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Effects of Process Parameters on Friction Stir


Spot Welding of Aluminum Alloy to Advanced
High-Strength Steel

Conference Paper · July 2016

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Proceedings of the ASME 2016 International Manufacturing Science and Engineering Conference
MSEC2016
June 27-July 1, 2016, Blacksburg, Virginia, USA

MSEC2016-8589

EFFECTS OF PROCESS PARAMETERS ON FRICTION STIR SPOT WELDING OF


ALUMINUM ALLOY TO ADVANCED HIGH-STRENGTH STEEL

Kai Chen, Xun Liu, Jun Ni


University of Michigan
Ann Arbor, MI, USA

ABSTRACT (FSSW) is a promising solution to make spot joints between


dissimilar materials.
Friction stir spot welding (FSSW) process has been During FSSW, a rotating tool with a pin feature is gradually
successfully applied for joining aluminum alloy 6061 to TRIP plunged into the welding materials at a prescribed speed until a
780/800 steel. Effects of tool plunge speed and dwell time on desired plunge depth is reached. The tool is then held rotating at
the weld strength were studied through design of experiments that position and after a short period of dwell time, it is
and analysis of variance. It is shown that dwell time is a more retracted and a weld is achieved. FSSW joint strength closely
dominant parameter in affecting the weld strength than plunge depends on welding process parameters, including rotation
speed. Cross sections of weld specimens show the formation of speed, plunge speed, plunge depth and dwell time. Liu et al.[2]
hook with a swirling structure. Higher magnified SEM view did friction stir welding of 1.5mm thick Al 6061 alloy to 1.4mm
with EDS analysis reveals the swirling structure to be composed thick TRIP 780/800 steel with a butt configuration, and the
of alternating thin layers of steel and Al-Fe intermetallic maximum tensile strength was achieved about 85% of the base
compounds (IMCs). During tensile shear test, cross nugget Al alloy. Aldanondo et al. [3] welded 2mm thick DP1200 ultra
failure is the only failure mode. Cracks are initiated in the high strength steel and reported that dwell time and plunge
swirling structure at the tensile side of the weld nugget and depth were the most critical parameters on influencing shear
cleavage feature can be observed on the fractured surface. strength of the joints. Lathabai et al. [4] did FSSW on
aluminum alloy Al 6060-T5 and showed that the plunge depth
1. INTRODUCTION had a profound effect on the joint strength through its strong
In recent years, growing amount of attention has been correlation with the dimension of the annular bond area
drawn to studies of reducing vehicle weights in the automotive between the two sheets. Karthikeyan et al. [5] applied
industry considering both economic and environmental factors. response surface method to study effects of process parameters
One of the effective methods to achieve this goal is to replace on friction stir spot welding of aluminum alloy 2024. They
steel components with multi-material vehicle structures [1]. pointed out that plunge speed had a greater influence on tensile
Joining of dissimilar materials is therefore very important shear fracture load followed by plunge depth, dwell time, and
to meet this demand. It is generally difficult to join dissimilar tool rotation speed. Sakamura et al. [6] showed that larger
materials using conventional welding technologies, especially plunge depth produced higher strength for FSSW of aluminum
for aluminum alloys to advanced high strength steel, as they alloy 5052 to low carbon steel. Zhang et al. [7] applied FFSW
have quite different physical and chemical properties. In to join aluminum alloy 5052-H112 sheets. The maximum
addition, the formation of large amount of brittle intermetallic tensile-shear strength they achieved was from the condition
compounds is highly detrimental to joint quality. where rotation speed was 1541 rpm and dwell time was 5
Friction stir welding (FSW) is a solid state welding seconds. Lakshminarayanan et al. [8] studied FSSW on low
technique and can avoid bulk melting during the process. As a carbon automotive steels. In their works, tool rotating speed
variant of friction stir welding, friction stir spot welding ranged from 1200RPM to 1600RPM. Their plunge depth,

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which was defined as the distance from the top sheet surface to of steel, as a common experimental configuration in the
the tool shoulder surface, was ranged from 0 to 0.2mm. Dwell literature. The thickness of both sheets was 1.5mm. Tensile test
time varied from 5 seconds to 25 seconds. They figured out the specimens were prepared according to the JIS Z 3136:1999
maximum tensile shear strength was obtained with the operation standard and detailed dimensions are shown in Figure 1. During
condition of 1157 rpm rotating speed, 0.05mm plunge depth experiments, the tool axis was aligned with the center of the
and dwell time of 22 seconds. Besides, dwell time was indicated overlapped area. After welds, lap shear tensile tests were
to be the dominant parameter in determining joint properties. performed on a computer assisted INSTRON tensile machine
Several studies have been conducted on FSSW of with a loading speed of 1mm/min. Three replicates were tested
aluminum alloy to steel. Bozzi et al. [9] welded dissimilar for each welding condition.
materials of 1.2 mm aluminum alloy 6016 to 2 mm IF-steel. It
was pointed out that Intermetallic compound (IMC) layer was
necessary to guarantee the weld strength. However, if the
thickness of the IMC layer exceeded a certain value, cracks
were initiated and propagated easily through the brittle IMCs
tangles, which led to a weak weld strength. Chen et al. [10]
applied abrasion circle friction spot welding process for
welding 1mm aluminum alloy 6111-T4 to steel DC04. In their
process, a probe tool translated along a circular path to abrade
Figure 1. Dimensions of lap shear test (unit: mm)
the steel sheet, which was placed on the bottom. Their total
cycle time was close to 1 second. No IMCs were found at the
FSSW tool is made of ground and polished tungsten
interface between steel and aluminum. Sun et al. [11] welded
carbide with 10% cobalt and the hardness is 91.8 HRA. The
1mm aluminum alloy 6061 to mild steel with a flat spot FSW
tool consists of a non-threaded cylindrical pin and the detailed
technique, during which a probe-less rotating tool was applied
dimensions are presented in Figure 2.
to flatten the weld surface after making the spot weld. The
keyhole defect was eliminated, which improved physical
properties of the joints. No intermetallic compound layer was
found at the Al/Fe interface. Furthermore, they indicated the
length of the tool probe had little effect on the welding
properties. Figner et al. [12] welded aluminum alloy 5754 to
galvanized steel HX 340LAD. They found a longer dwell time
or slower spindle speed decreased the weld strength.
It can be noticed that a limited amount of literature has
discussed FSSW for joining aluminum alloy to advanced high
strength steel. Combination of different series of aluminum and Figure 2. Dimensions of FSSW tool
steel as base materials generally result in variations of the
welding performance even under the same operation Effects of two process parameters were studied in this
parameters. Besides, effects of plunge speed during FSSW of research, including plunge speed and dwell time, and each was
similar materials can be observed to be controversial from examined in three levels. All experiments were performed under
literature. Lathabai et al. [4] found that the plunge speed had the same rotation speed and plunge depth, which were
little effect on the weld strength. However, Baskoro et al. [13] 2000RPM and 0.4mm into steel sheet respectively. The
indicated that slower plunge speed would increase the tensile investigated welding conditions are summarized in Table 2.
strength. A Kistler dynamometer was mounted below the workpiece
In this research, friction stir spot welding was applied for for measurement of the axial plunge force during the welding
joining aluminum alloy 6061-T6 to one type of advanced high process. Obtained welds were sectioned in the center and then
strength steel, TRIP 780/800 steel. Rotation speed and plunge mounted, ground and polished. Joint cross-sections were
depth, which was the depth that the tool pin plunged into the characterized using both optical and scanning electron
steel, were kept constant during all the experiments. Effects of microscope. Energy dispersive X-ray spectroscopy (EDS)
plunge speed and dwell time on weld strength were studied analysis was further performed for determining elemental
based on design of experiments method. Microstructure of joint distributions at Al-Fe interfaces. Fractorgraphic examination
cross section was characterized and failure mechanisms were was also performed on the broken tensile specimens using
analyzed. Philips XL-30 SEM. Hardness distribution on joint cross
sections was measured with CLARK micro-hardness tester and
2. EXPERIMENTAL DETAILS a 100g load was applied for 15 seconds.
Chemical compositions of Aluminum 6061-T6 used in this
study are listed in Table 1. Aluminum sheet was placed on top

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Table 1. Chemical compositions of the base material Al 6061-T6
Chemical Composition (wt.%)
Material Al Mg Si Cr Mn Ti Cu Zn Fe other
Al6061-T6 95.1-98.2 0.8-1.2 0.4-0.8 0.05-0.4 <0.15 <0.15 0.05-0.4 <0.25 <0.7 <0.15

Table 2. Experimental design matrix


Experimental Plunge Speed Dwell Time
Order (mm/min) (s)
1 5 1
2 5 5
3 5 10
4 10 1
5 10 5
6 10 10
7 15 1
8 15 5
9 15 10

3. RESULTS AND DISCUSSION Figure 3. Plunge force as a function of the pin plunge
distance
3.1 Effects of plunge speed on force history (Plunge speed 5mm/min, dwell time 10s)
Figure 3 shows a typical curve of the axial plunge force
with regard to tool plunge distance. Plunge force reaches its The effect of different plunge speeds on the maximum axial
peak value when the bottom surface of the pin penetrates force at the end of plunge stage was studied and the relationship
0.4mm into steel, which corresponds to point 5 in the figure. is shown in Figure 4. It can be observed that the maximum
The history of plunge force can be roughly divided into five plunge force is positively correlated to plunge speed at all levels
regions. From the initial position to point 1, the rotating pin that have been investigated. Since higher plunge speed provides
starts to touch aluminum top surface and gradually moves into less amount of heat, the deformation resistance of materials
the workpiece. The plunge force increases due to the growing remains high and accordingly requires a larger maximum
amount of deformation materials. In this stage, only aluminum plunge force. In addition, the difference in maximum axial force
is stirred around the tool pin. From point 1 to point 2, as the pin due to different plunge speeds becomes smaller as the plunge
travels deeper into aluminum, the heat generated from both speed increases. For example, the maximum plunge force
friction and plastic deformation in the workpiece softens increased by 1.07KN when the plunge speed increased from
aluminum to an overheat level. This makes it easier for the pin 2mm/min to 5mm/min, while the increment was only 0.26KN
to further plunge into workpiece and results in a decreased when the plunge speed increased from 15mm/min to
plunge force. At point 2, the shoulder surface of FSSW tool 20mm/min.
begins to touch the squeezed out aluminum. As the entire
shoulder area starts to deform aluminum, plunge force increases
again. After that, as the rotating shoulder moves deeper into
aluminum, it interacts with the material as a pin with larger
diameter. Similar to the condition between point 1 and point 2,
the heat generated from friction and severe plastic deformation
will reach an overshoot level, which softens the material and
decreases the force increasing rate from point 3 to point 4. From
point 4 to point 5, a certain amount of steel starts to be
deformed by the tool pin. This portion of steel is then squeezed Figure 4. Maximum plunge force at different plunge speeds
to flow upward, which is further suppressed by the tool
shoulder. Therefore, plunge force increases rapidly in this 3.2 MICROSTRUCTURE
region. Finally from point 5 to point 6, which corresponds to the One of the typical cross sections of the weld zone is shown
dwell period and the force decreases as a consequence of in Figure 5 (a) and the corresponding welding parameters
continuing frictional heat generation at the interface between include plunge speed of 5mm/min and dwell time of 5 seconds.
tool and workpiece without further deformation. No obvious cracks exist at the interface between steel and
aluminum. A hook feature was observed around the weld

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nugget. A similar hook feature was also reported by Bozzi and
Figner [9, 12]. An enlarged view of this hook is presented in
Figure 5 (b). The extruded steel can be observed to flow
upward, which is primarily due to the downward squeezing
motion of the pin. In the meantime, the upward flow of steel is
restrained by the larger compression force from tool shoulder
surface. This portion of steel is therefore bent over and
embedded into the relatively soft aluminum matrix, which
finally forms the hook structure. Furthermore, a unique swirling
structure layer can be noticed at the Al-Fe interface, as marked
out by the region “A” in Figure 5 (b). This swirling structure
can generally be observed in all the investigated conditions, as
shown in Figure 6 (a), which corresponds to plunge speed of Figure 5. (a) Cross section view of the weld nugget
5mm/min and dwell time of 10s. The thickness of this layer is (b) Geometry of the hook
up to 0.2mm. In Figure 5 (a), the right side of the figure actually (c) Detailed view of the right end side of welding zone
corresponded to the squeezed aluminum that accumulated (Plunge speed 5mm/min, dwell time 5 seconds)
around the periphery of tool shoulder region rather than the
original aluminum sheet. It was mainly caused by the material
flow driven by tool shoulder. As the shoulder surface was
pressed into aluminum, the aluminum material below the tool
would be squeezed out, which flowed upward surrounding the
outside surface of the tool. In the meantime, a gap was
generated as indicated B in Figure 5 (c). Accordingly, the
thickness of accumulated aluminum in this region is larger than
1.5mm.

In order to analyze this feature in details, a further


magnified view was obtained from SEM and the result is
presented in Figure 6 (b). Moreover, elemental distribution was
analyzed through EDS line scanning, which was performed
along the arrow line shown in Figure 6 (b). A relatively constant
ratio between weight percentage of aluminum and that of iron Figure 6. (a) Typical hook geometry on the left side
can be observed in Figure 6 (c), which indicates formation of (b) EDS line test on the swirling structure
intermetallic compounds (IMCs) in the layer between point C (c) Element weight percentage from EDS line test
and D. The thickness of this IMC layer is around 3μm. A few (Plunge speed 5mm/min, dwell time 10seconds)
amount of carbon was also detected. Based on the Al-Fe phase
diagram, as shown in Figure 7 [14] and the Al-Fe atomic ratio
from the EDS results, the composition of this IMC layer is
likely to be Fe2Al5 or FeAl2. The swirling structure can
accordingly be concluded as composed of alternating thin layers
of steel and IMCs, which exhibits as a fence-shaped
morphology. Formation of IMCs can be contributed to the
upward flow of steel, which is embedded into aluminum.
Reactions between iron and aluminum are then likely to occur
under the combined condition of frictional heat generated by
tool rotational motion as well as the large compression force. In
the following analysis of joint tensile tests results, it can be Figure 7. Al-Fe phase diagram [14]
shown that the hook and IMC layer in the swirling feature are
key factors that determine FSSW joint strength. 3.3 MICROHARDNESS
Hardness distribution on the joint cross section was
measured along a line from point A to point B, which was
0.3mm above the interface of aluminum and steel. The results
are shown in Figure 8. Hardness of base steel is around 279HV
while that of base aluminum alloy is only around 80HV. A

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substantially higher hardness can be observed in the swirling
structure region, which is approximately 366HV on average and
is 131% of that of the base steel. This again reveals the
formation of IMCs and the associated high hardness indicates
its brittle properties, which accordingly plays an important role
in determining the weld strength.

Figure 9. Shear strength at different plunge speeds

Figure 8. Vickers hardness distribution


(Plunge speed 10mm/min, dwell time 5 seconds)

3.4 LAP SHEAR STRENGTH

3.4.1 EFFECTS OF PLUNGE SPEED Figure 10. Cross-sectional view of FSSW joint with plunge
Effects of plunge speed on lap shear strength of FSSW speed of 15mm/min
joints are shown in Figure 9 and the corresponding dwell time is
5 seconds. The joint strength varies from 2443N to 4083N, 3.4.2 DOE ANALYSIS ON EFFECTS OF WELD
which is approximately in the same range as reported by PARAMETERS
Lathabai et al [4].when they did FSSW for joining similar To further understand the influence of dwell time and
aluminum alloy Al 6060. The maximum shear strength of plunge speed on FSSW of aluminum alloy to TRIP steel, design
4083N is achieved at a plunge speed of 10mm/min. Moreover, of experiments (DOE) method was applied. DOE is an efficient
it can be observed that joint shear strength improves with approach to identify the most critical process parameters for the
increasing plunge speed from 2mm/min to 10mm/min. On the final output, understand interactions between different
other hand, further increasing the plunge speed will reduce the parameters and optimize process conditions. In this study, a
joint strength. Since plunge speed is closely related to the total three-level full-factorial design was adopted to investigate
amount of heat input during FSSW, slower plunge speed effects of dwell time and plunge speed on weld characteristics.
corresponds to longer contact period between shoulder and The experimental matrix is listed in Table 2 in the previous
material, which therefore leads to a greater amount of heat section. A statistical analysis of variance (ANOVA) was then
generation. Accordingly the IMC layer at the interface between performed to evaluate the relative significance of different
aluminum and steel becomes thicker and results in a negative process parameters as well as their interactions on joint tensile
effect on weld strength. On the other hand, when the plunge strength. The confidential level was set as 95% for all intervals.
speed reaches a higher value, axial plunge force increases as Degrees of freedom (DF), total sum of squares (SS), and the
shown in Figure 4. The large plunge force can initiate cracks on mean squares (MS) for each parameter are summarized in Table
brittle IMCs in the swirling structure during the welding 3. The F value is then determined as the average of mean square
process, which are left as defects on the weld before tensile deviation due to each parameter divided by the mean of squared
tests. Figure 10 shows the cross sectional view of the hook error, which is basically the ratio of “average between
obtained from a high plunge speed condition. A large crack can treatment” to “average within treatment”. Generally, F value
be observed in the swirling structure, which significantly larger than 4 indicates the corresponding parameter is relatively
deteriorates joint quality. significant [15]. P value is the probability that the null
hypothesis is rejected when it is actually true and null
hypothesis is that there is no difference in mean values for
different levels of a tested factor.
From Table 3, in the investigated range of operation
parameters, dwell time is shown to be the most influential factor
on joint tensile strength, followed by plunge speed and then the

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interaction of these two parameters. The P value for dwell time formation of cracks in the swirling structure thus the joint
is only 0.002, which further indicates it as a dominant factor. strength is reduced by this weld defect. For the dwell time of 5
Main effects of different process parameters on joint tensile seconds, the weld strength increases with the increasing plunge
strength are shown in Figure 11. The total average joint strength speed in the beginning but then decreases. This can be
obtained from all welding conditions is plotted as a baseline explained as the followings: at relatively low plunge speed,
value for reference. From Figure 11 (a), it can be observed that excessive amount of heat can be generated during the plunge
the overall effects of plunge speed averaged from different stage, which produces extra undesirable IMCs on the interface
levels of dwell time are consistent with the result in Figure 9, between steel and aluminum. The thick layer of brittle IMCs
which is for a specific dwell time of 5s. Maximum joint strength greatly deteriorates joint quality. On the other hand, when the
can be achieved at an intermediate level of plunge speed and plunge speed reaches a higher value as 15mm/min, the
either too high or too slow plunge speed will reduce joint associated larger plunge force can generate initial cracks, as in
strength. Figure 11 (b) shows the main effects of dwell time the condition of a shorter dwell time. To reduce the prejudicial
averaged under various plunge speeds. It can be observed the effects of both these factors, an intermediate value of plunge
shear strength decreases monotonically as dwell time increases. speed therefore achieves better joint performance. Finally, for
Dwell time of both 1 second and 5 seconds yields a higher the case of 10 seconds dwell time, the weld strength increases
strength than the average baseline value. When comparing as the plunge speed increases. This can be considered from the
Figure 11 (a) and Figure 11 (b), dwell time has an evidently aspect that a longer dwell time can increase the IMC thickness
larger influence on the joint strength, as is also indicated by the due to the larger amount of frictional heat input in dwell stage.
result of F value in Table 3. Less heat generation with faster plunge speed in plunge stage
Interaction plot of the processing parameters is given in can restrain IMCs formation and consequently improve joint
Figure 12. At dwell time of 1 second, the weld strength strength. It can be noticed that different effects of process
decreases with increasing plunge speed, which can be attributed parameters on weld strength are closely related to both the
to the associated large plunge force, as discussed in the previous associated heat input and plunge force.
session. The large plunge force increases the possibility of
Table 3. ANOVA of the weld strength under different process conditions
Source DF SS MS F-Value P-Value
Plunge Speed 2 1342589 671294 3.26 0.062
Dwell Time 2 3521958 1760979 8.55 0.002
Plunge Speed*Dwell Time 4 2404500 601125 2.92 0.05
Error 18 3705991 205888
Total 26 10975038

Figure 12. Interaction plot of different plunge speeds and


dwell time on joint shear strength

3.5 FAILURE MODE


According to the literature, there are generally two failure
modes for FSSW joints, including nugget pull out and cross
nugget failure. In the former one, cracks are generated in the
Figure 11. Main effects of different plunge speeds and shoulder area and propagate around the weld nugget, which
dwell time on joint shear strength leaves the nugget intact and corresponds to a ductile fracture.
The other failure mode is that the fracture happens across the
weld nugget and leaves a relatively brittle joint fracture [16-18].

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In this study, the cross nugget failure was the only observed IMCs in the swirling structure as it determines the fracture
failure mode, as shown in Figure 13 (a) and the welding strength on the tensile side of the nugget.
condition was 5 seconds dwell time and 10mm/min plunge
speed. The left side of Figure 13(a) is a top view of the weld on
steel sheet and the right is a back side view of aluminum.
Direction of the applied test load with regard to weld specimens
is illustrated in Figure 13 (b). It can be observed that on the
right side of nugget, the top aluminum sheet is subjected to
tensile loading. This force tries to pull aluminum away from the
nugget. Due to the existence of a considerable amount of brittle
IMC in the swirling structure, cracks are first initiated in this
region, as shown in Figure 14(a), which corresponds to the
beginning stage of tensile test and is obtained from an
interrupted loading condition. The cracks then propagate along
the interface between the swirling structure and steel. The joint Figure 13. (a) Cross nugget failure mode
eventually failed as shown in Figure 14(b). The entire loading (b) Schematic illustration of tensile shear test
process on this right side of the nugget is illustrated
schematically in Figure 15.
On the left side of nugget, the applied force is trying to
push the aluminum sheet towards the nugget, which results in a
compressive stress state in aluminum. As illustrated in Figure
16, the compressing force is applied on point 1 and then cracks
are generated on the swirling structure above the hook. Based
on stress state analysis, the compressive stress results in a large Figure 14. Cross section view of the fracture:
shear stress component in the 45o plane. Cracks then propagate (a) At the beginning of tensile test: Cracks formed in the IMCs,
along this path and the fractured geometry is shown in Figure (b) At the end of tensile test: Cracks propagate and fracture
17. It can also be noticed that the aluminum sheet was tilted occurs
upward with a small angle, which is more obvious in the bottom
region as in point 2. A different failure mechanism on the left
side was reported by Liyanage et al [19]. In their study, the
fracture is initiated at the interface between aluminum and steel
sheet and then propagated to the key hole. However, the hook
formed in this study provides a sufficiently high resistance to
Figure 15. Illustration of the failure process in the tensile side
the compression force, which helps prevent cracks from
propagating to the keyhole.
Figure 18 (a) compares the relative strength between
tension and compression side of the weld nugget. An enlarged
view of the fracture region is provided in figure 18 (b). It can be
observed the fracture already occurred in the tensile side while
steel and aluminum were still connected on the left compressive
Figure 16. Illustration of the failure process in the compressive
side. This indicates fracture first happened on the right side
side
during the tensile test and the specimen finally failed when the
compressive side was completely sheared through. Figure 19
shows SEM analysis on the fractured surface at the backside of
aluminum. The cleavage characteristics imply a brittle fracture
mechanism, which is very likely to be related to the fracture
path through the IMC layer in the swirling structure of the hook.
Base on the previous discussions, there are three major factors
that affect the joint strength. The first is hook geometry. A
strong hook is necessary to avoid nugget fracture. The second
factor is the remaining thickness of aluminum after penetration
of the tool shoulder, which is denoted as T in Figure 13 (b). Figure 17. Failure on the left side of the nugget
Increasing the thickness can reduce the effective applied
loading stress on the weld cross section, which enables a higher
loading before joint failure. The third one is the amount of

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only observed failure mode. The joint finally failed when the
aluminum sheet in compressive side of the weld nugget was
sheared through along the 45o plane.

5. ACKNOWLEDGMENTS
This work is supported by the CERC-CVC U.S.-China
Program of Clean Vehicle under Award Number DE-PI0000012
and National Science Foundation (Grant No. 1537582, Joining
of Dissimilar Materials through a Novel Hybrid Friction Stir
Resistance Spot Welding Process).

Figure 18. (a) Failure happened at the tensile side while the
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