increase the
• 1 part per volume of white cement hydraulic nature of the mortar. These types of cement
• Ratio of 3:1 aggregate to binder are preferable because they are generally devoid
of gypsum or soluble salts. With the use of white
In this recipe white cement replaces a portion of the
cements, however, it is very important to respect the
hydraulic lime in order to increase the amount of
proportions outlined. White cements have high com-
siliceous/aluminous material in the binder, replicat-
pressive strength (at least 425 kg/cm2) and a large rate
ing the nature of the siliceous stone in the masonry
of shrinkage during drying due to their lack of addi-
and increasing the amount of adhesion between the
tives. Too much white cement in a recipe can result in
mortar and the masonry. At the same time the ratio of
a mortar that is too hard and has low permeability to
aggregate to binder is increased to 3:1 to avoid creat-
water vapor and that may shrink considerably
ing a mortar that is too hard and impervious to
during drying.
water vapor.
Aggregates should vary in size to compensate for
C. Maximum Thickness of Mortar settlement within the mortar matrix while still plastic
and, importantly, to increase the elasticity, making
Maximum thickness refers to the thickness with which the mortar better able to expand and contract with
the mortar can be applied without resulting in fissur- temperature changes. For example, between two types
ing or cracking during drying, which ultimately will of sand with a grain size variation of 0–8 mm and
then be exacerbated by dimensional changes brought 4–8 mm, 0–8 mm is preferable because it contains a
about by cyclical changes in temperature. A study of greater range of particle sizes and will make a more
numerous old mortars that displayed good stability adaptable mortar.
showed a ratio of size of the aggregate to thickness of Sand aggregates should be washed prior to their
the mortar application of between 2.5 and 3.0 (Pulga use to remove any clay impurities and then fully dried.
1995). This same ratio was reproduced experimentally The above recipes are based on proportions for dry
with modern mortars and displayed optimal results in sand. If damp, sand can contain up to 30% water,
terms of density, firmness, and elasticity. which will produce a mortar that has too much binder
Based on these findings, care should be taken in and water. Sand is typically stored uncovered in stores
selecting an appropriate aggregate in terms of its prop- and on construction sites and thus usually contains a
erties and size. These can be easily verified or refined substantial amount of moisture. When used for con-
with the use of sieves or screens set to the appropriate servation, sand should ideally be stored under a cover-
particle size. Accordingly, mortar application should ing and frequently raked to ensure dryness.
not exceed three times the maximum grain size or The amount of water added to the mixture must be
dimension of the aggregate in one application (e.g., an very conservative and limited to creating a malleable
aggregate of 10 mm means that mortar of more than but not runny or overly liquid mortar. When worked
30 mm in thickness should not be applied). with a trowel, the mortar should maintain its form
without sagging. Unfortunately, the common use of
A Few Observations on Hydraulic Limes, and overreliance on cement mixers today means that
White Cement, and Aggregates most commercial cements require a greater amount of
Without delving too deeply into the complex chem- water to create an acceptably pliable mortar. This fact
istry of building materials, it is useful to elaborate on alone indicates that most mortars for conservation
should not be prepared with a cement mixer, as their The practice of overwetting mortars originates with
use is incompatible with creating a good lime mortar. masons’ overwhelming use of cement in today’s con-
Instead, commercially available static mixer attach- struction. Cement as a binder is very strong and will
ments for drills that allow for small quantities of mor- cure even if there are gross errors in proportions dur-
tar to be created with a proper consistency and with ing mixing. A more liquid cement can cover a large
limited amounts of water are recommended. surface area, even when applied to dry masonry. This
It is absolutely essential to not use too much water is incompatible with lime mortar, where the absorp-
when mixing mortar as excess water will produce: tion of moisture by the masonry, especially highly
porous materials like brick, will have a deleterious
• Excess dilution of the binder, which can result in
effect on the mortar. For this reason, the appropriate
an irregular mortar that is in parts too liquid and in
mortar mixture should be chosen according to the
parts too dense, leading to difficulty in application
three factors outlined above, and the masonry should
and uneven adhesion and drying
be well wetted prior to mortar application. If both are
• Excessive volume loss due to water evaporation
done correctly, this should result in a mortar that is
during setting, resulting in shrinkage cracks
well adhered and robust.
and fissures
• Inconsistencies in the mechanical properties
between the exterior surface of the mortar and
its interior
UNESCO Guidelines
123
art and architecture, each Member State being free financial resources make it impossible for all Member
to adopt the most appropriate criterion for assessing States to adopt a uniform system of organization in
the public interest of objects found on its territory. In the administrative services responsible for excava-
particular, the provisions of the present Recommenda- tions, certain common principles should nevertheless
tion should apply to any monuments and movable or apply to all national archaeological services:
immovable objects of archaeological interest consid- (a) The archaeological service should, so far as pos-
ered in the widest sense. sible, be a central State administration—or at any rate
an organization provided by law with the necessary
3. The criterion adopted for assessing the public inter- means for carrying out any emergency measures that
est of archaeological remains might vary according may be required. In addition to the general admin-
to whether it is a question of the preservation of such istration of archaeological work, this service should
property, or of the excavator’s or finder’s obligation to co-operate with research institutes and universities in
declare his discoveries. the technical training of excavators. This body should
(a) In the former case, the criterion based on pre- also set up a central documentation, including maps,
serving all objects originating before a certain date of its movable and immovable monuments and addi-
should be abandoned, and replaced by one whereby tional documentation for every important museum or
protection is extended to all objects belonging to a ceramic or iconographic collection, etc.
given period or of a minimum age fixed by law. (b) Steps should be taken to ensure in particular
(b) In the latter case, each Member State should the regular provision of funds: (i) to administer the
adopt far wider criteria, compelling the excavator or services in a satisfactory manner; (ii) to carry out a
finder to declare any object, of archaeological char- programme of work proportionate to the archaeo-
acter, whether movable or immovable, which he may logical resources of the country, including scientific
discover. publications; (iii) to exercise control over accidental
discoveries; (iv) to provide for the upkeep of excava-
II. General Principles tion sites and monuments.
p r o t e c t i o n o f t h e a r c h a e o l o g i c a l h e r i ta g e
4. Each Member State should ensure the protection of 7. Careful supervision should be exercised by each
its archaeological heritage, taking fully into account Member State over the restoration of archaeological
problems arising in connexion with excavations, remains and objects discovered.
and in conformity with the provisions of the present
Recommendation. 8. Prior approval should be obtained from the com-
petent authority for the removal of any monuments
5. Each Member State should in particular: which ought to be preserved in situ.
(a) Make archaeological explorations and excava-
tions subject to prior authorization by the competent 9. Each Member State should consider maintaining
authority; untouched, partially or totally, a certain number of
(b) Oblige any person finding archaeological archaeological sites of different periods in order that
remains to declare them at the earliest possible date to their excavation may benefit from improved tech-
the competent authority; niques and more advanced archaeological knowledge.
(c) Impose penalties for the infringement of these On each of the larger sites now being excavated, in so
regulations; far as the nature of the land permits, well-defined “wit-
(d) Make undeclared objects subject to ness” areas might be left unexcavated in several places
confiscation; in order to allow for eventual verification of the stratig-
(e) Define the legal status of the archaeological raphy and archaeological composition of the site.
sub-soil and, where State ownership of the said sub-
soil is recognized, specifically mention the fact in its f o r m at i o n o f c e n t r a l a n d r e g i o n a l
legislation; collections
(f) Consider classifying as historical monuments 10. Inasmuch as archaeology is a comparative sci-
the essential elements of its archaeological heritage. ence, account should be taken, in the setting up and
organizing of museums and reserve collections, of the
Resolutions need for facilitating the work of comparison as much
p r o t e c t i n g b o d y : a r c h a e o l o g i c a l e x c avat i o n s as possible. For this purpose, central and regional col-
6. Although differences of tradition and unequal lections might be formed or, in exceptional cases, local
collections on particularly important archaeological age excavations carried out by joint missions of sci-
sites—in preference to small scattered collections, entists from their own country and of archaeologists
accessible to comparatively few people. These estab- representing foreign institutions, or by international
lishments should command, on a permanent basis, the missions.
administrative facilities and scientific staff necessary
to ensure the preservation of the exhibits. 16. When a concession is granted to a foreign mission,
the representative of the conceding State—if such
11. On important archaeological sites, a small exhibit be appointed—should, as far as possible, also be an
of an educational nature—possibly a museum— archaeologist capable of helping the mission and col-
should be set up to convey to visitors the interest of laborating with it.
the archaeological remains.
17. Member States which lack the necessary resources
e d u c at i o n o f t h e p u b l i c for the organization of archaeological excavations
12. The competent authority should initiate edu- in foreign countries should be accorded facilities for
cational measures in order to arouse and develop sending archaeologists to sites being worked by other
respect and affection for the remains of the past by Member States, with the consent of the director of
the teaching of history, the participation of students excavations.
in certain excavations, the publication in the press of
archaeological information supplied by recognized 18. Member States whose techniques or other
specialists, the organization of guided tours, exhibi- resources are insufficient for the scientific carrying out
tions and lectures dealing with methods of excavation of an excavation should be able to call on the partici-
and results achieved, the clear display of archaeologi- pation of foreign experts or on a foreign mission to
cal sites explored and monuments discovered, and the undertake it.
publication of cheap and simply written monographs
and guides. In order to encourage the public to visit reciprocal guarantees
these sites, Member States should make all necessary 19. Authority to carry out excavations should be
arrangements to facilitate access to them. granted only to institutions represented by qualified
archaeologists or to persons offering such unimpeach-
III. Regulations Governing Excavations able scientific, moral and financial guarantees as to
and International Collaboration ensure that any excavations will be completed in
a u t h o r i t y t o e x c avat e g r a n t e d t o f o r e i g n e r s accordance with the terms of the deed of concession
13. Each Member State on whose territory excava- and within the period laid down.
tions are to take place should lay down general rules
governing the granting of excavation concessions, the 20. On the other hand, when authority to carry out
conditions to be observed by the excavator, in par- excavations is granted to foreign archaeologists, it
ticular as concerns the supervision exercised by the should guarantee them a period of work long enough,
national authorities, the period of the concession, the and conditions of security sufficient to facilitate their
reasons which may justify its withdrawal, the suspen- task and protect them from unjustified cancellation of
sion of work, or its transfer from the authorized exca- the concession in the event, for instance, of their being
vator to the national archaeological service. obliged, for reasons recognized as valid, to interrupt
their work for a given period of time.
14. The conditions imposed upon a foreign excavator
should be those applicable to nationals. Consequently, p r e s e r vat i o n o f a r c h a e o l o g i c a l r e m a i n s
the deed of concession should omit special stipula- 21. The deed of concession should define the obliga-
tions which are not imperative. tions of the excavator during and on completion of
his work. The deed should, in particular, provide for
i n t e r n at i o n a l c o l l a b o r at i o n guarding, maintenance and restoration of the site
15. In the higher interest of archaeology and of inter- together with the conservation, during and on com-
national collaboration, Member States should encour- pletion of his work, of objects and monuments uncov-
age excavations by a liberal policy. They might allow ered. The deed should moreover indicate what help if
qualified individuals or learned bodies, irrespective any the excavator might expect from the conceding
of nationality, to apply on an equal footing for the State in the discharge of his obligations should these
concession to excavate. Member States should encour- prove too onerous.
Classification of Materials
128
129
creates a mortar that becomes increasingly hard and react with silica, alumina, and iron oxides to create
durable as it loses water and reacts with atmospheric silico-aluminous bonds that react even in the presence
carbon dioxide. The acquisition of hardness and of excess water. Based on these discoveries, the indus-
durability is better known as “setting” and, chemically trial manufacture of hydraulic limes as we know them
speaking, is a carbonation. The physical/chemical today began.
changes that occur within the mortar mixture during Today there is a rough categorization of hydraulic
this process begin, at first, with the contraction of the limes:
lime mass due to the loss of water from absorption
• Natural, if obtained from clayey limestone baked at
into the surrounding masonry and from evaporation.
1000°C
The loss of water begins to create compactness in
• Artificial, if obtained by mixing hydraulic lime with
the lime mixture, inducing the initiation of absorp-
pozzolanic or hydraulic aggregates
tion and reaction with atmospheric carbon dioxide
(carbonation, reaction 3 above), which gives rise to The index of hydraulicity of lime (l) is expressed as
the formation of elongated crystals of calcium carbon- the following equation:
ate. These crystals create a regular, stable crystalline
Clay-based impurities: SiO2 + AlO3 + Fe2O3 = l
network with the added aggregates, making a viable
strong masonry mortar. Calcareous component: CaO
The higher the hydraulicity (l), the more hydraulic the
hydraulic lime quicklime. Traditionally limes are classed as follows:
In the third century bc the Romans developed tech-
niques and recipes to obtain so-called hydraulic lime • 0.01 (l) = aerated lime
mortars that could set underwater and remain resis- • 0.1 to 0.16 (l) = minimally hydraulic lime
tant to deterioration in submerged contexts. The cre- • 0.16 to 0.3 (l) = medium hydraulic lime
ation of these mortars allowed for the construction of • 0.3 to 0.4 (l) = hydraulic lime
aqueducts, sewers, and artificial harbors that are still • 0.4 to 0.5 (l) = highly hydraulic lime
in operation today. The significance of these accom- The compressive resistance of hydraulic lime–based
plishments is that they were created with mortars with mortars is directly proportional to the silica content.
slaked lime (Ca(OH)2 + n H2O) as their binder, which Setting occurs in two phases: rapid initial setting is
does not properly set in wet or high-humidity condi- due to the hydration of the hydraulic bonds; slow
tions and is susceptible to the effects of water. The setting is due to the carbonatization of the calcium
slaked lime was altered through the addition of spe- hydroxide (Ca(OH)2).
cific aggregates, so-called hydraulic or pozzolanic, that
endowed the mortar with water-resistant properties. Hydraulic (Pozzolanic) Behavior and Aggregates
The fact that the Romans did not discover hydrau- historical background
lic lime in itself can be attributed to strict regulation Both the Greeks and the Romans understood that
governing the manufacture of lime in the empire. volcanic aggregates, once pulverized and mixed with
Only calcium carbonate materials free of clay impuri- lime, gave a good-quality mortar that would set in and
ties were used to make lime, and after cooking the be resistant to fresh- and saltwater conditions. The
long duration in slaking pits automatically led to the Greeks used volcanic tufa from the island of Santorini,
segregation of any possible hydraulic constituents. The which still enjoys widespread use today in the eastern
need for mortars that could set underwater and not be Mediterranean under the trade name Santorini Earth.
adversely affected by prolonged exposure to moisture The Romans employed the reddish volcanic tufa wide-
led Roman architects to experiment with the types of spread around the Bay of Naples and, in particular,
aggregates that could be combined with lime. from Pozzuoli, which is what gives the name “poz-
Historically, beginning in the sixteenth century zolanic” to any volcanic aggregates that endow similar
stone materials with large amounts of clay impuri- properties. Where neither of these or other volcanic
ties began to be used as a source of lime, resulting tufa sources were available, both the Greeks and the
in a grayish-brown quicklime that had the ability to Romans employed tiles and bricks to achieve hydrau-
set in wet environments. These were the first true lic mortars. Accordingly, any aggregates derived
hydraulic limes. Only in the nineteenth century did from pulverized fired clay are known as “artificial
chemists demonstrate that firing limestone with clay pozzolanic.”
impurities to 1000°C would yield lime that would
properties u s e o f h y d r a u l i c a g g r e g at e s
ASTM on cements, Des. C340-58 T, defines hydraulic Many ancient features and structures contain lime
aggregates as “silica or silica-alumina based materials mortar with hydraulic aggregates to seal or protect
that, in and of themselves, do not have binder prop- them from the effects of water (aqueducts, water
erties. Once pulverized and combined with water, pipes, bath, cisterns, and the ground course on build-
however, they will react with calcium hydroxide ings, to name a few). Such aggregates were used inten-
(Ca(OH)2) at room temperature to form compounds tionally in these contexts to create a resistant hydraulic
with binding properties.” It should be noted that this lime that is distinct for its durability in the face of the
definition speaks not to the nature of the aggregates effects of water and wear. Lime mortars with such
but rather to their ability to combine with calcium aggregates are characterized by extreme hardness and
hydroxide in the presence of water. Consequently, the low porosity.
ability of aggregates to create hydraulic properties is, Even today hydraulic aggregates can be useful in
in the context of conservation, the capacity to react the treatment and preservation of ancient and his-
with calcium hydroxide and harden underwater. torical features and structures. The addition of such
aggregates to lime, whether hydrate or hydraulic, will
n at u r a l h y d r a u l i c a g g r e g at e s endow useful and interesting characteristics on the
Natural hydraulic aggregates are derived from molten mortar, such as:
rocks ejected and formed during volcanic eruptions
• The ability to set on damp/wet walls and in wet or
and activities. Liquid magma is typically broken into
humid conditions
small droplets when propelled into the air during an
• Good resistance to rain and runoff
eruption and undergoes sudden cooling that effec-
• Greater hardness than found in mortars of lime
tively crystallizes the unstable physical structure into a
and regular sand
solid. This instability renders such volcanically derived
sands and soils susceptible to attack by the high caus-
Aggregates
ticity of lime and leads to the particular chemical
As has already been mentioned, aggregates can be
reaction that creates hydraulic properties. Among the
defined as materials added to binders, as well as the
most common volcanic aggregates, one can list:
structural elements within a mortar and held together
• Pozzolanic soils themselves by the binder. Any classification of aggregates can at
• Soil from Santorini (Greece) best be considered incomplete and open to interpreta-
• Bavarian Trass tion. For this reason, only the primary physical char-
• Compact volcanic tufas (Tarquinian and Romanian acteristics of aggregates are listed here. The physical
tuffs) characteristics influence the strength and durability
• Natural clays, fired and hardened by volcanic of the mortar. In general ancient mortars used river
activity sands from the relative vicinity of the work site. The
• Diatomaceous earth preference for river sands was for specific reasons:
All these minerals have a very high silica content and • Near-total absence of soluble salts
can be used as hydraulic aggregates once pulverized or • Rough surface texture due to slow erosion by river
ground. currents
• Variable mineralogy and size, guaranteeing a
a r t i f i c i a l h y d r a u l i c a g g r e g at e s selection of grain size and limited porosity related
This category includes the following: to a sand’s location in a river, whether from the
riverbank or the river bed, leading to natural
• Calcined clays (brick, clay, or ceramic dust or
segregation
pieces)
• Fly ash, produced in large quantities by power All these properties help to ensure a good-quality
plants mortar. A rough surface guarantees proper bonding
between the added aggregate and the lime binder,
Both of these artificial aggregates are predominantly
while the varied mineralogy excludes overly porous
silica and alumina, making them analogous in behav-
sands that would be too absorbent. Variable grain size
ior to natural hydraulic aggregates.
limits shrinkage. Being river sourced eliminates the
possibility of soluble salts, ensuring that the mortar
will not be hygroscopic and eventually destroyed by excessive shrinkage from the loss of water that occurs
the constant cycling between dissolution and crystal- during setting. Soluble salts, on the other hand, can
lization of salt crystals. compromise the hardness of the mortar once the dry
Beach sands are practically antithetical in their phase is reached. Mortars prepared with marine sands
properties: are very rare, most likely because their instability leads
to limited preservation. Those that have survived
• Strong presence of soluble salts, predominantly
display very low cohesion, fragility, and susceptibility
sodium chlorides (NaCl)
to mechanical damage, as well as the tendency to salt
• Smoother grain surface due to the stronger and
efflorescence.
abrasive action of ocean currents, waves, and wind
Mortars prepared with crushed porous limestone
• A more uniform grain size due to continuous wave
aggregates, such as travertine, tend to have little hard-
motion
ness and are highly hygroscopic.
• A more uniform mineralogical composition due to
Siliceous sands yield hard mortars that can be too
coastal erosion
rigid in cases of extreme daily or seasonal thermal
A smoother grain surface allows for less bonding to changes, leading to detachment of the mortar from
the lime binder, while the more uniform grain size the applied archaeological or historical substrate.
creates the potential for cracking of the mortar due to
Consolidants
133
Primal®, mixed with 3 volumes, say, 300 ml may not be needed and thus have to be stored. This
of water, will yield a 400 ml solution in which is especially important because many polymers will
the Primal® is present at 100 ml. The actual progressively lose some of their physical and chemical
dilution ratio is therefore 100:400, or 1 to 4, and characteristics. Many polymers will eventually yellow.
the real dilution would be Accordingly, any stored solution that already has a yel-
100 × 100 lowish tinge or color should be discarded.
X= = 25% All containers are to some extent permeable to
400 vapors, especially more volatile (organic) solvents.
Rather than a percentage dilution, the proper Consequently, it is good practice to draw a line on
way to indicate this would be to give the ratio 1:3 the exterior of the container with an indelible marker
(v/v) as the dilution. (e.g., lead pencil) indicating the level of the solution
and the date. If the level of the solution is later found
Based on this, the three common forms of creating to be lower than the line, this can be used then as a
dilutions may appear to be similar but do not produce guide to top off the solution with solvent. As long as
the same percentage of dilution. the same solvent is used as in the original solution, the
desired concentration should be maintained. This is
an easy, yet necessary, control, as solutions can poten-
Labeling tially double in concentration in six months due to
To be of any use, a label should contain the following solvent evaporation.
types of information: In the case of emulsions, separation and sedimenta-
• Name of dissolved substance (e.g., consolidant or tion, with the heavier particulates sinking to the bot-
resin, Paraloid®) tom of the dilution, should be understood as common
• Concentration or dilution or ratio when stored. Consequently, before it is used an emul-
• Name of diluting liquid (solvent) sion should be agitated for a few minutes to ensure a
• Date of manufacture more homogeneous solution.
Care should be taken to store prepared consolidant
As an example: solutions away from direct sunlight and any electrical
sources or outlets, as well as areas of possible tem-
20% Paraloid® B-72 (w/v) perature fluctuations, such as near radiators or water
in Acetone pipes. Emulsions should not be exposed to freezing
04/04/2012 temperatures, as this will cause the separation of water
and resin and make them ultimately useless.
Finally, a fire extinguisher should be readily avail-
Storage able in any area where solvents and solvent solutions
In general, it is good practice to prepare solutions only are kept or stored.
as needed and not to prepare large quantities that
Silica Gel
(heating, ventilation, and air-conditioning) system that on-site (e.g., 250 ml, 500 ml, 1,000 ml, and 3,000 ml
regulates temperature and humidity. Conventional containers) and ready-made quantities of conditioned
measurements should thus be seen as a rough guide- silica gel in perforated plastic bags or small cloth
line but not fully applicable to archaeological contexts. sachets (bags of 10 g, 50 g, and 100 g).
Instead, in general, it is advisable to double or signifi-
cantly increase the amount of silica gel per volume of
air to mitigate less controlled ambient conditions of Duration of Efficacy for Activated
storage, such as using 40 grams per liter of air. Silica Gel
There are at least two reasons that increased silica Even the most hermetically sealed container will even-
gel is beneficial for the storage of metallic archaeologi- tually allow air to enter and its subsequent moisture.
cal materials: Any container with silica gel employed on-site dur-
• Artifacts or materials may contain discrete ing excavation should be used as a transitional and
amounts of moisture in the obscuring soiling or preservative measure between the potentially damag-
layers of corrosion. ing uncontrolled in situ environment and the more
• The moisture present within an artifact or material controlled conditions of the conservation laboratory
may exceed the capacity for absorption of the or medium- to long-term storage. When deployed
smaller amounts of silica gel, potentially negating on-site, especially for metal artifacts or other sensitive
its use altogether. materials, these containers should be moved to more
stable environs within 24 to 36 hours at the most.
For simplicity and ease of operations, it is beneficial
to have a range of airtight containers readily available
137
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
Date of input:
Prepared by:
Signature:
138
Unearthing Objects and Structures • Plastic stretch film (sold for food preparation and
storage, i.e., cling film or Saran Wrap);
(see chap. 4)
• Biocides;
• Semiflexible metal spatula, like those used for • Metal props, adjustable stakes and/or poles such as
painters’ palettes; wooden or plastic spatula, such those used for tents.
as tongue depressors;
• “Decorator”- and “artist”-type paintbrushes in both Straps and Bandages
round (gradations from 0 to 3 cm widths) and rect- • Nylon luggage straps or bungee cords;
angular (varying widths from 2 to 8 cm and 2 cm • Polypropylene webbing and strapping commonly
thickness) sections of soft and semisoft natural and used for packing and moving;
synthetic bristles of variable length; • Velcro strips;
• Hand brushes of the type typically used for brush- • Rubber bands or flat elastic bands (latex) for
ing clothing or polishing shoes, in natural and syn- clothing;
thetic bristles of variable hardness and length; • Polyethylene sheeting for industrial packing;
• Fine electric vacuum with filters; • Jute and cotton medical bandages;
• Natural and synthetic sponges of variable density; • Elastic medical bandaging, such as ACE™ bandages;
• Spray bottles to nebulize and mist water; • Elastic medical tubular net;
• Absorbent paper towels; • Lengths of wood for splints.
• Japanese tissue.
Temporary Facing
Stabilization during and after • Cotton gauze;
Excavation (see chap. 7) • Japanese tissue/paper;
• Paraloid® B-72, in a 20% w/v solution with a vola-
Temporary Shoring, Reinforcement, or Support tile solvent (e.g., Acetone);
• Wooden shoring and pickets; • Primal® 33 in a 5% dispersion, v/v;
• Various blocks and lengths of wood for creating • Various common solvents, such as water, acetone,
reinforcements, as well as wooden boards and ply- and ethyl alcohol;
wood sheets for supports; • Mowilith DMC2 (polyvinyl emulsion);
• Wooden wedges of differing dimensions and • Polyvinyl alcohol (PVAL) in grain/powder to dis-
angles, from thin shims to thick wedges; solve in hot water or polyvinyl acetate (PVAC) in
• Different types of wood saws (wood, Japanese, and grain/powder to dissolve in ethyl alcohol;
hack), hammers (claw and ball and ping), various • Natural-fiber brushes of varying length and
types of nails (from brads to roofing nails); softness;
• Polystyrene foam sheets or other forms of padding • Polyethylene containers for keeping solutions and
of a thickness of 2 to 3 mm; for rinsing and cleaning brushes.
• Geotextile;
• Polyethylene foam sheets, typically used as insula- “Emergency” Adhesive Preconsolidation
tion for houses, or other lightweight sheeting in 5, on Immovable Features (see chaps. 7 and 9
10, and 20 mm thicknesses; and Appendix 3)
• Polyurethane foam sold as an aerosol spray or as • Slaked lime putty and hydraulic lime;
two components to be mixed; • Pulverized brick (terracotta) or any other pozzo-
• Aluminum foil (sold for food preparation and lans in a pulverized form;
storage); • Fine sand (variable grain size from 0 to 2 mm);
139
Personal Protective Equipment • First aid kit complete with list of contents and
manual for use (periodically check for expiration of
• Suits, overalls, or protective garments in Tyvek, PE, pharmaceuticals and medicines);
or cotton; • Telephone numbers of pertinent professionals and
• Safety shoes and footwear; professional entities, including medical and fire
• Safety gloves of hide for medium- to heavy-duty department;
handling, as well as nitrile gloves for working with • Telephone numbers and addresses of relevant
most common solvents; services and suppliers, including art supplies, hard-
• Dust masks and protective filtered full- or half-face ware and lumber, packing and storage;
masks for smoke and chemical aerosols and vapors; • Common sense (not for sale).
• Polycarbonate face shield or protective glasses;
• Safety helmet of polyethylene or other suitable
material;
143
for his discussions on biocides and the timing and of Borgo San Dalmazzo, province of Cuneo, who, not
means of their application. being a conservator but a religious man, still perfectly
For the chapter on consolidation, once again I must understood and supported an intensive and ambi-
thank the aforementioned Vinicio Furlan, Renato tious conservation program of the splendid crypt and
Pancella, Ottorino Nonfarmale, Paolo Mora, and archaeological area of his parish church.
Laura Mora Sbordoni, as well as Eddy De Witte of the One last remembrance and acknowledgment of the
Royal Institute for Cultural Heritage (IRPA), Brussels. late Anne Feton for her steadfastness and respect for
I must also take the opportunity to thank all those the professional ethics that she always knew how to
who have made it possible for me to practice this pro- apply to the conservation of artistic and archaeologi-
fession for over thirty-five years. cal patrimony.
The section on techniques of detachment and A special thank-you to Corrado Pedelì, my coau-
lifting of wall and floor coverings would have been thor, for his precision and professionalism, which have
impossible to write without the firsthand experi- been a powerful incentive to constantly question the
ence of watching Paolo Mora, Laura Mora Sbordoni, accepted knowledge and to strive for greater under-
Sabino Giovannoni, Ottorino Nonfarmale, and Sergio standing. We found ourselves discussing conservation
Lancioni and the years of experience, at times with issues and techniques that we tend to take for granted.
my heart in my throat, thinking about and re-creating His ability to see things from a different perspective,
that which they had taught me. especially that of those who may not know or be of the
The section on labeling and data recording is based same opinion, was a great stimulus and influence on
on various principles masterfully expressed by Liliane the ultimate shape of this book.
Masschelein-Kleiner at the IRPA, Brussels, and the And finally a special thanks to Gian Carlo Bojani
late Jeanne-Laurence Guinand. and Anna Lega, formerly director of the International
Long-term preservation is a topic that I was able Museum of Ceramics (MIC) in Faenza and coor-
to develop only because of my various discussions dinator of the Department of Conservation for the
and experiences over the years with Renato Perinetti, MIC, respectively, for their trust and support in this
Luisella Peyrani Baricco, and Charles Bonnet. I should endeavor.
also add thanks to Don Giovanni Quaranta, pastor Stefano Pulga
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Note: Page numbers followed by f and t indicate archaeological excavation. See excavation
figures and tables, respectively. archaeological relevance, 4–5
archaeological sites. See sites
absolute humidity (AH) architectural elements. See immovable features
in burial environment, 15–16 artifacts. See also specific types
definition of, 16, 16f reliability of information from, 7
and temperature, 15–18, 16f, 17f assessment of materials, 39–52
acrylic emulsions in immovable features, 39–42
in consolidation, 81 in movable objects, 43–52
in stabilization, 68, 68f, 69f atmospheric gases, in soils, 13
acrylic resins awning fabrics and textiles, 55
in consolidation, 78–79, 81
in detachment, 85 bacteria, biological attack by, 73, 74–75
adhesive consolidation, 77–78, 80–81 bactericides, 74–75
adhesives bandages
in detachment, 84–85 in detachment and removal, 88t
in stabilization, 68–69 in stabilization, 66–67, 66f, 67f, 139
aerated lime, 129–30 barium hydroxide, 79
aerial binders, 21–22 binders, 21–23, 129–31
aggregates, 21–23, 130–32 definition of, 21
in capping and repointing, 118, 120–21 deterioration of, 21–23
definition of, 21, 23, 131 in immovable structures, 21–23
deterioration of, 23 properties of, 21–23, 129–31
in immovable structures, 21–23 biochemical treatments, 76
properties of, 23, 130–32 biocides, 72, 74–76
AH. See absolute humidity biodeterioration, definition of, 71. See also biological
algaecides, 74–75 attack
alloys, 23–25, 23t biological attack, 71–76
deterioration of, 24–25 biochemical treatments for, 76
identification and assessment of, 44–46 biocides for, 72, 74–76
life cycle of, 24, 24f criteria for treating, 71–72, 73f
properties of, 24 definition of, 71
alteration direct vs. indirect methods of prevention of,
of buried objects, 14–15 71–72
cleaning as cause of, 93 identifying type of, 73–74
definition of, 21 recognizing signs of, 73
vs. deterioration, 21 bleach, 74
of excavated objects, 3 block lifting, 88–92
aluminum foil, in climate wafers, 62 supported, 90–92, 92f
aluminum powder, in consolidation, 81 unsupported, 89–90, 90f
animal glues, in detachment, 84–85 bone, 28
antibiotics, 76 deterioration of, 28
Aosta Valley (Italy) identification and assessment of, 50, 50t, 51t
Department of Cultural Heritage of, 9, 61, 62, 72 properties of, 28
first aid operational units in, 10 bracing, stabilization with, 63–64, 64f
151
62, 72 emulsions
Culture, Italian Ministry of, 83 acrylic, 68, 68f, 69f, 81
cushioning, in preliminary packing, 97t, 101–2, in consolidation, 78, 81, 133–34
101t, 102t documentation of, 134
cyclododecane, 88t in stabilization, 68, 68f, 69f
environmental issues, 13–20. See also climate; soil
damage. See deterioration with buried objects, 13–18, 14t, 15t
damp cleaning, 95 in preliminary packing, 97t
debris, in consolidation, 82 enzymes, 76
decomposition, definition of, 71 equilibrium
decorative elements. See also specific types of buried objects, 13, 14, 15, 17, 18
detachment of, 85–86 loss of, in corrosion of metals, 24–25
stabilization of, 67–68 in organic materials, 27, 28
degradation. See deterioration silica gel and, 104
detachment ethyl silicates, 79–80
criteria for using, 83 Europe, climate of, 137
history of use, 83 excavation(s). See also specific types
of immovable features, 83–86 vs. conservation, goals of, vii, viii, 1, 2
of movable objects, 86–92, 88t, 89t conservation after, 4
principles of, 84 conservation during, 3–4, 6–10, 8f
deterioration, 21–29 factors influencing, 4–6
vs. alteration, 21 vs. messa in luce, 31
of buried objects, 14–15 types of, 4–5
cleaning as cause of, 36, 37n1, 93 UNESCO definition of, 123
definition of, 21 exposed conservation measures, 114–15
of excavated objects, 3
of immovable structures, 21–23 fabrics
of inorganic materials, 21–27 for coverings, 55–56
in messa in luce, 18–20 in detachment, 84
of movable objects, 23–29 in preliminary packing, 101–2, 101t, 102t
of organic materials, 27–29 facing
in storage, 107, 108f in detachment, 84
di-chlorofene, 75 in stabilization, 68, 68f, 69f, 139
dilutions, 133–34 faience, 26t
disintegration, definition of, 71 FAOU. See first aid operational unit
documentation, 111–12 financing
of conservation measures, 111–12 influence on excavations, 6
equipment and materials list for, 140 in planning for conservation, 10
in messa in luce, 33 fine earthenware, 26t
registration and labeling in, 105–6, 140 first aid operational unit (FAOU), 10–11
of stratigraphic layers, 3, 4 duties and responsibilities of, 10–11
template for, 138 equipment and materials list for, 139–41
dry cleaning, 95 profile of, 10–11
fixed features. See immovable features
earthenware, fine, 26t flooding, 83
edging, stabilization with, 69–70 floors. See also specific types
Education, Italian Ministry of, 6 binders in, 22
elastic bandages, 67 detachment and removal of, 83–86
elastic bands, 66 identification and assessment of, 41–42
emergency excavations messa in luce of, 34–36, 35f
challenges of, 7 stabilization of, 67–70
planning for conservation in, 8, 9, 10 types of, 41
rise in frequency of, 7 Florence (Italy), 1966 floods in, 83
long-term conservation of sites in, 117f, 118f, 119f messa in luce, 31–37
ivory, 28 conservation issues in, 18–20, 31–32
deterioration of, 28 conservation techniques in, 34–37
identification and assessment of, 50, 50t, 51t definition of, 18, 20n3, 31
properties of, 28 vs. excavation, 31
phases of, 18, 19f
jute bandages, 66–67 preliminary cleaning in, 31, 32, 34–37
principles of, 18–20, 32–33
labeling, 105–6 of small objects, 36–37
basic requirements for, 106 of structural features, 34–36
materials for, 106, 140 tools for, 34–37, 139
of solutions and emulsions, 134 metal alloys, 23–25, 23t
lead, identification and assessment of, 46, 46t, 47t metal objects, 23–25, 23t
lead alloys, identification and assessment of, 46, deterioration of, 19–20, 24–25
46t, 47t identification and assessment of, 43–46
leather, 29 life cycle of, 24, 24f
deterioration of, 20, 29 properties of, 24
identification and assessment of, 50, 52t pure, rarity of, 23–24
properties of, 29 relative humidity and, 19–20
relative humidity and, 20 metal rods, in block lifting, 91–92, 92f
lifting microclimate
block, 88–92 in coverings and shelters, 53, 54, 55, 56, 61
of detached features, 86 in messa in luce, 32–33
of movable objects, 87–92, 88t, 89t, 140 in preliminary packing, 103–4
lime, 129–30. See also hydraulic lime in stabilization, 65, 66, 67
as binder in structures, 22, 23 minerals. See stone
in capping and repointing, 120 mortar. See masonry
in consolidation, 79, 80–81 mosaic floors
cycle of, 129–30 detachment and removal of, 83–84, 85–86
deterioration of, 23 identification and assessment of, 42
properties of, 23, 129–30 vs. opus signinum floors, 85
types of, 129–30 stabilization of, 68–70
lime water, 79 movable objects. See also specific types
lime-based floors detachment and removal of, 86–92, 88t, 89t
detachment and removal of, 86 vs. immovable features, approach to conservation
identification and assessment of, 42 of, 3, 4, 7
stabilization of, 69 inorganic
localized shelters, 60–62 identification and assessment of, 43–49
logistics, influence on excavations, 5 properties and deterioration of, 23–27
logs, conservation, 111–12 messa in luce of, 36–37
organic
Management of Archaeological Projects (MAP2), 6 identification and assessment of, 50–52
markers, 106 properties and deterioration of, 27–29
masonry walls preliminary cleaning of, 36–37, 93–96, 140
aggregates in, 23 preliminary packing of, 97–104
binders in, 22 stabilization of, 65–67
identification and assessment of, 39–40
long-term conservation of, 116–21 needle-punch textiles, 56
mortar-bound vs. dry, 39–40 netting, 55, 56
mechanical interventions nylon plastic sheeting, 54
for biological attack, 72 nylon straps, 65
stabilization with, 67–70
mercury derivatives, 75 OPD. See Opificio delle Pietre Dure
159
PULGA
PEDELÌ
Conservation Practices on Archaeological Excavations
The relationship between archaeology
and conservation has long been a complex
and challenging one. Yet it is often initial
conservation in the field that determines the
long-term survival and intelligibility of both
movable artifacts and fixed architectural
features. For this reason archaeologists and
conservators must work successfully together
to ensure that recovered material culture—
and the many meanings it carries—is properly
preserved for future generations.
Conservation Practices
on Archaeological Excavations
Getty Publications
(800) 223-3431
www.getty.edu/publications
PRINCIPLES AND METHODS
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