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Welding International

ISSN: 0950-7116 (Print) 1754-2138 (Online) Journal homepage: http://www.tandfonline.com/loi/twld20

Joint microstructures, mechanical properties and


fatigue behaviour of ferritic stainless steel SUS 430
welds with different filler metals

Masayuki Akita, Yoshihiko Uematsu, Toshifumi Kakiuchi, Masaki Nakajima,


Yukio Agata & Kohei Takino

To cite this article: Masayuki Akita, Yoshihiko Uematsu, Toshifumi Kakiuchi, Masaki Nakajima,
Yukio Agata & Kohei Takino (2018) Joint microstructures, mechanical properties and fatigue
behaviour of ferritic stainless steel SUS 430 welds with different filler metals, Welding International,
32:6, 427-435

To link to this article: https://doi.org/10.1080/09507116.2017.1346860

Published online: 23 Oct 2018.

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WELDING INTERNATIONAL
2018, VOL. 32, NO. 6, 427–435
https://doi.org/10.1080/09507116.2017.1346860

ARTICLE

Joint microstructures, mechanical properties and fatigue behaviour of ferritic


stainless steel SUS 430 welds with different filler metals
Masayuki Akitaa, Yoshihiko Uematsub, Toshifumi Kakiuchib, Masaki Nakajimac, Yukio Agatad
and Kohei Takinoe
a
Faculty of Engineering, Gifu University; bDepartment of Mechanical Engineering, Faculty of Engineering, Gifu University; cToyota
College, National Institute of Technology; dNippon Welding Rod Co. Ltd.; eNTN Corporation

ABSTRACT KEYWORDS
Joint microstructures, mechanical properties and fatigue behavior of ferritic stainless steel Ferritic stainless steel; MIG
SUS430 welds with different filler metals were investigated. Two filler metals with different weld; microstructure; fatigue
chemical compositions, Filler I and II, had been used for the MIG butt welding of SUS430. strength; hardness
Filler I showed coarser grains in the microstructure than Filler II including Al and Ti. In both
welded joints, the hardness of heat affected zone (HAZ) was the highest due to the formation
of hard needle-like martensite. The welding heat input of Filler I welded joint was higher than
that of Filler II. Consequently, martensite content of Filler I was more numerous and bigger
than the Filler II. Fully reversed axial fatigue tests had been performed using smooth speci-
mens of welded joints and base-metal specimens at ambient temperature in laboratory air. In
both welded joints, fatigue fracture took place at base metal region due to the higher
hardness in weld metals and HAZ regions than the base metal.

1. Introduction metal, it is accompanied by structural changes such


as coarsening of the microstructure and particles in
Because of its excellent corrosion resistance and oxi-
the peripheral region of the weld [10–15]. If the
dation resistance at high temperatures, stainless steel
welding conditions are inappropriate, weld defects
is used for applications where thermal resistance is
such as penetration failure and blowholes may occur
required, such as boilers, electricity generation plant
and there are many factors that affect mechanical
and chemical plants [1]. Since among these stainless
characteristics. Since, improved ferritic stainless steel
steels, ferritic stainless steel has better stress corrosion
weld materials have been developed in recent years, it
cracking (SCC) resistance characteristics, smaller
is necessary to gain an understanding of the depen-
coefficient of linear expansion and better thermal
dency on filler metals and also to understand the
conductivity than austenitic steel, it is widely used
hardness, tensile strength and fatigue strength and
for boilers, heaters and other combustion devices
other physical properties of joints. The present
and motor vehicle exhaust systems [2–4]. When fer-
authors, in previous studies, have investigated MIG
ritic stainless steel is used as automotive exhaust
welding of the ferritic stainless steel SUS444 (19Cr–
members, SUS409 (13Cr–Ti) is generally used but
2Mo) with ferritic stainless welding materials with
internal corrosion of exhaust system members due
two different chemical compositions, inspected the
to exhaust condensates means that SUS430 (18Cr)
microstructure of the weld region and investigated
and other high-chromium ferritic stainless steels
the mechanical properties and fatigue behaviour
(16%–19% Cr) have come into use because of their
[16]. As a result they found that the weld microstruc-
excellent corrosion resistance [5].
ture differed greatly depending on the weld metals.
Welding is widely used in the fabrication of auto-
Since, however, there were weld defects such as
motive exhaust systems but since they are parts used
incomplete penetration and intergranular precipita-
at high temperatures, ferritic stainless steel of the
tion in the same joint it was not possible to go on to
same type as the base metal is used as welding
evaluate the mechanical properties of a sound joint.
metal [6,7] with the principal aim of high-tempera-
In the present study, SUS430, which is widely used
ture crack prevention [8]. On the other hand, in
in automotive exhaust system parts and has a Cr
almost all cracking failures of welded structures the
content lower than SUS444 and therefore is more
cracks initiate from the weld and then propagate until
effective in terms of cost reduction, was MIG welded
final failure [9] so a grasp of the mechanical charac-
with ferritic stainless steel filler metals of two differ-
teristics is an engineering requirement. Since welding
ent chemical compositions and a detailed examina-
is a joining technique which involves localized melt-
tion made of the microstructural appearance of the
ing and solidification of base metal and welding
weld region. The welding conditions were optimized
© 2018 Informa UK Limited, trading as Taylor & Francis Group
428 A. MASAYUKI ET AL.

Table 1. Chemical compositions of the base metal and filler metals (wt. %).
Material C Si Mn P S Ni Nb Cr Mo Al Ti Fe
SUS430 0.04 0.24 0.67 0.31 0.05 0.17 – 16.3 – – – Bal.
Filler I 0.016 0.43 0.45 0.016 0.002 0.35 0.44 17.69 0.25 – – Bal.
Filler II 0.017 0.39 0.39 – – 0.4 0.45 19.23 0.34 Inc. Inc. Bal.

so that there were no welding defects and the was 6 mm with X-shaped groove and two passes of
mechanical properties of a sound joint, not only the welding were performed, which resulted in weld
joint hardness and tensile strength but also the fati- defects. Accordingly in this study, the sheet thickness
gue strength and fatigue strength mechanism were was reduced slightly and one pass welding performed
discovered and compared to the base metal. so that a sound weld without defects was achieved.
The welding conditions and welding heat inputs are
shown in Table 2. Welding heat input was found
2. Materials and experimental methods
using the following equation [22]:
2.1 Specimens Welding heat input
The specimens were 4-mm thick ferritic stainless steel current ½A  voltage½V 
½J=mm ¼   (1)
SUS430 (18Cr). No prior heat treatment had been welding speed mm s
carried out on the specimens and they were welded
in their as-received state. The filler metals used were It can be found by using this equation that the
Fillers 1 and 2, ferritic stainless steel welding wires of welding heat input when welding was performed
different chemical compositions. Both of the welding with Filler I (470 J/mm) was slightly higher than
wires were developed for the welding of automotive with Filler 2 (440 J/mm); the difference was
exhaust system parts. Their chemical compositions approximately 7%.
(mass%) are shown in Table 1. Both of the fillers Tensile tests and fatigue tests were conducted
have added Nb to inhibit sensitization [17,18] caused using specimens as shown in Figure 2 to investigate
by welding [19]. Since Filler II (Cr content: 19.23%) the physical properties of the joints. The specimens
had a greater Cr content than Filler I (Cr content: were sheets with a parallel section length of 30 mm.
17.69%), it had superior heat resistance and corrosion The welding line was normal to the axis of the
resistance [20]. The filler metals design also involved specimen and the specimen was taken from the
the addition of Al and Ti to ensure minutely stabi- welded sheet so that this line was at the centre of
lized weld compositions [4,21]. the parallel section. Specimens were also taken
from unwelded base metal. The reinforcement was
machined off the welded joint specimens to pro-
2.2 Welding conditions and experimental duce smooth specimens with no stress concentra-
methods tion at the weld toe. This is because when there is
MIG welding was used, and a V-shaped groove was stress concentration at the weld toe, the stress con-
made at the ends of 4-mm thick sheets before one- centration dependent on the toe shape becomes
pass welding was then carried out (Figure 1). In the one of the principal affectors on fatigue strength
previous report [16], on SUS444 the sheet thickness [16]. The surfaces of fatigue specimens from which
the reinforcement had been removed were polished
with #2000 emery paper and then buffed to a mir-
ror finish before being used in the tests. Below, the
welded joint specimens welded using Filler I and
Filler 2 are referred to, respectively, as Filler I joint
and Filler II joint.
SEM was used for the inspection of the micro-
structures of the weld regions. Hardness was mea-
sured using a microVickers gauge (test force 4.9 N,
Figure 1. Dimensional details of welding groove. hold time 30s). A universal tensile tester was used
for tensile tests. A 49-kN fatigue tester with an
Table 2. Welding parameters. electrohydraulic servo was used for fatigue tests
Welding Welding and the load waveform was a sine wave with a
Welding Welding average Root heat frequency f = 10 Hz and stress ratio R = −1. The
Filler current voltage speed gap input
metal (A) (V) (mm/sec) (mm) (J/mm)
test environment was the laboratory atmosphere.
Filler I 180 24 9.2 0 470 An X-ray diffractometer (XRD) was used to mea-
Filler II 200 22 10 0.4 440 sure residual stress.
WELDING INTERNATIONAL 429

Figure 2. Configuration of fatigue specimen.

Figure 3. Microstructures in SUS430 welded joint using Filler Figure 4. Microstructures in SUS430 welded joint using Filler
I: (a) macroscopic appearance, (b) base metal, (c) HAZ and (d) II:(a) macroscopic appearance, (b) base metal, (c) HAZ and (d)
fusion zone. fusion zone.

3. Experimental results metal used. In the fusion zone of Filler I joint, a coarse
3.1 Microstructure of the welds (d = approximately 180 µm or greater) columnar
microstructure was observed. No such columnar
The cross-sectional surfaces of Fillers I and II joints microstructure was observed in the Filler II joint;
were polished and then etched with etchant (distilled
instead, there was a structure of uniaxial particles
water: hydrochloric acid: nitric acid = 5:5:1) for inspec- (Figure 4(d)) and d was approximately 120 µm,
tion of their microstructure. The results are shown in which was smaller than that in Filler I joint
Figures 3 and 4. In all joints, the average crystal grain (d = approximately 180 µm or greater). This is thought
size of the base metal d was approximately 30 µm to be due to the Al and Ti added to Filler II [4,21].
(Figure 3(b), Figure 4(b)). When the crystal grains
are not uniaxial, the average value for the projected
area diameter of the crystal grains was taken as the 3.2 Hardness distribution and tensile strength of
average crystal grain size. It was clear that the crystal the weld region
grains were coarsened by the heat input at the heat-
The average hardness of the base metal was 161HV for an
affected zone (HAZ) during welding. The crystal grain
average of 20 points. Figure 5 shows the lateral sectional
size d in Filler I joint (Figure 3(c)) and in Filler II joint
surface hardness distributions of the weld zone regions
(Figure 4(c)) was, respectively, approximately 100 µm
(measured at a position 1mm from the upper surface).
and approximately 110 µm. In the fusion zone where
With the weld centre line originating on the x-axis,
fusion and resolidification occur, the microstructure
hardness was measured at 0.25-mm intervals over a
had a very different appearance depending on the filler
range of 7 mm to one side of the weld centre. Dotted
430 A. MASAYUKI ET AL.

Figure 6. S–N diagrams.

the HAZ. Specifically, the fracture site is near the


boundary between the parallel section and the R
section and, as shown in Figure 2, at a position at
some distance from the fusion zone and HAZ.

3.3 Fatigue strength and fracture surface


observations
The S–N curve is shown in Figure 6. The results for the
base metal specimen are also shown as a comparison.
The fatigue strength of the Filler I joint and the Filler II
joint were approximately the same as that of the base
metal and the fatigue limits σw were, respectively,
200MPa and 220Mpa, thus rising to slightly higher
than that of the base metal (180 MPa). SEM micrographs
of the fracture surfaces near the crack initiation site in the
Figure 5. Vickers hardness distributions of welded joints: (a) base metal specimen, Filler I joint and Filler II joint are
welded joint using Filler I and (b) welded joint using Filler II. shown in Figure 7(a)–(c). In the base metal specimen
Dotted lines show the average of base-metal specimen and (Figure 7(a)), as in the results for other ferritic stainless
grey area indicate scatter of the hardness. steels, cracking initiates from the surface by repeated
sliding deformation [23–27]. On the other hand, in all
welded joint specimens (Figure. 7(b), (c)), like the base
lines in the figure show the average hardness (161 HV) of
metal specimen, cracking initiates in the specimen sur-
the base metal and the grey strips give the variations in
face by repeated sliding deformation from the base metal.
hardness in the base material. Due to the differences in
the welding conditions (Table 2), the fusion zone of Filler
I joint is narrower than that of Filler II joint and the HAZ 3.4 Residual stress
is wider. In both of the joints the HAZ is hardest, fol-
lowed by the fusion zone and the base metal. The max- The residual stress caused by welding is thought to be
imum hardness (275 HV) of the Filler I joint HAZ was one factor that affects the strength characteristics of the
greater than that of the Filler II joint (240 HV). welded joint [28,29]. The longitudinal residual stress of
Tensile tests of the base metal and both welded Filler I joint and of Filler II joint, the reinforcement
joints were performed three times for each and the having been removed from both, were measured by
tensile strength was obtained as an average value. The XRD. The spot diameter was 0.5mm and the surface of
resulting σB was 481 MPa for the base metal, 450 the measured specimen was machined and then buffed.
MPa for Filler I joint and 448 MPa for Filler II The residual stress distributions are shown in Figure 8.
joint, showing a tendency for the σB of the welded In the weld region where the measurements were
joints to be slightly lower than that of the base metal. made, compressive residual stress of −280 to −105
The fracture site of the joints was the base metal, MPa was identified in the Filler I joint and −280 to
which has lower hardness than the fusion zone and −155 MPa in the Filler II joint. Generally, marked
residual stress is created in the weld region when
WELDING INTERNATIONAL 431

Figure 8. Residual stress distributions of SUS430 welded


joints: (a) Filler I welded joint, (b) Filler II welded joint.

polishing and the value of this was smaller than that of


the welded joint specimens.

Figure 7. SEM micrographs of fracture surface near crack


4. Discussion
initiation site (a) base-metal (σa= 280MPa, Nf = 2.0 × 104)
and (c) Filler II welded joint (σa= 240MPa, Nf= 4.2 × 105). 4.1 Microstructure and mechanical properties of
Arrows indicate crack initiation site. the heat-affected zone
As shown in Figure 5, the hardness of the weld regions
welding is carried out. In the residual stress distribu- of each of the welded joints was greatest in the HAZ
tions shown in Figure 8, however, almost completely followed by the fusion zone, and the base metal was
uniform compressive residual stress was detected in least hard. Detailed structural inspections of the weld
the fusion zone, HAZ and base metal with no great regions were carried out to investigate the causes of
difference found between the amounts of residual distribution of different hardness. Figure 9 shows the
stress in the various zones. As a comparison, the resi- results of optical microscopy of the microstructure
dual stress was measured in the specimen parallel sec- around the boundary between the fusion zone and
tion region using the base metal specimen. HAZ. Figure 10 shows the results of SEM microscopy
Compressive residual stress of −60 to −30 MPa was of the different HAZs. In the optical micrographs of the
detected at the surface of the base metal specimen. Filler I joint (Figure 9(a)) and the Filler II joint
Since the surface of the base metal sample had not (Figure 9(b)), in the HAZ enclosed by the broken
been ground, as in reinforcement removal, this was lines there are black parts principally along the grain
compressive residual stress introduced by the surface boundaries. Figure 10 shows enlargements of these, in
432 A. MASAYUKI ET AL.

Figure 9. Microstructures of fusion zone and HAZ: (a) Filler I


welded joint and (b) Filler II welded joint. The black lines Figure 10. Magnified views of HAZ: (a) Filler I welded joint
indicate needle-like martensite in HAZ. The width of distribu- and (b) Filler II welded joint. Arrows indicate needle-like
tion of needle-like martensite (dotted line) in Filler I welded martensite.
joint is wider than in Filler II welded joint.
fusion zone was the same as in the filler. Since the
which it is evident that this black part is an acicular FF of the SUS430, which is the base metal, was 14.12
martensitic structure. As can be seen from Figures 9(a) (%), and thus < 17(%), it is thought that acicular
and 10(a), the acicular structure in the Filler I joint martensite has been precipitated into the HAZ, as
was greater in quantity than in the Filler II joint shown in Figures 9 and 10. As shown in Figure 9,
(Figures 9(b) and 10(b)) and the range of distribution on the other hand, there is no martensitic structure in
was greater. Also, there was much acicular martensite the weld metal. This indicates that it is because the
in the particles as well as in the particle boundaries in filler FF is adequately large and the ferrite phase is
the Filler I joint. Alizadeh-Sh et al.[14] and Zheng et al. stable. Also Zheng et al.[15] have reported that when
[15] have reported that, when ferritic stainless steel is low C· 12% Cr stainless steel is welded, and the
welded, and the ferrite factor (FF) is lower than 17(%), welding heat input is high, a large quantity of acicular
acicular martensite is precipitated in the HAZ. The FF martensite is precipitated. The fact that, although the
is as follows [14,15]: base metal is the same, the quantity of acicular mar-
tensite in Filler I joint is greater than that in Filler II
FF ¼ %Cr þ 6%Si þ 8%Ti þ 4%mo þ 2%Al is thought to be, as described in Section 2.2, the
þ 4%Nb  2%Mn  4%Ni  40% ðC þ N Þ welding heat input when welding was performed
(2) with Filler I (470 J/mm) was higher than with Filler
2 (440 J/mm).
SUS430: 16.3 + 6 × 0.24 – 2 × 0.67 – 4 × 0.17 – The hardness of the HAZ region is correlated
40 × 0.04 = 14.12 with the weld structure described above. It can
Filler I: 17.69 + 6 × 0.43 + 4 × 0.25 + 4 × 0.44 – 2 × 0.45 – thus be concluded that the hardness of the HAZ
4 × 0.35 – 40 × 0.016 = 20.09 is higher than in the base metal and the weld, as
Filler II: 19.23 + 6 × 0.39 + 8× Inc. + 4 × 0.34 + 2× Inc. shown in Figure 5, because hard acicular marten-
+ 4 × 0.45 – 2 × 0.39 – 4 × 0.4 × 0.017 > 21.67 site is precipitated. Alizadeh-Sh et al.[14] and
Strictly speaking, the chemical composition in the Ramkurar et al.[30] have reported that when mar-
fusion zone is thought to change in a graduated tensite is precipitated into the HAZ of a weld of
manner from the filler to the base metal but it was ferritic stainless steel, the hardness of the HAZ
calculated with the assumption that the FF in the
WELDING INTERNATIONAL 433

increases in comparison with the base metal. The fatigue strength is sensitive to residual stress, the
fact that the weld hardness is higher than the base strength of Filler I and Filler II joints was a little higher
metal hardness is because there is a large quantity than the base metal, despite the fact that fracture
of solid solution strengthening elements such as occurred in the base metal.
Ni and Nb in the weld metal. Tensile strength is In the present tests, the parallel section of the welded
slightly lower in the joint than in the base metal. joint specimen was elongated and each of the welded
On the other hand, the tensile strength of a joints fractured at the base metal. The fatigue strength
welded joint where the weld is harder and stron- of the joints had increased slightly more than the base
ger than the base metal is sometimes greater than metal, due to effect of the residual stress noted above,
that of the base metal. This is thought to be but the effect of the filler on the tensile strength and
because the deformation of the contiguous low- fatigue strength remains obscure. However, if the joint
hardness metal is constrained by the high-strength is sound, it is important in the engineering context that,
weld and enters a multiaxial stress state that whatever the weld metal, a strength similar to that of the
requires a deformational stress greater than that base metal should be achieved. As described in Section
required by the base metal alone requires [31]. In 4.1, when the ferritic stainless steel SUS430 is welded
the present tensile tests also, the fracture site was with different fillers, there are differences in the micro-
the base metal. However, the parallel section of structure of the weld region which are dependent on the
the tensile test specimen is 30 mm (Figure 2) and chemical composition and a correlation between hard-
if the HAZ, strengthened by the precipitation of ness distribution and structure also becomes apparent.
acicular martensite, is also included in the weld, This is because in the joint part of the two different
the parallel section is comparatively short. As a joints, there may be differences not only in fatigue
result, there is what is known as an R section strength but also in other phenomena such as cracking
fracture, in which tensile fracture occurs around initiation and propagation behaviour and the fatigue
the boundary between the parallel section and the fracture surface. It can also be anticipated that marten-
R section, and the tensile strength of the joint site content of the HAZs will differ and that environ-
specimen is thus a little lower than that of the mental sensitivity may also differ in the base metal,
base metal. In tensile tests of the base metal speci- fusion zone and HAZ. There is therefore a need to
mens, fracture occurred at the centre of the gauge. investigate the failure mode in welds in a structure
where the distance from the base metal is short and
fracture occurs in the weld metal and a detailed study of
4.2 Fatigue behaviour of the welded joint
this will be made in the future.
specimen
The fatigue test results showed that fatigue cracking,
5. Conclusion
leading to fracture, occurred in the base metal of all the
welded joint specimens (Figure 7). Generally, fatigue In the present study SUS430 ferritic stainless steel was
strength is more sensitive to welding defects than tensile MIG welded using two ferritic stainless steel fillers
strength. However, the fact that fatigue cracking with different chemical constituents and detailed
occurred in the base metal, unlike the previously study was made of the differences in the weld region
reported [16] SUS444, indicates that a sound joint microstructures thus obtained. The mechanical prop-
with no weld defects has been fabricated whatever the erties and fatigue behaviour under an axial load were
filler. Also, unlike tensile strength, the fatigue strength also investigated using specimens where the reinfor-
of the joint has become slightly higher than the base cement had been machined off. The following con-
metal, despite the fact that fracture occurs in the base clusions were made.
metal. Generally, when welding is carried out, a com-
plex residual stress is created in the weld region. (1) The microstructure of the fusion zone made with
However, Figure 8 shows the detection of almost com- Filler I was a coarse structure of columnar crystal
pletely uniform compressive residual stresses in the grains. In the Filler II joint, coarsening of the
stress distributions in the fusion zone, HAZ and base grains was inhibited so that, compared to Filler I
metal with no great difference found between the joint, the grains were uniaxial and fine. This was
amounts of residual stress in the various zones. From thought to result from the addition of Al and Ti
these findings it is thought that, as shown in Figure 8, to Filler II.
almost completely uniform compressive residual stress (2) In the HAZ of each of the welded joints the
has been introduced due to the effect of grinding and crystal grains were coarsened due to the welding
surface polishing to remove the reinforcement of the heat input. With SUS430, which has a low FF, an
specimens. The welded joint specimens had higher acicular martensitic structure was precipitated
compressive residual stress than the base metal speci- along the grain boundaries of the HAZ but in
men, which only underwent surface polishing. Since the weld metal, since the FF is high and the
434 A. MASAYUKI ET AL.

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