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Original Article

Effect of laser welding heat input on fatigue crack


growth and CTOD fracture toughness of HSLA steel
joints

Henrique Varella Ribeiro a,b,*, Carlos Antonio Reis Pereira Baptista b,


Milton Sergio Fernandes Lima c, Marcelo Augusto Santos Torres d,
Jose Benedito Marcomini e
a
Centro Federal de Educaça ~o Tecnologica Celso Suckow da Fonseca, CEFET/RJ, Rua do Areal, 522, Parque
Mambucaba, CEP 23953-030, Angra dos Reis, RJ, Brazil
b
Department of Materials Engineering, EEL-USP, University of Sa ~ o Paulo, Polo Urbo-Industrial, s/N, CEP 12602-810,
Lorena, SP, Brazil
c
Institute for Advanced Studies, IEAv-DCTA. Trevo Cel, Av. Jose Alberto Albano do Amarante, CEP 12228-001, Sa ~o
Jose dos Campos, SP, Brazil
d
Department of Mechanics, Sa ~o Paulo State University, Av. Ariberto Pereira da Cunha, 333, CEP 12516-410,
Guaratingueta  , SP, Brazil
e
Materials Engineering Department, SMM, EESC-USP, University of Sa ~ o Paulo, Av. Joa
~ o Dagnone, 1100, CEP 13563-
120, Sa ~ o Carlos, SP, Brazil

article info abstract

Article history: High strength low alloy steels are employed in structural elements and, despite presenting
Received 18 June 2020 good weldability, the welded joint is always a critical issue and its evaluation is funda-
Accepted 11 January 2021 mental in guaranteeing structural integrity. The mechanical properties of weld beads can
Available online 20 January 2021 be significantly different from the base material’s properties due to metallurgical alter-
ations caused by the welding process. One of the factors leading to significant impact is the
Keywords: heat input. This paper evaluates the hardness, fracture toughness and fatigue crack growth
Laser welding in weld beads obtained via a Laser process with two different heat inputs, which resulted in
Fatigue crack growth weld beads with distinct microstructures: one composed of ferrite presenting different
Fracture toughness morphologies and the other composed of martensite and bainite. The aims of this work are
Welding metallurgy evaluating the effect of Laser welding heat input on microstructures in the weld beads, and
HSLA steel the correlation of the microstructure with fatigue crack growth and crack-tip opening
displacement fracture toughness. Fracture toughness presented itself to be more sensitive
to the microstructural alterations caused by the heat input than hardness and fatigue crack
growth. Weld beads showed higher resistance to fatigue crack growth when compared to
the base metal, even though there were no significant differences between them.
© 2021 The Authors. Published by Elsevier B.V. This is an open access article under the CC
BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).

* Corresponding author.
E-mail addresses: prof.henriquevarella@gmail.com (H.V. Ribeiro), carlos.baptista@usp.br (C.A. Reis Pereira Baptista), miltonsflima@
gmail.com (M.S. Fernandes Lima), mastorres@uol.com.br (M.A. Santos Torres), jmarcomini@usp.br (J.B. Marcomini).
https://doi.org/10.1016/j.jmrt.2021.01.038
2238-7854/© 2021 The Authors. Published by Elsevier B.V. This is an open access article under the CC BY-NC-ND license (http://
creativecommons.org/licenses/by-nc-nd/4.0/).
802 j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 1 ; 1 1 : 8 0 1 e8 1 0

1. Introduction interlocking nature of acicular ferrite, plus its fine grains,


promotes maximum fracture resistance. For another condi-
High strength low alloy (HSLA) steels are employed in struc- tion, the microstructure presented is coarse, contains M-A
tural elements due to the fine combination of mechanical constituent consisting of martensitic laths, upper bainite, and
resistance and fracture toughness, as well as good formability of grain boundary ferrite. The formation of grain boundary
and weldability. In the automobile industry, they are used in ferrite and upper bainite provides an easy pathway for crack
the manufacture of chassis, wheels (rim and disc), pieces of propagation, resulting in lower fracture resistance. Yang et al.
suspensions and other parts [1]. Among these are the micro- [8] evaluated fracture toughness of the materials in welded
alloyed steels that allowed an advance in some joint, by Submerged arc welding (SAW), of X80 pipeline steel,
manufacturing processes such as the fractured connecting and concluded that the weld metal zone is relatively poor in
rods and the Thermomechanical Controlled Processing plasticity and fracture toughness because of Widmansta € tten
(TMCP) in the manufacturing of crankshafts, for example, by ferrite, and the welding process resulted in embrittlement in
using the DIN38MnSiVS5 steel in the automotive industry and the heat-affected zone (HAZ) of the X80 steel welded joint. The
the API 5LX70/80 steels in the manufacture of oil pipeline occurrence of a lot of strip martensite-austenite (MeA) con-
tubes in the petrochemical industry. Controlled forging and stituents and the mutual permeation of the structures
rolling are a few examples of TMCP. Although these alloys noticeably deteriorate the fracture toughness of the
present good weldability, the welded joint is always a critical structures.
spot in structural elements due to metallurgical alterations, Neves e Loureiro [9] examined the effect of the welding
complex stressestrain states due to joint geometry and procedure (SAW), the heat input in particular, on the changes
possible presence of discontinuities and residual stresses. induced in the mechanical behavior of welds on a high
The application of these steels in structural elements strength quenched and tempered steel. The microstructure of
generates the need for more detailed analysis of the joint’s the deposited weld metal is composed by a very refined
mechanical behavior due to the previously mentioned factors acicular ferrite, and it was observed that an increase in heat
and to the nature of the loadings, which taken together can input also caused softening of the weld metal due to the
nucleate cracks in the welding region. Taking into account the coarsening of the microstructure, and a decrease in toughness
presence of cracks, this analysis must be done under static was observed in the weld metal and HAZ due to microstruc-
and cyclic loads, with fracture toughness and fatigue proper- tural changes. Ranganath, Kumar and Pandey [10] investi-
ties quantifications [2]. The mechanical properties of a welded gated fracture toughness characterization of a weldment, by
joint depend on the microstructures in the different regions of Shielded Metal Arc Welding (SMAW), in a microalloyed steel.
the weld bead. Due to metallurgical alterations caused by the The weld zone, dominantly of acicular ferrite, exhibits
welding process because of the thermal cycles, added ele- maximum initiation toughness and strength. The base metal
ments (when there are ones) and distinct cooling rates, these and HAZ, composed of greater proportion of polygonal ferrite
different regions may present microstructures that vary from and grain boundary ferrite together with lath martensite,
that of the base metal. Liu and Varga [3] report that fracture exhibit almost equal values of initiation toughness. The
toughness and crack growth resistance depends mainly on acicular ferrite appears to be responsible for high toughness in
the microstructural inhomogeneity including the size and the weld zone whereas the lath martensite and grain bound-
distribution of various zones in the ligament or along the ary ferrite reduce the toughness in the HAZ.
crack front. For mechanical components with the presence of cracks,
Thermal input control is important in order to optimize the fatigue life can be quantified by the fatigue crack growth (FCG)
metallurgical alterations caused by this process. Processing/ stage. There are several factors that affect the FCG, and in
welding conditions with high heat input tend to generate relation to microstructures, it is widely reported on literature
coarser structures with bigger delta ferrite dendrites and that it affects significantly the propagations of short cracks
austenitic grains, which, in general, result in inferior me- and the beginning of the growth of long cracks, while it has
chanical properties [4], in addition to influencing the decom- little influence on stable fracture propagation (108 to 105 m/
position of austenite, as well as the formation of inclusions cycle) [11,12]. However, there are works that show that mi-
and discontinuities [5]. Santos et al. [6] analyzed fracture crostructures affect stable fracture propagation, being the
toughness of API 5 L X80 steel friction stir welds. They checked most significant influence on smaller values of tension in-
that the process parameters variation resulted in appreciable tensity. Several works show distinct fatigue crack growth
microstructural changes, e.g., the higher heat input joints rates (FCGR) for the different microstructures obtained from
resulted in degenerated upper bainite associated with the thermal-treated steels [13e17]. The studies from Bhambri
elongated MA and high carbide (cementite) content which was et al. [14] have shown that tempered martensite presented
detrimental to fracture toughness. On the other hand, the higher resistance to FCG, followed by tempered bainite,
lower heat inputs joints presented massive MA associated martensite and ferrite-pearlite, in order. In the studies of Ravi
with acicular ferrite (granular bainite) and lower carbide et al. [18], after analyzing the different weld beads (SMAW -
content which was beneficial to fracture toughness. Dirisu HSLA steel), the one with the biggest volumetric fraction of
et al. [7] analyzed of fracture toughness properties of acicular ferrite present higher FCG resistance. However, in the
wire þ arc additive manufactured HSLA steel with different studies of Magudeeswaran et al. [19], that evaluated the effect
welding conditions and wires. For a given condition, the of welding processes (SMAW and Flux Cored Arc Welding) on
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Table 1 e Chemical composition (wt.%) of the base metal.


C Mn Cr Mo V Cu Ni P S Si Nb Ti Others
0.085 1.169 0.016 0.005 0.003 0.007 0.008 0.017 0.005 0.053 0.035 0.013 0.03

FCG behaviour in quenched and tempered steel joints, the fiber Laser (IPG Photonics, model YLR 2000). A series of Laser
weld bead composed with the most acicular ferrite presented beam welding experiments were realized to chose two pa-
lower FCG resistance than the base metal (acicular rameters representing different welding routes. The Laser
martensite), while it presented the bigger FCG resistance beam power was fixed at 2 kW (current maximum value) and
when compared to a weld bead composed primarily of grain then the Laser speed was varied between 5 and 100 mm/s,
boundary ferrite. For Han et al. [17], the weld bead (SAW - representing the extreme parameters of the CNC process
micro-alloyed steel) composed primarily of Widmansta € tten table. At the end, the full penetration weld was achieved at a
ferrite presented lower FCG resistance than the base metal speed of 8 mm/s, which are too low for Laser beam welding
(ferritic-pearlitic). Due to the complex microstructures origi- and similar to GTAW. This condition usually leads to excesses
nated from the weld beads’ thermal cycles, the relation be- weld bead and HAZ due to a high heat input. Therefore, it was
tween microstructure and FCG resistance isn’t obvious. decided to use two runs instead of a single one at the top and
Depending on the phases/micro-constituents formed, the bottom of the sheet. Using two weld runs, the speed could be
microstructure may present high FCG resistance. increased to 30 mm/s reducing both the fusion and heat-
There are, in literature, recent papers on the correlation affected regions. This condition was latter called low heat
between microstructure and mechanical performance of weld input. Therefore, two welding conditions were utilized:
beads obtained by Laser welding on HSLA steels [20e22], with employing high heat input (HI) and low heat input (LI), with
basic mechanical properties such as hardness and tensile the parameters shown in Table 2.
properties, but this evaluation alone is insufficient to char- The validation process of weld quality was done by quan-
acterize the mechanical behavior of the weld bead. Informa- tifying weld bead discontinuity (pores, lack of penetration,
tion on fracture toughness and FCG in microstructures etc.) and by tensile testing conducted in specimens cut
obtained by the process of Laser welding in HSLA steels with transversally to the weld bead, which fractured beyond the
different thermal inputs is still lacking, and therefore this weld region. The tensile tests were conducted in accordance
research can contribute. This paper evaluates the effects on to ASTM E08 [23].
two distinct microstructures obtained in weld beads that Microstructural characterization was done via Nital
resulted from Laser welding with high and low heat inputs, etching (2% nitric acid in ethanol) and Le’Pera (an aqueous
under static loading, evaluating the fracture toughness by solution of sodium metabisulfite and a solution of picric acid
Crack-Tip Opening Displacement (CTOD) and under cyclic in ethyl alcohol), by optical microscopy (OM) and scanning
loading, evaluating the FCG behavior. electron microscopy (SEM), based around ASTM E407 [24].
Microhardness was determined in conformity with ASTM
E384 [25], with loads of 200 gf per 15 s.
2. Material and experimental procedure The CTOD testing of fracture toughness was done with an
SE(B) type specimen, with a notch in the center of the weld
The steel in question is classified as HSLA ferritic-pearlitic, bead (Fig. 2(a)). The pre-cracking of the specimens was done
with the chemical composition shown in Table 1. The steel with constant amplitude loading with sinusoidal wave shape,
plates (200  100 mm x 4,5 mm) were butt welded (Fig.1 (a) and ratio of 0.1 and frequency of 20 Hz. The testing was done by
(b)) autogenously via a Laser process that utilizes a high power applying monotonic load with a constant displacement rate of

Fig. 1 e (a) Microalloyed steel plates being Laser welding (b) execution of a butt welded joint.
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0.2 mm/min. The crack tip opening displacement was interior of the austenitic grain, through well-defined planes.
measured indirectly by a clip gage attached to the notch’s Allotriomorphic ferrite, however, is favored in higher tem-
extremity. After fracture, crack length measurements were peratures, nucleates in austenite grains to which it presents a
done at nine equally spaced points throughout the sample’s defined crystallographic orientation and grows toward the
thickness with a precision of 0.1 mm, in conformity with interior of the grain with a random orientation and
ASTM E1290 [26]. In these tests the crack propagation occurred throughout the austenitic grain boundary, presenting a
in the weld beads and close to their center, as recommended lenticular shape [30,31].
by BS 7448 - Part 2 [27]. For the LI weld beads obtained via low heat input and two
FCG tests were performed according to ASTM E647 Stan- passes, one on each side of the plate, martensite and bainite
dard [28], under constant amplitude loading with a load ratio microstructures were found (Fig. 3 (d)e(f)). Fig. 3(e), obtained
of 0.1 and sine waveshape. Compact tension C(T) specimens via Le’Pera, shows martensite (white) and bainite (black) and
with side grooves were chosen for FCG tests. Crack length was Fig. 3(f), obtained via Nital, shows the bainite micro-
indirectly measured using the compliance method. The tests constituent, formed by fine ferrite needles that are separated
were carried out in MTS servo-hydraulic system 810. A fre- by cementite. The use of optical and scanning electron mi-
quency of 10 Hz was used, and crack length data were croscopy does not allow for the distinction between inferior,
collected with 0.2 mm intervals. The FCG tests were carried on upper (or others) bainite; therefore, bainite has not been
the base metal (BM) (Fig. 2(b)), and on the weld beads in a classified by microstructural analysis. The high cooling rate
longitudinal direction, with crack propagation near the mid- favored the formation of phases/microconstituents that are
dle of the weld bead (Fig. 2(c)). formed at lower temperatures, such as martensite laths. In it,
the nuclei grow rapidly in the shape of platelets and only stop
their growth when met by austenitic grain boundaries, other
3. Results and discussion martensite platelets or other types of hindrances, and may
have a high aspect ratio or disorientation. Upper bainite nu-
3.1. Microstructural analysis and hardness cleates preferably around austenite grain boundaries and it is
measurements formed by fine ferrite needles that grow in sets called blades or
platelets, while inside each platelet the ferrite needles are
The base metal microstructure is composed by equiaxial separated by cementite particles [30e32].
ferritic grains refined by the controlled rolling process and The hardness values obtained, presented in Table 3 with
pearlitic colonies elongated in the direction of the rolling microstructures, are compatible with the phases/micro-
(Fig. 3(a)). This banded structure is favored by Mn segregation constituents of the different weld beads and the base metal.
in the interdendritic region, when the ingot solidifies. It must The base metal has the lowest hardness value, and, among
be considered that the steel utilized in this work has a high Mn beads, the LI weld bead obtained the highest value. Miranda
presence (1.169wt.%). There are retained austenite spots, see et al. [29] found similar results using Laser Welding on API 5 L -
the red arrows in Fig. 3(b), found in HSLA steels [6,29] due to X100 steel as a base metal: approximately 360 HV0.5 on weld
the presence of austenite stabilizing elements such as C, Mn beads generated with low heat input, which had microstruc-
and Ni. tures composed primarily by martensite and bainite, and
The welding conditions for weld bead microstructures are approximately 290 HV0.5 in weld beads obtained by high heat
verified to influence austenite decomposition. The highest input, which had microstructures composed primarily by
heat input and the use of a single pass resulted in the biggest ferrite. Coelho et al. [33] also obtained similar results in the
volume of molten material, which generated a lower cooling bonding of a Laser Welding on HSLA steel: approximately 365
rate, favoring the formation of acicular ferrite, primary Wid- HV0.01 in weld beads which had microstructures composed
mansta € tten ferrite and grain boundary ferrite (allo- primarily by martensite and bainite and approximately 255
triomorphic/proeutectoid) (Fig. 3(c)) in the HI beads. Among HV0.01 in weld beads which had microstructures composed
them, acicular ferrite is favored the most in lower tempera- primarily by acicular ferrite, polygonal ferrite and grain
tures and nucleates grain boundaries, in heterogeneous boundary ferrite.
nucleation points such as precipitate, inclusions and it grows
with a high aspect ratio (10:1). Primary Widmansta € tten ferrite 3.2. CTOD fracture toughness
nucleates austenite grain boundaries and grows toward the
The HI weld bead, composed primarily by acicular ferrite,
€ tten ferrite and grain boundary ferrite, presented
Widmansta
higher fracture toughness than the LI bead composed pri-
Table 2 e Laser welding parameters adopted in this work. marily by martensite and bainite, as shown in Table 4.
Parameters/Condition HI LI The presence of acicular ferrite in HI weld beads has
contributed to their fracture toughness. Acicular ferrite is
Heat input 175 J/mm 46,6 J/mm
Weld speed 8 mm/s 30 mm/s
formed by a group of fine ferrite blades (with a high aspect
Number of passes 1 2 (one on each side) ratio and high orientation in relation to the matrix) and by
Laser power 2000 W disperse carbides in the matrix. Since the Dolby work (1982)
Shielding gas Helium [34] it is known that the acicular ferrite promotes a reduction
Gas flow rate 30 L/min of the crack path length. Acicular ferrite nucleation in
Laser focus on the surface
microalloyed steels like the present one occurs in precipitate
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Fig. 2 e Cutting scheme of specimens for (a) CTOD tests, (b) FCG in the base metal, (c) FCG in the longitudinal direction of the
weld bead.

particles as carbonitrides, leading to a fine structure. This mechanical resistance, low ductility [32] and low fracture
phenomenon is more effective in increasing the fracture toughness [7,37]. Between upper and inferior bainite, only
toughness than the austenite grain refinement. The acicular inferior bainite has high toughness and high fracture propa-
ferrite transformation kinetics leads a random orientation of gation resistance [38] due both to the fine precipitate of car-
the acicular ferrite grain boundaries and high dislocation bides inside the ferrite needles and to the refined acicular
density which contribute to increase the fracture toughness structure. The presence of martensite and, possibly, upper
[7,10,35,36]. The structure of the acicular ferrite (as just bainite has affected the fracture toughness of LI weld beads.
explained) leads to a higher mechanical resistance and hard- Bunaziv et al. [5] also verified that a microstructure composed
ness but not so high as martensite which presents a more of martensite and bainite negatively affected the welding
brittle behavior. Neves and Loureiro [9] and Santos et al. [6] metal’s fracture toughness, resulting in an average CTOD of
also obtained high fracture toughness (relative in each paper) 0.10 mm.
on weld beads with the presence of acicular ferrite. Both It has been verified that fracture toughness is more sensi-
Widmansta € tten ferrite and grain boundary ferrite, however tive to the microstructural alterations caused by heat input
present relatively large crystallites and have few crystallo- than by hardness [39]. Other researchers [6,7,10] have also
graphic differences, which are characteristics that do not in- found significant differences in fracture toughness regarding
crease fracture toughness [7,8]. Yang et al. [8] obtained a heat input/welding conditions. Santos et al. [6] have applied
decrease in the toughness of weld beads (API 5 L X80 steel) different heat inputs and the highest fracture toughness
composed by acicular ferrite, Widmansta € tten ferrite and (CTODm ¼ 0.75 mm) was found in beads obtained by the
polygonal ferrite among others, due to the presence of Wid- lowest heat inputs, which were composed massively of MA
mansta € tten ferrite, obtaining d0.2BL ¼ 0.24 mm. associated with acicular ferrite (granular bainite) and lower
Martensite usually presents itself in lath packets and has carbide content, whilst the lowest fracture toughness
carbon atoms retained in the octahedral interstices of the (CTODm ¼ 0.19 mm) was found in weld beads obtained by the
crystalline structure and carbides finely dispersed in the highest heat inputs, which were composed of degenerated
martensitic matrix, which has the ability to generate a high upper bainite associated with elongated MA and high carbide
tangled dislocations density, which may lead to elevated content (cementite). Dirisu et al. [7] have found different weld
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Fig. 3 e Optical micrographs (a), (c) to (e) and SEM micrographs (b) and (f), showing the microstructures of (a, b) the base metal
with equiaxial ferritic, pearlitic colonies and retained austenite (yellow arrows), (c) HI weld bead with acicular ferrite,
primary Widmansta € tten ferrite and grain boundary ferrite, and (d,e,f) LI weld bead with martensite (white in (e)) and bainite
(black in (e)).

beads by altering added wires and deposition methods, The higher fracture toughness of the HI beads is related to
generating weld beads with complex microstructures. The the presence of ferritic structures. (Fig. 4(a) and (c)). It can be
weld bead with the highest fracture toughness (640 kJ/m2) was observed that the fracture micro-mechanism consists of void
formed due to the presence of acicular ferrite, whilst the nucleation and coalescence, with deep dimple presence (Fig. 4
lowest fracture toughness (350 kJ/m2) occurred, primarily due (e)) due to the microstructure’s high deformation potential.
to the formation of grain boundary ferrite and upper bainite. For the LI beads, though, the fracture surface is characteristic

Table 3 e Vickers hardness (HV) and microstructures constituents.


Region Primary microstructure HV0.2
HI Acicular ferrite, Widmansta € tten ferrite and Grain boundary ferrite 250 ± 10
LI Martensite and bainite 382 ± 20
BM Equiaxial ferrite and pearlite 203 ± 9
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characteristics, similar to the ones presented in this paper, on


Table 4 e Calculated CTOD values.
samples with low toughness.
Weld beads d eot (mm)
HI 0.42 ± 0.14 3.3. Fatigue crack propagation
LI 0.14 ± 0.03
Fig. 5 presents, in bi-logarithmic scale, the relation between
the rate of crack propagation longitudinal to the weld bead
of a brittle microstructure, with no significant deformation and the stress intensity factor (SIF) range (DK) correspondent
(Fig. 4 (b) and (d)) and low energy absorption in the crack, yet to the stage of stable crack propagation (108 to 106 m/cycle)
the presence of a ductile micro-mechanism was observed, as on the base metal and weld beads. The obtained results are
shown by the presence of dimples (Fig. 4 (f)). However, these compared to the International Institute of Welding (IIW)
are shallow due to the low plastic deformation capacity. recommendation for steel [41], in which intercept
Garcia et al. [40] have also found dimples with distinct char- pffiffiffiffiffi
C ¼ 1.65  1011 [1/(MPa3 m cycle)] and exponent n ¼ 3 are
acteristics in different weld beads: the beads with higher adopted. The weld beads presented higher FCG resistance
toughness presented deep dimples, while the beads with than the base metal and as recommended by IIW. The dif-
lower toughness presented cleavage planes and dimples with ference between FCG resistances was more significant for
shallow depth, similar to the ones found in LI beads. Neves lower DK values. Regarding the weld beads, there is no FCG
and Loureiro [9] have also found fracture surfaces with brittle

Fig. 4 e SEM fractographs of the CTOD specimens (a, b, c, d) showing the fracture surfaces of (a, c) HI and (b, d) LI conditions
and the fracture micro-mechanism of (e) HI and (f) LI conditions.
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martensite and acicular ferrite, while the ones that have the
lowest FCG resistances are ferrite-pearlite, grain boundary
ferrite and Widmansta € tten ferrite.
Among the obtained weld beads, the HI presents higher
fracture toughness, which contributes to FCG resistance,
although lower hardness. The LI beads present higher hard-
ness, which contributes to FCG resistance, although they
present lower fracture toughness. Bhambri et al. [14] have
found similar FCG rates for different microstructures
(martensite and ferrite-pearlite), where martensite had high
mechanical resistance and low deformation capacity, whilst
ferrite-pearlite had low mechanical resistance and high
deformation capacity.
In relation to the microstructural composition of the HI and
LI beads, acicular ferrite present in HI beads has, in function of
its microstructure, good mechanical resistance and toughness
and its morphology makes the crack path harsher, dampening
Fig. 5 e Fatigue crack growth results for the base metal and crack growth, which results in low FCG rates [18,19]. However,
welding conditions. Comparison between crack Widmansta € tten ferrite and grain boundary ferrite do not have
propagation longitudinal to the weld beads and IIW high FCG resistance [17,19]. For LI beads, concerning bainite,
recommendations. upper bainite may present lower FCG resistance than low
carbon martensite [43], while inferior bainite presents higher
FCG resistance [15], therefore, upper bainite does not increase
FCG resistance. The acicular morphology of the martensite
resistance difference between LI and HI beads. The FCG was
may have favored high FCG resistance [44,45].
less sensitive to the microstructural alterations than the
In function of their mechanical properties and micro-
fracture toughness, which has been observed by other re-
structure morphologies, the HI and LI weld beads FCGR are
searchers as well [13,42].
similar, although lower than that found for the base metal,
FCGR is determined by the stressestrain state ahead of the
which has lower mechanical resistance, equiaxial
crack. The crack advance in stage II is associated with the high
morphology and coarse structures. Several researches [44e47]
stress levels that cause cyclic plastic deformation at the crack
have found a lower weld bead FCGR when compared to the
tip and with the plastic deformation in the matrix, primarily
base metal’s FCGR, mainly for smaller DK values. In all of
the plastic zone. In some research, FCG resistance is associ-
them, the martensite or acicular ferrite microstructures have
ated with the best overall mechanical properties [19,20], such
contributed to the increase in FCG resistance.
as tensile strength, deformation capacity and toughness. Of
By analyzing the fracture surfaces referred to cracks lon-
the data extracted from the literature [15,17e19] it has been
gitudinal to the weld beads on HI and LI conditions, we found
verified, in each work, the difference between the FCGR in
no significant differences between them, therefore only one
function of microstructures and mechanical properties.
weld bead is presented in Fig. 6. In both there is the presence
However, the correlation between microstructure, mechani-
of deformation signs, secondary cracks and fatigue striations,
cal properties and FCGR isn’t obvious. It has been observed
the latter being more evident at the beginning of the stable
that solely microstructures which have high mechanical
crack growth (arrows in Fig. 6(a)), whilst the end of the growth
resistance and high deformation capacity or toughness pre-
indicates coarse striations (rectangle in Fig. 6(b)) and tearing
sent higher FCG resistance. Amidst the microstructures with
ridge.
higher FCG resistances one can quote tempered martensite,

Fig. 6 e SEM micrographs showing the fatigue fracture surfaces of (a) initial crack and (b) end of the FCG process. Rectangle
indicates coarse striations. Crack growth is oriented vertically, from top to bottom.
j o u r n a l o f m a t e r i a l s r e s e a r c h a n d t e c h n o l o g y 2 0 2 1 ; 1 1 : 8 0 1 e8 1 0 809

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