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Pergamon Chemical Enoineerin 0 Science, Vol. 50, No. 16, pp.

2531-2543, 1995
Elsevier Science Ltd
Printed in Great Britain.
0009-2509/95 $9.50 + 0.00
0009-2509(95)00107-7

THE S I N G L E SCREW E X T R U S I O N O F PASTES t

A.S. BURBIDGE and J. BRIDGWATER


Department of Chemical Engineering, University of Cambridge, Pembroke Street,
Cambridge CB2 3RA, U.K.

(Received 18 August 1994)


Abstract--Screw extrusion is widely used but little is known about the design and operation of this type of
equipment save in the polymer industry. Particularly with the advent of high-performance, high-value
ceramic materials, it has become important to extend knowledge. Here a mathematical model for a flooded
screw brings together recent paste rheology and a model of screw extrusion developed previously for
frictional solids flow. The model suggests that helix angles in current use are significantly below the
optimum. Furthermore it appears that the deepest channel screws will produce the highest pressure
gradients, a fact already established in practice which is in contrast with screws for polymers. Experiments
both with and without flow on a 20 mm diameter laboratory extruder used screws of varying angle and
channel depth with pastes of various rheologles. Pressure measurements from experiments without flow
could show a marked offset from predictions with screws of low helix angles, this apparently being the result
of an increased surface shear stress at the barrel-paste interface. The effects of changing the screw speed
were reliably predicted. Experiments with flow carried out on a 76 mm diameter industrial machine showed
general consistency with predictions.

INTRODUCTION metal extrusion for use with stiff pastes thus allowing
Ceramic extrusion requires the mixing of a refractory prediction of the effects of changing die length and
powder (the solid phase) with a liquid phase such as diameter. They were the first to separate and analyse
water with starch, glucose or methyl-cellulose added the flow into two distinctly different regions, firstly
as rheology modifiers to improve the paste flow prop- a die entry region in which the effects arise due to bulk
erties. Solid phases such as clay may be added as deformation and secondly a dieland region in which
binders in order that the green product has sufficient wall frictional shearing terms dominate. It will be
strength and can be handled. These also influence the noted that there is a large extensional flow component
rheology. An extrudate so formed can then be dried in the die entry region. Benhow (1971) showed that
and sintered, removing the liquid phase and burning pressure generated, P, due to extension in the flow of
out any binders that may have been added, to form catalyst pastes from a barrel of diameter Do into
a finished ceramic product. Similar thinking applies in a circular dieland of diameter D and length L was
many other areas including food processing which given by
have been listed by Benbow and Bridgwater (1993).
Until recently paste extrusion has remained poorly P = 2(a0 + ~V)ln(Do/D) + 4(L/D)(To + flV) (1)
understood with the only reported applications being
empirical ones largely concerned with the extrusion of where V is the mean extrudate velocity in the dieland
bricks and china clays. Processing conditions were and the extrusion parameters are as follows: a0 is the
not as critical as for plastics since the final product is initial bulk yield stress of paste, • is the velocity of
made to a lower tolerance. The requirement for low- bulk yield stress, z0 is the initial wall shear stress of
cost, poor-tolerance products can be associated his- paste and fl is the velocity factor of wall shear stress.
torically with a "black art" approach to ceramic screw The parameters a0 and ~ describe the influences due
extruder design. Scientific publications concerned to extension caused by changes in cross-sectional area
with the theory of single screw extrusion of paste are and Zo and fl describe these due to shear during flow
therefore very limited. along a duct of constant cross-section. The material
However, Ovenston and Benbow (1968) studied the flows as a plug due to the existence of lubricating
effects of die geometry on the extrusion of clay-like layers at external surfaces. Zo and fl are related both to
material in the preparation of catalyst supports. Ex- the properties of the solid phase and those of thin
perimental results were used to make critical compari- layers of uncertain structure near to the surface.
sons between the expressions developed by previous Recently, Benbow et al. (1987) further developed
workers. They further developed the theory of soft the theory to deal with dies of more complex ge-
ometry. They modified the previous expression as
follows:
Work performed at IRC in Materials for High Perfor-
mance Applications and Department of Chemical Engineer- P = (go + ~V)In(Ao/A) + L(C/A)(zo + flV) (2)
ing, The University of Birmingham, Edgbaston, Birmingham
BI5 2TT, UK. where the nomenclature is as before except that
2531
2532 A.S. BURBIDGE and J. BRIDGWATER

Ao and A are the cross-sectional areas of the die entry others, argued that this system may best be described
and dieland regions, respectively, and C is the wetted by a modified McKelvey et al. (1953) approach, i.e. by
perimeter of the dieland. solution of Navier-Stokes-type equations for a power
The present purpose is to develop the theories of law fluid.
Benbow et al. to provide a method of predicting the
ANALYSIS
pressure generation in a single screw extruder for
Consider a single screw extruder of average screw
pastes and to assess the validity of the approach.
helix angle ~b(Fig. 1) that is fully flooded with paste. In
SINGLE SCREW OPERATION addition let the screw be of constant pitch and chan-
nel depth and fitting closely inside of the barrel such
A simple representation of the process of single
that there is no clearance between the screw flight and
screw extrusion can be given as follows. The ceramic
the internal wall of the barrel. There is then no leak-
is first dropped into a feeding hopper from whence it
age of paste between the flight tips and the constrain-
falls onto a rotating single flighted screw. The screw is
ing wall of the barrel. If the pitch and channel depth
driven by a motor through a linkage and gearbox
were not constant, then the analysis to follow would
assembly. Friction between the material and the bar-
be more difficult since the extension of the paste in the
rel causes the paste to be conveyed towards the die
channel would also be need to be included.
assembly, where sufficient pressure is generated to
Let an angular velocity be imposed on the whole
drive the paste through the die to give an extruded
system such that the channel of the screw is stationary
product. Use of the single screw extruder is widely
and the barrel rotates to compensate for this. If the
established in forming processes. Many variants of the
effect of curvature of the channel is assumed to be
basic design exist and there are also twin and multiple
small as is commonly the case, then the channel can be
screw machines, the analysis of which is beyond the
unrolled and treated as a long rectangular groove
present scope. A theoretical analysis of a single screw
[Fig. l(c)]. The groove containing the paste will then
system processing pastes has remained elusive, design
have the moving surface of the barrel sliding across
being either empirical or copied from machines used
the top surface providing a force component which
in the polymer industry.
generates pressure and conveys paste along the chan-
Grunwell (1928) reported on extensive experiments
nel. It is further assumed that the screw is single
out on a high-tonnage industrial brick extruder. He
frighted, i.e. it is a single helix, and that the width of
produced machine-specific correlations for the effi-
the flight is negligible; these restrictions could be re-
ciency of single, double and triple winged augers but
laxed readily. The screw is taken to be fully flooded
was unable to develop any generally applicable in-
having paste contact with all three sides of the screw
sights. Similar studies were carried out by Reed (1962),
and with the barrel internal surface. Adaption to
by Johnson (1962), who experimented with clay pipe
account for the existence of one free screw surface
extruders, and by Lund et al. (1962), who empirically
requires a simple adjustment, leaving open the ques-
established optimum design characteristics for many
tion as to what conditions cause a face to lose contact
types of auger.
with the paste. Forces due to the weight of the paste
Parks and Hill (1959) appear to have produced the
are insignificant and may be expected to only be
only design model for screw extruders with ceramics
influential near the paste inlet. It is further assumed
to date. They took the work of Darnell and Mol
that the inner wall of the barrel is of sufficient rough-
(1956) who sought to develop a model for stress gen-
ness to ensure that the paste does not slip over the
eration during the feeding of solid particles, the mater-
surface. Work by Benbow and Bridgwater (1993) illus-
ial behaving as a frictional solid. A change was incorp-
trates that although gross surface roughness (rough-
orated such that the plug was assumed to be in con-
ness height/radius of dieland = 0.28) produced an
tact with only two of the three surfaces of the screw,
increase in pressure gradient in a circular pipe, smaller
i.e. the trailing face of the flight was assumed to be
(0.10) surface undulations produced little detectable
a free surface. This feature was included since such
pressure rise. It is thus likely that the effect of surface
behaviour had been observed widely in screw ex-
finish on the operation of a machine will not be great
truders working with clay. The weakness of this model
provided excessive surface lubrication is avoided.
is that it relies upon coefficients of friction between the
Consider now a stationary screw of diameter
surfaces of the machine and the extruding material.
D, with a channel depth h and average helix angle
Not only have these proven difficult to measure accu-
around which a barrel is allowed to rotate at a rate
rately even for single-phase systems composed of
N [Fig. l(a)]. Paste is extruded at a volumetric flow-
powders and granular solids (Darnell and Mol, 1956),
rate Q. Let the width of the channel measured normal
this tribology is not appropriate for a paste.
to the flights be w. The development proceeds in two
Work similar to that of Parks and Hill (1959) has
stages. Firstly geometric relationships between the
been done by Jasberg et al. (1979) for the extrusion of
barrel and paste plug velocities are derived. Secondly
defatted soy flakes. They argued that the flakes flowed
these are employed in a force balance on the paste.
as a solid plug and that the approach of Darnell and
v,, the relative velocity vector of the barrel surface
Mol could be effective. Experiments on the hot extru-
with respect to the paste plug, is given by
sion of polymer/ceramic mixtures designed for injec-
tion moulding by Mutsuddy (1987, 1989) amongst v, = v~ - vp (3)
The single screw extrusion of pastes 2533
l Flowrate,
Q
(a)
vb = 7r.D,N

Velocity triangle (b)


n-Ds

L
Geometric triangle

I
I I

I I
I I

(c)
I Section of unrolled channel
Ds ~.-1
I
I

Fig. 1. Notation for and modelling of the single screw extruder.

where vb is the relative velocity vector of the screw and By the geometry of the velocity triangle [Fig. l(b)]
barrel and vp is the velocity vector of the paste plug
along the channel [-Fig. l(b)], va is the vector velocity
Ivz,I tan ~ nD~N tan ~b
Iv, I =
component of the paste plug along the axis of the (tan 0 + tan tp) cos 0 = (tan 0 + tan ~b)cos 0"
screw, i.e. perpendicular to the plane of rotation. Now, (6)
[va [ = Ivr [ sin 0 (4) Using eq. (4),

where 0 is the forward angle of movement of the paste riD, N tan 0 tan ~b
Iv~[ = (7)
relative to the plane of rotation. The overall flowrate tan 0 + tan q~
Q is given by the product of the flow area measured
perpendicular to the axis of the channel and the axial and also
velocity, i.e.
I%1 tan ~ sin 0 7tD~N tan 0
7l" 2 ]Vpl = (tan 0 + tan ~)cos 0 sin ~ = (tan 0 + tan ~p)cos ~"
O = ~[D~ - ( D s - 2h)2]lval (5)
(8)
2534 A.S. BURBIDGE a n d J. BRIDGWATER

Expressions for Iv, I, Ivol and Iv~l have thus now been Cs
P = Fv, cos (0 + ~b) - --Fvp (15)
established in terms of nD~N. A relationship between Cb
the superficial speed of the barrel wall, Ivbl, and the
volumetric flowrate of the paste is thus or alternatively, using the geometry of a rectangular
channel,
7t 2 nD~ N tan 0 tan q~
Q=~[D~-(D,-2h) 2] tan0+tanq~ P=fv, cos(O+dp)- l+ Fvp (15a)
(9)
P provides a description of the pressure generation
or, in a dimensionless form,
per unit length of screw, and is controlled by the
4S tan 0 tan 4~ (10) values of the other five groups. ~b is the mean helix
R =
-- ~z2EI - - ( I - - T ) 2 ] tan 0 + tan ~b angle of the screw, and Tis a geometric factor describ-
ing the channel depth of the screw. Fvr and F~p provide
and so a description of the rheology of the paste coupled with
= x R . a geometric allowance for the relative surface vel-
0 tan- I(ta--ntan~b)
- R_]l (11) ocities at the barrel and screw surfaces respectively.
Since the rheology of the paste is the same in both
Here cases, Fo, and Fop are related and are not independent.
Finally there is S, a flowrate function.
Q (a dimensionless flow rate)
s=gb2 The steady-state operation of a rectangular chan-
neled screw can therefore be described by eq. (15)
2h together with eqs(10) and (11). Equation (15) can
T = -- (a dimensionless channel depth).
- - Ds readily be developed to use a four-parameter rheology
where % = Zo + f l v
We now have a set of relationships for the movement
of the barrel and the plug in terms of the forward feed AsincpdP_(zo + fllv, I) c~(~o+/~lv.I) (16)
angle of the plug 0, rotational speed N, inner diameter co Zo d x Zo CbZo
of the barrel Ds, and helix angle 4~ of the screw.
or a six-parameter rheoiogy (Benbow and Bridgwater,
In steady-state operation, the force balance acting
on a paste plug over an elemental length of the chan- 1993) where % = z0 + fltv"
nel dL [Fig. l(c)-I indicates that the component of Asin~b dP (Zo + / ~ l v , l") c~(ro +/~alvpl")
- (17)
barrel surface force acting along the screw channel Cbro dx *o Cb"C0
opposes the drag force due to the screw surface and
the force due to the back pressure. Thus
DISCUSSION OF M O D E L
c~%, cos(0 + $)dL = C,%pdL + A d P (12)
We now turn to consider the consequences of the
Where %, is the surface shear stress acting in the model and also provide some experimental evidence
direction of v,, %p is the surface shear stress acting in from equipment of two different scales.
the direction of Vp and c~, c, are the perimeters of (i) Numerical evaluation--current systems. Equation
contact between the paste and the inside surface of the (15) contains the related groups _Fo, and _Fvp. Thus,
barrel and the paste and the screw respectively. A de- introducing
notes the cross-sectional area of the channel. Hence,
G = finDs N
dP
A~=c~,%,cos(O+dp)-Cs%p. (13) -- "~0

we get
Introducing the length variable x which is measured
along the screw axis [Fig. l(b)] and rearranging, we { [ tan~p l } c o s ( 0 + cp)
have P= I+G (tan 0 + tan 40 cos 0

Asin~dP
Cb~o d x
%,
= --cos(0
~o
+ ~b) -
Cs%p
---
cb Zo "
(14)
T 1+ _[,tan0+-~a~-~)cos
tan0 6J)
(18)
This describes the behaviour of an extruding channel
whatever the geometry. Defining further dimension- with 0 defined by eqs (11) and (10) and thereby being
less groups as follows, a function of S, T and ~b. Hence the dimensionless
pressure gradient P. can be defined by G, S, T and 4~.
A sin q~dP Some standard values of G, S, T and ~b are known
P = - - (a dimensionless pressure gradient)
-- cb Zo dx from the design of extrusion machines but, for some,
a more detailed analysis is required. We consider each
ox = zv--5~ (a ratio of dynamic to static shear stresses) of the four dimensionless groups in turn:
Zo q~, the average helix angle of the screw, is usually
yields between 18 and 25 ° in the plastics industry, and from
The single screw extrusion of pastes 2535

20 to 22 ° in the ceramics industry. The values of 18, If the helix angle ~bis increased from 18 to 24 ° with
20, 22 and 24 ° are chosen for assessment here. all other variables held constant, then the pressure
T is the value of 2h/D, which is commonly 0.6 for gradient increases by a factor of about three with little
ceramic systems. Values of T examined are 0.4, 0.5, 0.6 drop in the forward feed angle, 0. This suggests that
and 0.7. a 24 ° screw could deliver the same volumetric flow as
G covers a broader range of values being dependent an 18° screw but at a higher outlet pressure. Thus
on the size of machine and the type of paste being a helix angle of 24° would give a shorter axial length
extruded. For practical machines, the values of D are of screw.
approximately between 0.02 and 0.50 m, with the Increasing the channel depth Tofthe screw predicts
screws generally rotating at around 0.5 rev/s. The an increase in the pressure gradient and a decrease in
values of ~o and fl can be found from typical paste the forward feed angle 0. This is due to continuity
formulations: ro varies between 0.030 MPa for an since the volume flowrate is constant and the cross-
alumina gel to about 0.048 MPa for an alumina and sectional area of the channel is proportional to T.
clay mixture; values of fl range between 0.200 MPa Hence the pressure increases since the value of Iv~ and
s/m for plasticene to about 3 MPa s/m for alumina hence the drag at the screw surface are inversely
gels heavily loaded with zeolites. The maximum and related to the flow area. This effect is partly opposed
minimum values of _G calculated are therefore 78.5 by the small increase of resisting surface area due to
and 0.13 respectively. The values of G_Gconsidered
_ are the increase in channel depth. This leads to the con-
0, 10.0, 30.0 and 50.0. clusion that the deeper the screw channel, the greater
S is a flowrate function, and cannot be assessed the pressure gradient it can generate. This may ex-
without knowledge of the die used. Dimensional anal- plain why screws designed for extruding ceramics are
ysis and analysis of data on the range of conditions generally deeper than those used for polymers.
employed by manufacturers (Benbow and Bridgwater, Considering the effect of varying _G reveals much
1993) suggest that Q should be proportional to D~. In greater scope for variation. The lowest value of G in-
practice, unrestricted values of S are found to lie vestigated was 0, equating to a paste with no velocity
between 0.22 and 0.35. To allow for die restrictions, dependence (i.e. fl = 0). Then Fob and Fvp both become
S was taken as 0.06,0.10,0.14 and 0.18. unity. Consequently the screw term (Fvp) dominates
A summary of predictions made by the model can the equation because of its larger contacting area
be found in Table 1; it is to be seen that negative (ca > Cb)and the pressure gradient is negative. In prac-
values of _P can arise, this meaning that the screw in rice the screw would simply generate no pressure and
these circumstances acts as a pressure sink, and not fail to extrude unless the machine is fed by force.
a pressure generator. The feed is being forced through Increasing G increases the pressure gradient. For
the system with the rotating screw restricting rather example when G is increased from 10 to 50, the value
than enhancing flow. of P increases from 1.93 to 12.3. Changing G will
necessarily have no effect on the value of the forward
feed angle 0, since 0 is geometric in its origin and
defined independently of _G.
Table 1. Predicted effect of design parameters on ceramic Finally, increasing the flowrate function S has
screw systems in current use through continuity the effect of increasing the forward
feed angle 0 and reducing the pressure gradient P.
~b(deg) G T S O(deg) P (ii) Numerical evaluation--full range of parameters.
Effect of varying ~p We now extend the discussion to consider the effects
18 10.0 0.60 0.06 7.19 1.09 of using extreme values of _G,_S, T and ~b. Table
20 10.0 0.60 0.06 6.91 1.93 2 shows the effects predicted for using an average
22 10.0 0.60 0.06 6.69 2.55 screw helix angle over a much larger range than is
24 10.0 0.60 0.06 6.51 3.01 used in industry. There is a peak in performance at

Effect of varying T about 35°, which is much higher than that in standard
20 10.0 0.40 0.06 10.1 0.62
20 10.0 0.50 0.06 8.04 1.47
20 10.0 0.60 0.06 6.91 1.93
20 10.0 0.70 0.06 6.23 2.13 Table 2. Predicted effect of extreme values of screw helix
angle, ~b, on pressure generation P
Effect of varying G
20 0.0 0.60 0.06 6.91 -- 0.67 ~b(deg) G T S 0(deg) P
20 10.0 0.60 0.06 6.91 1.93
20 30.0 0.60 0.06 6.91 7.12 11 10.0 0.60 0.06 9.69 -- 5.55
20 50.0 0.60 0.06 6.91 12.30 21 10.0 0.60 0.06 6.79 2.26
31 10.0 0.60 0.06 6.11 3.81
Effect of varying S 41 10.0 0.60 0.06 5.79 3.76
24 30.0 0.60 0.06 6.91 1.93 51 10.0 0.60 0.06 5.60 2.97
24 30.0 0.60 0.10 14.5 -- 2.68 61 10.0 0.60 0.06 5.46 1.72
24 30.0 0.60 0.14 26.9 -- 7.35 71 10.0 0.60 0.06 5.36 0.17
24 30.0 0.60 0.18 47.4 - 12.2 81 10.0 0.60 0.06 5.27 -- 1.58
2536 A.S. BURBIDGE and J. BRIDGWATER

use, but coincides with predictions made by Adams inevitable that the paste is being pumped through the
et al. (1993) who used a technique of complex non- rotating screw. It is interesting to note that for very
isothermal Darnell and Mol modelling for food paste deep channels (large values of T__)there would appear
systems with a number of parameters differing from to be an optimum at around 0.80 (compared with
those used here. Experimental details were not given T = 0.70 from Table 1) which is about the deepest
by these workers; an empirically determined Tresca channelled screw that could be used in a practical
boundary condition was employed. The selection of machine. It should be noted that the error due to the
a helix angle is dependent on the values of the other "unrolling" of the screw channel is increasingly signifi-
design groups G, T, S and P for the system, so con- cant as T is increased.
cluding that helix angles in current use are generally Table 5 investigates the effects of extreme values of
too small would perhaps be imprudent at this junc- the flowrate function, S. If we consider the case of
ture. However, from a study of the open literature the a screw pumping against a blocked channel (S = 0)
reasoning for selecting ~b to be around 22 ° is certainly the maximum pressure gradient is obtained. Increas-
not clear. ing the values of S leads ultimately to large adverse
Table 3 demonstrates that pressure is roughly pro- pressure gradients and large forward feed angles.
portional to values of__Gover the full range of values
tested. The higher values of G are unlikely to be Laboratory evaluation
achieved in practice without significant shear-thicken- A small single screw extruder was designed and
ing since the shear rate dependence of the paste must built to allow laboratory-scale experimentation on
be large. This kind of behaviour is not desirable since model systems (Fig. 2). The rig was designed around
it is difficult to control and machine damage could a constant pitch brass screw of outside diameter
easily occur. 20 mm, core diameter 9 mm, helix angle 16.7 C' and
Values of T are physically constrained because of length 110 mm. It sits inside a close-fitting stainless
the need for the core of the screw to provide mechan- steel barrel 150 m m in length and 20 mm inside dia-
ical strength. When possible leakage effects around meter allowing feed to a point 109 mm measured
the flight tip are considered also, it is difficult to axially from the tip of the screw. At the feed port
envisage a practical screw with a value of T outside of a short vertical tube of 20 mm inside diameter termin-
the range from 0.8 to 0.1. However, for completeness, ates in a flange of 76 mm allowing for the attachment
extreme values of T are considered in Table 4. For of dies of varying length and diameter. The screw is
very shallow channels (small values o f T ) , the forward connected to a gearbox which is driven by a 150 W
feed angle 0 is forced to take on very large values. In electric motor via a moulded soft plastic linkage.
physical terms, the largest possible value of 0 is Control of the screw speed is by means of a poten-
90 ° - ~b, since any value larger than this implies that tiometer. A one-eighth inch nominal diameter
Iv~l is greater than the barrel velocity and it is then threaded tap situated 20 mm behind the die allows for
attachment of a small pressure transducer, 4. Three
other threaded pressure taps are positioned along the
barrel as shown.
Table 3. Predicted effect ofextreme values of G, on pressure
generation The two model pastes used in this study were de-
noted mix25A and plastic body. Mix25A is a laborat-
~b(deg) G T S 0(deg) P ory standard formulated as 25.5 w t % each of 280, 400
and 1200 grade Universal Abrasives a-alumina pow-
20 1.0 0.60 0.06 6.91 - 0.41 der, 2.91 wt% each of potato starch and bentonite,
20 2.0 0.60 0.06 6.91 - 0.15
20 3.0 0.60 0.06 6.91 0.11 and finally 17.6 wt% of deionised water. The powders
20 10.0 0.60 0.06 6.91 1.93 were dry mixed in a Hobart paddle mixer for 20 min,
20 30.0 0.60 0.06 6.91 7.12
20 3110 0.60 0.06 6.91 77.2
20 30110 0.60 0.06 6.91 778
Table 5. Predicted effect ofextreme values of S on pressure
generation

Table 4. Predicted effect of extreme values T on pressure q~(deg) G T S 0(deg) P


generation
20 10.0 0.60 0.00 0.00 8.78
gb(deg) G T S 0(deg) P 20 10.0 0.60 0.005 0.44 8.21
20 10.0 0.60 0.010 0.91 7.64
20 10.0 0.05 0.06 145 - 37.6 20 10.0 0.60 0.015 1.39 7.06
20 10.0 0.10 0.06 104 - 15.7 20 10.0 0.60 0.030 2.97 5.36
20 10.0 0.15 0.06 48.4 - 8.60 20 10.0 0.60 0.200 61.1 - 14.7
20 10.0 0.20 0.06 26.9 - 4.67 20 10.0 0.60 0.210 68.4 - 15.9
20 10.0 0.30 0.06 14.3 - 1.04 20 10.0 0.60 0.220 75.8 - 17.2
20 10.0 0.80 0.06 5.81 2.17 20 10.0 0.60 0.230 83.0 - 18.5
20 10.0 0.90 0.06 5.59 2.06 20 10.0 0.60 0.240 89.8 - 19.7
20 10.0 0.95 0.06 5.53 1.96 20 10.0 0.60 0.250 96.3 - 20.1
The single screw extrusion of pastes 2537

---imm0
Fig. 2. Laboratory-scale single screw extruder.

the liquid having then being added before a further S subminiature 20 M P a pressure transducers. These
20 min of wet mixing. Finally the paste was pugged were positioned in 4 mm threaded holes numbered
twice by passing it through the Hobart screw mincer sequentially from 1 to 4, 1 being at the inlet and 4 at
attachment to improve its extrusion properties. Plas- the die end of the screw extruder (Fig. 2). Hence three
tic body is a commercial clay produced by British axial pressure gradients were derived as follows: G r l
Industrial Sand Ltd for pottery use and consequently are the measured axial pressure gradients at the feed
is not very homogeneous. It was used for industrial- end of the screw and have been calculated from
scale experiments due to its availability in the large measurements by transducers 1 and 2; Gr2 are the
quantities required. Plastic body was also used with corresponding calculated values for tile centre section
the 20 mm extruder as a paste of contrasting rheology of the screw and are from data for transducers 2 and 3;
to mix25A. Gr3 are the corresponding calculated values for the
The calculation of rheological parameters Zo, delivery section of the screw being from data for
fll and n followed the procedure presented by Benbow transducers 3 and 4 (Fig. 2). Pressure measurements
and Bridgwater (1993). Briefly, this consisted of in- close to the inlet proved unsuitable due to the bulk
strumented ram extrusion through a set of dies of consolidation process taking place and those close to
identical diameter but differing lengths. Subtraction of the die dependent on the particular die used. The
pressure drop vs dieland extrusion speed character- pressure gradient calculated for the centre section of
istic curves for dies of different lengths allowed the the screw (Gr2) is therefore considered as the best
calculation of surface shear stress as a function of characteristic of the system.
velocity. Curve fitting techniques implemented on An important prediction of the model is that the
a PC were then used to derive values of either Zo, fll pressure gradient is constant along the screw, this
and n or z0 and fl as required. being at odds with models based on frictional bound-
It should be noted that the ratio of the pressure ary conditions such as that of Parks and Hill (1959).
drop due to the die entrance to that due to the dieland Experimental work presented here presents no in-
shearing is large. The effect of this is such that the formation in this respect, although considerable ex-
measurement of the parameters z0, fll and n becomes perimental work has been carried out by Laenger
relatively inaccurate adversely affecting any predic- (1992). This lends significant support since he found
tions made by the screw model using these data. It is that the pressure gradient was constant along the
probable then that in the future the predictions may length of a single screw extruder working with clay.
be improved by redesigning the ram extrusion system. Experiments were carried out using the 20 mm dia-
To this end systems based around a long die with meter laboratory machine to drive paste through a die
radial stress transducers at points along the axis are of 3 mm diameter and 48 mm axial length at various
currently under investigation. volumetric flowrates. The volumetric flowrate was
Pressure measurement along the 20 mm screw ex- maintained at a constant rate by an Instron strain
truder barrel were made with four Sensotec model frame (Fig. 2). In this way the paste flowrate could be
2538 A.S. BURmDGEand J. BIUDGWATER
controlled independently of the screw speed and However, use of McKelvey's "unrolled" channel re-
hence in some cases negative pressure gradients were mains appropriate for polymer extruders where the
maintained across the screw. Experiments at a zero channels are generally shallow and the error in the
flowrate were performed by the use of a blank die. screw polymer contact area is small.
Figure 3 compares experimental measurements Figures 4, 5 and 6 compare experiment with predic-
with predictions made for an "unrolled" rectangular tion for screws of identical pitch, but varying channel
screw channel. Predictions consistently underestimate depth; the predictions are all for curved channels.
the pressure for these experiments. Allowance can be Comparison suggests that the greatest pressure gradi-
made for the reduction of the screw-channel paste ents are generated by the shallowest screw. In general,
contact area due to the curvature of the channel, in the effect of screw speed is predicted reasonably for
which case the predictions are significantly improved higher volumetric flowrates although there is con-
(Fig. 4) taking siderable deviation as the throughput is reduced. It
can be argued that the phenomena of liquid migration
co = 2h + 7rD sin ~b and consolidation will cause localised variations in
~o,/~1 and n at the barrel surface especially as the paste
for an unrolled rectangular channel and
at this surface is not exchanged radially or able to
move axially. If the values of Zo are consequently
assumed to be higher at this fast moving barrel surface
then the predictions can be improved. These consoli-
dation phenomena will require further investigation
for a helical channel. in the future.

25

20

15 ¸
• Q=O m31s
• Q=-1.29E-8 m3/s
@ 1o • Q=1.72E-8 m3/s
o Q=2.15E-8 m3/s
Q=O m 3 / s
5
-- -- Q=1.29E-8 m 3 / s
o ..... Q = 1.72E-8m3/s
- Q=2.15E-8 m31s

0.05 _ ~ .---~-~ -~G='.'.~ -'-='--~ ~-~ ""='~'~ 0.15 0.2 0.25

-5

screw speed ffevl=)

Fig. 3. Axial pressure gradient vs screw speed and volumetric flowrate for mix25A Zo = 0.01 MPa,/~2 =
0.8 MPa(s/m) °'45, n = 0.45; screw o f mean hefix angle 16.3 °, outside diameter 20 mm and core diameter
7.4 mm. Predictions for fiat unrolled rectangular channel.

25

20

15

• Q=l.29E-8 m3/s
10
• Q=l.72E-8 m 3 / s
• Q=2.15E-8 m 3 / s
Q=0 m3/s
5
• - Q=l.29E.5 m3/s I
.... Q,=1.72E-8m3/s
• - - - -- Q=2.15E-8 m 3 / s
I I t I I
0.05 0.1 0.15 0.2 0.25

~w meeo 0~vl=)

Fig. 4. Axial pressure gradient vs speed and volumetric flowrate for mix25A Zo = 0.01 MPa, ~1 =

0.8 MPa(s/m) °''s, n = 0.45; screw o f mean helix angle 16.3 °, outside diameter 20 mm and core diameter
TA rnm. Predictions for curved channel.
The single screw extrusion of pastes 2539

2O

15-
• II
• Q = O m3/s
• ~-8.58E-9 m31s
10- • Q=I.72E-8 m3/s
"o
e Q=2.15E-8 m3/s
Q = O m3/s
5" -- -- Q=8.58E-9 rn3/s
.- Q=1.72E-8m3/s
- - Q=2.15E-8 m3/s
0 I I i I L
0.0.5 0.1 0.15 0.2 0.25
screw ~ (roy/8)

FiB. 5. Axial pressure gradient vs screw speed and volumetric flowrate for mix25A To = 0.01 MPa, fll =
0.8 MPa(s/m)°'`s, n = 0.45; screw of mean helix angle 14.9°, outside diameter 20 mm and core diameter
8.5 ram. Predictions for curved channel.

20.

18-

16

14.

~ 12

• Q = O m3/s

~s
'o


Q=1.29E-8 m3/s
Q=1.72E-8 rn3/s

6 o Q=2.15E-8 m3/s

~ ~_,..~ ~ ~.r.~ ~ ~ ~ ~--'~ ~ "~'-~ Q = O m3/s


4 .
-- -- Q=1.29E-8 m3/s
.... Q=1.72E-Sm3/s
2
o - Q=2.15E-8 m3/s
0 • • e i t
0.05 0.1 0.15 0.2 0.25

~:mw ~ (mvls)

Fig. 6. Axial pressure gradient vs screw speed and volumetric flowrate for mix25A Zo = 0.01 MPa, flj =
0.8 MPa(s/m)°'`s, n = 0.45; screw of mean helix angle 18.7°, outside diameter 20 mm and core diameter
6.0 mm. Predictions for curved channel.

Overall comparison between experimental data for all speeds. The relationship is different from that for
different screws becomes easier if only the dynamic mix25A (Figs 3-6) and the predictions still show good
part of the pressure gradient is considered. The dy- agreement. This suggests that the dynamic effects of
namic part will be defined as the difference in the the paste rheology have been correctly included in the
pressure gradient generated for N = 0.245 and model system.
N = 0.0245 rev/s. Figure 7 shows these dynamic pres-
sure gradients for all of the screws tested at zero Industrial-scale evaluation
volumetric flowrate. It is dear that there is an opti- Industrial-scale experiments were also carried out
mum dimensionless channel depth somewhere be- although here the control of the paste was quite diffi-
tween 0.22 and 0.32 and also that higher pressure cult. A Bennett and Sayer single screw extruder
gradients are generated at the lower screw angles. It is (Fig. 9) was used having a maximum unrestricted
unclear how changing the volumetric throughput of flowrate (i.e. the conveying rate with no die plate at
the screw system will affect these values. maximum speed) of 600 kg/h and a screw speed con-
Finally, Fig. 8 illustrates the effects of another tinuously variable between 10 and 60 rpm. Paste is fed
paste. Dynamic pressure gradients are again used to into a hopper above a pair of counter-rotating shafts.
remove any effects caused by consolidation at the One shaft, section AA, drives a deep grooved feeding
barrel surface, the value of pressure gradient at roller similar to that found on some types of pelletiz-
N = 0.0245 rev/s being subtracted from the data for ing roll extrusion presses; the second drives the feed
2540 A.S. BURBIDGE and J. BRIDGWATER
12 ¸

10

- e . - h/D=0.221
- - I I - - h/D--0.29 /
8
--;~- h/D=0.32 /
X WD=0.35|

• 6
l,<

"0
4

0 b I I I I I I I I
5 10 15 20 25 30 35 40 45 50

helix angle (degrees)

Fig. 7. Experimental dynamic axial pressure gradient (pressure change between N = 0.0245 and
0.245 rev/s) vs helix angle with screw channel depth as a parameter for mix25A To = 0.01 MPa,
/~1 = 0.8 MPa(s/m) °'45, n = 0.45; at zero volumetric flowrate.

5.00¸

4.50

4.00¸

3.50

3.00

L•, 2.50
x

•o 2.OO

1.50 -
t- prs,,,oo I
t • expenment J
1.00.

0.50.

0.00 JL j I i I J
0.00 0.05 0.10 0.15 0.20 0.25 0.30
screw speed (rev/s)

Fig. 8. Dynamic axial pressure gradient (pressure change between N = 0.0245 and 0.245 rev/s) vs screw
speed at zero volumetric flowrate for plastic body To = 0.01 MPa, fll = 2.9 MPa(s/m) 1"2, n = 1.2; screw of
m e a n helix angle 35.3 °, outside diameter 20 m m and core diameter 7.4 mm. Predictions for curved channel.
The single screw extrusion of pastes 2541

AA I BB I CC I DD
I I I

I I I
Feed.
I I scre~l Output
screw screw

Feed screw Feed roller


screw
~_~ ,oiler 2
Section through Section through Section through Section through
plane AA plane BB plane CC plane DD

Fig. 9. Bennett and Sayer 3 in. diameter single screw extruder.

12
screw, section BB. Paste falls onto the roller and is
then forced into the single flighted helical screw (sec-
tion AA). The paste is then conveyed along the feeding ~ "

o° l,\ leoeeO
]Increasing screw

I
• lO RPM

.20.
screw (section BB) into a vacuum chamber from 5= & 30 RPM

whence it drops onto a second roller (section CC) Q • X 50 RPM


which then feeds the final pressure generating screw
(section DD). 2

The final screw, the one to which the pressure and 0


0 2 4 6 8 10
flow measurements relate, is of outside diameter
Volumetric f l o w r a ~ , Q (m3"le-,~e)
80 mm, internal diameter 40 mm and has flight spac-
ings of 61, 61, 40, 40 and 40 mm measured along the Fig. 10. Axial pressure gradient for Bennett and Sayer ma-
axis of the machine. The spacing is defined as the chine extruding plastic body for which To = 0.01 MPa,
distance from the front tip of one screw flight to an fll = 2.90 MPa(s/m)1"2, n = 1.2.
identical point on the adjacent downstream flight
along the axis of the screw. The mean helix angles for
the screw are deduced as ~ = 19.7° for the first two nitudes and trends of the predictions being broadly
turns, and ~ = 13.4° for the delivery part of the screw. correct. The influence of screw speed was satisfactorily
The change in the period occurs just as the screw predicted with the flowrate at a given pressure differ-
enters the enclosed portion, i.e. where the barrel sec- ing by a factor of up to two. There is thus evidence,
tion begins. The flight width perpendicular to the within the acctiracy of the experiment, that the effects
helix is 12 mm and the part of the screw enclosed by of scale are satisfactorily included.
the barrel section is of length 124 mm and internal
diameter 83 ram. There is therefore a tip to wall gap of CONCLUSIONS
1.5 mm through which paste leakage can occur. The A theory based upon a model of paste rheology has
dimensionless channel depth ._T= 2h/D = 0.5. been coupled to the approach of Darnell and Mol to
Figure 10 illustrates the results of pressure measure- yield a model for the rate of pressure generation in
ments taken at the die for this single screw extruder. a fully flooded single screw.
The pressure gradients were calculated on the basis Generalisations about the predictions made are
that only the 13.4° part of the screw was fully flooded, rather awkward to make due to the interaction of the
but it was not possible to ascertain whether this was design parameters. It is found that (i) the screw should
attained. The material was of variable quality and the have a dimensionless channel depth close to 0.30 and
quantities required rendered conditions difficult. The (ii) the surface shear stress of the paste should exhibit
measurements are comparable with the predictions of a considerable velocity dependence since it is this
the model when the intrinsic accuracy of the experi- shearing force that is directly responsible for the pres-
ment is taken into consideration, with both the mag- sure generation.
2542 A.S. BURmDGEand J. BRIDGWATER
Experiments show that the dynamic trends of the N angular rotation rate, s-1
data were predicted to good agreement in all cases. P pressure, M P a
However, in the case of low or zero flowrates, there Q volumetric flowrate, m3/s
appear to be changes in the surface properties of vo axial ' velocity vector of paste plug in screw
pastes that affect the shear stresses causing the abso- extruder, m/s
lute values of the predictions to b e too low. This Vb relative velocity vector of screw and barrel,
becomes insignificant when the flowrate is higher. m/s
From separate larger scale work, the effect of scale vo velocity vector of paste plug, m/s
appears to have been correctly identified although v, relative velocity of paste plug and barrel,
more reliable data are desirable. m/s
Some of the difficulty in the model predictions was V mean extrudate velocity in dieland, m/s
due to the characterisation of the paste rheology w width of channel normal to the flights, m
which was used as an input for the predictive systems; x Cartesian length axis measured along axis of
despite this, the dynamic rheological effects in particu- screw
lar seem to have been correctly identified. One
method of improving the measurement of the dieland Greek letters
paste parameters (~0,/~ and n) is to design a very long velocity factor of bulk yield stress, MPa s/m
die with pressure transducers at intervals along its fl velocity factor of wall shear stress, MPa s/m
length and this is in hand. An advantage of such fll power law velocity factor for wall shear
a method is that it could allow for measurement of the stress, MPa(s/m)"
dieland parameters completely separately from those 0 forward feed angle of paste
for the die entry region, ao initial bulk yield stress of paste, MPa
The work also indicates that the physical mecha- %p shear stress at velocity Vp, M P a
nism arising when pastes are exposed for a long time %, shear stress at velocity v,, MPa
to shear need study together with direct measure- Xo initial wall shear stress of paste, MPa
ments of the surface shear stress. helix angle of screw
There are a number of further challenges. It is
known that sometimes pastes lose contact with the Dimensionless groups
trailing face of the screw. Analysis of this is of interest Fvv ratio of dynamic to static shear stress at
in its own right and is important in that it influences Ivpl -- xvdz0
the wetted area of the paste in contact with the screw. Fvr ratio of dynamic to static shear stress at
The more difficult issue of flow between the tips of the Iv,I = ~p/T0
screw flights and the barrel awaits analysis as do the G surface velocity independent shear stress ra-
more complex flows in twin screws. tio ( = BnDN/~o)
P dimensionless pressure gradient ( = ((A sin ~p)/
Acknowledaements--The work presented in this paper was (Cb~o))/(dS/dx)
carried out under the financial support of the Institut R_ dimensionless flowrate group { = 4 Q /
Fran~ais du P&role, CEDI, Solaize, France. Thanks are also 7r2D~N[D~ -- (Ds - 2h)2])
due to the Department of Industrial Ceramics in the Univer-
sity of Staffordshire for use of their Bennett and Sayer 76 mm _S dimensionless flowrate ( = Q/ND~)
screw extruder. T dimensionless channel depth ( = 2h/D,)

NOTATION REFERENCES
Ao cross-sectional area of die entry, m 2 Adams, M. J., E~imonson, B. and Briscoe, B. J., 1993, Non-
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A cross-sectional area of dieland or screw
single screw extrusion of pastes. Proceedings of the
channel, m 2 I ChemE Research Event, pp. 114-116.
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DKG 69, 266-272. Ovenston, A. and Benbow, J. J., 1968, Effects of die geometry
Lund, H. H., Boritz, S. A. and Reed, A. J., 1962, Auger design on extrusion of clay-like material. Trans. Br. Ceramic. Soc.
for clay extrusion. Ceramic Bull. 41, 554-559. 67, 543-567.
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Chem. 45, 970-993. Am. Ceramic Soc. 42, 1-6.
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